#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:49:11 +0300 (Thu, 24 May 2018) $
#$Revision: 798 $
#$URL: svn://172.16.1.111/rod/cif/1/00/02/1000292.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000292
loop_
_publ_author_name
'Kolitsch, U.'
'Giester, G.'
_publ_section_title
;
 The crystal structure of namibite, Cu(BiO)2VO4(OH), and a revision of its
 symmetry
;
_journal_name_full               'American Mineralogist'
_journal_page_first              1298
_journal_page_last               1301
_journal_volume                  85
_journal_year                    2000
_chemical_compound_source        R100182
_chemical_formula_sum            'Bi2 Cu H O7 V'
_chemical_name_mineral           Namibite
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                90.10
_cell_angle_beta                 108.73
_cell_angle_gamma                107.47
_cell_length_a                   6.210
_cell_length_b                   7.398
_cell_length_c                   7.471
_cell_volume                     308.224
_exptl_crystal_density_diffrn    6.955
_cod_original_formula_sum        'Bi2 Cu V O7 H'
_cod_database_code               9002427
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R100182.rod
_rod_data_source.block           3500000
_rod_database.code               1000292
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9002427 COD http://www.crystallography.net/cod/9002427.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
134.9078 0.0000000E+00
135.3899 5.863655
135.8721 3.809082
136.3542 1.555862
136.8363 2.512024
137.3184 1.142746
137.8005 9.761795
138.2826 23.43571
138.7648 38.90472
139.2469 54.37784
139.7290 70.68564
140.2111 93.49295
140.6932 123.9027
141.1753 158.8853
141.6575 195.3917
142.1396 234.0661
142.6217 273.4130
143.1038 312.6575
143.5859 352.0593
144.0681 393.3755
144.5502 437.5552
145.0323 483.0876
145.5144 529.3474
145.9965 576.8003
146.4786 623.6446
146.9608 667.4594
147.4429 707.1212
147.9250 751.3865
148.4071 798.0771
148.8892 850.2874
149.3713 911.3434
149.8535 981.6033
150.3356 1061.237
150.8177 1151.961
151.2998 1260.552
151.7819 1365.340
152.2640 1476.240
152.7462 1582.813
153.2283 1663.997
153.7104 1731.878
154.1925 1763.573
154.6746 1748.893
155.1567 1675.295
155.6389 1576.397
156.1210 1439.544
156.6031 1278.555
157.0852 1126.177
157.5673 983.3096
158.0495 855.1086
158.5316 742.8741
159.0137 649.2368
159.4958 569.7488
159.9779 505.2511
160.4600 454.0101
160.9422 410.3588
161.4243 374.2501
161.9064 344.0292
162.3885 318.7957
162.8706 299.4184
163.3527 283.3380
163.8349 269.0363
164.3170 256.7702
164.7991 247.9586
165.2812 244.3105
165.7633 243.9966
166.2454 245.4181
166.7276 249.3874
167.2097 253.8049
167.6918 257.1788
168.1739 259.6724
168.6560 262.9606
169.1381 268.5040
169.6203 274.9854
170.1024 276.2290
170.5845 275.4512
171.0666 274.0106
171.5487 270.3173
172.0309 264.6316
172.5130 259.2921
172.9951 257.0434
173.4772 256.2615
173.9593 254.1437
174.4414 249.6570
174.9236 244.1582
175.4057 238.6655
175.8878 232.8513
176.3699 227.2137
176.8520 222.3352
177.3341 217.9352
177.8163 213.4017
178.2984 208.4929
178.7805 203.3092
179.2626 197.9865
179.7447 192.6099
180.2268 187.0642
180.7090 181.1666
181.1911 175.0364
181.6732 169.1063
182.1553 163.6517
182.6374 158.5325
183.1195 153.5950
183.6017 148.7669
184.0838 144.1614
184.5659 139.3155
185.0480 134.4929
185.5301 130.8609
186.0123 129.9777
186.4944 130.8159
186.9765 130.0310
187.4586 127.2781
187.9407 123.7277
188.4228 121.0013
