#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:47:49 +0300 (Thu, 24 May 2018) $
#$Revision: 778 $
#$URL: svn://172.16.1.111/rod/cif/1/00/02/1000276.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000276
loop_
_publ_author_name
'Bonazzi, P.'
'Keutsch, F. N.'
'Bindi, L.'
_publ_section_title
;
 Manganoquadratite, AgMnAsS3, a new manganese-bearing sulfosalt from the
 Uchucchacua polymetallic deposit, Lima Department, Peru: Description and
 crystal structure
;
_journal_name_full               'American Mineralogist'
_journal_page_first              1199
_journal_page_last               1205
_journal_paper_doi               10.2138/am.2012.4004
_journal_volume                  97
_journal_year                    2012
_chemical_compound_source
'Uchucchacua polymetallic deposit, Lima Department, Peru'
_chemical_formula_sum            'Ag As Mn S3'
_chemical_name_mineral           Manganoquadratite
_space_group_IT_number           95
_symmetry_space_group_name_Hall  'P 4cw 2c'
_symmetry_space_group_name_H-M   'P 43 2 2'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   5.4496
_cell_length_b                   5.4496
_cell_length_c                   32.949
_cell_volume                     978.524
_exptl_crystal_density_diffrn    4.533
_cod_original_formula_sum        'Ag Mn As S3'
_cod_database_code               9014926
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R090021.rod
_rod_data_source.block           3500000
_rod_database.code               1000276
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9014926 COD http://www.crystallography.net/cod/9014926.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
194.0990 0.0000000E+00
194.5811 2.450195
195.0633 2.853027
195.5454 7.397461
196.0275 13.98193
196.5096 24.80908
196.9917 43.54688
197.4738 50.72705
197.9560 44.55762
198.4381 26.07080
198.9202 14.94482
199.4023 11.37891
199.8844 13.72363
200.3665 19.22559
200.8487 30.02002
201.3308 40.70947
201.8129 45.23047
202.2950 37.81641
202.7771 31.89453
203.2592 31.24170
203.7414 36.50684
204.2235 38.69287
204.7056 42.99512
205.1877 46.79395
205.6698 45.56299
206.1519 42.14258
206.6341 38.94531
207.1162 33.93506
207.5983 25.89209
208.0804 19.06836
208.5625 15.72949
209.0446 14.93652
209.5268 15.48877
210.0089 20.91748
210.4910 25.02100
210.9731 27.55908
211.4552 28.29053
211.9373 24.53271
212.4195 15.94336
212.9016 8.677734
213.3837 6.618164
213.8658 11.28125
214.3479 12.41016
214.8300 8.335449
215.3121 1.682617
215.7943 0.8403320
216.2764 2.137207
216.7585 6.078125
217.2406 9.638672
217.7227 13.71387
218.2048 13.17725
218.6870 4.835449
219.1691 6.710449
219.6512 9.465332
220.1333 2.083984
220.6154 12.18896
221.0975 13.81006
221.5797 3.585938
222.0618 5.660645
222.5439 14.48438
223.0260 21.93945
223.5081 25.45410
223.9902 22.56592
224.4724 19.73389
224.9545 20.07031
225.4366 25.21143
225.9187 28.06445
226.4008 27.75781
226.8829 25.42480
227.3651 23.68750
227.8472 23.56299
