#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:49:32 +0300 (Thu, 24 May 2018) $
#$Revision: 803 $
#$URL: svn://172.16.1.111/rod/cif/1/00/02/1000296.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000296
loop_
_publ_author_name
'Kampf, A. R.'
'Downs, R. T.'
'Housley, R. M.'
'Jenkins, R. A.'
'Hyrsl, J.'
_publ_section_title
;
 Anorpiment, As2S3, the triclinic dimorph of orpiment
;
_journal_name_full               'Mineralogical Magazine'
_journal_page_first              2857
_journal_page_last               2867
_journal_paper_doi               10.1180/minmag.2011.075.6.2857
_journal_volume                  75
_journal_year                    2011
_chemical_compound_source
'Palomo mine, Castrovirreyna Province, Huancavelica Department, Peru'
_chemical_formula_sum            'As2 S3'
_chemical_name_mineral           Anorpiment
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                78.152
_cell_angle_beta                 75.817
_cell_angle_gamma                89.861
_cell_length_a                   5.7577
_cell_length_b                   8.7169
_cell_length_c                   10.2682
_cell_volume                     488.377
_exptl_crystal_density_diffrn    3.346
_cod_database_code               9015549
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R110016.rod
_rod_data_source.block           3500000
_rod_database.code               1000296
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9015549 COD http://www.crystallography.net/cod/9015549.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
139.7290 0.0000000E+00
140.2111 0.1707110
140.6932 2.057850
141.1753 4.830626
141.6575 5.886719
142.1396 7.028217
142.6217 8.712254
143.1038 6.100824
143.5859 3.275572
144.0681 1.064077
144.5502 0.7209490
145.0323 1.749884
145.5144 1.512726
145.9965 0.6577800
146.4786 3.024811
146.9608 5.107113
147.4429 6.923103
147.9250 8.602966
148.4071 9.504776
148.8892 10.51006
149.3713 12.86883
149.8535 18.05827
150.3356 23.19498
150.8177 27.38328
151.2998 29.72596
151.7819 33.03541
152.2640 37.29725
152.7462 42.54302
153.2283 48.72037
153.7104 55.05948
154.1925 62.96220
154.6746 73.09965
155.1567 86.76101
155.6389 100.1835
156.1210 111.8751
156.6031 122.9877
157.0852 136.4829
157.5673 156.3949
158.0495 176.3343
158.5316 193.4691
159.0137 207.3411
159.4958 218.0548
159.9779 224.2094
160.4600 226.9596
160.9422 230.0801
161.4243 234.2145
161.9064 239.5027
162.3885 246.0531
162.8706 254.8140
163.3527 263.8917
163.8349 271.7700
164.3170 279.0177
164.7991 288.3550
165.2812 300.8122
165.7633 316.0566
166.2454 333.8387
166.7276 355.5537
167.2097 378.4451
167.6918 400.4015
168.1739 421.6110
168.6560 445.3906
169.1381 471.5619
169.6203 501.7189
170.1024 533.5278
170.5845 572.8589
171.0666 616.1658
171.5487 657.4542
172.0309 696.9276
172.5130 740.5242
172.9951 790.4113
173.4772 847.1387
173.9593 911.9697
174.4414 983.3199
174.9236 1063.453
175.4057 1159.060
175.8878 1271.155
176.3699 1378.972
176.8520 1491.479
177.3341 1589.425
177.8163 1629.880
178.2984 1582.747
178.7805 1472.855
179.2626 1319.646
179.7447 1122.547
180.2268 925.3832
180.7090 766.6275
181.1911 643.8297
181.6732 553.0864
182.1553 500.1806
182.6374 476.8993
183.1195 469.7708
183.6017 479.2140
184.0838 499.2728
184.5659 525.3214
185.0480 556.6962
185.5301 591.0192
186.0123 628.5515
186.4944 668.2208
186.9765 709.0490
187.4586 754.4614
187.9407 790.0632
188.4228 793.0244
188.9050 765.4842
189.3871 727.7197
189.8692 681.2733
