#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:48:30 +0300 (Thu, 24 May 2018) $
#$Revision: 788 $
#$URL: svn://172.16.1.111/rod/cif/1/00/02/1000284.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000284
loop_
_publ_author_name
'Araki, T.'
'Moore, P. B.'
_publ_section_title
;
 Dixenite, CuMn14Fe(OH)6(AsO3)5(SiO4)2(AsO4): Metallic [As4Cu] clusters in
 an oxide matrix
;
_journal_name_full               'American Mineralogist'
_journal_page_first              1263
_journal_page_last               1273
_journal_volume                  66
_journal_year                    1981
_chemical_compound_source        R100044
_chemical_formula_sum            'As6.3 Cu0.843 Fe H6 Mg0.1 Mn12.9 O33 Si1.7'
_chemical_name_mineral           Dixenite
_space_group_IT_number           146
_symmetry_space_group_name_Hall  'R 3'
_symmetry_space_group_name_H-M   'R 3 :H'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_length_a                   8.233
_cell_length_b                   8.233
_cell_length_c                   37.499
_cell_volume                     2201.236
_exptl_crystal_density_diffrn    4.242
_cod_original_sg_symbol_H-M      'R 3'
_cod_original_formula_sum        'Mn12.9 Mg.1 Fe Cu.843 Si1.7 As6.3 O33 H6'
_cod_database_code               9000836
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R100044.rod
_rod_data_source.block           3500000
_rod_database.code               1000284
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9000836 COD http://www.crystallography.net/cod/9000836.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
165.7633 0.0000000E+00
166.2454 7.8491002E-02
166.7276 2.659203
167.2097 5.958099
167.6918 7.398186
168.1739 7.114906
168.6560 6.907982
169.1381 7.955521
169.6203 9.568695
170.1024 10.32812
170.5845 10.34430
171.0666 10.05787
171.5487 9.281143
172.0309 8.068993
172.5130 7.243568
172.9951 7.951988
173.4772 9.324524
173.9593 10.00516
174.4414 8.906158
174.9236 7.165985
175.4057 5.920799
175.8878 5.160812
176.3699 4.773514
176.8520 4.797310
177.3341 5.113693
177.8163 5.472672
178.2984 5.909042
178.7805 6.279541
179.2626 6.349182
179.7447 6.107956
180.2268 5.633560
180.7090 4.834930
181.1911 3.827339
181.6732 2.977707
182.1553 2.266846
182.6374 1.849998
183.1195 2.254196
183.6017 3.608818
184.0838 5.121674
184.5659 6.067337
185.0480 6.452660
185.5301 6.335869
186.0123 5.230125
186.4944 3.590065
186.9765 3.084389
187.4586 3.972145
187.9407 5.204987
188.4228 5.150810
188.9050 3.935890
189.3871 2.881950
189.8692 2.825790
190.3513 3.582275
190.8334 4.178177
191.3155 4.430130
191.7977 4.394539
192.2798 4.609947
192.7619 5.076408
193.2440 5.461830
193.7261 5.556076
194.2082 5.382782
194.6904 5.130890
195.1725 4.630646
195.6546 4.421951
196.1367 6.114479
196.6188 9.930710
197.1009 12.86597
197.5831 12.54695
198.0652 8.992775
198.5473 7.285355
199.0294 8.063118
199.5115 10.28851
199.9937 12.00941
200.4758 13.19197
200.9579 13.98336
201.4400 14.35381
201.9221 14.27196
202.4042 14.24318
202.8864 14.38892
203.3685 14.51084
203.8506 14.01080
204.3327 12.71938
204.8148 11.51014
205.2969 10.98987
205.7791 11.30740
206.2612 11.20954
206.7433 10.54143
207.2254 9.482567
207.7075 8.466072
208.1896 7.488602
208.6718 6.552635
209.1539 5.639824
209.6360 4.748642
210.1181 3.915192
210.6002 3.079269
211.0823 2.335480
211.5645 2.041023
212.0466 2.420586
212.5287 2.718597
213.0108 2.482864
213.4929 1.562164
213.9750 0.6999970