228.3293 22.21680
228.8114 18.25928
229.2935 10.62500
229.7757 3.763672
230.2578 3.151855
230.7399 8.619141
231.2220 9.158203
231.7041 0.5751950
232.1862 6.529297
232.6684 8.455566
233.1505 4.376465
233.6326 2.320313
234.1147 13.26562
234.5968 25.93506
235.0789 35.31641
235.5611 39.82520
236.0432 43.65967
236.5253 49.08105
237.0074 57.91357
237.4895 60.69238
237.9716 53.48291
238.4538 42.68896
238.9359 38.95801
239.4180 46.36084
239.9001 54.28516
240.3822 58.96240
240.8643 58.74023
241.3465 62.72803
241.8286 72.07227
242.3107 84.77246
242.7928 98.63477
243.2749 116.4233
243.7570 130.4551
244.2392 137.8452
244.7213 137.3784
245.2034 137.6758
245.6855 138.6357
246.1676 140.5156
246.6497 143.5220
247.1319 147.1299
247.6140 153.0566
248.0961 162.3711
248.5782 175.6611
249.0603 187.8467
249.5424 198.1602
250.0246 208.3682
250.5067 220.9321
250.9888 237.8140
251.4709 253.0977
251.9530 263.3032
252.4351 268.9243
252.9173 280.0249
253.3994 299.7144
253.8815 321.3374
254.3636 338.5015
254.8457 349.4756
255.3278 358.4985
255.8100 363.8403
256.2921 365.8506
256.7742 379.0615
257.2563 409.8330
257.7384 443.2622
258.2205 465.8701
258.7026 473.9233
259.1848 480.6943
259.6669 486.4473
260.1490 492.1147
260.6311 505.3872
261.1132 530.4048
261.5953 556.4834
262.0775 574.0664
262.5596 578.5137
263.0417 588.8228
263.5238 608.0859
264.0059 634.8276
264.4880 664.0278
264.9702 697.2642
265.4523 729.1377
265.9344 755.7939
266.4165 776.2490
266.8986 794.9761
267.3807 810.7490
267.8629 826.0039
268.3450 849.9419
268.8271 886.8350
269.3092 922.7314
269.7913 949.1768
270.2734 962.8960
270.7556 982.7886
271.2377 1012.334
271.7198 1047.622
272.2019 1077.570
272.6840 1099.393
273.1661 1125.138
273.6483 1163.530
274.1304 1217.144
274.6125 1262.112
275.0946 1294.676
275.5767 1322.132
276.0588 1359.149
276.5410 1407.792
277.0231 1453.218
277.5052 1485.454
277.9873 1504.551
278.4694 1534.841
278.9515 1578.197
279.4337 1628.113
279.9158 1676.862
280.3979 1724.301
280.8800 1768.472
281.3621 1806.512
281.8442 1839.716
282.3264 1877.385
282.8085 1920.830
283.2906 1964.134
283.7727 2000.594
284.2548 2030.390
284.7369 2057.843
285.2191 2082.889
285.7012 2106.642
286.1833 2135.903
286.6654 2171.537
287.1475 2207.734
287.6296 2236.402
288.1118 2258.628
288.5939 2285.591
289.0760 2321.690
289.5581 2362.570
290.0402 2398.512
290.5223 2429.543
291.0045 2458.080
291.4866 2484.187
291.9687 2508.917
292.4508 2538.946
292.9329 2578.645
293.4150 2619.420
293.8972 2645.832
294.3793 2659.006
294.8614 2671.232
295.3435 2689.863
295.8256 2713.856
296.3077 2740.733
296.7899 2770.615
297.2720 2801.627
297.7541 2832.057
298.2362 2861.357
298.7183 2887.643
299.2004 2908.496
299.6826 2925.689
300.1647 2942.477
300.6468 2958.698
301.1289 2975.544
301.6110 2995.132
302.0931 3016.334
302.5753 3036.950
303.0574 3056.532
303.5395 3074.470
304.0216 3087.950
304.5037 3096.924
304.9858 3107.812
305.4680 3133.331
305.9501 3163.659
306.4322 3181.640
306.9143 3168.544
