#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:36:06 +0300 (Thu, 24 May 2018) $
#$Revision: 761 $
#$URL: svn://172.16.1.111/rod/cif/1/00/02/1000265.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000265
loop_
_publ_author_name
'Novak, G. A.'
'Gibbs, G. V.'
_publ_section_title
;
 The crystal chemistry of the silicate garnets sample An
;
_journal_name_full               'American Mineralogist'
_journal_page_first              791
_journal_page_last               823
_journal_volume                  56
_journal_year                    1971
_chemical_compound_source        R070722
_chemical_formula_sum            'Ca3 Fe2 O12 Si3'
_chemical_name_mineral           Andradite
_space_group_IT_number           230
_symmetry_space_group_name_Hall  '-I 4bd 2c 3'
_symmetry_space_group_name_H-M   'I a -3 d'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   12.058
_cell_length_b                   12.058
_cell_length_c                   12.058
_cell_volume                     1753.177
_exptl_crystal_density_diffrn    3.851
_cod_original_formula_sum        'Si3 Fe2 Ca3 O12'
_cod_database_code               9000239
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R070722.rod
_rod_data_source.block           3500000
_rod_database.code               1000265
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9000239 COD http://www.crystallography.net/cod/9000239.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
161.1072 0.0000000E+00
161.5893 31.74902
162.0714 81.33984
162.5536 132.7988
163.0357 166.8164
163.5178 171.8506
163.9999 234.8184
164.4820 213.0498
164.9641 184.0039
165.4463 147.2744
165.9284 74.36719
166.4105 1.025391
166.8926 34.18652
167.3747 19.23633
167.8568 89.12109
168.3390 127.0225
168.8211 128.9531
169.3032 123.0322
169.7853 124.8037
170.2674 130.9482
170.7495 135.8408
171.2317 136.1025
171.7138 134.2148
172.1959 131.7568
172.6780 128.1387
173.1601 127.0332
173.6422 139.0791
174.1244 158.7139
174.6065 167.0518
175.0886 140.3730
175.5707 98.82324
176.0528 70.46191
176.5349 58.79297
177.0171 65.51953
177.4992 109.8721
177.9813 185.5996
178.4634 244.2080
178.9455 226.7559
179.4276 162.8271
179.9098 121.1240
180.3919 135.0791
180.8740 176.7607
181.3561 203.3496
181.8382 214.2646
182.3203 213.3389
182.8025 197.8018
183.2846 171.4814
183.7667 149.2734
184.2488 137.7764
184.7309 135.6914
185.2130 131.9395
185.6951 121.2061
186.1773 131.5195
186.6594 242.3711
187.1415 439.6211
187.6236 574.5850
188.1057 524.6641
188.5878 330.2637
189.0700 183.6475
189.5521 107.7441
190.0342 81.15137
190.5163 72.90527
190.9984 83.01660
191.4805 99.44922
191.9627 111.0586
192.4448 118.7227
192.9269 138.4570
193.4090 178.4990
193.8911 228.8389
194.3732 256.1904
194.8554 257.4541
195.3375 255.6465
195.8196 282.2754
196.3017 338.8457
196.7838 366.0088
197.2659 335.1055
197.7481 258.9473
198.2302 226.0859
198.7123 245.4932
199.1944 283.5518
199.6765 300.4502
200.1586 294.2705
200.6408 284.8330
201.1229 276.1895
201.6050 268.1895
202.0871 270.9561
202.5692 287.3672
203.0513 309.6357
203.5335 323.3008
204.0156 325.4346
204.4977 330.0449
204.9798 340.6240
205.4619 355.3008
205.9440 390.0195
206.4262 455.2256
206.9083 532.9512
207.3904 573.1982
207.8725 563.6572
208.3546 549.8418
208.8367 566.2861
209.3189 618.7646
209.8010 653.7305
210.2831 658.3770
210.7652 624.9941
211.2473 616.4414
211.7294 648.0088
212.2116 690.5918
212.6937 717.8389
213.1758 735.4902
213.6579 771.4912
214.1400 820.7031
214.6221 871.3389
215.1043 913.7275
215.5864 951.1396
216.0685 980.9121
216.5506 994.7070
