#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:47:37 +0300 (Thu, 24 May 2018) $
#$Revision: 775 $
#$URL: svn://172.16.1.111/rod/cif/1/00/02/1000273.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000273
loop_
_publ_author_name
'Rozhdestvenskaya, I. V.'
'Bannova, I. I.'
'Nikishova, L. V.'
'Soboleva, T. V.'
_publ_section_title
;
 The crystal structure of fenaksite K2Na2Fe2Si8O20 Locality: synthetic
;
_journal_name_full               'Doklady Earth Sciences'
_journal_page_first              1029
_journal_page_last               1033
_journal_volume                  398
_journal_year                    2004
_chemical_compound_source        R080135
_chemical_formula_sum            'Fe K Na O10 Si4'
_chemical_name_mineral           Fenaksite
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                100.21
_cell_angle_beta                 114.13
_cell_angle_gamma                105.87
_cell_length_a                   8.142
_cell_length_b                   9.954
_cell_length_c                   6.983
_cell_volume                     469.098
_exptl_crystal_density_diffrn    2.763
_cod_original_formula_sum        'K Na Fe Si4 O10'
_cod_database_code               9012902
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R080135.rod
_rod_data_source.block           3500000
_rod_database.code               1000273
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9012902 COD http://www.crystallography.net/cod/9012902.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
115.1136 0.0000000E+00
115.5958 0.1648940
116.0779 0.2567440
116.5600 0.6575390
117.0421 2.363937
117.5242 4.603333
118.0063 7.363907
118.4885 10.74307
118.9706 14.74684
119.4527 18.99467
119.9348 23.15038
120.4169 27.33961
120.8990 31.92645
121.3812 37.42136
121.8633 43.17912
122.3454 48.58653
122.8275 53.68896
123.3096 58.17905
123.7917 61.50462
124.2739 63.88547
124.7560 66.13597
125.2381 69.19925
125.7202 72.42091
126.2023 74.59543
126.6844 75.30074
127.1666 75.10219
127.6487 74.75276
128.1308 74.23558
128.6129 73.30212
129.0950 71.22879
129.5771 68.43513
130.0593 66.47430
130.5414 66.11586
131.0235 66.76001
131.5056 66.78342
131.9877 65.30553
132.4698 62.32108
132.9520 59.16223
133.4341 55.82602
133.9162 51.96725
134.3983 47.20314
134.8804 41.73434
135.3625 36.92964
135.8447 32.81465
136.3268 29.24760
136.8089 26.05632
137.2910 23.26373
137.7731 20.55032
138.2552 17.62941
138.7374 14.39445
139.2195 11.93161
139.7016 10.42955
140.1837 9.464905
140.6658 8.039398
141.1479 5.706589
141.6301 3.895065
142.1122 3.410416
142.5943 4.920044
143.0764 5.862427
143.5585 5.889603
144.0406 5.337601
144.5228 5.457443
145.0049 6.544830
145.4870 7.917831
145.9691 9.232620
146.4512 10.85069
146.9333 11.85287
147.4155 11.82353
147.8976 10.94205
148.3797 10.83824
148.8618 12.15186
149.3439 13.86887
149.8260 15.39134
150.3082 16.38928
150.7903 17.55524
151.2724 18.67992
151.7545 19.76892
152.2366 20.77707
152.7188 21.15523
153.2009 21.79622
153.6830 23.36580
154.1651 27.04736
154.6472 30.55768
155.1293 33.28322
155.6115 35.14830
156.0936 36.87512
156.5757 38.43497
157.0578 40.19890
157.5399 42.42131
158.0220 45.02579
158.5042 47.68971
158.9863 50.63477
159.4684 53.79092
159.9505 56.42532
160.4326 57.81525
160.9147 58.68109
161.3969 60.09161
161.8790 62.80847
162.3611 65.88304
162.8432 68.85016
163.3253 71.60281
163.8074 74.27026
164.2896 76.80069
164.7717 79.27686
165.2538 81.86627
165.7359 84.29327
166.2180 87.05011
166.7001 90.66922
167.1823 95.60130
