#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:50:21 +0300 (Thu, 24 May 2018) $
#$Revision: 817 $
#$URL: svn://172.16.1.111/rod/cif/1/00/03/1000307.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000307
loop_
_publ_author_name
'Leone, P.'
'Palvadeau, P.'
'Moelo, Y.'
_publ_section_title
;
 Structure cristalline d'un nouvel hydroxyphosphate naturel de strontium,
 fer et aluminium (lulzacite), Sr2Fe(Fe0,63Mg0,37)2Al4(PO4)4(OH)10
;
_journal_name_full               'Chimie de l etat Solide et Cristallochimie'
_journal_page_first              301
_journal_page_last               308
_journal_volume                  3
_journal_year                    2000
_chemical_compound_source
'Saint-Aubin-des-Chateaux, Loire-Atlantique, France'
_chemical_formula_sum
'Al4 Ba0.08 Fe2.26 H4 Mg0.74 O26 P3.92 Sr1.92 V0.08'
_chemical_name_mineral           Lulzacite
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                108.47
_cell_angle_beta                 91.72
_cell_angle_gamma                97.44
_cell_length_a                   5.457
_cell_length_b                   9.131
_cell_length_c                   9.769
_cell_volume                     456.500
_exptl_crystal_density_diffrn    3.553
_cod_original_formula_sum
'(Sr1.92 Ba.08) (P3.92 V.08) Fe2.26 Al4 Mg.74 O26 H4'
_cod_database_code               9014177
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R110147.rod
_rod_data_source.block           3500000
_rod_database.code               1000307
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9014177 COD http://www.crystallography.net/cod/9014177.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
147.3820 0.0000000E+00
147.8641 0.2816640
148.3462 0.4520820
148.8283 0.7357130
149.3104 0.9460500
149.7925 1.528280
150.2747 1.817363
150.7568 1.193858
151.2389 0.6430890
151.7210 0.2124910
152.2031 0.1211890
152.6852 0.2707460
153.1674 9.7791001E-02
153.6495 0.2301090
154.1316 0.4740300
154.6137 0.5199720
155.0958 0.5603710
155.5779 0.6538880
156.0601 0.8154150
156.5422 1.000091
157.0243 1.227362
157.5064 1.469082
157.9885 1.671221
158.4706 1.506451
158.9528 1.529728
159.4349 2.072412
159.9170 3.634447
160.3991 4.917377
160.8812 5.321920
161.3633 5.145891
161.8455 5.171400
162.3276 5.748461
162.8097 6.561434
163.2918 7.444265
163.7739 8.439583
164.2560 9.374916
164.7382 10.21047
165.2203 10.93538
165.7024 11.50842
166.1845 11.89808
166.6666 12.13421
167.1487 12.21410
167.6309 11.81757
168.1130 11.60568
168.5951 12.00475
169.0772 12.96629
169.5593 14.19541
170.0414 15.91433
170.5236 17.69374
171.0057 18.99288
171.4878 19.46720
171.9699 19.54510
172.4520 19.35423
172.9341 18.93437
173.4163 18.79970
173.8984 19.58809
174.3805 20.89151
174.8626 21.99626
175.3447 22.57287
175.8268 22.87835
176.3090 23.15138
176.7911 23.38622
177.2732 23.64042
177.7553 23.77916
178.2374 23.74223
178.7195 23.63234
179.2017 23.35740
179.6838 23.09414
180.1659 23.15880
180.6480 23.56957
181.1301 24.06933
181.6122 24.46244
182.0944 24.75870
182.5765 24.97043
183.0586 25.19684
183.5407 25.33653
184.0228 25.08732
184.5049 24.38740
184.9871 23.65378
185.4692 23.52311
185.9513 23.87211
186.4334 24.03603
186.9155 23.47136
187.3976 22.45130
187.8798 21.93657
188.3619 22.02378
188.8440 22.35492
189.3261 22.53393
189.8082 22.56033
190.2903 22.35377
190.7725 21.69040
191.2546 20.68277
191.7367 20.07131
192.2188 19.95418
192.7009 20.05506
193.1830 19.90936
193.6652 19.51644
194.1473 19.13680
