#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:48:14 +0300 (Thu, 24 May 2018) $
#$Revision: 784 $
#$URL: svn://172.16.1.111/rod/cif/1/00/02/1000281.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000281
loop_
_publ_author_name
'Kampf, A. R.'
'Yang, H.'
'Downs, R. T.'
'Pinch, W. W.'
_publ_section_title
;
 The crystal structures and Raman spectra of aravaipaite and
 calcioaravaipaite
;
_journal_name_full               'American Mineralogist'
_journal_page_first              402
_journal_page_last               407
_journal_paper_doi               10.2138/am.2011.3620
_journal_volume                  96
_journal_year                    2011
_chemical_compound_source
'Grand Reef mine, Aravaipa mining district, Arizona, USA'
_chemical_formula_sum            'Al F9 H2 O Pb3'
_chemical_name_mineral           Aravaipaite
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                98.725
_cell_angle_beta                 94.020
_cell_angle_gamma                90.683
_cell_length_a                   5.6637
_cell_length_b                   5.8659
_cell_length_c                   12.7041
_cell_volume                     416.045
_exptl_crystal_density_diffrn    6.686
_cod_original_formula_sum        'Pb3 Al F9 O H2'
_cod_database_code               9014374
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R100004.rod
_rod_data_source.block           3500000
_rod_database.code               1000281
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9014374 COD http://www.crystallography.net/cod/9014374.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
144.9714 0.0000000E+00
145.4535 5.992004
145.9356 5.247528
146.4177 0.9055480
146.8998 2.346954
147.3820 0.1496580
147.8641 3.974060
148.3462 10.43530
148.8283 17.36499
149.3104 23.90442
149.7925 28.68396
150.2747 34.30261
150.7568 41.06842
151.2389 48.76819
151.7210 55.49677
152.2031 60.37201
152.6852 64.54462
153.1674 68.86304
153.6495 72.53314
154.1316 76.99933
154.6137 83.48529
155.0958 92.04449
155.5779 97.94739
156.0601 97.25958
156.5422 95.18878
157.0243 96.12463
157.5064 102.9929
157.9885 110.9220
158.4706 118.6008
158.9528 125.8682
159.4349 133.5602
159.9170 140.7783
160.3991 148.8354
160.8812 159.2542
161.3633 175.5336
161.8455 191.7982
162.3276 205.3340
162.8097 215.1771
163.2918 224.6613
163.7739 234.2105
164.2560 239.8201
164.7382 245.9124
165.2203 249.0376
165.7024 252.5911
166.1845 255.3184
166.6666 257.0564
167.1487 258.1448
167.6309 258.8098
168.1130 259.0399
168.5951 258.7393
169.0772 256.7302
169.5593 254.8107
170.0414 254.7990
170.5236 257.7895
171.0057 260.8473
171.4878 261.5331
171.9699 260.5179
172.4520 259.7635
172.9341 260.6867
173.4163 262.3795
173.8984 263.6479
174.3805 263.7593
174.8626 264.0328
175.3447 266.5089
175.8268 270.6449
176.3090 273.9328
176.7911 274.4857
177.2732 273.0831
177.7553 270.9030
178.2374 268.1281
178.7195 264.8251
179.2017 260.9309
179.6838 256.4728
180.1659 251.8927
180.6480 247.5431
181.1301 243.3214
181.6122 238.9515
182.0944 234.4814
182.5765 229.7386
183.0586 223.9691
183.5407 217.2556
184.0228 210.8752
184.5049 206.4611
184.9871 203.4887
185.4692 200.2639
185.9513 196.8949
186.4334 192.6937
186.9155 184.5552
187.3976 172.0804
187.8798 160.6240
188.3619 156.7180
188.8440 159.3152
189.3261 161.9023
189.8082 162.1980
190.2903 160.8121
190.7725 159.8384
191.2546 159.2692
191.7367 159.1517
192.2188 160.1482
192.7009 162.1581
193.1830 162.8977
193.6652 160.7473
194.1473 156.3264
194.6294 153.8063
195.1115 153.4974