190.3513 630.7194
190.8334 599.4258
191.3155 590.3703
191.7977 596.4424
192.2798 611.7536
192.7619 635.9860
193.2440 653.8314
193.7261 661.5973
194.2082 658.2360
194.6904 632.3380
195.1725 580.7886
195.6546 512.6077
196.1367 440.5249
196.6188 363.2212
197.1009 294.1879
197.5831 241.1936
198.0652 204.0288
198.5473 174.8018
199.0294 153.9384
199.5115 139.5230
199.9937 128.0848
200.4758 119.8007
200.9579 113.6055
201.4400 109.8751
201.9221 108.8625
202.4042 105.7894
202.8864 99.77759
203.3685 92.40822
203.8506 87.28580
204.3327 84.73990
204.8148 82.95789
205.2969 81.04759
205.7791 78.94107
206.2612 76.31305
206.7433 73.10408
207.2254 69.66609
207.7075 66.66922
208.1896 64.12837
208.6718 61.44611
209.1539 58.19313
209.6360 54.17607
210.1181 51.16403
210.6002 49.46461
211.0823 48.72807
211.5645 48.00461
212.0466 47.33311
212.5287 46.47575
213.0108 45.37598
213.4929 44.09781
213.9750 42.37668
214.4572 39.77927
214.9393 36.88676
215.4214 35.63181
215.9035 36.82971
216.3856 37.92584
216.8678 37.41495
217.3499 34.75276
217.8320 32.36766
218.3141 30.46394
218.7962 28.87808
219.2783 27.05702
219.7605 24.75182
220.2426 22.65523
220.7247 21.25394
221.2068 20.95987
221.6889 20.11655
222.1710 18.33388
222.6532 16.03314
223.1353 14.62143
223.6174 14.55806
224.0995 14.62152
224.5816 14.10284
225.0637 12.50961
225.5459 11.69370
226.0280 12.17258
226.5101 13.36929
226.9922 13.27924
227.4743 10.82819
227.9564 8.794220
228.4386 8.762665
228.9207 12.03186
229.4028 14.05020
229.8849 14.32864
230.3670 13.42123
230.8492 12.94241
231.3313 13.17728
231.8134 13.39655
232.2955 13.19333
232.7776 12.04330
233.2597 11.72760
233.7419 12.72482
234.2240 14.44446
234.7061 15.26285
235.1882 14.84650
235.6703 14.05264
236.1524 13.16367
236.6346 11.89352
237.1167 11.24194
237.5988 11.53336
238.0809 12.32461
238.5630 12.64258
239.0451 12.51468
239.5273 11.84229
240.0094 10.43478
240.4915 7.716980
240.9736 5.793488
241.4557 5.068146
241.9378 4.940491
242.4200 4.122253
242.9021 2.146637
243.3842 0.1975400
243.8663 1.330139
244.3484 2.462006
244.8306 3.032532
245.3127 2.635132
245.7948 1.895691
246.2769 2.060150
246.7590 3.734741
247.2411 5.296448
247.7233 6.189850
248.2054 6.294037
248.6875 6.109070
249.1696 5.338501
249.6517 4.485229
250.1338 4.498871
250.6160 6.065826
251.0981 7.251007
251.5802 7.356232
252.0623 6.127869
252.5444 5.094055
253.0265 4.316315
253.5087 3.693665
253.9908 3.089355
254.4729 2.359650
254.9550 1.898712
255.4371 1.777863
255.9192 1.989868
256.4014 2.746094
256.8835 4.429779
257.3656 6.278961
257.8477 7.381439
258.3298 7.581543
258.8120 7.355621
259.2941 6.619263
259.7762 5.297882
260.2583 4.676514
260.7404 4.893036
261.2225 5.627075
261.7047 6.721283
262.1868 8.667023
262.6689 9.632172
263.1510 8.777222
263.6331 6.203644
264.1152 5.241150
264.5974 6.747925
265.0795 8.561188
265.5616 8.370239
266.0437 5.341370
266.5258 2.999878
267.0079 2.071014
267.4901 2.400665
267.9722 2.918030
268.4543 3.784241
268.9364 4.485992
269.4185 4.457123
269.9006 3.435638
270.3828 2.833282
270.8649 2.971222
271.3470 3.673767
271.8291 4.166565
272.3112 4.524658
272.7933 4.480530
273.2755 3.685760
273.7576 1.992645
274.2397 0.6411440
274.7218 0.1307070
275.2039 0.4943240
275.6860 0.8727420
276.1682 1.193909
276.6503 1.847290
277.1324 3.011780
277.6145 4.654114
278.0966 7.158905
278.5787 10.79590
279.0609 15.03043
279.5430 18.59579
280.0251 21.31076
280.5072 24.42618
280.9893 28.76575
281.4715 34.28479
281.9536 40.03214