194.6294 18.98296
195.1115 19.02435
195.5936 18.81333
196.0757 18.23913
196.5579 17.55110
197.0400 17.26521
197.5221 17.41450
198.0042 17.63718
198.4863 17.75314
198.9684 17.77704
199.4506 17.80085
199.9327 17.79497
200.4148 17.80917
200.8969 18.09129
201.3790 18.71643
201.8611 19.05383
202.3433 18.60394
202.8254 17.26464
203.3075 16.41683
203.7896 16.30613
204.2717 16.62077
204.7538 16.51205
205.2360 15.81558
205.7181 15.16513
206.2002 15.01741
206.6823 15.49763
207.1644 15.60125
207.6465 15.06868
208.1287 14.20502
208.6108 13.99285
209.0929 14.63029
209.5750 15.35680
210.0571 15.69799
210.5392 15.60444
211.0214 15.43209
211.5035 15.15113
211.9856 14.81282
212.4677 14.65876
212.9498 14.79421
213.4319 14.88227
213.9140 14.64373
214.3962 13.89705
214.8783 13.48905
215.3604 13.56107
215.8425 14.01520
216.3246 14.49860
216.8067 15.12002
217.2889 15.57443
217.7710 15.62689
218.2531 15.10189
218.7352 14.67955
219.2173 14.36569
219.6994 14.19470
220.1816 14.36893
220.6637 15.05882
221.1458 15.80315
221.6279 16.30821
222.1100 16.52167
222.5921 16.63564
223.0743 16.60112
223.5564 16.47583
224.0385 16.57732
224.5206 17.07092
225.0027 17.52470
225.4848 17.63979
225.9670 17.22538
226.4491 16.95179
226.9312 16.99095
227.4133 17.22356
227.8954 17.04441
228.3775 16.27466
228.8597 15.35881
229.3418 14.57030
229.8239 13.98023
230.3060 13.36264
230.7881 12.75306
231.2702 12.10776
231.7524 11.17868
232.2345 9.660702
232.7166 8.300381
233.1987 7.618671
233.6808 8.066254
234.1629 8.176899
234.6451 7.715565
235.1272 6.837288
235.6093 6.248211
236.0914 6.179520
236.5735 6.083187
237.0556 5.618313
237.5378 4.521198
238.0199 3.641201
238.5020 3.100040
238.9841 2.809586
239.4662 2.407959
239.9483 1.741875
240.4305 1.176285
240.9126 0.9271510
241.3947 1.180946
241.8768 1.344574
242.3589 1.385319
242.8410 1.319538
243.3232 1.197723
243.8053 0.9921300
244.2874 0.7677150
244.7695 0.5619430
245.2516 0.3954850
245.7337 0.1880570
246.2159 0.1163410
246.6980 0.4589880
247.1801 0.6469800
247.6622 0.6300050
248.1443 0.5303420
248.6264 0.3945050
249.1086 0.1645010
249.5907 5.7610001E-02
250.0728 0.1352690
250.5549 0.3199460
251.0370 0.4030530
251.5191 0.3384020
252.0013 0.2412870
252.4834 0.1319200
252.9655 6.4762004E-02
253.4476 5.0934002E-02
253.9297 0.3720590
254.4118 0.9328310
254.8940 1.023071
255.3761 0.4215930
255.8582 0.2615200
256.3403 0.7942620
256.8224 1.175957
257.3046 1.391041
257.7867 1.374802
258.2688 1.229279
258.7509 1.150532
259.2330 1.161835
259.7151 1.189758
260.1973 1.202381
260.6794 1.185135
261.1615 1.219021
261.6436 1.343300
262.1257 1.484245
262.6078 1.443871
263.0900 1.013992
263.5721 0.9137610
264.0542 1.540668
264.5363 3.098389
265.0184 4.033386
265.5005 4.149147
265.9827 3.900124
266.4648 3.971363
266.9469 4.504135
267.4290 4.935566
267.9111 4.997044
268.3932 4.638962
268.8754 4.766090
269.3575 5.515938
269.8396 6.534187
270.3217 7.384731
270.8038 8.044540
271.2859 8.605511
271.7681 9.046860
272.2502 9.372791
272.7323 9.841331
273.2144 10.51653
273.6965 11.18502
274.1786 11.53249
274.6608 11.46114
275.1429 11.65290
275.6250 12.44065
276.1071 13.67953
276.5892 14.16167
277.0714 13.65950
277.5535 13.02701
278.0356 13.12249
278.5177 14.02000
278.9998 14.88763
279.4819 15.60434
279.9641 16.15532
280.4462 16.40855
280.9283 16.32608
281.4104 16.10994
281.8925 15.82745
282.3746 15.47379
282.8568 15.42640
283.3389 15.84558
283.8210 16.53408
284.3031 16.93319
284.7852 17.02276