307.3964 3149.989
307.8785 3153.731
308.3607 3177.344
308.8428 3196.936
309.3249 3195.062
309.8070 3180.965
310.2891 3165.005
310.7712 3147.153
311.2534 3131.572
311.7355 3124.445
312.2176 3122.839
312.6997 3116.336
313.1818 3095.717
313.6639 3069.928
314.1461 3046.428
314.6282 3029.213
315.1103 3009.252
315.5924 2980.346
316.0745 2945.581
316.5566 2910.842
317.0388 2881.251
317.5209 2850.857
318.0030 2817.303
318.4851 2781.621
318.9672 2737.642
319.4493 2678.869
319.9315 2612.116
320.4136 2545.496
320.8957 2477.357
321.3778 2414.048
321.8599 2358.577
322.3420 2311.594
322.8242 2265.890
323.3063 2224.271
323.7884 2181.593
324.2705 2133.398
324.7526 2070.117
325.2347 2008.932
325.7169 1955.094
326.1990 1908.087
326.6811 1862.116
327.1632 1816.679
327.6453 1771.299
328.1274 1725.862
328.6096 1680.490
329.0917 1636.070
329.5738 1590.971
330.0559 1546.612
330.5380 1508.152
331.0201 1480.309
331.5023 1453.419
331.9844 1422.933
332.4665 1385.458
332.9486 1353.142
333.4307 1327.812
333.9128 1307.214
334.3950 1287.804
334.8771 1269.176
335.3592 1250.754
335.8413 1232.039
336.3234 1212.547
336.8055 1198.044
337.2877 1190.312
337.7698 1186.883
338.2519 1184.384
338.7340 1182.710
339.2161 1177.341
339.6982 1164.999
340.1803 1148.499
340.6624 1146.083
341.1446 1161.579
341.6267 1177.843
342.1088 1180.365
342.5909 1168.891
343.0730 1161.370
343.5551 1160.565
344.0373 1163.412
344.5194 1163.680
345.0015 1161.354
345.4836 1162.510
345.9657 1170.651
346.4478 1184.864
346.9300 1203.262
347.4121 1227.410
347.8942 1250.911
348.3763 1263.669
348.8584 1267.313
349.3405 1271.532
349.8227 1283.664
350.3048 1298.767
350.7869 1307.061
351.2690 1308.659
351.7511 1305.319
352.2332 1296.792
352.7154 1284.530
353.1975 1271.894
353.6796 1261.729
354.1617 1249.745
354.6438 1230.579
355.1259 1204.645
355.6081 1175.553
356.0902 1146.109
356.5723 1114.389
357.0544 1077.459
357.5365 1033.792
358.0186 986.3042
358.5008 935.3530
358.9829 882.3921
359.4650 830.4487
359.9471 778.5928
360.4292 730.0234
360.9113 687.9238
361.3935 653.9517
361.8756 619.3394
362.3577 577.9849
362.8398 535.0845
363.3219 496.6611
363.8040 469.7275
364.2862 442.7432
364.7683 411.0044
365.2504 374.6533
365.7325 340.8647
366.2146 310.1782
366.6967 282.7354
367.1789 258.6880
367.6610 238.0288
368.1431 220.9941
368.6252 211.8901
369.1073 206.7188
369.5894 193.3755
370.0716 161.7798
370.5537 132.3130
371.0358 112.5083
371.5179 106.1714
372.0000 97.51465
372.4821 84.52344
372.9643 70.50537
373.4464 60.47803
373.9285 57.01611
374.4106 52.31543
374.8927 43.37354
375.3748 30.27197
375.8570 21.04736
376.3391 16.32910
376.8212 14.00195
377.3033 13.17383
377.7854 14.43701
378.2675 11.73877
378.7497 2.824707
379.2318 9.018066
379.7139 14.97949
380.1960 14.45117
380.6781 14.71631
381.1602 22.06543
381.6424 34.66846
382.1245 39.87891
382.6066 35.84668
383.0887 29.73096
383.5708 32.29004
384.0529 41.31006
384.5351 46.88818
385.0172 41.89697
385.4993 32.80322
385.9814 32.28418
