#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:49:15 +0300 (Thu, 24 May 2018) $
#$Revision: 799 $
#$URL: svn://172.16.1.111/rod/cif/1/00/02/1000293.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000293
loop_
_publ_author_name
'Hofmeister, W.'
'Tillmanns, E.'
_publ_section_title
;
 Strukturelle untersuchungen an arsenbrackebuschit
;
_journal_name_full
'Tschermaks Mineralogische und Petrographische Mitteilungen'
_journal_page_first              153
_journal_page_last               163
_journal_volume                  25
_journal_year                    1978
_chemical_compound_source        R100184
_chemical_formula_sum            'As2 Fe0.65 H2.65 O9 Pb2 Zn0.35'
_chemical_name_mineral           Arsenbrackebuschite
_space_group_IT_number           11
_symmetry_space_group_name_Hall  '-P 2yb'
_symmetry_space_group_name_H-M   'P 1 21/m 1'
_cell_angle_alpha                90
_cell_angle_beta                 112.5
_cell_angle_gamma                90
_cell_length_a                   7.763
_cell_length_b                   6.046
_cell_length_c                   9.022
_cell_volume                     391.215
_exptl_crystal_density_diffrn    6.537
_cod_original_formula_sum        'Pb2 (Fe.65 Zn.35) As2 O9 H2.65'
_cod_database_code               9009598
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R100184.rod
_rod_data_source.block           3500000
_rod_database.code               1000293
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9009598 COD http://www.crystallography.net/cod/9009598.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
150.8177 0.0000000E+00
151.2998 0.5313420
151.7819 1.523407
152.2640 6.119293
152.7462 12.35901
153.2283 19.79941
153.7104 28.69888
154.1925 37.80789
154.6746 46.66150
155.1567 55.47787
155.6389 62.98160
156.1210 68.58734
156.6031 72.68204
157.0852 76.39767
157.5673 80.24747
158.0495 83.47937
158.5316 85.76028
159.0137 86.82483
159.4958 87.15067
159.9779 86.30441
160.4600 84.67551
160.9422 83.56335
161.4243 83.58801
161.9064 84.13892
162.3885 84.77853
162.8706 84.97894
163.3527 85.74057
163.8349 87.60229
164.3170 90.43240
164.7991 93.63208
165.2812 96.67392
165.7633 100.0814
166.2454 104.3492
166.7276 110.0941
167.2097 116.2481
167.6918 122.2029
168.1739 127.9546
168.6560 134.1097
169.1381 141.7862
169.6203 149.6563
170.1024 153.1295
170.5845 152.5908
171.0666 151.6398
171.5487 151.7984
172.0309 152.9940
172.5130 154.4846
172.9951 156.6134
173.4772 158.5920
173.9593 159.1690
174.4414 157.1669
174.9236 153.9320
175.4057 150.7498
175.8878 147.5922
176.3699 144.6185
176.8520 142.2823
177.3341 140.2010
177.8163 137.5695
178.2984 134.2729
178.7805 130.1955
179.2626 125.1514
179.7447 119.4964
180.2268 113.8056
180.7090 108.5623
181.1911 103.9971
181.6732 99.91571
182.1553 96.66959
182.6374 93.42474
183.1195 88.67017
183.6017 82.51770
184.0838 76.50140
184.5659 71.76511
185.0480 67.78275
185.5301 64.22668
186.0123 61.11459
186.4944 58.51544
186.9765 56.47983
187.4586 54.18845
187.9407 51.89105
188.4228 49.45569
188.9050 46.43893
189.3871 43.96542
189.8692 42.53729
190.3513 41.65918
190.8334 40.07269
191.3155 37.48148
191.7977 34.37271
192.2798 31.71896
192.7619 29.61548
193.2440 27.57870
193.7261 25.06754
194.2082 22.20197
194.6904 20.46771
195.1725 20.26688
195.6546 20.58911
196.1367 19.44672
196.6188 16.74622
197.1009 13.86554
197.5831 11.39874
198.0652 9.322815
198.5473 7.810760
199.0294 6.949554
199.5115 6.528717
199.9937 6.213287
200.4758 6.036163
200.9579 5.742157
201.4400 5.046112