217.0327 980.1846
217.5148 988.3750
217.9970 1032.558
218.4791 1115.889
218.9612 1206.776
219.4433 1319.372
219.9254 1434.969
220.4075 1526.759
220.8897 1590.643
221.3718 1635.977
221.8539 1659.748
222.3360 1656.306
222.8181 1659.989
223.3002 1669.036
223.7824 1685.995
224.2645 1717.802
224.7466 1780.099
225.2287 1833.045
225.7108 1853.247
226.1929 1822.840
226.6750 1810.863
227.1572 1829.225
227.6393 1862.842
228.1214 1871.745
228.6035 1845.453
229.0856 1810.065
229.5677 1778.820
230.0499 1758.906
230.5320 1726.385
231.0141 1673.634
231.4962 1607.282
231.9783 1555.831
232.4604 1533.157
232.9426 1507.812
233.4247 1458.703
233.9068 1372.300
234.3889 1291.152
234.8710 1219.110
235.3531 1155.394
235.8353 1098.390
236.3174 1052.550
236.7995 1008.765
237.2816 960.4727
237.7637 907.0654
238.2458 850.7607
238.7280 792.1494
239.2101 731.2510
239.6922 664.1348
240.1743 577.3125
240.6564 497.4932
241.1385 452.6377
241.6207 466.1738
242.1028 471.6357
242.5849 452.1885
243.0670 404.6143
243.5491 372.1113
244.0313 358.5771
244.5134 356.8125
244.9955 361.9072
245.4776 389.8389
245.9597 396.2178
246.4418 361.5547
246.9240 273.3281
247.4061 219.0488
247.8882 215.3086
248.3703 234.0752
248.8524 233.4189
249.3345 198.0303
249.8167 169.9424
250.2988 166.4111
250.7809 199.8809
251.2630 206.3604
251.7451 172.2607
252.2272 118.8711
252.7094 85.40430
253.1915 81.93750
253.6736 80.77344
254.1557 71.89062
254.6378 52.78223
255.1199 32.93652
255.6021 9.263672
256.0842 13.54590
256.5663 21.82910
257.0484 1.725586
257.5305 8.938477
258.0126 12.94629
258.4948 92.56152
258.9769 131.0576
259.4590 112.0391
259.9411 56.74512
260.4232 22.11035
260.9053 12.90918
261.3875 15.18750
261.8696 26.44434
262.3517 56.23438
262.8338 60.95117
263.3159 23.67773
263.7980 36.60449
264.2802 49.43262
264.7623 4.099609
265.2444 67.39844
265.7265 111.9873
266.2086 139.8984
266.6907 137.9639
267.1729 95.39941
267.6550 24.58789
268.1371 31.34473
268.6192 72.63867
269.1013 96.67871
269.5834 96.41309
270.0656 65.39258
270.5477 39.95117
271.0298 26.44043
271.5119 21.57227
271.9940 10.41602
272.4761 9.133789
272.9583 28.79395
273.4404 40.63867
273.9225 42.09863
274.4046 50.68457
274.8867 75.81738
275.3688 109.0723
275.8510 106.7617
276.3331 59.29785
276.8152 4.855469
277.2973 22.17480
277.7794 18.50684
278.2615 19.94238
278.7437 36.35938
279.2258 62.71973
279.7079 74.14551
280.1900 67.77539
280.6721 57.84961
281.1542 57.90918
281.6364 68.53223
282.1185 77.96387
282.6006 83.26367
283.0827 85.76855
283.5648 89.95703
284.0469 95.58984
284.5291 104.5273
285.0112 116.1504
285.4933 130.6660
285.9754 157.1572
286.4575 202.0625
286.9396 259.0322
287.4217 306.1377
287.9038 342.6465
288.3860 372.6504
288.8681 393.6895
289.3502 407.4824
289.8323 434.3105
290.3144 481.8545
290.7965 545.1621
291.2787 617.8887
291.7608 702.2168
292.2429 774.0781
292.7250 799.3975
293.2071 788.1602
293.6892 789.6807
294.1714 822.8574
294.6535 877.8838
295.1356 936.1826
295.6177 998.4365
296.0998 1062.068
296.5819 1123.998
297.0641 1186.294
297.5462 1253.827
298.0283 1328.119
298.5104 1408.710
298.9925 1507.111
299.4746 1624.020
299.9568 1720.197
300.4389 1738.552
300.9210 1709.456
301.4031 1704.604
301.8852 1761.340
302.3673 1848.241
302.8495 1931.771
303.3316 2010.816
303.8137 2081.417
304.2958 2136.677
304.7779 2180.708
305.2600 2219.807
305.7422 2258.601
306.2243 2292.001
306.7064 2308.148
307.1885 2308.460
307.6706 2317.347
308.1527 2375.521
308.6349 2448.221
309.1170 2486.078
309.5991 2434.979
310.0812 2369.635
310.5633 2351.259
311.0454 2377.056