214.4572 9.6473999E-02
214.9393 0.7949910
215.4214 1.373138
215.9035 1.970474
216.3856 2.166458
216.8678 1.569618
217.3499 0.2507170
217.8320 1.432793
218.3141 1.678764
218.7962 1.285332
219.2783 1.223274
219.7605 1.760132
220.2426 2.135941
220.7247 1.828247
221.2068 0.4076160
221.6889 0.4522170
222.1710 0.5292740
222.6532 3.3546001E-02
223.1353 0.3719330
223.6174 0.5186310
224.0995 0.7502060
224.5816 1.310829
225.0637 2.547935
225.5459 3.171982
226.0280 2.860306
226.5101 1.974586
226.9922 1.667480
227.4743 2.270988
227.9564 2.923805
228.4386 3.172836
228.9207 2.727852
229.4028 2.572067
229.8849 2.787949
230.3670 3.282143
230.8492 3.863449
231.3313 4.775230
231.8134 5.399727
232.2955 5.375069
232.7776 4.190659
233.2597 3.517746
233.7419 3.483086
234.2240 3.974541
234.7061 4.620621
235.1882 5.396446
235.6703 6.251137
236.1524 7.264305
236.6346 8.735435
237.1167 9.650009
237.5988 9.734138
238.0809 9.363716
238.5630 9.455078
239.0451 10.33013
239.5273 11.22458
240.0094 11.76826
240.4915 11.73485
240.9736 11.82030
241.4557 12.10369
241.9378 12.49619
242.4200 12.74549
242.9021 12.53123
243.3842 12.64257
243.8663 13.40771
244.3484 15.00795
244.8306 16.78115
245.3127 18.94337
245.7948 21.19585
246.2769 22.88409
246.7590 23.72997
247.2411 24.30910
247.7233 24.75024
248.2054 24.89831
248.6875 25.62167
249.1696 27.08979
249.6517 28.97140
250.1338 30.82038
250.6160 32.93365
251.0981 34.45975
251.5802 34.93571
252.0623 34.03897
252.5444 33.84276
253.0265 34.59003
253.5087 35.86995
253.9908 37.08313
254.4729 38.21541
254.9550 39.28143
255.4371 40.31268
255.9192 41.33852
256.4014 42.25543
256.8835 42.98550
257.3656 43.56915
257.8477 44.11884
258.3298 44.89442
258.8120 45.03151
259.2941 44.12085
259.7762 42.07011
260.2583 40.47011
260.7404 39.35361
261.2225 38.65199
261.7047 38.39303
262.1868 38.87585
262.6689 38.94710
263.1510 38.27866
263.6331 36.88545
264.1152 35.20434
264.5974 33.07792
265.0795 30.95018
265.5616 29.32238
266.0437 28.29688
266.5258 27.38927
267.0079 26.63102
267.4901 25.99445
267.9722 25.18677
268.4543 24.05451
268.9364 22.84716
269.4185 21.78226
269.9006 20.97814
270.3828 20.03781
270.8649 18.80568
271.3470 17.45144
271.8291 16.59743
272.3112 16.35120
272.7933 16.24138
273.2755 15.92137
273.7576 15.41507
274.2397 14.81524
274.7218 14.07538
275.2039 13.19522
275.6860 12.04512
276.1682 10.52245
276.6503 9.111450
277.1324 8.145401
277.6145 7.661957
278.0966 7.253258
278.5787 6.913589
279.0609 6.611267
279.5430 6.240959
280.0251 5.810982
280.5072 5.450455
280.9893 5.161667
281.4715 4.920975
281.9536 5.011757
282.4357 5.635292
282.9178 6.263382
283.3999 5.540703
283.8820 3.360451
284.3642 1.719353
284.8463 2.015907
285.3284 4.016304
285.8105 4.848022
286.2926 4.283844
286.7747 3.237595
287.2569 3.132927
287.7390 3.919258
288.2211 4.270096
288.7032 3.308777
289.1853 1.419342
289.6674 0.3706970
290.1496 0.2358550
290.6317 0.4204860
291.1138 0.1920390
291.5959 0.3662490
292.0780 0.6099090
292.5602 0.1572340
293.0423 0.6887280
293.5244 1.142143
294.0065 1.189789
294.4886 1.105560
294.9707 1.205528
295.4529 1.397873
295.9350 1.308678
296.4171 0.6535490
296.8992 0.1572800
297.3813 0.2906720
297.8634 0.1993870
298.3456 0.7104340
298.8277 0.6951220
299.3098 0.3639760
299.7919 0.1781850
300.2740 0.2523270
300.7561 0.4760740
301.2383 0.8679660
301.7204 1.352776
302.2025 1.551300
302.6846 0.8762210
303.1667 0.1336140
303.6488 0.6086040
304.1310 0.2891390
304.6131 0.1864930