201.9221 3.884308
202.4042 3.252014
202.8864 3.412201
203.3685 3.916443
203.8506 3.600586
204.3327 2.269745
204.8148 0.9123230
205.2969 6.3568003E-02
205.7791 0.2265320
206.2612 0.3426510
206.7433 0.1977840
207.2254 2.4901999E-02
207.7075 0.1946720
208.1896 0.9828800
208.6718 1.980194
209.1539 2.665436
209.6360 2.912354
210.1181 3.466400
210.6002 4.531952
211.0823 5.848419
211.5645 6.684113
212.0466 6.990234
212.5287 6.931335
213.0108 6.530548
213.4929 5.679810
213.9750 4.860901
214.4572 3.989014
214.9393 3.208893
215.4214 2.989410
215.9035 3.542999
216.3856 4.233398
216.8678 4.808472
217.3499 5.435272
217.8320 5.394836
218.3141 4.365051
218.7962 2.745819
219.2783 1.796173
219.7605 1.695923
220.2426 1.972839
220.7247 2.429871
221.2068 3.149536
221.6889 3.879211
222.1710 4.856964
222.6532 5.777252
223.1353 5.459473
223.6174 2.984955
224.0995 0.7881470
224.5816 0.2617190
225.0637 2.347809
225.5459 3.637268
226.0280 3.700043
226.5101 2.970764
226.9922 2.843567
227.4743 3.780884
227.9564 4.589264
228.4386 4.628784
228.9207 3.470367
229.4028 2.610504
229.8849 2.209686
230.3670 2.090973
230.8492 1.734589
231.3313 1.063538
231.8134 0.2807920
232.2955 0.5426640
232.7776 1.398499
233.2597 2.291626
233.7419 3.224640
234.2240 4.206299
234.7061 5.204407
235.1882 6.115662
235.6703 7.207397
236.1524 8.684082
236.6346 10.93732
237.1167 12.65686
237.5988 13.69427
238.0809 14.26102
238.5630 14.77579
239.0451 14.82767
239.5273 15.43317
240.0094 17.19083
240.4915 20.93921
240.9736 23.55374
241.4557 24.30722
241.9378 24.25385
242.4200 25.69220
242.9021 29.60355
243.3842 33.50540
243.8663 36.42328
244.3484 37.96503
244.8306 39.67499
245.3127 41.50284
245.7948 43.51157
246.2769 45.83298
246.7590 48.56122
247.2411 51.39545
247.7233 54.18228
248.2054 56.79553
248.6875 59.88193
249.1696 63.55200
249.6517 67.59445
250.1338 71.61432
250.6160 75.42978
251.0981 79.58313
251.5802 84.29907
252.0623 89.77200
252.5444 94.94940
253.0265 99.67596
253.5087 104.2026
253.9908 108.7590
254.4729 113.3235
254.9550 118.0211
255.4371 122.8452
255.9192 127.7033
256.4014 133.1093
256.8835 139.2972
257.3656 145.8044
257.8477 152.3713
258.3298 159.3418
258.8120 165.5919
259.2941 170.5834
259.7762 174.2049
260.2583 178.9052
260.7404 185.2546
261.2225 192.0161
261.7047 197.9982
262.1868 202.9286
262.6689 207.7816
263.1510 212.8263
263.6331 218.0246
264.1152 223.1062
264.5974 228.2302
265.0795 232.9707
265.5616 236.6150
266.0437 238.8214
266.5258 241.1851
267.0079 244.2104
267.4901 247.7903
267.9722 250.5073
268.4543 252.4679
268.9364 253.3541
269.4185 252.9084
269.9006 251.0695
270.3828 248.3452
270.8649 244.6115
271.3470 240.0931
271.8291 235.8162
272.3112 231.9930
272.7933 227.6927
273.2755 222.1811
273.7576 215.2960
274.2397 207.9119
274.7218 200.1554
275.2039 191.9956
275.6860 183.3860
276.1682 174.2577
276.6503 164.9437
277.1324 155.4180
277.6145 145.6827
278.0966 136.3171
278.5787 127.5376
279.0609 118.9924
279.5430 109.4389
280.0251 98.64487
280.5072 88.54745
280.9893 80.56970
281.4715 74.88110
281.9536 68.92621
282.4357 62.40305
282.9178 55.54349
283.3999 48.85574
283.8820 42.37573
284.3642 36.56619
284.8463 31.51331
285.3284 27.14789
285.8105 23.76868
286.2926 21.52496
286.7747 19.92355
287.2569 18.20432
287.7390 16.35172
288.2211 14.68295
288.7032 13.07065
289.1853 11.74139
289.6674 11.69061
290.1496 12.99017
290.6317 15.07761
291.1138 17.44360
291.5959 20.09073
292.0780 22.97159
292.5602 26.04364
293.0423 29.38043
293.5244 33.05554
294.0065 37.04349
294.4886 41.71191