311.5276 2397.866
312.0097 2383.532
312.4918 2348.708
312.9739 2309.464
313.4560 2272.164
313.9381 2230.303
314.4203 2173.709
314.9024 2105.522
315.3845 2055.304
315.8666 2050.475
316.3487 2059.003
316.8308 2055.745
317.3130 2022.530
317.7951 1993.524
318.2772 1978.076
318.7593 1974.642
319.2414 1980.825
319.7235 2006.886
320.2057 2035.120
320.6878 2053.684
321.1699 2054.120
321.6520 2054.421
322.1341 2046.619
322.6162 2033.865
323.0984 2048.867
323.5805 2130.789
324.0626 2226.181
324.5447 2300.189
325.0268 2327.921
325.5089 2362.680
325.9911 2411.719
326.4732 2471.852
326.9553 2527.602
327.4374 2562.805
327.9195 2602.929
328.4016 2663.223
328.8838 2776.298
329.3659 2867.474
329.8480 2923.061
330.3301 2948.301
330.8122 2980.786
331.2943 3021.968
331.7765 3069.848
332.2586 3124.774
332.7407 3200.963
333.2228 3254.483
333.7049 3273.675
334.1870 3272.713
334.6692 3302.006
335.1513 3374.465
335.6334 3451.918
336.1155 3509.683
336.5976 3536.259
337.0797 3582.915
337.5619 3658.432
338.0440 3752.922
338.5261 3838.512
339.0082 3916.932
339.4903 3980.071
339.9724 4011.913
340.4546 4005.395
340.9367 4031.217
341.4188 4096.048
341.9009 4191.829
342.3830 4307.191
342.8651 4443.352
343.3473 4585.544
343.8294 4723.812
344.3115 4860.471
344.7936 5002.691
345.2757 5151.396
345.7578 5309.291
346.2400 5481.908
346.7221 5667.737
347.2042 5872.871
347.6863 6108.328
348.1684 6366.922
348.6505 6624.367
349.1327 6880.305
349.6148 7147.361
350.0969 7443.249
350.5790 7765.893
351.0611 8103.400
351.5432 8451.442
352.0254 8808.098
352.5075 9176.360
352.9896 9553.919
353.4717 9940.404
353.9538 10320.20
354.4359 10709.41
354.9181 11128.42
355.4002 11615.19
355.8823 12119.52
356.3644 12587.61
356.8465 13018.49
357.3286 13459.08
357.8108 13938.84
358.2929 14451.64
358.7750 14998.84
359.2571 15604.01
359.7392 16225.39
360.2213 16849.39
360.7035 17474.29
361.1856 18081.94
361.6677 18686.33
362.1498 19256.55
362.6319 19772.63
363.1140 20236.53
363.5962 20634.76
364.0783 20990.99
364.5604 21293.77
365.0425 21458.83
365.5246 21414.82
366.0067 21259.99
366.4889 21056.26
366.9710 20895.12
367.4531 20589.08
367.9352 20072.70
368.4173 19380.93
368.8994 18669.13
369.3815 17965.41
369.8636 17230.82
370.3458 16454.50
370.8279 15590.22
371.3100 14742.95
371.7921 13902.27
372.2742 13079.97
372.7563 12301.89
373.2385 11582.76
373.7206 10893.50
374.2027 10228.26
374.6848 9588.306
375.1669 8972.714
375.6490 8381.742
376.1312 7808.458
376.6133 7270.086
377.0954 6734.149
377.5775 6229.443
378.0596 5748.606
378.5417 5300.592
379.0239 4919.047
379.5060 4615.291
379.9881 4354.137
380.4702 4102.100
380.9523 3857.248
381.4344 3626.159
381.9166 3406.943
382.3987 3202.963
382.8808 3013.573
383.3629 2840.413
383.8450 2677.896
384.3271 2529.341
384.8093 2389.020
385.2914 2241.898
385.7735 2073.972
386.2556 1907.645
386.7377 1787.941
387.2198 1709.358
387.7020 1625.248
388.1841 1485.691
388.6662 1327.490
389.1483 1199.469
389.6304 1124.029
390.1125 1067.140
390.5947 1004.865
391.0768 939.8945
391.5589 881.8184
392.0410 840.5410
392.5231 805.2637
393.0052 766.9375
393.4874 721.2090
393.9695 679.8594
394.4516 655.2070
394.9337 636.7129
395.4158 605.1465
395.8979 541.9893
396.3801 475.3076
396.8622 415.8135
397.3443 364.8359
397.8264 318.0049
398.3085 261.5713
398.7906 213.4551
399.2728 196.4844
399.7549 254.5000
400.2370 295.0713
400.7191 300.4492
401.2012 269.3115
401.6833 222.7500
402.1655 143.1318
402.6476 66.62109
403.1297 27.37305
403.6118 42.14160
404.0939 56.20508
404.5760 63.75293
405.0582 62.04688
405.5403 44.48047