386.4635 39.85938
386.9456 47.17725
387.4278 47.09033
387.9099 42.63965
388.3920 38.54639
388.8741 36.20850
389.3562 34.17822
389.8383 30.70410
390.3205 26.48486
390.8026 23.42627
391.2847 25.26465
391.7668 26.87305
392.2489 23.54590
392.7310 13.74561
393.2132 4.733398
393.6953 2.538086
394.1774 6.272461
394.6595 4.222168
395.1416 14.41455
395.6237 29.18994
396.1059 30.46680
396.5880 18.99219
397.0701 9.768066
397.5522 7.715332
398.0343 7.511719
398.5164 6.032227
398.9986 0.2749020
399.4807 3.166504
399.9628 1.335938
400.4449 2.719727
400.9270 1.624023
401.4091 10.28760
401.8913 20.10986
402.3734 22.46240
402.8555 15.03857
403.3376 13.29785
403.8197 19.04590
404.3018 28.33447
404.7840 38.16406
405.2661 50.39990
405.7482 55.68652
406.2303 49.59326
406.7124 35.79053
407.1945 30.04883
407.6767 33.51172
408.1588 39.08691
408.6409 41.75049
409.1230 41.73486
409.6051 43.86523
410.0872 49.32080
410.5694 54.55176
411.0515 52.64795
411.5336 44.91797
412.0157 39.16650
412.4978 41.47559
412.9799 47.32129
413.4621 45.70850
413.9442 36.91699
414.4263 29.88574
414.9084 34.76904
415.3905 45.53174
415.8727 52.39014
416.3548 52.01514
416.8369 48.56348
417.3190 43.78564
417.8011 38.55371
418.2832 35.04248
418.7654 34.25977
419.2475 35.60303
419.7296 39.27197
420.2117 45.83887
420.6938 51.21338
421.1759 52.68359
421.6581 52.52051
422.1402 53.12061
422.6223 55.08691
423.1044 57.77100
423.5865 62.21533
424.0686 67.85107
424.5508 70.57471
425.0329 66.76123
425.5150 62.64600
425.9971 61.19678
426.4792 64.46631
426.9613 66.27344
427.4435 65.82764
427.9256 64.45996
428.4077 63.99219
428.8898 64.00391
429.3719 66.31592
429.8540 73.11426
430.3362 83.67773
430.8183 86.89453
431.3004 80.79541
431.7825 74.27832
432.2646 76.30762
432.7467 86.89697
433.2289 92.45312
433.7110 89.68750
434.1931 83.43311
434.6752 83.39209
435.1573 88.90039
435.6394 92.99805
436.1216 89.79297
436.6036 82.96484
437.0858 80.96094
437.5679 84.00977
438.0500 88.33594
438.5321 91.44336
439.0142 92.91406
439.4963 92.35107
439.9785 90.52051
440.4606 86.89746
440.9427 76.78125
441.4248 63.22559
441.9069 56.35742
442.3890 72.03564
442.8712 89.39062
443.3533 92.59326
443.8354 75.80859
444.3175 62.18262
444.7996 63.10693
445.2817 70.25732
445.7639 74.73389
446.2460 72.78857
446.7281 70.17285
447.2102 68.00537
447.6923 66.12256
448.1744 62.89014
448.6566 54.69678
449.1387 48.31055
449.6208 47.17969
450.1029 53.58984
450.5850 60.13818
451.0671 67.40088
451.5493 73.80811
452.0314 77.46729
452.5135 78.02148
452.9956 76.62256
453.4777 74.45996
453.9598 71.76025
454.4420 65.63916
454.9241 55.56055
455.4062 45.89844
455.8883 39.92188
456.3704 37.37305
456.8525 37.99316
457.3347 42.40869
457.8168 46.40039
458.2989 43.91602
458.7810 36.97510
459.2631 31.21826
459.7452 29.29395
460.2274 28.67969
460.7095 25.72656
461.1916 21.08496
461.6737 18.95850
462.1558 22.19678
462.6379 28.73047
463.1201 37.74170
463.6022 52.31396
464.0843 61.69580
464.5664 58.07861
465.0485 46.95020
