#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:48:59 +0300 (Thu, 24 May 2018) $
#$Revision: 795 $
#$URL: svn://172.16.1.111/rod/cif/1/00/02/1000290.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000290
loop_
_publ_author_name
'Gatehouse, B. M.'
'Leverett, P.'
_publ_section_title
;
 Lithium triniobate(V), LiNb3O8 Note: isostructural with lithiotantite
;
_journal_name_full               'Crystal Structure Communications'
_journal_page_first              83
_journal_page_last               86
_journal_volume                  1
_journal_year                    1972
_chemical_compound_source        Synthetic
_chemical_formula_sum            'Li Nb3 O8'
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 107.33
_cell_angle_gamma                90
_cell_length_a                   7.459
_cell_length_b                   5.034
_cell_length_c                   15.270
_cell_volume                     547.339
_exptl_crystal_density_diffrn    5.020
_cod_database_code               9014478
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R100165.rod
_rod_data_source.block           3500000
_rod_database.code               1000290
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9014478 COD http://www.crystallography.net/cod/9014478.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
147.9250 0.0000000E+00
148.4071 25.90332
148.8892 19.61450
149.3713 5.308838
149.8535 5.454102
150.3356 9.581299
150.8177 37.07715
151.2998 77.85425
151.7819 125.0664
152.2640 179.3794
152.7462 239.3308
153.2283 300.7068
153.7104 370.7195
154.1925 435.3513
154.6746 489.5071
155.1567 532.3594
155.6389 562.8281
156.1210 579.2446
156.6031 582.9980
157.0852 578.5078
157.5673 566.5029
158.0495 546.2991
158.5316 517.2363
159.0137 475.1860
159.4958 429.6377
159.9779 379.4150
160.4600 326.6387
160.9422 278.5366
161.4243 232.8296
161.9064 195.3218
162.3885 169.8462
162.8706 158.3125
163.3527 157.6567
163.8349 166.9639
164.3170 186.1699
164.7991 215.0815
165.2812 252.8530
165.7633 300.5820
166.2454 359.4409
166.7276 436.2280
167.2097 518.3423
167.6918 600.1162
168.1739 681.0166
168.6560 764.0049
169.1381 850.8521
169.6203 938.6011
170.1024 989.4019
170.5845 1025.829
171.0666 1061.937
171.5487 1091.396
172.0309 1114.773
172.5130 1140.882
172.9951 1178.721
173.4772 1224.513
173.9593 1271.310
174.4414 1310.195
174.9236 1345.794
175.4057 1384.890
175.8878 1428.019
176.3699 1468.862
176.8520 1503.807
177.3341 1533.320
177.8163 1559.037
178.2984 1579.387
178.7805 1596.804
179.2626 1616.612
179.7447 1638.936
180.2268 1657.157
180.7090 1662.805
181.1911 1658.293
181.6732 1650.583
182.1553 1644.794
182.6374 1637.824
183.1195 1622.410
183.6017 1597.812
184.0838 1568.026
184.5659 1534.673
185.0480 1498.834
185.5301 1464.878
186.0123 1434.660
186.4944 1407.865
186.9765 1385.487
187.4586 1368.215
187.9407 1351.937
188.4228 1332.466
188.9050 1309.684
189.3871 1281.430
189.8692 1249.548
190.3513 1212.575
190.8334 1160.664
191.3155 1092.354
191.7977 1012.673
192.2798 928.2979
192.7619 839.3130
193.2440 746.8110
193.7261 646.6938
194.2082 540.6621
194.6904 443.3130
195.1725 355.6152
195.6546 276.1992
196.1367 205.4502
196.6188 142.9746
197.1009 88.70117
197.5831 43.86914
198.0652 8.140625
198.5473 23.79980
199.0294 53.11182
199.5115 77.70752
199.9937 92.96973
200.4758 98.42725
200.9579 97.61768
201.4400 91.60010
201.9221 80.26025
202.4042 67.12988
202.8864 53.08252
203.3685 37.09473
203.8506 16.57275
204.3327 8.267090
204.8148 37.30371