285.2673 17.02145
285.7495 17.05093
286.2316 17.11474
286.7137 17.29510
287.1958 17.69408
287.6779 18.08125
288.1600 17.86187
288.6422 17.02550
289.1243 16.21327
289.6064 15.93472
290.0885 16.06951
290.5706 16.01387
291.0527 15.69917
291.5349 15.20695
292.0170 14.64732
292.4991 14.02327
292.9812 13.32255
293.4633 12.45521
293.9454 11.50205
294.4276 10.79852
294.9097 10.42599
295.3918 10.05022
295.8739 9.132210
296.3560 7.796196
296.8381 6.584743
297.3203 5.819389
297.8024 5.356049
298.2845 4.952484
298.7666 4.617023
299.2487 4.193584
299.7308 3.415287
300.2130 2.397762
300.6951 1.483974
301.1772 0.7777020
301.6593 0.2699010
302.1414 2.2864999E-02
302.6235 0.1010970
303.1057 8.0959000E-02
303.5878 2.3705000E-02
304.0699 0.1510960
304.5520 0.1758840
305.0341 2.1492001E-02
305.5162 0.2558290
305.9984 0.3309630
306.4805 0.2610970
306.9626 0.1522830
307.4447 3.6858000E-02
307.9268 5.6159999E-02
308.4089 8.7569997E-02
308.8911 4.3437999E-02
309.3732 5.1383998E-02
309.8553 0.3105810
310.3374 0.6409990
310.8195 0.7292020
311.3016 0.1268200
311.7838 0.6508900
312.2659 1.136993
312.7480 1.186253
313.2301 1.117462
313.7122 0.9134520
314.1943 0.7048450
314.6765 0.7875400
315.1586 1.773739
315.6407 2.755482
316.1228 3.060886
316.6049 2.422012
317.0870 1.888515
317.5692 2.000008
318.0513 2.485989
318.5334 2.960243
319.0155 3.241474
319.4976 3.544762
319.9797 4.049820
320.4619 4.789036
320.9440 5.405987
321.4261 5.707653
321.9082 5.863983
322.3903 6.034649
322.8724 6.159866
323.3546 6.416584
323.8367 6.954113
324.3188 7.740219
324.8009 8.313370
325.2830 8.428596
325.7651 8.408382
326.2473 8.462128
326.7294 8.720245
327.2115 8.944916
327.6936 9.231377
328.1757 9.484386
328.6578 9.346596
329.1400 8.378239
329.6221 7.436661
330.1042 6.898289
330.5863 7.180798
331.0684 7.113686
331.5505 6.409279
332.0327 5.423817
332.5148 4.960457
332.9969 5.304222
333.4790 5.793148
333.9611 6.284267
334.4432 6.886375
334.9254 7.000191
335.4075 6.371387
335.8896 5.465626
336.3717 4.906273
336.8538 4.738953
337.3359 4.833969
337.8180 5.257027
338.3001 5.997921
338.7823 6.467102
339.2644 6.614071
339.7465 6.584942
340.2286 6.478119
340.7107 6.270401
341.1928 6.136848
341.6750 6.114990
342.1571 6.193745
342.6392 6.342606
343.1213 6.568962
343.6034 6.833534
344.0855 7.151688
344.5677 7.515236
345.0498 7.758202
345.5319 7.838825
346.0140 7.823837
346.4961 7.815182
346.9782 7.814091
347.4604 7.853527
347.9425 7.964863
348.4246 8.134220
348.9067 8.305695
349.3888 8.472878
349.8709 8.659554
350.3531 8.897362
350.8352 9.179935
351.3173 9.482712
351.7994 9.857918
352.2815 10.22722
352.7636 10.45912
353.2458 10.55293
353.7279 10.56152
354.2100 10.47746
354.6921 10.34554
355.1742 10.24231
355.6563 10.18118
356.1385 10.16597
356.6206 10.18702
357.1027 10.25114
357.5848 10.39154
358.0669 10.67889
358.5490 11.02685
359.0312 11.37886
359.5133 11.79086
359.9954 12.05772
360.4775 11.87264
360.9596 11.46000
361.4417 11.29468
361.9239 11.82012
362.4060 12.44553
362.8881 12.86245
363.3702 13.02041
363.8523 13.04515
364.3344 12.94654
364.8166 12.75278
365.2987 12.49235
365.7808 11.99848
366.2629 11.61671
366.7450 11.56118
367.2271 11.82652
367.7093 11.80650
368.1914 11.34288
368.6735 10.62937
369.1556 9.795910
369.6377 8.401310
370.1198 7.442829
370.6020 7.248783
371.0841 7.558674
371.5662 7.416996
372.0483 6.558357
372.5304 5.573696
373.0125 4.689999
373.4947 3.934662
373.9768 3.202885
374.4589 2.402496
374.9410 1.690350
