#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-05-24 15:50:25 +0300 (Thu, 24 May 2018) $ #$Revision: 818 $ #$URL: svn://172.16.1.111/rod/cif/1/00/03/1000308.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_1000308 loop_ _publ_author_name 'Cooper, M. A.' 'Ball, N. A.' 'Hawthorne, F. C.' 'Paar, W. H.' 'Roberts, A. C.' 'Moffatt, E.' _publ_section_title ; Georgerobinsonite, Pb4(CrO4)2(OH)2FCl, a new chromate mineral from the Mammoth-St. Anthony mine, Tiger, Pinal County, Arizona: description and crystal structure ; _journal_name_full 'The Canadian Mineralogist' _journal_page_first 865 _journal_page_last 876 _journal_paper_doi 10.3749/canmin.49.3.865 _journal_volume 49 _journal_year 2011 _chemical_compound_source 'Mammoth-St. Anthony mine, Tiger, Pinal County, Arizona, USA' _chemical_formula_sum 'Cl Cr2 F H2 O10 Pb4' _chemical_name_mineral Georgerobinsonite _space_group_IT_number 59 _symmetry_space_group_name_Hall '-P 2ab 2a' _symmetry_space_group_name_H-M 'P m m n :2' _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_length_a 7.6256 _cell_length_b 11.6081 _cell_length_c 6.8961 _cell_volume 610.434 _exptl_crystal_density_diffrn 6.253 _cod_original_sg_symbol_H-M 'P m m n' _cod_original_formula_sum 'Pb4 Cr2 Cl F O10 H2' _cod_database_code 9016621 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type other _raman_measurement_device.excitation_laser_wavelength 532 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 15 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R110148.rod _rod_data_source.block 3500000 _rod_database.code 1000308 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9016621 COD http://www.crystallography.net/cod/9016621.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 89.78320 0.0000000E+00 90.26532 2.143509 90.74744 0.2792360 91.22955 0.1953740 91.71167 2.321548 92.19379 4.706451 92.67590 7.372375 93.15802 10.22353 93.64014 13.04552 94.12225 15.93887 94.60437 19.15990 95.08649 22.82323 95.56860 26.71217 96.05072 30.54352 96.53284 34.41022 97.01495 38.60606 97.49707 43.48820 97.97919 49.03236 98.46130 54.67976 98.94342 60.30223 99.42554 65.92238 99.90765 71.56918 100.3898 77.30618 100.8719 83.08968 101.3540 88.98425 101.8361 95.23401 102.3182 100.8161 102.8004 105.4672 103.2825 109.2219 103.7646 112.0139 104.2467 113.6924 104.7288 114.5663 105.2109 115.3349 105.6931 116.2491 106.1752 116.7864 106.6573 116.7589 107.1394 116.3681 107.6215 115.2172 108.1036 113.3015 108.5858 110.6788 109.0679 107.5083 109.5500 103.3590 110.0321 99.00250 110.5142 94.88405 110.9963 91.82642 111.4785 88.66202 111.9606 84.51889 112.4427 79.59244 112.9248 75.30968 113.4069 72.44646 113.8890 70.29213 114.3712 67.61728 114.8533 63.88016 115.3354 60.28821 115.8175 57.35855 116.2996 55.11594 116.7817 52.82082 117.2639 49.99942 117.7460 46.99434 118.2281 44.24086 118.7102 41.60431 119.1923 39.44695 119.6744 38.18823 120.1566 38.04507 120.6387 37.94522 121.1208 37.53534 121.6029 36.69713 122.0850 35.19394 122.5671 32.46263 123.0493 29.19124 123.5314 26.02705 124.0135 23.02266 124.4956 20.23091 124.9777 17.77109 125.4598 15.59644 125.9420 13.59656 126.4241 11.68022 126.9062 9.888092 127.3883 8.309647 127.8704 6.999847 128.3525 5.857605 128.8347 4.706070 129.3168 3.546555 129.7989 2.533447 130.2810 1.910355 130.7631 1.572495 131.2452 1.019470 131.7274 1.6541000E-02 132.2095 1.278976 132.6916 2.031113 133.1737 2.232407 133.6558 2.237045 134.1379 2.459564 134.6201 2.893021 135.1022 