465.5306 37.41455
466.0128 31.25098
466.4949 27.18555
466.9770 26.11230
467.4591 28.19873
467.9412 27.58057
468.4233 20.14258
468.9055 13.43311
469.3876 12.20410
469.8697 20.97412
470.3518 25.25635
470.8339 22.91992
471.3160 17.39209
471.7982 14.85889
472.2803 15.56982
472.7624 18.90332
473.2445 26.25293
473.7266 36.10547
474.2087 39.70947
474.6909 36.56738
475.1730 30.78320
475.6551 23.17188
476.1372 14.34619
476.6193 12.05469
477.1014 19.01221
477.5836 29.30762
478.0657 36.69727
478.5478 41.24951
479.0299 43.17822
479.5120 40.97070
479.9941 37.32812
480.4763 34.05029
480.9584 31.35596
481.4405 30.68311
481.9226 35.92871
482.4047 41.73779
482.8868 43.76758
483.3690 39.31982
483.8511 33.92285
484.3332 27.44531
484.8153 21.50342
485.2974 18.59814
485.7795 25.26074
486.2617 28.38232
486.7438 21.64355
487.2259 5.441895
487.7080 1.305176
488.1901 16.03369
488.6722 33.35400
489.1544 43.99414
489.6365 47.00537
490.1186 45.75684
490.6007 38.10254
491.0828 29.68115
491.5649 32.13428
492.0471 46.13477
492.5292 53.43018
493.0113 44.33545
493.4934 26.23340
493.9755 19.64990
494.4576 24.11719
494.9398 30.71484
495.4219 32.89209
495.9040 32.69629
496.3861 34.01904
496.8682 37.67041
497.3503 40.85742
497.8325 42.05127
498.3146 41.14355
498.7967 37.95264
499.2788 30.88672
499.7609 23.05469
500.2430 14.38037
500.7252 5.978027
501.2073 2.674805
501.6894 13.78857
502.1715 24.02441
502.6536 25.29785
503.1357 12.01270
503.6179 4.647949
504.1000 7.123535
504.5821 12.56348
505.0642 13.57080
505.5463 7.012695
506.0284 2.937988
506.5106 3.883789
506.9927 7.721680
507.4748 6.443848
507.9569 1.536133
508.4390 6.957031
508.9211 4.471191
509.4033 5.007813
509.8854 16.01123
510.3675 29.14355
510.8496 38.51953
511.3317 33.61865
511.8138 20.21191
512.2960 15.15918
512.7781 25.85986
513.2602 38.30078
513.7423 35.25928
514.2244 22.40918
514.7065 13.49805
515.1887 20.34277
515.6708 29.31934
516.1529 30.71094
516.6350 24.39160
517.1171 18.89062
517.5992 17.46924
518.0814 17.79980
518.5635 18.28613
519.0456 17.55371
519.5277 19.06982
520.0098 26.84863
520.4919 35.48340
520.9741 35.87354
521.4562 21.29932
521.9383 11.92773
522.4204 13.71777
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1284.165 24.78271
1284.647 29.36670
1285.129 37.93408
1285.611 42.93994
1286.093 35.06006
1286.575 26.74170
1287.057 24.79297
1287.539 24.32568
1288.021 18.33936
1288.504 8.873047
1288.986 10.08398
1289.468 20.19043
1289.950 25.79395
1290.432 14.20605
1290.914 6.861816
1291.396 10.07617
1291.878 14.95264
1292.360 9.352539
1292.843 9.7699999E-04
1293.325 7.666016
1293.807 27.02246
1294.289 38.21631
1294.771 29.04492
1295.253 19.29248
1295.735 8.628418
1296.217 0.9604490
1296.700 1.152832
1297.182 2.208984
1297.664 14.56592
1298.146 31.27441
1298.628 41.87549
1299.110 45.74170
1299.592 46.45117
1300.074 43.74609
1300.557 40.06006
1301.039 40.55957
1301.521 38.47754
1302.003 24.31104
1302.485 6.890625
1302.967 7.9590000E-02
1303.449 0.0000000E+00