167.6644 100.4752
168.1465 104.4527
168.6286 107.6796
169.1107 110.5666
169.5928 113.9478
170.0750 116.8470
170.5571 118.2410
171.0392 117.5436
171.5213 115.8614
172.0034 114.5032
172.4855 113.1304
172.9677 110.0031
173.4498 103.5247
173.9319 95.24414
174.4140 87.37871
174.8961 80.83124
175.3782 74.53018
175.8604 66.67899
176.3425 57.46837
176.8246 48.82625
177.3067 42.43381
177.7888 37.53911
178.2709 32.67572
178.7531 27.06604
179.2352 21.46902
179.7173 17.06195
180.1994 13.79623
180.6815 11.03912
181.1636 8.287170
181.6458 5.606628
182.1279 3.272079
182.6100 1.374817
183.0921 0.1387180
183.5742 1.341171
184.0563 2.211700
184.5385 2.964218
185.0206 3.971680
185.5027 5.114197
185.9848 5.773239
186.4669 5.560547
186.9490 4.731781
187.4312 3.999069
187.9133 3.395035
188.3954 2.815506
188.8775 2.199402
189.3596 1.545822
189.8417 0.7770230
190.3239 0.2361300
190.8060 1.417740
191.2881 2.298782
191.7702 2.841263
192.2523 3.194733
192.7344 3.577682
193.2166 3.988617
193.6987 4.236053
194.1808 4.290024
194.6629 4.140488
195.1450 3.618057
195.6271 2.642456
196.1093 1.501526
196.5914 0.6522980
197.0735 0.1224520
197.5556 0.4740600
198.0377 1.363571
198.5198 2.555679
199.0020 3.641068
199.4841 4.711975
199.9662 5.522919
200.4483 5.539215
200.9304 4.632553
201.4125 3.724899
201.8947 3.397614
202.3768 3.751968
202.8589 3.309631
203.3410 1.822449
203.8231 0.1547850
204.3052 1.594849
204.7874 2.458801
205.2695 3.014557
205.7516 3.259979
206.2337 3.102386
206.7158 3.314117
207.1979 4.033386
207.6801 5.000397
208.1622 5.551117
208.6443 5.455750
209.1264 5.664978
209.6085 6.750061
210.0906 8.978577
210.5728 10.81513
211.0549 12.01175
211.5370 12.95752
212.0191 14.52249
212.5012 16.88345
212.9833 19.46603
213.4655 21.83383
213.9476 23.67618
214.4297 26.59393
214.9118 31.01434
215.3939 36.31552
215.8760 41.10172
216.3581 45.19998
216.8403 49.05435
217.3224 52.71274
217.8045 55.94998
218.2866 59.80054
218.7687 64.44968
219.2508 69.64197
219.7330 74.47818
220.2151 78.55927
220.6972 82.98062
221.1793 88.29022
221.6614 94.95035
222.1435 101.3126
222.6257 107.1617
223.1078 112.7614
223.5899 119.0735
224.0720 126.5023
224.5541 134.0349
225.0362 141.4119
225.5184 148.6857
226.0005 155.5114
226.4826 161.7420
226.9647 167.5876
227.4468 174.0493
227.9289 182.1915
228.4111 189.2625
228.8932 193.9224
229.3753 195.4388
229.8574 196.3659
230.3395 197.1378
230.8216 197.2557
231.3038 195.2564
231.7859 190.6754
232.2680 184.6579
232.7501 177.6414
233.2322 169.4412
233.7143 160.6324
234.1965 150.8488
234.6786 140.4711
235.1607 130.4192
235.6428 120.6336
236.1249 111.2437
236.6070 102.3478
237.0892 94.17737
237.5713 85.91138
238.0534 77.10043
238.5355 68.30710
239.0176 61.04153
239.4997 55.68091
239.9819 51.17657
240.4640 47.15726
240.9461 43.64001
241.4282 40.44919
241.9103 37.54559
242.3924 34.99283
242.8746 32.90231
243.3567 31.19418
243.8388 30.07962
244.3209 29.72928
244.8030 30.39777
245.2851 31.24496
245.7673 32.25400
246.2494 33.44510
246.7315 34.82159
247.2136 36.19009
247.6957 38.06027
248.1778 40.70370
248.6600 44.31622
249.1421 47.94589
249.6242 51.51431
250.1063 55.25122
250.5884 59.47427
251.0705 64.13983
251.5527 69.22070
252.0348 74.75510
252.5169 81.02667
252.9990 86.93637
253.4811 92.53275
253.9632 97.82224
254.4454 102.6383
254.9275 106.6368
255.4096 110.8503
255.8917 115.7032
256.3738 121.3375
256.8560 126.7690
257.3381 132.0790
257.8202 137.1701
258.3023 142.0351
258.7844 146.6947
259.2665 151.0782
259.7487 155.0609
260.2308 158.5038