406.0224 4.296875
406.5045 27.69824
406.9866 22.65820
407.4688 22.53418
407.9509 48.52539
408.4330 44.44922
408.9151 22.41895
409.3972 4.935547
409.8793 7.271484
410.3615 10.08984
410.8436 6.764648
411.3257 35.53320
411.8078 48.07812
412.2899 40.99414
412.7720 25.92969
413.2542 12.03906
413.7363 0.9121090
414.2184 3.057617
414.7005 13.87793
415.1826 33.31543
415.6647 30.48926
416.1469 4.416992
416.6290 24.83789
417.1111 45.26953
417.5932 59.87109
418.0753 71.87793
418.5574 86.37988
419.0396 95.89258
419.5217 97.44141
420.0038 91.14844
420.4859 77.33984
420.9680 42.45020
421.4501 8.178711
421.9323 9.836914
422.4144 2.290039
422.8965 11.03516
423.3786 27.85645
423.8607 47.48047
424.3428 68.57910
424.8250 108.1533
425.3071 132.9834
425.7892 127.3721
426.2713 71.81641
426.7534 38.44922
427.2355 42.91211
427.7177 60.00684
428.1998 48.94434
428.6819 10.00293
429.1640 50.83691
429.6461 48.52148
430.1282 3.833008
430.6104 24.04590
431.0925 34.16602
431.5746 31.47559
432.0567 15.17188
432.5388 15.18359
433.0209 34.63574
433.5031 34.36816
433.9852 22.93359
434.4673 18.98633
434.9494 22.72754
435.4315 35.64746
435.9136 72.19922
436.3958 119.1074
436.8779 139.6611
437.3600 124.2715
437.8421 94.85742
438.3242 66.53906
438.8063 42.49805
439.2885 31.42871
439.7706 48.18262
440.2527 73.72070
440.7348 90.04492
441.2169 94.88477
441.6990 99.28027
442.1812 107.2412
442.6633 118.6768
443.1454 133.6904
443.6275 167.4580
444.1096 189.5820
444.5917 176.0020
445.0739 130.6582
445.5560 111.2012
446.0381 151.4697
446.5202 205.7041
447.0023 247.1074
447.4844 273.1562
447.9666 287.3711
448.4487 284.3828
448.9308 270.3613
449.4129 261.6660
449.8950 260.3369
450.3771 261.5146
450.8592 262.8389
451.3413 263.3398
451.8235 269.8389
452.3056 282.4854
452.7877 301.1396
453.2698 336.3623
453.7519 392.1660
454.2340 412.5371
454.7162 362.1992
455.1983 268.0732
455.6804 229.6631
456.1625 249.2588
456.6446 282.7324
457.1267 309.0527
457.6089 320.4766
458.0910 289.5146
458.5731 190.5625
459.0552 84.14746
459.5373 54.93262
460.0194 82.79492
460.5016 100.6289
460.9837 50.77148
461.4658 14.89551
461.9479 47.26855
462.4300 35.52246
462.9121 20.12207
463.3943 20.62695
463.8764 29.84473
464.3585 39.93848
464.8406 53.13281
465.3227 57.29590
465.8048 50.39453
466.2870 32.36035
466.7691 6.181641
467.2512 42.46777
467.7333 88.54199
468.2154 115.2637
468.6975 85.28320
469.1797 102.6953
469.6618 204.7637
470.1439 347.0713
470.6260 401.4150
471.1081 327.1084
471.5902 262.3467
472.0724 276.3984
472.5545 377.2988
473.0366 434.1953
473.5187 435.9258
474.0008 421.2666
474.4829 441.4141
474.9651 493.4375
475.4472 534.5977
475.9293 545.0049
476.4114 541.5059
476.8935 559.8691
477.3756 599.3525
477.8578 645.6055
478.3399 689.5996
478.8220 735.0859
479.3041 782.9434
479.7862 827.2676
480.2683 885.0762
480.7505 993.6973
481.2326 1125.070
481.7147 1221.001
482.1968 1213.050
482.6789 1199.033
483.1610 1219.413
483.6432 1276.522
484.1253 1397.618
484.6074 1699.885
485.0895 2005.665
485.5716 2164.188
486.0537 1990.599
486.5359 1878.827
487.0180 1873.460
487.5001 1953.877
487.9822 2032.705
488.4643 2119.941
488.9464 2188.430
489.4286 2213.253
489.9107 2176.847
490.3928 2206.078
490.8749 2324.439
491.3570 2465.436
491.8391 2528.554
492.3213 2514.104
492.8034 2492.233
493.2855 2486.101
493.7676 2490.873
494.2497 2497.053
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1261.297 76.23242
1261.779 62.62695
1262.261 55.18555
1262.743 61.33789
1263.226 92.55859
1263.708 86.09766
1264.190 34.87500
1264.672 0.3261720
1265.154 0.0000000E+00
