#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:48:26 +0300 (Thu, 24 May 2018) $
#$Revision: 787 $
#$URL: svn://172.16.1.111/rod/cif/1/00/02/1000283.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000283
loop_
_publ_author_name
'Kampf, A. R.'
'Foord, E. E.'
_publ_section_title
;
 Artroeite, PbAlF3(OH)2, a new mineral from the Grand Reef mine, Graham
 County, Arizona: Description and crystal structure
;
_journal_name_full               'American Mineralogist'
_journal_page_first              179
_journal_page_last               183
_journal_volume                  80
_journal_year                    1995
_chemical_compound_source        R100034
_chemical_formula_sum            'Al F3 H2 O2 Pb'
_chemical_name_mineral           Artroeite
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                90.68
_cell_angle_beta                 107.69
_cell_angle_gamma                104.46
_cell_length_a                   6.270
_cell_length_b                   6.821
_cell_length_c                   5.057
_cell_volume                     198.618
_exptl_crystal_density_diffrn    5.438
_cod_original_formula_sum        'Pb Al F3 O2 H2'
_cod_database_code               9001665
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R100034.rod
_rod_data_source.block           3500000
_rod_database.code               1000283
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9001665 COD http://www.crystallography.net/cod/9001665.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
155.5779 0.0000000E+00
156.0601 0.1220090
156.5422 0.8417360
157.0243 2.468445
157.5064 3.630341
157.9885 5.549042
158.4706 8.567566
158.9528 12.71948
159.4349 17.29547
159.9170 22.55502
160.3991 27.93060
160.8812 32.78143
161.3633 35.59259
161.8455 38.95032
162.3276 44.46054
162.8097 52.74243
163.2918 60.04935
163.7739 64.18027
164.2560 66.02170
164.7382 65.36609
165.2203 64.65137
165.7024 64.46179
166.1845 65.07721
166.6666 67.16333
167.1487 68.12482
167.6309 66.34659
168.1130 62.10172
168.5951 57.33957
169.0772 52.35388
169.5593 47.61545
170.0414 43.64725
170.5236 40.66522
171.0057 38.04440
171.4878 35.58060
171.9699 33.13452
172.4520 30.32724
172.9341 26.56281
173.4163 22.43665
173.8984 18.59171
174.3805 15.00772
174.8626 11.96024
175.3447 9.763397
175.8268 8.311066
176.3090 7.141724
176.7911 6.310516
177.2732 5.495605
177.7553 4.076019
178.2374 3.748975
178.7195 3.293279
179.2017 2.822784
179.6838 2.973633
180.1659 2.651978
180.6480 2.352448
181.1301 2.051422
181.6122 1.675659
182.0944 1.205444
182.5765 0.6532900
183.0586 0.1072390
183.5407 1.053375
184.0228 1.818573
184.5049 1.862549
184.9871 1.380615
185.4692 1.081024
185.9513 1.232361
186.4334 1.691986
186.9155 2.221497
187.3976 2.832581
187.8798 3.340454
188.3619 3.187347
188.8440 2.567657
189.3261 2.767670
189.8082 4.748627
190.2903 7.875671
190.7725 9.652252
191.2546 9.891724
191.7367 9.912872
192.2188 11.27612
192.7009 13.93988
193.1830 16.91647
193.6652 20.05438
194.1473 23.28497
194.6294 25.58640
195.1115 26.57343
195.5936 27.89731
196.0757 31.94720
196.5579 38.78470
197.0400 46.31729
197.5221 53.78134
198.0042 61.17178
198.4863 69.05447
198.9684 77.48328
199.4506 86.23398