195.5936 154.0317
196.0757 153.5380
196.5579 151.9768
197.0400 150.6401
197.5221 150.2963
198.0042 150.8395
198.4863 150.5458
198.9684 149.2467
199.4506 147.4928
199.9327 146.1537
200.4148 145.2863
200.8969 144.2732
201.3790 142.3391
201.8611 139.3873
202.3433 138.9400
202.8254 140.1565
203.3075 142.3024
203.7896 140.3788
204.2717 133.4930
204.7538 127.1823
205.2360 124.1485
205.7181 124.7716
206.2002 124.3879
206.6823 122.6241
207.1644 120.2807
207.6465 119.0209
208.1287 119.2144
208.6108 119.1960
209.0929 117.9395
209.5750 114.9941
210.0571 113.4520
210.5392 113.8052
211.0214 115.1600
211.5035 115.4418
211.9856 114.0535
212.4677 113.2668
212.9498 114.2013
213.4319 117.1562
213.9140 120.5188
214.3962 124.3408
214.8783 128.5290
215.3604 132.5410
215.8425 135.7762
216.3246 140.2177
216.8067 147.1760
217.2889 157.5089
217.7710 167.0318
218.2531 175.4497
218.7352 183.0914
219.2173 190.8788
219.6994 198.6611
220.1816 206.9033
220.6637 215.9492
221.1458 225.9106
221.6279 236.5557
222.1100 248.5414
222.5921 261.0114
223.0743 271.8593
223.5564 279.9767
224.0385 288.3654
224.5206 298.2798
225.0027 310.4069
225.4848 322.5781
225.9670 334.4271
226.4491 346.3116
226.9312 359.6171
227.4133 375.2520
227.8954 390.7173
228.3775 404.5844
228.8597 416.8975
229.3418 427.9360
229.8239 437.3381
230.3060 445.5350
230.7881 453.4407
231.2702 461.0620
231.7524 468.4398
232.2345 475.6488
232.7166 483.4348
233.1987 489.4969
233.6808 493.6450
234.1629 496.1069
234.6451 497.5182
235.1272 497.9438
235.6093 497.2726
236.0914 495.3375
236.5735 491.5153
237.0556 488.0325
237.5378 485.2646
238.0199 482.8162
238.5020 479.6352
238.9841 475.4170
239.4662 470.8663
239.9483 466.3786
240.4305 462.6870
240.9126 457.4080
241.3947 450.2670
241.8768 441.6304
242.3589 432.1111
242.8410 420.4733
243.3232 409.7275
243.8053 401.5497
244.2874 397.6187
244.7695 392.1285
245.2516 384.4871
245.7337 375.4276
246.2159 366.5627
246.6980 357.7268
247.1801 349.3881
247.6622 341.5765
248.1443 334.0844
248.6264 327.7493
249.1086 323.1962
249.5907 319.4898
250.0728 314.3979
250.5549 306.2924
251.0370 299.5510
251.5191 296.3488
252.0013 298.4624
252.4834 298.0958
252.9655 294.2057
253.4476 288.4530
253.9297 283.9434
254.4118 281.2860
254.8940 278.7935
255.3761 275.6487
255.8582 271.2667
256.3403 268.6682
256.8224 268.6589
257.3046 269.8248
257.7867 269.7817
258.2688 267.9697
258.7509 266.1701
259.2330 265.1935
259.7151 265.3722
260.1973 264.3312
260.6794 261.5739
261.1615 258.1831
261.6436 255.9397
262.1257 255.3831
262.6078 254.5938
263.0900 252.9572
263.5721 250.3468
264.0542 247.8613
264.5363 245.6573
265.0184 243.3178
265.5005 240.2171
265.9827 236.3923
266.4648 231.7615
266.9469 226.2961
267.4290 220.0206
267.9111 212.9478
268.3932 204.7452
268.8754 196.3381
269.3575 188.9901
269.8396 183.0356
270.3217 176.7784
270.8038 169.6436
271.2859 161.6545
271.7681 154.6603
272.2502 149.0192
272.7323 143.7825
273.2144 138.3064
273.6965 132.5658
274.1786 126.1219
274.6608 118.3782
275.1429 109.7394
275.6250 102.5655
276.1071 97.15491
276.5892 92.89899
277.0714 89.75470
277.5535 87.79663
278.0356 85.01886
278.5177 80.94550
278.9998 75.97253
279.4819 71.73090
279.9641 68.30145
280.4462 64.95923
280.9283 60.65094
281.4104 55.35425
281.8925 51.56104
282.3746 50.09393
282.8568 50.06976
283.3389 48.82935
283.8210 46.11359
284.3031 43.60529
284.7852 43.02216
285.2673 44.22687
285.7495 43.99384
286.2316 41.49097
286.7137 37.86401
287.1958 35.65839
287.6779 34.93549
288.1600 34.10028
288.6422 31.87213
289.1243 28.43860