305.0952 0.1462630
305.5773 0.2538220
306.0594 0.5912630
306.5415 0.6464610
307.0237 0.5266190
307.5058 0.2929460
307.9879 7.2540000E-02
308.4700 0.3718950
308.9521 0.4494930
309.4343 0.3585360
309.9164 0.1992190
310.3985 0.2438960
310.8806 0.5641940
311.3627 0.2662730
311.8448 0.6826710
312.3270 1.390358
312.8091 0.8912280
313.2912 1.1627000E-02
313.7733 0.3696670
314.2554 0.8303220
314.7375 2.075150
315.2197 2.496979
315.7018 2.183708
316.1839 1.882843
316.6660 2.155167
317.1481 2.467888
317.6302 2.368240
318.1124 1.379799
318.5945 0.4265060
319.0766 0.3143080
319.5587 0.8051680
320.0408 0.9315110
320.5229 0.3667530
321.0051 0.3682330
321.4872 1.021385
321.9693 1.666359
322.4514 1.999535
322.9335 1.917336
323.4156 1.485764
323.8978 0.8314060
324.3799 0.6382450
324.8620 1.794014
325.3441 2.181976
325.8262 1.558929
326.3083 0.8269580
326.7905 0.3774490
327.2726 1.520576
327.7547 1.931030
328.2368 0.3228680
328.7189 0.6905820
329.2010 0.2087940
329.6832 2.005089
330.1653 3.000648
330.6474 1.794052
331.1295 7.7843003E-02
331.6116 0.7720640
332.0938 0.1947400
332.5759 0.3653260
333.0580 0.7622910
333.5401 1.006470
334.0222 1.120796
334.5043 1.002708
334.9865 0.8984830
335.4686 1.014336
335.9507 1.574158
336.4328 1.715836
336.9149 1.250771
337.3970 0.4083560
337.8792 0.2736430
338.3613 0.9177170
338.8434 1.085106
339.3255 0.3200840
339.8076 1.614250
340.2898 2.578156
340.7719 2.310753
341.2540 1.544197
341.7361 1.437912
342.2182 2.079170
342.7003 2.519089
343.1825 2.151062
343.6646 1.216904
344.1467 1.614815
344.6288 3.589386
345.1109 5.678818
345.5930 6.424377
346.0752 5.899246
346.5573 4.925140
347.0394 3.435974
347.5215 1.826942
348.0036 0.8640520
348.4857 0.5628740
348.9679 0.9783480
349.4500 2.640160
349.9321 5.091751
350.4142 7.000778
350.8963 8.145958
351.3784 8.734955
351.8606 8.753174
352.3427 8.359940
352.8248 8.155006
353.3069 8.825043
353.7890 9.746902
354.2711 9.933258
354.7533 9.201080
355.2354 8.496727
355.7175 8.762802
356.1996 9.610443
356.6817 10.37276
357.1638 10.72626
357.6460 10.91275
358.1281 10.91637
358.6102 10.79388
359.0923 11.16834
359.5744 13.22936
360.0565 15.56812
360.5387 16.81340
361.0208 15.83012
361.5029 14.56849
361.9850 13.58859
362.4671 13.00356
362.9492 13.12789
363.4314 14.95137
363.9135 16.84887
364.3956 17.91145
364.8777 17.75034
365.3598 17.43169
365.8419 17.02367
366.3241 16.62958
366.8062 16.40733
367.2883 16.33929
367.7704 16.46831
368.2526 16.90861
368.7347 17.78870
369.2168 18.31355
369.6989 18.12373
370.1810 17.80341
370.6631 17.86633
371.1453 18.80366
371.6274 19.32757
372.1095 19.20746
372.5916 18.53232
373.0737 18.15565
373.5558 18.17867
374.0380 18.34085
374.5201 18.48246
375.0022 18.51772
375.4843 18.86603
375.9664 19.76700
376.4485 20.76306
376.9307 20.83952
377.4128 19.77538
377.8949 18.78616
378.3770 18.38451
378.8591 18.55559
379.3412 18.99014
379.8234 19.74287
380.3055 20.50349
380.7876 20.88342
381.2697 20.90259
381.7518 20.86654
382.2339 20.74525
382.7161 20.60165
383.1982 20.75960
383.6803 21.26358
384.1624 21.67663
384.6445 21.51598
385.1266 20.98940
385.6088 20.74802
386.0909 20.94231
386.5730 21.13169
387.0551 20.81421
387.5372 20.18970
388.0193 19.69846
388.5015 19.49932
388.9836 19.58416
389.4657 20.12128
389.9478 21.22015
390.4299 22.25941
390.9120 22.84912
391.3942 23.09949
391.8763 23.13670
392.3584 22.80955
392.8405 22.46150
393.3226 22.25475
393.8047 22.17776
394.2869 22.16545