199.9327 95.16891
200.4148 104.4706
200.8969 112.7415
201.3790 119.0804
201.8611 123.3624
202.3433 128.4424
202.8254 134.5396
203.3075 141.0977
203.7896 147.1965
204.2717 152.8923
204.7538 157.9912
205.2360 162.1759
205.7181 165.2886
206.2002 168.9042
206.6823 173.1151
207.1644 177.7057
207.6465 182.0076
208.1287 185.5393
208.6108 190.2947
209.0929 197.1330
209.5750 206.2124
210.0571 216.6356
210.5392 228.2390
211.0214 241.3996
211.5035 257.0649
211.9856 275.3500
212.4677 295.3689
212.9498 317.5828
213.4319 342.7830
213.9140 365.1785
214.3962 384.8481
214.8783 401.6874
215.3604 416.1014
215.8425 430.4818
216.3246 437.3988
216.8067 433.0363
217.2889 415.6875
217.7710 392.7357
218.2531 362.5515
218.7352 327.7577
219.2173 293.4011
219.6994 258.2656
220.1816 225.6398
220.6637 196.3895
221.1458 170.5338
221.6279 147.8087
222.1100 128.0308
222.5921 111.3430
223.0743 97.81949
223.5564 88.43109
224.0385 80.67087
224.5206 73.65613
225.0027 67.33908
225.4848 61.64441
225.9670 56.60791
226.4491 52.23459
226.9312 48.47971
227.4133 45.44135
227.8954 42.89761
228.3775 40.84995
228.8597 39.45712
229.3418 38.06232
229.8239 36.59415
230.3060 35.11584
230.7881 33.84378
231.2702 32.74142
231.7524 31.85513
232.2345 31.21133
232.7166 30.81882
233.1987 30.59750
233.6808 30.47241
234.1629 30.53348
234.6451 30.99414
235.1272 31.68796
235.6093 33.03928
236.0914 35.38535
236.5735 39.45499
237.0556 42.73944
237.5378 44.89044
238.0199 46.43387
238.5020 48.73251
238.9841 52.50934
239.4662 56.03217
239.9483 58.67209
240.4305 60.57260
240.9126 61.19171
241.3947 60.41013
241.8768 58.53119
242.3589 55.80783
242.8410 51.75647
243.3232 47.10675
243.8053 42.09680
244.2874 36.15826
244.7695 31.42163
245.2516 28.10001
245.7337 26.04877
246.2159 24.78717
246.6980 24.38632
247.1801 24.22397
247.6622 24.10849
248.1443 23.99939
248.6264 24.26370
249.1086 25.03461
249.5907 26.14380
250.0728 27.22610
250.5549 28.21939
251.0370 29.44669
251.5191 31.00458
252.0013 32.93176
252.4834 34.80121
252.9655 36.62308
253.4476 38.41113
253.9297 40.15295
254.4118 41.79370
254.8940 43.51547
255.3761 45.27927
255.8582 47.01807
256.3403 48.80438
256.8224 50.71939
257.3046 52.78931
257.7867 54.99750
258.2688 57.40982
258.7509 59.92300
259.2330 62.48743
259.7151 65.12833
260.1973 67.47003
260.6794 69.33322
261.1615 71.06903
261.6436 73.07010
262.1257 75.31116
262.6078 77.95703
263.0900 81.28690
263.5721 85.51138
264.0542 88.48709
264.5363 89.76294
265.0184 90.35330
265.5005 91.80170
265.9827 94.67096
266.4648 96.69278
266.9469 97.09943
267.4290 95.86218
267.9111 94.38724
268.3932 92.67917
268.8754 90.73395
269.3575 88.47769
269.8396 85.76593
270.3217 83.21588
270.8038 81.06259
271.2859 79.26071
271.7681 77.11673
272.2502 74.43735
272.7323 71.82242
273.2144 69.98636
273.6965 69.02600
274.1786 68.25964
274.6608 67.52655
275.1429 66.85788
275.6250 66.46552
276.1071 66.37701
276.5892 66.48737
277.0714 66.75601
277.5535 67.21048
278.0356 67.60001
278.5177 67.86545
278.9998 68.03836
279.4819 68.55753
279.9641 69.73004
280.4462 70.00967
280.9283 67.40457
281.4104 61.80020
281.8925 57.94644
282.3746 57.28049
282.8568 58.28519
283.3389 56.44464
283.8210 51.49069
284.3031 45.74405
284.7852 40.37180