282.4357 46.16568
282.9178 52.13126
283.3999 56.73608
283.8820 59.91006
284.3642 63.12817
284.8463 66.79123
285.3284 70.94962
285.8105 76.55502
286.2926 84.08527
286.7747 91.77737
287.2569 96.80548
287.7390 99.25479
288.2211 101.6005
288.7032 104.9028
289.1853 108.9226
289.6674 112.5904
290.1496 115.8705
290.6317 119.1953
291.1138 123.2264
291.5959 127.8650
292.0780 132.1664
292.5602 135.3914
293.0423 138.2796
293.5244 142.8336
294.0065 149.0768
294.4886 156.0778
294.9707 163.5555
295.4529 171.2892
295.9350 178.1998
296.4171 183.6025
296.8992 188.5357
297.3813 194.6872
297.8634 201.9799
298.3456 209.9765
298.8277 218.0192
299.3098 226.4527
299.7919 235.7143
300.2740 245.1708
300.7561 256.5821
301.2383 271.8470
301.7204 290.9322
302.2025 312.6904
302.6846 336.0516
303.1667 361.9276
303.6488 391.7519
304.1310 424.9163
304.6131 463.4699
305.0952 509.2727
305.5773 561.8657
306.0594 619.6992
306.5415 682.2516
307.0237 749.8416
307.5058 824.8765
307.9879 907.7629
308.4700 993.2518
308.9521 1078.344
309.4343 1163.641
309.9164 1252.013
310.3985 1344.616
310.8806 1441.647
311.3627 1542.645
311.8448 1648.441
312.3270 1760.148
312.8091 1871.600
313.2912 1991.653
313.7733 2130.773
314.2554 2279.430
314.7375 2459.375
315.2197 2672.856
315.7018 2924.007
316.1839 3230.847
316.6660 3589.040
317.1481 4014.949
317.6302 4518.448
318.1124 5133.501
318.5945 5788.969
319.0766 6497.264
319.5587 7237.357
320.0408 7946.867
320.5229 8626.204
321.0051 9255.830
321.4872 9829.083
321.9693 10346.60
322.4514 10791.72
322.9335 11149.92
323.4156 11434.12
323.8978 11669.09
324.3799 11808.80
324.8620 11943.63
325.3441 12099.36
325.8262 12268.05
326.3083 12483.82
326.7905 12713.48
327.2726 13004.39
327.7547 13410.81
328.2368 13844.84
328.7189 14490.33
329.2010 15401.31
329.6832 16579.73
330.1653 17906.15
330.6474 19459.75
331.1295 21102.76
331.6116 22745.46
332.0938 24405.24
332.5759 26055.14
333.0580 27781.59
333.5401 29537.20
334.0222 30918.39
334.5043 32236.78
334.9865 32772.41
335.4686 32065.77
335.9507 29881.49
336.4328 26995.37
336.9149 23125.88
337.3970 18688.32
337.8792 14876.74
338.3613 11642.03
338.8434 9005.439
339.3255 7015.418
339.8076 5718.604
340.2898 4693.373
340.7719 3964.813
341.2540 3447.998
341.7361 3027.519
342.2182 2715.882
342.7003 2448.679
343.1825 2212.939
343.6646 2005.537
344.1467 1820.581
344.6288 1655.939
345.1109 1516.185
345.5930 1405.742
346.0752 1324.987
346.5573 1262.673
347.0394 1217.659
347.5215 1187.473
348.0036 1166.789
348.4857 1155.605
348.9679 1151.584
349.4500 1158.238
349.9321 1171.231
350.4142 1180.220
350.8963 1186.944
351.3784 1180.928
351.8606 1148.823
352.3427 1092.585
352.8248 1017.951
353.3069 914.7368
353.7890 800.9797
354.2711 696.9005
354.7533 603.8416
355.2354 524.6240
355.7175 463.7830
356.1996 419.3948
356.6817 387.9807
357.1638 372.2009
357.6460 365.7176
358.1281 364.4488
358.6102 368.3192
359.0923 376.8845
359.5744 391.5777
360.0565 409.9638
360.5387 429.8549
361.0208 451.8578
361.5029 473.9942
361.9850 496.8337
362.4671 519.3262
362.9492 537.8501
363.4314 547.3876
363.9135 555.2905
364.3956 565.2415
364.8777 577.3777
365.3598 592.5392
365.8419 608.5526
366.3241 628.2092
366.8062 655.6569
367.2883 688.9055
367.7704 732.5118
368.2526 787.0962
368.7347 852.5595
369.2168 930.9570
369.6989 1019.581
370.1810 1122.858
370.6631 1245.889
371.1453 1397.076
371.6274 1556.212
372.1095 1724.035
372.5916 1900.104
373.0737 2075.531
373.5558 2251.259
374.0380 2427.102
374.5201 2609.965