260.7129 162.1859
261.1950 166.1021
261.6771 170.3222
262.1592 174.9359
262.6414 180.0680
263.1235 185.1522
263.6056 189.8821
264.0877 194.2457
264.5698 199.1925
265.0519 205.1250
265.5341 211.0724
266.0162 215.8984
266.4983 219.2917
266.9804 222.3962
267.4625 225.3799
267.9446 228.2271
268.4268 231.7404
268.9089 236.2435
269.3910 240.7231
269.8731 244.0517
270.3552 245.9228
270.8373 247.8128
271.3195 250.2007
271.8016 252.9663
272.2837 255.1011
272.7658 256.7897
273.2479 257.4629
273.7300 256.3717
274.2122 253.2684
274.6943 250.0349
275.1764 247.1572
275.6585 244.4637
276.1406 240.8992
276.6227 236.2550
277.1049 231.4472
277.5870 226.9602
278.0691 222.7250
278.5512 219.6727
279.0333 218.1055
279.5154 217.7439
279.9976 217.5014
280.4797 217.2459
280.9618 217.9781
281.4439 220.6663
281.9260 225.3383
282.4081 230.3378
282.8903 235.4846
283.3724 240.8361
283.8545 246.4828
284.3366 252.3636
284.8187 258.6889
285.3008 265.9592
285.7830 274.0774
286.2651 281.2777
286.7472 287.4622
287.2293 292.5818
287.7114 296.8057
288.1935 300.1260
288.6757 301.6132
289.1578 300.8485
289.6399 297.7963
290.1220 292.3604
290.6041 284.4524
291.0862 274.3961
291.5684 262.3003
292.0505 248.1958
292.5326 233.0987
293.0147 216.6986
293.4968 199.6323
293.9789 183.1649
294.4611 167.4835
294.9432 152.5197
295.4253 138.2197
295.9074 124.5720
296.3895 111.8696
296.8716 100.1081
297.3538 89.28378
297.8359 79.34421
298.3180 70.20613
298.8001 61.87924
299.2822 54.34047
299.7643 47.49918
300.2465 41.23633
300.7286 35.58548
301.2107 30.44699
301.6928 25.53555
302.1749 20.91263
302.6570 16.83360
303.1392 13.70645
303.6213 11.26575
304.1034 9.137131
304.5855 7.193756
305.0676 5.505142
305.5497 4.184982
306.0319 3.187729
306.5140 2.200653
306.9961 0.7011260
307.4782 0.7710720
307.9603 1.563080
308.4424 1.381638
308.9246 0.7429200
309.4067 0.1395420
309.8888 1.183853
310.3709 2.173920
310.8530 2.888046
311.3351 3.544449
311.8173 4.312546
312.2994 5.217468
312.7815 6.263977
313.2636 7.471008
313.7457 8.811859
314.2278 10.25121
314.7100 11.57503
315.1921 13.13037
315.6742 15.20015
316.1563 17.87367
316.6384 20.64607
317.1205 23.35588
317.6027 25.98814
318.0848 28.50909
318.5669 30.85910
319.0490 33.13866
319.5311 35.25491
320.0132 37.18715
320.4954 39.50308
320.9775 42.54135
321.4596 45.92584
321.9417 49.29701
322.4238 52.54019
322.9059 55.80606
323.3881 59.34360
323.8702 63.05899
324.3523 66.20490
324.8344 68.59048
325.3165 70.42871
325.7986 71.87003
326.2808 72.84555
326.7629 73.52557
327.2450 74.23383
327.7271 74.73825
328.2092 74.12094
328.6913 71.64629
329.1735 68.69505
329.6556 65.78902
330.1377 63.27411
330.6198 60.13744
331.1019 56.22394
331.5840 51.74069
332.0662 46.93903
332.5483 41.42296
333.0304 36.10538
333.5125 31.38055
333.9946 27.26352
334.4767 23.32822
334.9589 19.48639
335.4410 15.95950
335.9231 13.11955
336.4052 11.25311
336.8873 9.381790
337.3694 7.222687
337.8516 4.820740
338.3336 2.838028
338.8158 1.416458
339.2979 0.1131900
339.7800 1.654739
340.2621 4.025070
340.7442 5.734940
341.2263 6.363007
341.7085 6.254486
342.1906 6.573822
342.6727 7.403549
343.1548 8.164673
343.6369 8.387329
344.1190 8.108643
344.6012 8.022354
345.0833 8.307465
345.5654 8.614609
346.0475 8.252838
346.5296 7.260361
347.0117 6.166183
347.4939 5.270615
347.9760 4.508987
348.4581 3.662964
348.9402 2.722336
349.4223 1.710373
349.9044 0.7447660
350.3866 0.2635500
350.8687 1.623154
351.3508 3.695526
351.8329 6.107040
352.3150 8.333191
352.7971 10.38463
353.2793 12.28737