285.2673 35.44839
285.7495 31.73853
286.2316 29.61801
286.7137 28.33765
287.1958 26.28998
287.6779 23.44400
288.1600 20.64423
288.6422 18.25366
289.1243 16.28775
289.6064 15.16824
290.0885 15.14667
290.5706 15.38947
291.0527 14.48318
291.5349 12.49225
292.0170 10.30890
292.4991 7.982605
292.9812 5.795807
293.4633 5.213745
293.9454 6.625000
294.4276 8.306488
294.9097 7.646240
295.3918 5.059814
295.8739 2.727570
296.3560 1.857269
296.8381 1.982788
297.3203 2.287384
297.8024 2.819489
298.2845 2.895081
298.7666 1.023376
299.2487 2.044861
299.7308 1.253216
300.2130 3.303314
300.6951 1.203156
301.1772 0.2492070
301.6593 1.055847
302.1414 1.076019
302.6235 0.7223210
303.1057 3.364685
303.5878 4.815125
304.0699 3.725769
304.5520 1.660065
305.0341 0.2396240
305.5162 0.5607600
305.9984 0.9768680
306.4805 1.161072
306.9626 1.058746
307.4447 0.5199890
307.9268 0.8876650
308.4089 2.235657
308.8911 2.572815
309.3732 2.099396
309.8553 1.628601
310.3374 1.594147
310.8195 1.821930
311.3016 2.276093
311.7838 3.314453
312.2659 3.791534
312.7480 2.689697
313.2301 4.166976
313.7122 2.016998
314.1943 5.472778
314.6765 8.107635
315.1586 8.143433
315.6407 4.473389
316.1228 1.269501
316.6049 1.018524
317.0870 2.486633
317.5692 3.639435
318.0513 3.195343
318.5334 2.714264
319.0155 3.144897
319.4976 4.749390
319.9797 5.890900
320.4619 5.336853
320.9440 4.270294
321.4261 4.019440
321.9082 5.340576
322.3903 7.085785
322.8724 9.163086
323.3546 11.57141
323.8367 13.47513
324.3188 14.37076
324.8009 14.90500
325.2830 15.56519
325.7651 15.88739
326.2473 16.96701
326.7294 19.62863
327.2115 23.52792
327.6936 26.26215
328.1757 26.37155
328.6578 26.28448
329.1400 27.20551
329.6221 29.76035
330.1042 32.48837
330.5863 35.57712
331.0684 38.81531
331.5505 41.70947
332.0327 44.14822
332.5148 46.50119
332.9969 48.97180
333.4790 51.55365
333.9611 53.83456
334.4432 55.53320
334.9254 57.20306
335.4075 59.74997
335.8896 63.25116
336.3717 67.20538
336.8538 71.56058
337.3359 76.47668
337.8180 81.40735
338.3001 86.58081
338.7823 91.32596
339.2644 94.66428
339.7465 96.29852
340.2286 97.96436
340.7107 100.1703
341.1928 102.7872
341.6750 104.7748
342.1571 106.2061
342.6392 106.8550
343.1213 106.3440
343.6034 104.6573
344.0855 102.7693
344.5677 100.6620
345.0498 98.63431
345.5319 97.55225
346.0140 97.43689
346.4961 97.66812
346.9782 98.01151
347.4604 98.41550
347.9425 98.52441
348.4246 98.23013
348.9067 97.89386
349.3888 97.99481
349.8709 98.51004
350.3531 99.28918
350.8352 100.2537
351.3173 101.4308
351.7994 102.9048
352.2815 104.6782
352.7636 106.6928
353.2458 108.9525
353.7279 111.4092
354.2100 113.9717
354.6921 116.9996
355.1742 119.8297
355.6563 121.7033
356.1385 122.6614
356.6206 123.2801
357.1027 123.6692
357.5848 123.8709
358.0669 124.0767
358.5490 124.4720
359.0312 124.7565
359.5133 124.6765
359.9954 124.2577
360.4775 123.5922
360.9596 123.4221
361.4417 122.5582
361.9239 120.0633
362.4060 115.2337
362.8881 110.5393
363.3702 106.5639
363.8523 103.3047
364.3344 100.7893
364.8166 100.2272
365.2987 99.29630
365.7808 96.90198
366.2629 92.80917
366.7450 88.85681
367.2271 85.57971
367.7093 82.51627
368.1914 79.23541
368.6735 75.62573
369.1556 71.81812
369.6377 67.79309
370.1198 63.58133