205.2969 70.94531
205.7791 101.5483
206.2612 133.1602
206.7433 163.8911
207.2254 196.8901
207.7075 241.8379
208.1896 301.4985
208.6718 364.5698
209.1539 425.5049
209.6360 482.5420
210.1181 542.6758
210.6002 604.9097
211.0823 671.2192
211.5645 747.1177
212.0466 833.4653
212.5287 928.5654
213.0108 1031.614
213.4929 1143.654
213.9750 1261.623
214.4572 1384.623
214.9393 1513.483
215.4214 1655.520
215.9035 1814.184
216.3856 1980.373
216.8678 2146.339
217.3499 2314.192
217.8320 2481.897
218.3141 2649.227
218.7962 2814.979
219.2783 2974.564
219.7605 3127.787
220.2426 3272.153
220.7247 3406.302
221.2068 3533.106
221.6889 3640.532
222.1710 3727.193
222.6532 3794.083
223.1353 3841.152
223.6174 3868.002
224.0995 3876.955
224.5816 3868.921
225.0637 3842.381
225.5459 3802.325
226.0280 3746.194
226.5101 3677.261
226.9922 3607.173
227.4743 3536.118
227.9564 3462.744
228.4386 3384.565
228.9207 3300.103
229.4028 3217.384
229.8849 3134.948
230.3670 3054.396
230.8492 2977.195
231.3313 2901.168
231.8134 2832.769
232.2955 2774.792
232.7776 2732.132
233.2597 2691.033
233.7419 2651.417
234.2240 2613.375
234.7061 2578.585
235.1882 2550.275
235.6703 2520.776
236.1524 2486.918
236.6346 2449.406
237.1167 2406.151
237.5988 2356.079
238.0809 2300.687
238.5630 2242.675
239.0451 2184.098
239.5273 2120.118
240.0094 2046.964
240.4915 1957.038
240.9736 1876.350
241.4557 1803.552
241.9378 1739.755
242.4200 1687.591
242.9021 1646.979
243.3842 1617.059
243.8663 1597.477
244.3484 1588.342
244.8306 1588.951
245.3127 1598.364
245.7948 1618.290
246.2769 1653.545
246.7590 1706.552
247.2411 1771.468
247.7233 1846.665
248.2054 1932.814
248.6875 2025.420
249.1696 2121.464
249.6517 2224.301
250.1338 2339.795
250.6160 2471.725
251.0981 2609.311
251.5802 2747.840
252.0623 2886.821
252.5444 3032.477
253.0265 3184.226
253.5087 3342.025
253.9908 3503.842
254.4729 3672.625
254.9550 3840.718
255.4371 4007.565
255.9192 4172.471
256.4014 4327.704
256.8835 4474.091
257.3656 4609.056
257.8477 4735.552
258.3298 4860.341
258.8120 4961.413
259.2941 5036.433
259.7762 5087.381
260.2583 5110.553
260.7404 5103.849
261.2225 5071.991
261.7047 5018.494
262.1868 4940.204
262.6689 4846.593
263.1510 4736.633
263.6331 4611.548
264.1152 4479.412
264.5974 4338.765
265.0795 4194.499
265.5616 4054.319
266.0437 3915.210
266.5258 3782.781
267.0079 3656.220
267.4901 3535.877
267.9722 3435.003
268.4543 3354.420
268.9364 3289.917
269.4185 3236.187
269.9006 3190.628
270.3828 3166.912
270.8649 3165.508
271.3470 3187.482
271.8291 3239.292
272.3112 3325.229
272.7933 3431.082
273.2755 3543.496
273.7576 3659.519
274.2397 3799.582
274.7218 3963.748
275.2039 4153.481
275.6860 4373.591
276.1682 4627.409
276.6503 4906.740
277.1324 5210.713
277.6145 5537.454
278.0966 5880.669
278.5787 6243.879
279.0609 6617.492
279.5430 6996.647
280.0251 7385.715
280.5072 7744.136
280.9893 8061.729
281.4715 8336.144
281.9536 8540.345
282.4357 8678.412
282.9178 8736.136
283.3999 8679.003
283.8820 8503.967
284.3642 8264.559
284.8463 7966.651
285.3284 7613.612
285.8105 7262.289
286.2926 6908.054
286.7747 6563.998
287.2569 6247.697
287.7390 5958.762
288.2211 5689.225
288.7032 5437.324
289.1853 5202.781
289.6674 4981.041
290.1496 4771.532
290.6317 4571.898
291.1138 4384.432
291.5959 4206.399
292.0780 4025.523
292.5602 3838.432
293.0423 3644.186
293.5244 3439.555
294.0065 3225.441
294.4886 3002.725
294.9707 2764.796
295.4529 2514.961
295.9350 2270.030
296.4171 2029.854
296.8992 1797.404
297.3813 1578.799
297.8634 1375.084