375.4231 1.422802
375.9052 1.858185
376.3874 1.992661
376.8695 1.381401
377.3516 4.5479000E-02
377.8337 0.7261310
378.3158 0.8376050
378.7979 0.6881030
379.2801 0.6206470
379.7622 0.6346280
380.2443 0.7516980
380.7264 1.037880
381.2085 1.380836
381.6906 1.459362
382.1728 1.270367
382.6549 1.010719
383.1370 0.7853550
383.6191 0.5952340
384.1012 0.4879650
384.5833 0.5079880
385.0655 0.4752960
385.5476 2.4878999E-02
386.0297 0.7201390
386.5118 1.290638
386.9939 1.194794
387.4760 0.9024280
387.9582 1.103909
388.4403 1.817886
388.9224 2.770664
389.4045 4.111496
389.8866 5.449547
390.3687 6.199821
390.8509 5.634823
391.3330 4.992771
391.8151 5.179939
392.2972 6.052189
392.7793 7.016361
393.2614 8.203808
393.7436 9.100250
394.2257 9.237297
394.7078 8.132454
395.1899 7.246342
395.6720 7.178951
396.1541 7.641632
396.6363 8.170815
397.1184 8.791615
397.6005 9.332493
398.0826 9.674812
398.5647 9.772835
399.0468 10.02802
399.5290 10.53642
400.0111 11.18507
400.4932 11.88335
400.9753 12.62497
401.4574 13.42690
401.9395 14.29038
402.4217 15.21351
402.9038 16.17294
403.3859 17.17623
403.8680 18.20543
404.3501 19.27002
404.8322 20.39226
405.3144 21.42216
405.7965 22.28732
406.2786 23.13208
406.7607 24.22214
407.2428 25.61254
407.7249 26.95107
408.2071 28.10198
408.6892 29.10445
409.1713 30.14120
409.6534 31.20538
410.1355 32.21818
410.6176 33.08019
411.0998 33.82267
411.5819 34.56626
412.0640 35.32825
412.5461 36.19427
413.0282 37.43227
413.5103 38.94630
413.9925 40.31266
414.4746 41.21252
414.9567 41.86512
415.4388 42.53192
415.9209 43.21554
416.4030 44.04351
416.8852 45.32353
417.3673 46.79649
417.8494 48.04309
418.3315 48.80006
418.8136 49.39326
419.2957 50.15038
419.7779 50.99182
420.2600 51.41722
420.7421 51.06025
421.2242 50.28087
421.7063 49.36330
422.1884 48.45845
422.6706 47.21127
423.1527 45.25710
423.6348 42.92570
424.1169 40.83173
424.5990 39.33493
425.0811 37.80045
425.5633 36.04308
426.0454 34.04189
426.5275 31.92780
427.0096 29.41698
427.4917 26.99212
427.9738 25.04774
428.4560 23.72399
428.9381 22.60108
429.4202 21.68601
429.9023 20.94334
430.3844 20.21739
430.8665 19.52523
431.3487 18.81363
431.8308 18.01006
432.3129 17.10440
432.7950 16.36911
433.2771 15.79757
433.7592 15.43005
434.2414 15.39219
434.7235 15.64978
435.2056 15.79561
435.6877 15.68372
436.1698 15.44677
436.6519 15.29836
437.1341 15.23028
437.6162 15.16684
438.0983 15.06950
438.5804 14.92120
439.0625 14.67837
439.5446 14.31295
440.0268 14.01049
440.5089 14.00203
440.9910 14.16853
441.4731 14.26712
441.9552 14.27104
442.4373 14.09300
442.9195 13.59655
443.4016 12.81468
443.8837 12.12887
444.3658 11.74838
444.8479 11.44762
445.3300 11.05381
445.8122 10.26532
446.2943 9.769066
446.7764 9.852005
447.2585 10.29830
447.7406 10.56609
448.2227 10.60895
448.7049 10.47278
449.1870 10.05709
449.6691 9.241135
450.1512 8.925537
450.6333 9.364525
451.1154 10.03118
451.5976 10.42801
452.0797 10.47810
452.5618 10.52473
453.0439 10.68224
453.5260 10.83872
454.0081 10.56913
454.4903 9.801975
454.9724 9.068550
455.4545 8.679878
455.9366 8.596043
456.4187 8.555218
456.9008 8.574299
457.3830 8.498695
457.8651 8.146431
458.3472 7.549644
458.8293 6.803047
459.3114 5.754200
459.7935 4.750626
460.2757 4.352325
460.7578 4.444023
461.2399 4.432808
461.7220 3.806248
462.2041 2.982857
462.6862 2.356022
463.1684 1.999405
463.6505 1.770653
464.1326 1.778950
464.6147 1.824013
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