188.9050 119.0232
189.3871 116.9192
189.8692 114.5393
190.3513 111.7821
190.8334 107.8170
191.3155 102.3940
191.7977 96.38712
192.2798 91.08386
192.7619 85.01935
193.2440 79.37091
193.7261 74.04044
194.2082 69.05594
194.6904 64.46490
195.1725 60.55084
195.6546 56.53012
196.1367 50.50363
196.6188 42.27792
197.1009 34.85803
197.5831 30.04324
198.0652 27.74261
198.5473 25.78806
199.0294 24.16812
199.5115 22.61288
199.9937 20.34488
200.4758 17.18469
200.9579 14.19916
201.4400 12.11853
201.9221 11.05618
202.4042 10.32468
202.8864 9.728455
203.3685 9.229706
203.8506 9.245300
204.3327 10.08835
204.8148 10.55029
205.2969 9.512970
205.7791 6.543427
206.2612 4.842743
206.7433 5.148743
207.2254 6.481903
207.7075 5.915771
208.1896 2.644836
208.6718 0.7487180
209.1539 2.268188
209.6360 1.116852
210.1181 1.485748
210.6002 4.412323
211.0823 8.539001
211.5645 9.733917
212.0466 6.954498
212.5287 3.693054
213.0108 1.734222
213.4929 1.208344
213.9750 1.487915
214.4572 3.018036
214.9393 5.134888
215.4214 5.893280
215.9035 5.040466
216.3856 3.348206
216.8678 1.084900
217.3499 2.104645
217.8320 4.764252
218.3141 6.754517
218.7962 8.161957
219.2783 9.026764
219.7605 8.668243
220.2426 8.960388
220.7247 11.13681
221.2068 16.11978
221.6889 20.18658
222.1710 22.48343
222.6532 23.92035
223.1353 27.47650
223.6174 34.39996
224.0995 41.43668
224.5816 46.91428
225.0637 50.34067
225.5459 53.58749
226.0280 56.60760
226.5101 59.52563
226.9922 62.66547
227.4743 66.31024
227.9564 69.77298
228.4386 72.81207
228.9207 75.46793
229.4028 77.48056
229.8849 78.86835
230.3670 79.60828
230.8492 79.61700
231.3313 78.65829
231.8134 77.33099
232.2955 75.78357
232.7776 73.67737
233.2597 72.21689
233.7419 71.46606
234.2240 71.35852
234.7061 71.73041
235.1882 72.54498
235.6703 73.90421
236.1524 75.91705
236.6346 78.83850
237.1167 81.80051
237.5988 84.55756
238.0809 87.44025
238.5630 91.36047
239.0451 96.84360
239.5273 102.5307
240.0094 107.9629
240.4915 113.3441
240.9736 117.9332
241.4557 121.7109
241.9378 124.7197
242.4200 127.1059
242.9021 129.1948
243.3842 130.1649
243.8663 129.6107
244.3484 127.1437
244.8306 124.4165
245.3127 122.2320
245.7948 119.4046
246.2769 113.3632
246.7590 102.0818
247.2411 91.18420
247.7233 82.99109
248.2054 78.76453
248.6875 72.35861
249.1696 62.65561
249.6517 51.60681
250.1338 42.51355
250.6160 36.30713
251.0981 30.36185
251.5802 23.74817
252.0623 16.03769
252.5444 9.714783
253.0265 5.290802
253.5087 1.881775
253.9908 1.676910
254.4729 5.643036
254.9550 9.296600
255.4371 12.45636
255.9192 15.07571
256.4014 17.38159
256.8835 19.52808
257.3656 21.21158
257.8477 21.96802
258.3298 21.20810
258.8120 20.90149
259.2941 21.92282
259.7762 24.45493
260.2583 25.12247
260.7404 23.18762
261.2225 20.32889
261.7047 18.40598
262.1868 17.97330
262.6689 17.02130
263.1510 14.99255
263.6331 11.93802
264.1152 9.194977
264.5974 7.325714
265.0795 4.915344
265.5616 0.2964170
266.0437 7.583984
266.5258 14.34933
267.0079 18.77521
267.4901 21.29453
267.9722 25.15405
268.4543 30.74112
268.9364 36.82712
269.4185 42.41367
269.9006 47.32559
270.3828 53.02673
270.8649 59.66324
271.3470 67.22842
271.8291 76.03839
272.3112 86.43994
272.7933 97.32535
273.2755 107.7982
273.7576 117.7846
274.2397 128.1153
274.7218 138.6347
275.2039 149.5892
275.6860 161.7802
276.1682 175.4157
276.6503 189.9231
277.1324 205.2672
277.6145 221.3974
278.0966 237.3225
278.5787 252.8446
279.0609 268.2323
279.5430 284.2411
280.0251 300.8002
280.5072 318.1139
280.9893 336.8757
281.4715 356.9332