394.7690 22.31473
395.2511 22.42342
395.7332 22.35344
396.2154 22.02998
396.6975 21.66377
397.1796 21.18372
397.6617 20.77114
398.1438 20.67165
398.6259 21.83222
399.1081 22.48608
399.5902 21.81369
400.0723 19.49168
400.5544 17.87794
401.0365 17.28859
401.5186 17.17845
402.0008 17.16995
402.4829 17.72414
402.9650 17.45650
403.4471 15.73811
403.9292 13.11212
404.4113 11.98886
404.8935 12.97099
405.3756 14.03452
405.8577 14.09141
406.3398 12.99101
406.8219 11.62751
407.3040 9.873634
407.7862 8.242996
408.2683 7.523415
408.7504 7.742462
409.2325 8.000214
409.7146 8.104431
410.1967 7.994385
410.6789 7.300369
411.1610 5.998138
411.6431 4.773560
412.1252 4.451859
412.6073 4.701096
413.0894 4.499802
413.5716 3.480881
414.0537 2.329163
414.5358 2.060440
415.0179 2.410706
415.5000 2.513367
415.9821 1.401733
416.4643 6.6086002E-02
416.9464 0.3719640
417.4285 0.2176670
417.9106 0.9709320
418.3927 1.414932
418.8748 1.675491
419.3570 1.893341
419.8391 1.876892
420.3212 2.060623
420.8033 2.978149
421.2854 4.382126
421.7675 5.133987
422.2497 3.819687
422.7318 2.562012
423.2139 2.652191
423.6960 5.199539
424.1781 6.975296
424.6602 7.111649
425.1424 6.416428
425.6245 6.041473
426.1066 5.813889
426.5887 6.162674
427.0709 7.496674
427.5530 9.813583
428.0351 11.16245
428.5172 11.16467
428.9993 10.73308
429.4814 10.44003
429.9636 10.22789
430.4457 10.38962
430.9278 11.00810
431.4099 11.95314
431.8920 13.02226
432.3741 14.26163
432.8563 15.34502
433.3384 16.18874
433.8205 16.77350
434.3026 16.81387
434.7847 16.24644
435.2668 15.65143
435.7490 15.64378
436.2311 16.10866
436.7132 16.67287
437.1953 17.35345
437.6774 17.92668
438.1595 17.89354
438.6417 17.42194
439.1238 17.20566
439.6059 18.28542
440.0880 19.51718
440.5701 19.48347
441.0522 17.85518
441.5344 16.21466
442.0165 15.65811
442.4986 15.63005
442.9807 15.45438
443.4628 14.93547
443.9449 14.20006
444.4271 13.10138
444.9092 11.74275
445.3913 10.69109
445.8734 10.39542
446.3555 10.22522
446.8376 9.879303
447.3198 9.295074
447.8019 8.605362
448.2840 7.722366
448.7661 6.780609
449.2482 5.973206
449.7303 5.382324
450.2125 4.806488
450.6946 4.245010
451.1767 3.681671
451.6588 2.795166
452.1409 1.301865
452.6230 0.1276090
453.1052 0.1733550
453.5873 1.571045
454.0694 2.453156
454.5515 2.673538
455.0337 2.330093
455.5158 1.284882
455.9979 0.4019780
456.4800 1.696457
456.9621 1.999222
457.4442 1.662109
457.9264 1.525986
458.4085 1.580673
458.8906 1.541946
459.3727 0.8952330
459.8548 7.0556998E-02
460.3369 0.1958470
460.8191 0.3747410
461.3012 1.234482
461.7833 2.256165
462.2654 3.232834
462.7475 3.733154
463.2296 3.676392
463.7118 3.010223
464.1939 1.278946
464.6760 1.574677
465.1581 3.598526
465.6402 3.603180
466.1223 2.891312
466.6045 2.370819
467.0866 2.037933
467.5687 2.053986
468.0508 2.485687
468.5329 3.261826
469.0150 4.292450
469.4972 5.972168
469.9793 7.287354
470.4614 7.851028
470.9435 7.627380
471.4256 7.322037
471.9077 6.799469
472.3899 6.469803
472.8720 6.893158
473.3541 8.181702
473.8362 8.836029
474.3183 8.423660
474.8004 7.630188
475.2826 8.210236
475.7647 10.01808
476.2468 11.17622
476.7289 9.852570
477.2110 7.368286
477.6931 6.863586
478.1753 8.351303
478.6574 10.27260
479.1395 11.60191
479.6216 12.47173
480.1037 13.02054
480.5858 13.08165
481.0680 13.21516
481.5501 14.05498
482.0322 15.24426
482.5143 16.02977
482.9964 15.47856
483.4786 15.01035
483.9607 15.43431
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