353.7614 13.99664
354.2435 15.62218
354.7256 17.34383
355.2077 19.16736
355.6898 21.15329
356.1720 23.52429
356.6541 26.18228
357.1362 28.69002
357.6183 30.59164
358.1004 32.36559
358.5826 34.46069
359.0647 37.04416
359.5468 39.73749
360.0289 42.21028
360.5110 44.65628
360.9931 47.45605
361.4753 50.92624
361.9574 54.61702
362.4395 58.32333
362.9216 62.02782
363.4037 65.73224
363.8858 69.16428
364.3680 72.70004
364.8501 76.72974
365.3322 81.73721
365.8143 86.73917
366.2964 91.62119
366.7785 96.42233
367.2607 101.0208
367.7428 105.0732
368.2249 109.1564
368.7070 113.6515
369.1891 119.4285
369.6712 124.4032
370.1534 128.5159
370.6355 131.8054
371.1176 134.4135
371.5997 136.5222
372.0818 137.6916
372.5639 137.6689
373.0461 136.1540
373.5282 134.3390
374.0103 132.1460
374.4924 129.6772
374.9745 127.0369
375.4566 124.0572
375.9388 121.3899
376.4209 119.3299
376.9030 117.8158
377.3851 116.0611
377.8672 113.8402
378.3493 112.0396
378.8315 111.7383
379.3136 112.9679
379.7957 114.0994
380.2778 114.7195
380.7599 115.1931
381.2420 116.5333
381.7242 118.7164
382.2063 121.0565
382.6884 123.1508
383.1705 125.0291
383.6526 126.6754
384.1347 128.0269
384.6169 129.3486
385.0990 131.2264
385.5811 133.3947
386.0632 134.9113
386.5453 135.4621
387.0274 135.0571
387.5096 133.6353
387.9917 131.2130
388.4738 127.9845
388.9559 124.1923
389.4380 119.7417
389.9201 114.4124
390.4023 107.6541
390.8844 100.6241
391.3665 93.97072
391.8486 87.62500
392.3307 81.56439
392.8128 76.05814
393.2950 70.63898
393.7771 64.81242
394.2592 58.16840
394.7413 52.04732
395.2234 46.89676
395.7055 42.54346
396.1877 38.75427
396.6698 35.69637
397.1519 32.96889
397.6340 30.35921
398.1161 27.79936
398.5982 25.61426
399.0804 24.05009
399.5625 22.89476
400.0446 21.94531
400.5267 21.22180
401.0088 20.60304
401.4909 19.97784
401.9731 19.50694
402.4552 19.74916
402.9373 20.99104
403.4194 22.42035
403.9015 23.58102
404.3836 24.21928
404.8658 25.91475
405.3479 28.96945
405.8300 32.59573
406.3121 35.53088
406.7942 37.60536
407.2763 40.21506
407.7585 43.93083
408.2406 48.57704
408.7227 53.07025
409.2048 57.36832
409.6869 61.61624
410.1690 65.84183
410.6512 70.03641
411.1333 74.50740
411.6154 79.45004
412.0975 84.44980
412.5796 89.05356
413.0617 93.25298
413.5439 97.09290
414.0260 100.7093
414.5081 104.0132
414.9902 106.6263
415.4723 108.4625
415.9544 110.4183
416.4366 113.6648
416.9187 117.4025
417.4008 120.4043
417.8829 121.1257
418.3650 121.8705
418.8471 124.2646
419.3293 127.9956
419.8114 131.3937
420.2935 133.3611
420.7756 134.9983
421.2577 137.1418
421.7398 140.7473
422.2220 143.2839
422.7041 143.6943
423.1862 142.8358
423.6683 142.1815
424.1504 142.2206
424.6325 142.1633
425.1147 141.9220
425.5968 141.5482
426.0789 140.4544
426.5610 137.9030
427.0431 135.3001
427.5252 133.8186
428.0074 133.7702
428.4895 134.1156
428.9716 134.7459
429.4537 135.6887
429.9358 136.9337
430.4179 138.3321
430.9001 140.5153
431.3822 143.9068
431.8643 148.5193
432.3464 153.4675
432.8285 158.7481
433.3106 164.3699
433.7928 170.0544
434.2749 175.9199
434.7570 183.0105
435.2391 191.8817
435.7212 201.9888
436.2033 212.4347
436.6855 223.1375
437.1676 234.1643
437.6497 245.7270
438.1318 257.5732
438.6139 269.4626
439.0960 281.5273
439.5782 293.0110
440.0603 303.7825
440.5424 313.5296
441.0245 321.5182
441.5066 328.7747
441.9887 333.2041
442.4709 333.6229
442.9530 330.0082
443.4351 322.9565
443.9172 312.0002
444.3993 298.1140
444.8814 282.0927
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