281.9536 375.6664
282.4357 392.5778
282.9178 408.8972
283.3999 426.7638
283.8820 446.2302
284.3642 466.0992
284.8463 485.7379
285.3284 505.2718
285.8105 525.4147
286.2926 546.4368
286.7747 567.4543
287.2569 587.1038
287.7390 605.4152
288.2211 623.6282
288.7032 642.6386
289.1853 661.9965
289.6674 679.9918
290.1496 696.6589
290.6317 712.3791
291.1138 728.1191
291.5959 743.6603
292.0780 756.8706
292.5602 766.8074
293.0423 774.1920
293.5244 781.3888
294.0065 788.4668
294.4886 793.0637
294.9707 793.2177
295.4529 789.1575
295.9350 781.6773
296.4171 770.4519
296.8992 756.3374
297.3813 740.9379
297.8634 724.2920
298.3456 705.7841
298.8277 684.6108
299.3098 661.4214
299.7919 637.3478
300.2740 612.0280
300.7561 587.2996
301.2383 566.9751
301.7204 550.1164
302.2025 533.8663
302.6846 515.5334
303.1667 496.7811
303.6488 479.5948
304.1310 464.3658
304.6131 450.9905
305.0952 439.7982
305.5773 430.5865
306.0594 422.8448
306.5415 416.0734
307.0237 410.6766
307.5058 407.4801
307.9879 406.8868
308.4700 406.3813
308.9521 403.2166
309.4343 398.8928
309.9164 395.9663
310.3985 396.2256
310.8806 397.7167
311.3627 399.0924
311.8448 400.2542
312.3270 401.3322
312.8091 402.3398
313.2912 403.3870
313.7733 404.6010
314.2554 406.4073
314.7375 408.0965
315.2197 409.1905
315.7018 409.8314
316.1839 410.7185
316.6660 412.4539
317.1481 414.2926
317.6302 415.6159
318.1124 417.0345
318.5945 417.4034
319.0766 416.1494
319.5587 413.4563
320.0408 410.0782
320.5229 405.5990
321.0051 401.0863
321.4872 397.1223
321.9693 393.8209
322.4514 390.9845
322.9335 389.3531
323.4156 388.2660
323.8978 386.3096
324.3799 381.8569
324.8620 377.1853
325.3441 373.2920
325.8262 370.8491
326.3083 367.4252
326.7905 361.7134
327.2726 355.2656
327.7547 350.0741
328.2368 347.8787
328.7189 345.1447
329.2010 341.0211
329.6832 335.4060
330.1653 330.0310
330.6474 325.1141
331.1295 320.3055
331.6116 315.3176
332.0938 310.5807
332.5759 305.1856
333.0580 298.4686
333.5401 290.5723
334.0222 284.4652
334.5043 281.6452
334.9865 278.5359
335.4686 272.4986
335.9507 261.6197
336.4328 252.6019
336.9149 246.3469
337.3970 241.9985
337.8792 237.2985
338.3613 232.1322
338.8434 226.3715
339.3255 219.6019
339.8076 211.5414
340.2898 204.9217
340.7719 200.0361
341.2540 195.7777
341.7361 190.3484
342.2182 183.7754
342.7003 177.6946
343.1825 172.9164
343.6646 169.0815
344.1467 164.4165
344.6288 158.7194
345.1109 153.1318
345.5930 148.4014
346.0752 144.6433
346.5573 142.2590
347.0394 141.6910
347.5215 142.2055
348.0036 141.8352
348.4857 140.6184
348.9679 140.1520
349.4500 141.4903
349.9321 144.5254
350.4142 149.0249
350.8963 155.1749
351.3784 162.1966
351.8606 169.1287
352.3427 176.0076
352.8248 183.1097
353.3069 190.5721
353.7890 198.2839
354.2711 206.1880
354.7533 214.2369
355.2354 222.5585
355.7175 231.4218
356.1996 240.5360
356.6817 249.3930
357.1638 256.9856
357.6460 264.8053
358.1281 273.8635
358.6102 284.1391
359.0923 295.7433
359.5744 308.9909
360.0565 323.3867
360.5387 338.3972
361.0208 353.0756
361.5029 369.4102
361.9850 387.7112
362.4671 408.1914
362.9492 431.3391
363.4314 458.8545
363.9135 487.9703
364.3956 517.1953
364.8777 546.2469
365.3598 575.8884
365.8419 607.1511
366.3241 638.9120
366.8062 669.2878
367.2883 700.2182
367.7704 727.6208
368.2526 751.8919
368.7347 774.3109
369.2168 785.9566
369.6989 786.7435
370.1810 776.9589
370.6631 756.5254
371.1453 721.4777
371.6274 681.3717
372.1095 635.2894
372.5916 584.0293
373.0737 534.2545
373.5558 484.1762
374.0380 437.5862
374.5201 396.0031
375.0022 360.2085