298.3456 1187.419
298.8277 1021.895
299.3098 874.6538
299.7919 738.5522
300.2740 613.3174
300.7561 498.4419
301.2383 398.5688
301.7204 311.4028
302.2025 233.4849
302.6846 162.0332
303.1667 97.89502
303.6488 41.17627
304.1310 7.096680
304.6131 49.38281
305.0952 87.20947
305.5773 120.4341
306.0594 148.5063
306.5415 170.5303
307.0237 187.8325
307.5058 201.6997
307.9879 211.9492
308.4700 220.2773
308.9521 228.2339
309.4343 235.1953
309.9164 240.2734
310.3985 243.9937
310.8806 245.1411
311.3627 243.6201
311.8448 239.4316
312.3270 229.9614
312.8091 212.9351
313.2912 189.9585
313.7733 162.9341
314.2554 134.2915
314.7375 100.1992
315.2197 58.95068
315.7018 10.25488
316.1839 44.83936
316.6660 105.2720
317.1481 172.6343
317.6302 247.5547
318.1124 333.6123
318.5945 423.3848
319.0766 514.7715
319.5587 608.2310
320.0408 706.6401
320.5229 808.4131
321.0051 917.0996
321.4872 1035.293
321.9693 1163.435
322.4514 1298.455
322.9335 1439.021
323.4156 1586.029
323.8978 1741.206
324.3799 1905.803
324.8620 2077.787
325.3441 2256.717
325.8262 2439.818
326.3083 2632.898
326.7905 2842.691
327.2726 3061.510
327.7547 3276.970
328.2368 3484.277
328.7189 3694.696
329.2010 3913.479
329.6832 4140.120
330.1653 4359.319
330.6474 4567.383
331.1295 4770.443
331.6116 4975.519
332.0938 5181.781
332.5759 5392.079
333.0580 5603.491
333.5401 5818.573
334.0222 6040.133
334.5043 6265.614
334.9865 6503.534
335.4686 6760.634
335.9507 7038.052
336.4328 7333.751
336.9149 7650.010
337.3970 7988.029
337.8792 8337.836
338.3613 8703.997
338.8434 9082.968
339.3255 9483.105
339.8076 9911.814
340.2898 10321.26
340.7719 10722.29
341.2540 11092.33
341.7361 11414.19
342.2182 11685.02
342.7003 11887.43
343.1825 12025.29
343.6646 12091.63
344.1467 12029.50
344.6288 11834.93
345.1109 11529.72
345.5930 11113.75
346.0752 10596.27
346.5573 10019.33
347.0394 9373.315
347.5215 8686.726
348.0036 7990.113
348.4857 7287.260
348.9679 6614.827
349.4500 5986.266
349.9321 5402.499
350.4142 4869.159
350.8963 4385.460
351.3784 3948.394
351.8606 3564.633
352.3427 3233.149
352.8248 2942.313
353.3069 2693.495
353.7890 2482.763
354.2711 2302.532
354.7533 2153.420
355.2354 2029.441
355.7175 1931.905
356.1996 1856.925
356.6817 1797.727
357.1638 1750.601
357.6460 1718.861
358.1281 1705.667
358.6102 1710.573
359.0923 1728.515
359.5744 1760.200
360.0565 1801.919
360.5387 1850.330
361.0208 1906.992
361.5029 1964.738
361.9850 2019.293
362.4671 2072.162
362.9492 2127.039
363.4314 2191.927
363.9135 2254.878
364.3956 2310.018
364.8777 2357.097
365.3598 2396.812
365.8419 2429.674
366.3241 2455.693
366.8062 2474.292
367.2883 2484.515
367.7704 2488.411
368.2526 2485.387
368.7347 2474.582
369.2168 2463.380
369.6989 2452.718
370.1810 2441.880
370.6631 2430.696
371.1453 2420.670
371.6274 2409.324
372.1095 2397.128
372.5916 2384.041
373.0737 2368.524
373.5558 2353.134
374.0380 2332.547
374.5201 2303.107
375.0022 2264.246
375.4843 2211.897
375.9664 2144.955
376.4485 2065.348
376.9307 1974.008
377.4128 1870.672
377.8949 1759.772
378.3770 1641.938
378.8591 1518.070
379.3412 1395.323
379.8234 1274.768
380.3055 1155.191
380.7876 1035.037
381.2697 913.8413
381.7518 801.6821
382.2339 701.8311
382.7161 612.4473
383.1982 526.9829
383.6803 446.2900
384.1624 373.4663
384.6445 313.9854
385.1266 264.7993
385.6088 217.5425
386.0909 169.9272
386.5730 127.6211
387.0551 97.69238
387.5372 79.09570
388.0193 68.41699
388.5015 64.85840
388.9836 68.01025
389.4657 78.08789
389.9478 95.14990
390.4299 116.7056