289.6064 25.68048
290.0885 23.78284
290.5706 22.27783
291.0527 20.59930
291.5349 18.76337
292.0170 16.56958
292.4991 14.01392
292.9812 11.04016
293.4633 7.377258
293.9454 6.425206
294.4276 5.915603
294.9097 5.062683
295.3918 7.187500
295.8739 8.530396
296.3560 9.108093
296.8381 9.061035
297.3203 8.457703
297.8024 7.236206
298.2845 6.069519
298.7666 5.954651
299.2487 6.525696
299.7308 6.697998
300.2130 5.391907
300.6951 3.652283
301.1772 3.470886
301.6593 4.828308
302.1414 6.210022
302.6235 6.025818
303.1057 4.892029
303.5878 4.029297
304.0699 4.208191
304.5520 4.572571
305.0341 3.979980
305.5162 2.531738
305.9984 1.146484
306.4805 0.6922610
306.9626 0.6554570
307.4447 0.2813110
307.9268 0.7396850
308.4089 1.971741
308.8911 2.909546
309.3732 3.670593
309.8553 4.757568
310.3374 6.823425
310.8195 9.188110
311.3016 11.17731
311.7838 12.59534
312.2659 13.74011
312.7480 14.67383
313.2301 15.48553
313.7122 16.36823
314.1943 17.27618
314.6765 18.37860
315.1586 19.88477
315.6407 21.97760
316.1228 23.95026
316.6049 25.42047
317.0870 26.55383
317.5692 27.63068
318.0513 28.98676
318.5334 30.09747
319.0155 30.79584
319.4976 31.08411
319.9797 30.66559
320.4619 28.87518
320.9440 26.49005
321.4261 24.43286
321.9082 23.45319
322.3903 22.27173
322.8724 20.44611
323.3546 17.95459
323.8367 15.36572
324.3188 12.37952
324.8009 9.554993
325.2830 7.374878
325.7651 6.575012
326.2473 5.650391
326.7294 4.386230
327.2115 2.817505
327.6936 1.173279
328.1757 0.4925540
328.6578 2.215881
329.1400 4.046387
329.6221 6.764771
330.1042 8.476501
330.5863 8.740173
331.0684 7.994080
331.5505 7.422058
332.0327 6.557434
332.5148 6.453186
332.9969 7.917175
333.4790 12.30981
333.9611 14.25195
334.4432 12.51642
334.9254 9.047852
335.4075 7.178833
335.8896 7.525452
336.3717 8.233582
336.8538 8.841248
337.3359 9.395569
337.8180 9.428040
338.3001 8.735901
338.7823 7.818909
339.2644 7.381958
339.7465 7.691223
340.2286 7.282410
340.7107 5.503906
341.1928 2.642395
341.6750 0.8969120
342.1571 0.5289310
342.6392 0.2948610
343.1213 0.9703370
343.6034 3.282166
344.0855 5.296753
344.5677 6.751648
345.0498 7.813110
345.5319 8.718018
346.0140 9.449097
346.4961 10.51172
346.9782 12.28717
347.4604 14.70062
347.9425 17.53955
348.4246 21.01550
348.9067 24.29236
349.3888 25.75354
349.8709 25.73969
350.3531 26.11246
350.8352 27.70322
351.3173 30.34109
351.7994 33.81281
352.2815 38.11459
352.7636 42.94830
353.2458 48.54218
353.7279 54.47891
354.2100 59.86212
354.6921 63.95212
355.1742 67.54926
355.6563 71.67319
356.1385 76.25769
356.6206 80.59491
357.1027 83.12384
357.5848 85.46277
358.0669 89.75616
358.5490 97.74289
359.0312 106.0693
359.5133 112.8999
359.9954 118.3862
360.4775 123.1580
360.9596 126.4234
361.4417 129.7921
361.9239 134.4561
362.4060 140.8945
362.8881 147.6156
363.3702 154.7521
363.8523 161.7868
364.3344 167.8458
364.8166 172.4652
365.2987 176.1140
365.7808 178.7914
366.2629 180.4753
366.7450 181.9400
367.2271 183.6536
367.7093 185.1001
368.1914 185.7624
368.6735 184.6833
369.1556 183.6718
369.6377 183.5247
370.1198 184.0314
370.6020 183.0501
371.0841 180.1199
371.5662 176.0860
372.0483 171.4060
372.5304 165.7229
373.0125 159.9631
373.4947 153.8461
373.9768 147.8119
374.4589 142.9957
374.9410 140.0658
375.4231 136.9540
375.9052 132.5471
376.3874 126.4855
376.8695 121.8394
377.3516 118.8568
377.8337 116.8253
378.3158 114.7526
378.7979 112.5803
379.2801 110.6866
379.7622 109.0116
380.2443 107.7047
380.7264 107.8671
381.2085 109.7919
381.6906 111.1031
382.1728 108.6152
382.6549 103.1518