375.4843 328.2986
375.9664 300.6658
376.4485 276.5234
376.9307 253.7223
377.4128 232.4040
377.8949 212.6698
378.3770 194.9450
378.8591 179.2343
379.3412 164.1696
379.8234 149.9075
380.3055 136.2068
380.7876 122.9827
381.2697 110.1398
381.7518 98.11868
382.2339 87.01773
382.7161 76.85019
383.1982 67.62686
383.6803 59.41309
384.1624 51.55838
384.6445 43.50763
385.1266 35.53619
385.6088 28.26352
386.0909 21.74908
386.5730 16.11383
387.0551 11.72153
387.5372 8.452209
388.0193 5.874176
388.5015 4.705475
388.9836 3.654053
389.4657 0.8663330
389.9478 3.825165
390.4299 7.948120
390.9120 9.432892
391.3942 9.504425
391.8763 9.636932
392.3584 10.87030
392.8405 11.78568
393.3226 11.15762
393.8047 9.399170
394.2869 8.401031
394.7690 9.832947
395.2511 11.61624
395.7332 12.42810
396.2154 11.61966
396.6975 10.75809
397.1796 10.42194
397.6617 10.19791
398.1438 9.379974
398.6259 6.929352
399.1081 4.797913
399.5902 3.743896
400.0723 4.018311
400.5544 3.642029
401.0365 2.208740
401.5186 0.4297180
402.0008 1.146576
402.4829 2.649536
402.9650 3.689331
403.4471 4.066223
403.9292 3.944672
404.4113 3.996490
404.8935 4.188965
405.3756 4.617157
405.8577 5.419556
406.3398 6.674500
406.8219 7.694336
407.3040 8.403656
407.7862 9.019379
408.2683 9.849976
408.7504 10.90247
409.2325 12.06839
409.7146 13.44876
410.1967 14.88974
410.6789 15.67154
411.1610 15.75818
411.6431 16.15222
412.1252 18.14703
412.6073 21.16605
413.0894 23.44473
413.5716 24.34601
414.0537 24.98572
414.5358 26.70065
415.0179 29.28281
415.5000 32.09760
415.9821 35.05518
416.4643 37.89542
416.9464 40.09363
417.4285 41.53613
417.9106 43.42688
418.3927 47.14438
418.8748 51.55545
419.3570 55.25974
419.8391 56.90671
420.3212 58.63235
420.8033 61.33701
421.2854 64.90024
421.7675 68.76361
422.2497 72.57153
422.7318 76.78137
423.2139 81.76381
423.6960 88.27292
424.1781 93.98085
424.6602 98.23505
425.1424 101.6403
425.6245 105.0032
426.1066 107.7791
426.5887 111.1928
427.0709 115.8057
427.5530 121.6148
428.0351 126.4996
428.5172 130.3183
428.9993 133.4613
429.4814 136.1387
429.9636 138.2470
430.4457 140.3109
430.9278 142.4397
431.4099 144.4761
431.8920 146.2176
432.3741 147.7402
432.8563 148.4425
433.3384 147.5255
433.8205 145.3507
434.3026 144.8099
434.7847 146.1191
435.2668 147.2600
435.7490 145.3902
436.2311 141.4627
436.7132 139.1285
437.1953 140.1330
437.6774 142.0426
438.1595 141.4628
438.6417 138.8380
439.1238 136.0231
439.6059 134.0036
440.0880 132.3929
440.5701 130.9598
441.0522 129.7834
441.5344 128.3091
442.0165 125.6731
442.4986 122.7500
442.9807 120.5581
443.4628 120.8077
443.9449 120.7472
444.4271 119.2161
444.9092 116.3100
445.3913 112.9124
445.8734 108.0609
446.3555 103.9426
446.8376 101.9283
447.3198 103.7957
447.8019 103.9256
448.2840 101.4671
448.7661 97.68994
449.2482 94.24611
449.7303 91.69402
450.2125 88.43719
450.6946 83.80225
451.1767 78.05856
451.6588 73.85072
452.1409 71.47537
452.6230 69.46497
453.1052 66.98714
453.5873 64.07143
454.0694 60.86165
454.5515 57.27664
455.0337 53.62521
455.5158 50.54366
455.9979 48.02045
456.4800 45.83287
456.9621 43.99216
457.4442 42.22940
457.9264 39.91818
458.4085 37.12531
458.8906 34.25227
459.3727 31.39011
459.8548 28.69249
460.3369 26.48183
460.8191 24.86015
461.3012 23.55283
461.7833 22.59424
462.2654 21.77847
462.7475 20.67711
463.2296 18.36905
463.7118 16.32140
464.1939 15.58359
464.6760 16.21663
465.1581 16.63142
465.6402 16.41331
466.1223 15.74530
466.6045 14.75684
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