375.0022 2809.901
375.4843 2984.861
375.9664 3154.326
376.4485 3279.459
376.9307 3285.228
377.4128 3164.969
377.8949 2952.069
378.3770 2628.441
378.8591 2203.353
379.3412 1828.049
379.8234 1503.614
380.3055 1236.840
380.7876 1049.895
381.2697 938.6107
381.7518 861.7900
382.2339 816.4847
382.7161 792.5182
383.1982 768.2370
383.6803 743.8810
384.1624 718.5521
384.6445 688.0146
385.1266 656.2657
385.6088 633.4048
386.0909 621.4247
386.5730 617.1984
387.0551 618.0342
387.5372 623.9150
388.0193 634.9495
388.5015 662.3459
388.9836 688.9135
389.4657 699.5038
389.9478 693.5021
390.4299 665.7180
390.9120 602.3511
391.3942 518.2069
391.8763 432.2622
392.3584 340.6040
392.8405 258.6830
393.3226 195.3649
393.8047 148.9297
394.2869 111.5485
394.7690 83.02451
395.2511 60.65637
395.7332 43.10986
396.2154 31.30640
396.6975 21.99103
397.1796 14.74158
397.6617 9.439575
398.1438 5.872711
398.6259 6.283936
399.1081 6.115265
399.5902 3.623199
400.0723 1.766449
400.5544 5.518097
401.0365 6.903900
401.5186 7.216583
402.0008 7.385605
402.4829 7.068558
402.9650 7.299423
403.4471 8.429413
403.9292 10.21678
404.4113 11.65947
404.8935 12.93642
405.3756 13.51454
405.8577 12.74753
406.3398 10.30484
406.8219 9.044937
407.3040 9.241653
407.7862 10.18608
408.2683 10.93501
408.7504 11.47404
409.2325 12.04785
409.7146 12.83653
410.1967 13.67128
410.6789 14.23558
411.1610 14.55183
411.6431 14.27031
412.1252 12.51857
412.6073 9.874084
413.0894 8.118088
413.5716 7.876999
414.0537 8.030090
414.5358 7.063690
415.0179 5.301178
415.5000 3.803665
415.9821 3.538940
416.4643 3.633179
416.9464 3.028030
417.4285 1.591415
417.9106 0.4028170
418.3927 0.2950590
418.8748 0.7937620
419.3570 1.318100
419.8391 1.975571
420.3212 2.334869
420.8033 2.213806
421.2854 1.634979
421.7675 0.7546540
422.2497 0.7177430
422.7318 2.217194
423.2139 3.485809
423.6960 4.616608
424.1781 5.258148
424.6602 4.729904
425.1424 3.872650
425.6245 3.956314
426.1066 6.098526
426.5887 7.796051
427.0709 8.484467
427.5530 8.162796
428.0351 7.548492
428.5172 6.291718
428.9993 5.187378
429.4814 4.878250
429.9636 5.610031
430.4457 6.283646
430.9278 6.999130
431.4099 7.422287
431.8920 6.449677
432.3741 3.809387
432.8563 1.780640
433.3384 1.921982
433.8205 3.773087
434.3026 3.697357
434.7847 1.385925
435.2668 0.4426730
435.7490 2.390381
436.2311 8.325851
436.7132 11.46140
437.1953 9.042816
437.6774 4.829559
438.1595 3.606247
438.6417 4.961823
439.1238 7.198624
439.6059 10.55525
440.0880 13.63034
440.5701 14.56421
441.0522 12.86441
441.5344 11.10286
442.0165 10.90623
442.4986 11.57593
442.9807 12.26578
443.4628 12.38353
443.9449 12.77461
444.4271 13.94543
444.9092 15.75671
445.3913 17.40759
445.8734 19.05304
446.3555 20.20137
446.8376 20.45381
447.3198 18.78447
447.8019 18.22955
448.2840 19.73341
448.7661 22.01270
449.2482 23.23280
449.7303 22.58122
450.2125 22.24559
450.6946 22.73029
451.1767 23.98569
451.6588 25.29639
452.1409 26.71667
452.6230 28.08031
453.1052 29.52089
453.5873 31.14426
454.0694 31.20488
454.5515 29.07845
455.0337 26.36159
455.5158 26.07101
455.9979 28.03131
456.4800 29.78052
456.9621 30.05676
457.4442 29.45979
457.9264 29.53146
458.4085 30.16718
458.8906 30.41502
459.3727 29.03804
459.8548 26.89639
460.3369 25.41151
460.8191 24.91081
461.3012 24.87987
461.7833 25.35651
462.2654 25.98630
462.7475 26.01729
463.2296 24.22891
463.7118 22.63614
464.1939 22.64394
464.6760 24.27736
465.1581 25.68919
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