294.9707 47.55698
295.4529 54.45218
295.9350 61.76791
296.4171 69.30591
296.8992 77.31464
297.3813 86.31812
297.8634 96.21500
298.3456 106.3949
298.8277 116.2718
299.3098 126.0008
299.7919 135.7245
300.2740 145.0449
300.7561 155.0236
301.2383 166.7642
301.7204 180.2388
302.2025 194.5722
302.6846 209.9375
303.1667 225.6997
303.6488 241.0367
304.1310 255.3988
304.6131 270.2015
305.0952 287.0734
305.5773 305.4160
306.0594 323.5358
306.5415 341.3360
307.0237 358.1802
307.5058 373.4264
307.9879 386.7612
308.4700 399.5653
308.9521 413.7803
309.4343 428.1457
309.9164 440.7790
310.3985 451.1996
310.8806 459.4624
311.3627 465.8624
311.8448 470.4781
312.3270 472.3352
312.8091 469.8937
313.2912 464.6897
313.7733 458.5389
314.2554 452.9397
314.7375 445.8224
315.2197 435.8304
315.7018 423.0821
316.1839 409.3430
316.6660 394.8541
317.1481 379.9220
317.6302 364.9289
318.1124 349.1593
318.5945 334.2216
319.0766 320.4848
319.5587 307.9279
320.0408 296.2517
320.5229 285.6062
321.0051 275.6417
321.4872 266.0919
321.9693 256.7970
322.4514 248.3495
322.9335 240.9614
323.4156 234.4997
323.8978 228.7079
324.3799 223.2964
324.8620 218.7623
325.3441 215.3492
325.8262 213.3336
326.3083 211.7450
326.7905 210.4717
327.2726 209.5958
327.7547 209.2350
328.2368 209.2794
328.7189 209.9455
329.2010 211.2810
329.6832 213.2772
330.1653 215.9220
330.6474 219.7282
331.1295 223.8112
331.6116 227.3901
332.0938 229.2348
332.5759 232.6038
333.0580 238.4814
333.5401 246.4824
334.0222 253.2933
334.5043 258.4272
334.9865 263.1160
335.4686 268.0486
335.9507 273.1236
336.4328 278.8387
336.9149 285.6201
337.3970 292.9588
337.8792 299.2562
338.3613 304.2800
338.8434 309.0599
339.3255 314.1138
339.8076 319.5035
340.2898 324.7153
340.7719 330.0294
341.2540 334.8293
341.7361 338.3511
342.2182 340.5486
342.7003 341.3262
343.1825 340.5086
343.6646 338.1720
344.1467 335.2177
344.6288 331.7816
345.1109 327.3148
345.5930 320.7156
346.0752 312.0864
346.5573 302.6508
347.0394 292.6461
347.5215 282.1970
348.0036 271.1511
348.4857 259.5520
348.9679 247.4614
349.4500 234.5698
349.9321 220.9934
350.4142 207.1794
350.8963 193.0323
351.3784 178.9601
351.8606 165.5930
352.3427 153.0317
352.8248 141.1758
353.3069 129.8143
353.7890 119.1190
354.2711 109.3542
354.7533 100.7076
355.2354 92.63898
355.7175 84.83990
356.1996 77.33145
356.6817 70.18536
357.1638 63.10306
357.6460 56.65814
358.1281 51.24789
358.6102 46.86954
359.0923 43.13452
359.5744 40.34793
360.0565 37.91919
360.5387 35.26602
361.0208 32.01129
361.5029 28.76108
361.9850 25.62366
362.4671 22.68570
362.9492 20.26944
363.4314 18.74625
363.9135 17.58716
364.3956 16.48251
364.8777 15.26746
365.3598 14.39246
365.8419 14.42731
366.3241 14.75696
366.8062 14.45917
367.2883 12.25540
367.7704 10.52026
368.2526 10.26199
368.7347 11.95166
369.2168 12.42206
369.6989 10.35352
370.1810 7.837524
370.6631 6.583862
371.1453 7.431610
371.6274 8.323242
372.1095 9.257507
372.5916 10.12088
373.0737 10.04950
373.5558 8.340424
374.0380 6.731171
374.5201 6.303894
375.0022 7.600586
375.4843 8.255707
375.9664 7.957031
376.4485 7.188324
376.9307 6.792969
377.4128 6.733185
377.8949 7.257263
378.3770 8.769562
378.8591 11.18155
379.3412 12.66995
379.8234 13.06342
380.3055 13.10657
380.7876 13.72745
381.2697 14.87985
381.7518 15.64429
382.2339 15.52261
382.7161 15.06226
383.1982 15.75241
383.6803 17.55237
384.1624 19.29105
384.6445 20.08481
385.1266 20.14789
385.6088 19.94693
386.0909 19.49030
386.5730 18.98929
387.0551 18.88382
387.5372 18.98138
388.0193 18.71027
388.5015 17.68097