390.9120 140.6567
391.3942 168.2598
391.8763 200.8188
392.3584 243.3506
392.8405 286.5991
393.3226 325.9541
393.8047 362.0093
394.2869 397.4673
394.7690 433.2207
395.2511 468.8423
395.7332 504.7109
396.2154 543.6343
396.6975 576.9766
397.1796 601.0156
397.6617 618.9502
398.1438 636.1460
398.6259 657.3662
399.1081 674.1440
399.5902 682.0156
400.0723 678.9736
400.5544 680.7593
401.0365 688.0947
401.5186 699.6133
402.0008 714.4229
402.4829 734.6396
402.9650 753.4766
403.4471 766.3032
403.9292 777.2456
404.4113 805.0684
404.8935 856.2104
405.3756 909.6694
405.8577 953.2368
406.3398 984.2529
406.8219 1022.278
407.3040 1067.443
407.7862 1120.130
408.2683 1183.931
408.7504 1259.241
409.2325 1335.191
409.7146 1408.642
410.1967 1479.543
410.6789 1552.668
411.1610 1628.216
411.6431 1703.429
412.1252 1777.338
412.6073 1848.751
413.0894 1914.341
413.5716 1973.431
414.0537 2023.494
414.5358 2061.383
415.0179 2086.915
415.5000 2100.799
415.9821 2103.083
416.4643 2093.657
416.9464 2073.085
417.4285 2041.672
417.9106 1995.667
418.3927 1926.127
418.8748 1842.845
419.3570 1758.720
419.8391 1674.377
420.3212 1592.765
420.8033 1513.106
421.2854 1436.254
421.7675 1364.292
422.2497 1298.190
422.7318 1237.193
423.2139 1180.906
423.6960 1125.405
424.1781 1083.118
424.6602 1055.402
425.1424 1041.887
425.6245 1042.651
426.1066 1060.225
426.5887 1088.763
427.0709 1128.425
427.5530 1179.081
428.0351 1234.440
428.5172 1298.099
428.9993 1362.068
429.4814 1422.790
429.9636 1482.450
430.4457 1528.720
430.9278 1560.105
431.4099 1577.693
431.8920 1582.991
432.3741 1575.426
432.8563 1558.806
433.3384 1534.463
433.8205 1502.160
434.3026 1461.580
434.7847 1412.136
435.2668 1356.957
435.7490 1296.124
436.2311 1231.197
436.7132 1170.252
437.1953 1114.895
437.6774 1064.736
438.1595 1018.733
438.6417 976.6138
439.1238 937.3848
439.6059 900.8042
440.0880 866.7373
440.5701 835.0825
441.0522 805.7388
441.5344 779.0112
442.0165 755.5566
442.4986 734.3569
442.9807 714.2832
443.4628 694.2607
443.9449 676.2969
444.4271 660.9229
444.9092 648.3096
445.3913 638.8413
445.8734 633.0942
446.3555 630.4072
446.8376 631.0854
447.3198 638.3784
447.8019 642.9541
448.2840 639.2993
448.7661 635.0083
449.2482 641.0142
449.7303 662.0396
450.2125 685.2285
450.6946 707.1855
451.1767 728.5249
451.6588 756.3628
452.1409 791.3267
452.6230 831.8105
453.1052 876.6001
453.5873 926.1543
454.0694 978.9199
454.5515 1034.460
455.0337 1093.539
455.5158 1155.891
455.9979 1222.059
456.4800 1292.429
456.9621 1370.505
457.4442 1452.587
457.9264 1531.994
458.4085 1608.381
458.8906 1680.559
459.3727 1747.985
459.8548 1809.898
460.3369 1864.289
460.8191 1912.640
461.3012 1950.584
461.7833 1974.469
462.2654 1985.596
462.7475 1986.624
463.2296 1982.370
463.7118 1965.338
464.1939 1930.011
464.6760 1875.650
465.1581 1811.578
465.6402 1738.038
466.1223 1657.784
466.6045 1573.612
467.0866 1483.665
467.5687 1392.696
468.0508 1298.073
468.5329 1202.296
469.0150 1109.600
469.4972 1021.657
469.9793 935.9644
470.4614 852.2476
470.9435 770.4380
471.4256 692.5640
471.9077 618.4604
472.3899 548.8052
472.8720 484.5029
473.3541 424.8843
473.8362 370.2661
474.3183 320.7378
474.8004 275.3213
475.2826 232.0039
475.7647 190.8481
476.2468 152.9771
476.7289 118.1655
477.2110 87.01074
477.6931 61.66895
478.1753 41.97900
478.6574 26.36768
479.1395 16.27100
479.6216 8.636230
480.1037 1.376953
480.5858 16.70117
481.0680 31.52588
481.5501 41.45557
482.0322 47.96777
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