370.6020 59.49500
371.0841 55.75092
371.5662 52.00839
372.0483 48.02533
372.5304 43.45084
373.0125 39.15314
373.4947 35.01334
373.9768 31.20166
374.4589 28.34531
374.9410 27.02350
375.4231 25.57272
375.9052 23.26279
376.3874 19.93829
376.8695 16.79266
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377.8337 10.92160
378.3158 9.281158
378.7979 8.831268
379.2801 8.585144
379.7622 8.407104
380.2443 8.206268
380.7264 7.500702
381.2085 6.243256
381.6906 4.816132
382.1728 3.448975
382.6549 2.150574
383.1370 1.017639
383.6191 2.4048001E-02
384.1012 -0.1546611
384.5833 0.6461790
385.0655 0.2123410
385.5476 1.112030
386.0297 1.944275
386.5118 2.482452
386.9939 2.069275
387.4760 0.5019840
387.9582 0.9527590
388.4403 0.7514340
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390.3687 0.7140500
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395.6720 9.6588001E-02
396.1541 2.422913
396.6363 4.733002
397.1184 5.477356
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398.0826 2.878601
398.5647 3.973999
399.0468 5.936859
399.5290 7.418274
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400.9753 9.478973
401.4574 11.95724
401.9395 13.76334
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403.3859 15.80139
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413.5103 31.54053
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419.2957 18.35123
419.7779 18.11304
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420.7421 17.30505
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422.1884 14.87399
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443.8837 21.74939
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446.2943 30.89166
446.7764 34.93802
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448.2227 38.63733
448.7049 43.81635
449.1870 48.26822
449.6691 51.21240
450.1512 53.69650
450.6333 57.42572
451.1154 63.29657
451.5976 68.86902
452.0797 73.27158
452.5618 76.57071
453.0439 80.34705
453.5260 84.57916
454.0081 89.25732
454.4903 94.45282
454.9724 100.1125
455.4545 105.6866
455.9366 110.9605
456.4187 116.3217
456.9008 122.3510
457.3830 129.0710
457.8651 135.9289
458.3472 142.7648
458.8293 149.6384
459.3114 157.2411
459.7935 165.4910
460.2757 172.9193
460.7578 177.9240
461.2399 181.4103
461.7220 184.7527
462.2041 189.0525
462.6862 192.0789
463.1684 192.1741
463.6505 189.9002
464.1326 186.5437
464.6147 183.3229
465.0968 178.5455
465.5789 171.0168
466.0611 160.3450
466.5432 149.4579
467.0253 139.1321
467.5074 128.7921
467.9895 117.9921
468.4716 104.9052
468.9538 93.46652
469.4359 84.48544
469.9180 77.38739
470.4001 70.32581
470.8822 63.22937
471.3643 56.38571
471.8465 49.77112
472.3286 43.30621
472.8107 37.99045
473.2928 33.99673
473.7749 30.87973
474.2570 28.45090
474.7392 26.70682
475.2213 24.86133
475.7034 22.74350
476.1855 20.42850
476.6676 18.00467
477.1497 15.47672
477.6319 13.01138
478.1140 10.17059
478.5961 7.592957
479.0782 6.656616
479.5603 7.550323
480.0424 8.618835
480.5246 8.685547
481.0067 8.032715
481.4888 7.055817
481.9709 5.664276
482.4530 4.224396
482.9352 2.542511
483.4173 0.8935550
483.8994 0.1486510
484.3815 1.803741
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