388.9836 16.18430
389.4657 14.35593
389.9478 12.18619
390.4299 10.24216
390.9120 9.197052
391.3942 8.505676
391.8763 7.515686
392.3584 5.497498
392.8405 3.605804
393.3226 2.656860
393.8047 2.428162
394.2869 1.898132
394.7690 0.2535100
395.2511 1.531311
395.7332 2.869812
396.2154 3.610535
396.6975 4.021851
397.1796 3.948120
397.6617 3.620758
398.1438 3.433899
398.6259 3.699646
399.1081 3.864227
399.5902 3.744049
400.0723 3.295380
400.5544 2.859863
401.0365 2.089722
401.5186 1.600586
402.0008 2.022430
402.4829 4.381927
402.9650 5.670227
403.4471 5.092743
403.9292 3.201660
404.4113 2.354187
404.8935 2.832947
405.3756 3.688660
405.8577 4.568115
406.3398 5.522247
406.8219 5.966904
407.3040 5.780685
407.7862 5.298676
408.2683 4.922134
408.7504 4.643021
409.2325 4.664795
409.7146 5.449890
410.1967 6.489487
410.6789 5.864777
411.1610 3.517212
411.6431 0.9557950
412.1252 0.3402860
412.6073 0.7951200
413.0894 1.578369
413.5716 2.893051
414.0537 4.641678
414.5358 6.841156
415.0179 9.394836
415.5000 12.05313
415.9821 14.53934
416.4643 17.10202
416.9464 20.13786
417.4285 23.69902
417.9106 27.07805
418.3927 29.33853
418.8748 31.31744
419.3570 33.97476
419.8391 38.30508
420.3212 42.74727
420.8033 46.60739
421.2854 50.01355
421.7675 53.63840
422.2497 57.83589
422.7318 62.20526
423.2139 66.57422
423.6960 71.15997
424.1781 75.22285
424.6602 78.15619
425.1424 80.65332
425.6245 83.72925
426.1066 88.36923
426.5887 92.28271
427.0709 94.58742
427.5530 95.28362
428.0351 97.16005
428.5172 100.9976
428.9993 104.9627
429.4814 107.7796
429.9636 109.3050
430.4457 110.1732
430.9278 110.3136
431.4099 109.9418
431.8920 109.4155
432.3741 108.6799
432.8563 108.1523
433.3384 108.2006
433.8205 108.6866
434.3026 108.7060
434.7847 108.2484
435.2668 107.4143
435.7490 106.3999
436.2311 105.1080
436.7132 103.1154
437.1953 99.85556
437.6774 96.48386
438.1595 94.67877
438.6417 94.15688
439.1238 93.74371
439.6059 92.54846
440.0880 91.19766
440.5701 90.38177
441.0522 90.21588
441.5344 90.28452
442.0165 90.37939
442.4986 90.53833
442.9807 90.80962
443.4628 91.13206
443.9449 91.64420
444.4271 92.32729
444.9092 93.21381
445.3913 94.49405
445.8734 96.58594
446.3555 98.77554
446.8376 100.6440
447.3198 101.6819
447.8019 103.3677
448.2840 106.0586
448.7661 109.2544
449.2482 112.2317
449.7303 114.5948
450.2125 117.3963
450.6946 121.0537
451.1767 125.4961
451.6588 129.2982
452.1409 132.1236
452.6230 135.1430
453.1052 139.3430
453.5873 144.9316
454.0694 149.5336
454.5515 152.6905
455.0337 155.4278
455.5158 159.3349
455.9979 164.3823
456.4800 169.7480
456.9621 175.1125
457.4442 180.6276
457.9264 186.7952
458.4085 193.5703
458.8906 200.5195
459.3727 206.8846
459.8548 213.1569
460.3369 220.0648
460.8191 228.1783
461.3012 236.5239
461.7833 244.0153
462.2654 251.1586
462.7475 259.0124
463.2296 269.0771
463.7118 279.2497
464.1939 288.0438
464.6760 295.4373
465.1581 303.5148
465.6402 313.1092
466.1223 323.4440
466.6045 333.8744
467.0866 344.4144
467.5687 354.7760
468.0508 365.1393
468.5329 375.4272
469.0150 385.5364
469.4972 395.5689
469.9793 405.0282
470.4614 413.5176
470.9435 420.9976
471.4256 428.8155
471.9077 437.4917
472.3899 445.4017
472.8720 450.9826
473.3541 454.1678
473.8362 456.6191
474.3183 458.7719
474.8004 460.0375
475.2826 459.3730
475.7647 456.7857
476.2468 452.3854
476.7289 445.9075
477.2110 437.6754
477.6931 428.5324
478.1753 418.4503
478.6574 407.2904
479.1395 394.6435
479.6216 380.9288
480.1037 366.7249
480.5858 352.0109
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