3.113861 135.5843 2.883011 136.0664 2.287796 136.5485 2.047348 137.0306 2.282745 137.5128 2.592606 137.9949 2.455368 138.4770 1.781143 138.9591 1.077393 139.4412 0.5153960 139.9233 0.1146700 140.4055 0.3081970 140.8876 0.7201540 141.3697 1.189331 141.8518 1.840622 142.3339 2.720825 142.8160 3.693619 143.2982 4.717026 143.7803 5.782852 144.2624 6.950378 144.7445 8.281662 145.2266 9.692093 145.7087 10.93265 146.1909 11.85149 146.6730 12.81942 147.1551 14.00362 147.6372 15.51492 148.1193 16.97524 148.6014 18.40548 149.0836 19.84179 149.5657 21.26451 150.0478 22.62646 150.5299 24.00763 151.0120 25.45118 151.4941 26.83163 151.9763 28.35696 152.4584 29.97820 152.9405 31.73326 153.4226 33.71970 153.9047 36.40567 154.3868 39.02858 154.8690 41.17249 155.3511 42.29079 155.8332 43.46147 156.3153 44.97356 156.7974 46.76043 157.2795 48.26991 157.7617 49.07794 158.2438 49.72770 158.7259 50.61398 159.2080 52.18089 159.6901 53.65440 160.1722 54.87794 160.6544 55.84480 161.1365 56.45327 161.6186 56.62747 162.1007 56.44659 162.5828 55.97539 163.0649 55.09727 163.5471 54.05486 164.0292 52.99571 164.5113 51.91477 164.9934 50.63876 165.4755 49.03074 165.9576 47.17395 166.4398 45.20181 166.9219 42.99789 167.4040 40.78006 167.8861 38.77193 168.3682 36.98643 168.8503 35.14395 169.3325 32.94394 169.8146 30.57338 170.2967 28.37581 170.7788 26.42764 171.2609 24.72063 171.7430 23.34891 172.2252 22.34398 172.7073 21.36900 173.1894 20.07232 173.6715 18.58697 174.1536 17.26602 174.6357 16.43643 175.1179 15.76282 175.6000 14.76052 176.0821 13.34103 176.5642 11.94279 177.0463 11.02196 177.5284 10.47910 178.0106 10.03139 178.4927 9.621796 178.9748 9.185593 179.4569 8.576950 179.9390 7.724617 180.4211 6.901466 180.9033 6.491920 181.3854 6.415260 181.8675 6.307327 182.3496 5.872726 182.8317 5.258614 183.3138 4.763092 183.7960 4.419701 184.2781 4.208923 184.7602 4.188026 185.2423 4.330025 185.7244 4.437523 186.2065 4.359062 186.6887 4.138573 187.1708 3.930962 187.6529 3.748238 188.1350 3.592239 188.6171 3.461792 189.0992 3.354744 189.5814 3.319923 190.0635 3.399963 190.5456 3.569618 191.0277 3.625565 191.5098 3.523544 191.9919 3.335938 192.4741 3.291679 192.9562 3.419533 193.4383 3.465721 193.9204 3.148773 194.4025 2.479080 194.8846 2.055779 195.3668 2.023293 195.8489 2.211792 196.3310 2.167686 196.8131 1.861046 197.2952 1.535622 197.7773 1.338295 198.2595 1.265427 198.7416 1.214310 199.2237 1.180786 199.7058 1.163567 200.1879 1.169838 200.6700 1.204468 201.1522 1.231407 201.6343 1.221558 202.1164 1.170609 202.5985 1.110382 203.0806 1.056282 203.5627 0.9974140 204.0449 0.8812560 204.5270 0.6850360 205.0091 0.5019760 205.4912 0.4228130 205.9733 0.4773860 206.4554 0.4338000 206.9376 0.2372280 207.4197 6.4834997E-02 207.9018 0.3516920 208.3839 0.6779400 208.8660 0.8377460 209.3481 0.6187740 209.8303 8.4624998E-02 210.3124 0.6086040 210.7945 0.8623890 211.2766 0.9023060 211.7587 0.9396900 212.2408 0.9942700 212.7230 1.005913 213.2051 0.9085850 213.6872 0.6457750 214.1693 0.4596180 214.6514 0.4028470 215.1335 0.4414600 215.6157 0.4230580 216.0978 0.3013000 216.5799 0.1995700 217.0620 0.2109990 217.5441 0.3898620 218.0262 0.5220410 218.5084 0.5828250 218.9905 0.5820690 219.4726 0.5713120 219.9547 0.5673450 220.4368 0.5065460 220.9189 0.3223720 221.4011 0.1007610 221.8832 0.3315430 222.3653 0.2745670 222.8474 2.3994001E-02 223.3295 0.2857060 223.8116 0.4894790 224.2938 0.6371460 224.7759 0.7358170 225.2580 0.7772370 225.7401 