383.1370 100.4054
383.6191 101.9012
384.1012 105.4846
384.5833 107.6478
385.0655 108.5004
385.5476 109.2893
386.0297 110.8691
386.5118 112.8700
386.9939 114.8326
387.4760 116.6940
387.9582 117.8090
388.4403 117.1581
388.9224 115.4507
389.4045 114.0046
389.8866 113.5130
390.3687 113.3785
390.8509 112.9912
391.3330 112.1929
391.8151 111.5291
392.2972 112.2428
392.7793 113.1883
393.2614 112.8715
393.7436 109.1129
394.2257 106.2284
394.7078 107.0454
395.1899 110.2542
395.6720 112.4242
396.1541 111.3585
396.6363 109.9901
397.1184 109.7388
397.6005 111.1028
398.0826 112.3558
398.5647 113.4963
399.0468 114.4973
399.5290 115.1675
400.0111 115.6332
400.4932 115.4228
400.9753 114.7261
401.4574 113.5987
401.9395 110.8583
402.4217 105.7840
402.9038 99.75793
403.3859 93.43591
403.8680 85.91107
404.3501 80.39407
404.8322 78.02228
405.3144 77.42902
405.7965 74.99841
406.2786 70.39456
406.7607 65.03973
407.2428 59.02893
407.7249 52.24744
408.2071 47.28558
408.6892 44.36899
409.1713 42.69421
409.6534 41.72952
410.1355 41.36325
410.6176 39.74744
411.0998 35.41153
411.5819 30.02240
412.0640 28.20322
412.5461 29.83286
413.0282 31.43774
413.5103 29.58578
413.9925 25.88458
414.4746 23.86487
414.9567 24.54456
415.4388 25.75555
415.9209 25.07242
416.4030 23.10162
416.8852 21.23761
417.3673 20.15802
417.8494 19.62503
418.3315 19.05975
418.8136 18.46255
419.2957 18.57175
419.7779 21.35886
420.2600 24.38535
420.7421 25.16205
421.2242 19.95682
421.7063 15.57285
422.1884 14.81720
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423.1527 18.11185
423.6348 17.86508
424.1169 16.86786
424.5990 15.24673
425.0811 12.11343
425.5633 10.48688
426.0454 11.49368
426.5275 13.61188
427.0096 14.92502
427.4917 14.82471
427.9738 14.84494
428.4560 15.46777
428.9381 16.67004
429.4202 17.05481
429.9023 16.26727
430.3844 15.23248
430.8665 14.61401
431.3487 14.52670
431.8308 14.37558
432.3129 14.04727
432.7950 13.82709
433.2771 14.58896
433.7592 16.35434
434.2414 17.72687
434.7235 17.86447
435.2056 17.08600
435.6877 16.71732
436.1698 16.78336
436.6519 16.91150
437.1341 16.76608
437.6162 16.39047
438.0983 15.88733
438.5804 15.22983
439.0625 14.54068
439.5446 14.07526
440.0268 13.73703
440.5089 13.16479
440.9910 11.64078
441.4731 10.09634
441.9552 9.553131
442.4373 10.35611
442.9195 10.89929
443.4016 9.680023
443.8837 7.966614
444.3658 7.300323
444.8479 9.830597
445.3300 11.77496
445.8122 11.58414
446.2943 9.490723
446.7764 7.768036
447.2585 6.723083
447.7406 6.141510
448.2227 5.997711
448.7049 6.850525
449.1870 7.009979
449.6691 5.872620
450.1512 4.340912
450.6333 3.941833
451.1154 5.285706
451.5976 6.451355
452.0797 6.915802
452.5618 6.722839
453.0439 6.415405
453.5260 5.973297
454.0081 5.480957
454.4903 5.021820
454.9724 4.595978
455.4545 4.055634
455.9366 3.348511
456.4187 2.598785
456.9008 1.849396
457.3830 1.156036
457.8651 0.9844970
458.3472 1.950409
458.8293 3.456787
459.3114 4.576355
459.7935 5.285614
460.2757 5.485229
460.7578 4.692749
461.2399 3.450134
461.7220 2.473602
462.2041 1.826904
462.6862 1.681274
463.1684 2.451996
463.6505 3.816620
464.1326 5.007721
464.6147 6.390411
465.0968 6.970062
465.5789 5.705811
466.0611 2.171967
466.5432 0.2766720
467.0253 0.2046200
467.5074 0.8255920
467.9895 1.505859
468.4716 1.169342
468.9538 1.265778
469.4359 2.154663
469.9180 3.515930
470.4001 4.377899
470.8822 4.813690
471.3643 4.559174
471.8465 3.071930
472.3286 7.5714000E-02
472.8107 0.6488950
473.2928 1.688110
473.7749 4.384888
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