0.8041920 226.2222 0.8348770 226.7043 0.8558040 227.1865 0.7778240 227.6686 0.5208740 228.1507 0.2961880 228.6328 0.2313610 229.1149 0.3852770 229.5970 0.5456240 230.0792 0.7453380 230.5613 0.9713130 231.0434 1.097229 231.5255 1.041992 232.0076 0.9563220 232.4897 0.9313740 232.9719 0.9965590 233.4540 1.067863 233.9361 1.147812 234.4182 1.265121 234.9003 1.462105 235.3824 1.738281 235.8646 2.015442 236.3467 2.296394 236.8288 2.650970 237.3109 2.929512 237.7930 3.055885 238.2751 3.042511 238.7573 3.019859 239.2394 3.034996 239.7215 3.045753 240.2036 3.000145 240.6857 2.809258 241.1678 2.719200 241.6500 2.775497 242.1321 2.938377 242.6142 3.089333 243.0963 3.219040 243.5784 3.317352 244.0605 3.389008 244.5427 3.422966 245.0248 3.492249 245.5069 3.601364 245.9890 3.714272 246.4711 3.776848 246.9532 3.806450 247.4354 3.778267 247.9175 3.659508 248.3996 3.381989 248.8817 3.256348 249.3638 3.398605 249.8459 3.628891 250.3281 3.584778 250.8102 3.071365 251.2923 2.625046 251.7744 2.423019 252.2565 2.502281 252.7386 2.691994 253.2208 3.088333 253.7029 3.528427 254.1850 3.739784 254.6671 3.602859 255.1492 3.465134 255.6313 3.456200 256.1135 3.615425 256.5956 3.627876 257.0777 3.428093 257.5598 3.142960 258.0419 2.920837 258.5240 2.722458 259.0062 2.690582 259.4883 2.963387 259.9704 3.580025 260.4525 3.792946 260.9346 3.442772 261.4167 2.884789 261.8989 2.506325 262.3810 2.326157 262.8631 2.294006 263.3452 2.475639 263.8273 2.874359 264.3094 3.011139 264.7916 2.824104 265.2737 2.460724 265.7558 2.010056 266.2379 1.380470 266.7200 0.9916530 267.2021 1.023499 267.6843 1.453690 268.1664 1.736732 268.6485 1.833359 269.1306 1.818954 269.6127 1.728127 270.0948 1.528839 270.5770 1.395088 271.0591 1.362167 271.5412 1.409851 272.0233 1.469551 272.5054 1.548698 272.9875 1.625313 273.4697 1.696419 273.9518 1.771805 274.4339 1.746902 274.9160 1.594879 275.3981 1.358200 275.8802 1.119568 276.3624 0.8648220 276.8445 0.6646420 277.3266 0.5915070 277.8087 0.6572650 278.2908 0.6883930 278.7729 0.6803280 279.2551 0.5948940 279.7372 0.3416900 280.2193 9.5177002E-02 280.7014 0.4469600 281.1835 0.5510180 281.6656 0.4173890 282.1478 0.3109820 282.6299 0.2437740 283.1120 0.2099150 283.5941 0.2025070 284.0762 0.2218630 284.5583 0.2544100 285.0405 0.3158110 285.5226 0.4040760 286.0047 0.4165500 286.4868 0.3172530 286.9689 0.2247470 287.4510 0.3819500 287.9332 0.7720950 288.4153 1.050262 288.8974 1.038895 289.3795 0.8127670 289.8616 0.5886610 290.3438 0.3493650 290.8259 0.2142330 291.3080 0.4400180 291.7901 0.9493330 292.2722 1.263748 292.7543 1.083122 293.2365 0.6679080 293.7186 0.7438890 294.2007 1.320847 294.6828 1.842476 295.1649 1.652336 295.6470 0.9751660 296.1292 0.5601880 296.6113 0.7053910 297.0934 1.098694 297.5755 1.238121 298.0576 1.144653 298.5397 1.040321 299.0219 1.146111 299.5040 1.350426 299.9861 1.388069 300.4682 1.140961 300.9503 0.8499760 301.4324 0.8724750 301.9146 1.130585 302.3967 1.295311 302.8788 1.055298 303.3609 0.6266630 303.8430 0.3332370 304.3251 0.2395170 304.8073 0.2079620 305.2894 0.1349790 305.7715 2.7884999E-02 306.2536 0.1003490 306.7357 0.2770310 307.2178 0.4551620 307.7000 0.5646740 308.1821 0.5895770 308.6642 0.6189270 309.1463 0.6478730 309.6284 0.7354580 310.1105 0.9796370 310.5927 1.508194 311.0748 2.141647 311.5569 2.840904 312.0390 3.595947 312.5211 4.164986 313.0032 4.218498 313.4854 4.098312 313.9675 4.165733 314.4496 4.667793 314.9317 5.268715 315.4138 5.770638 315.8959 6.210976 316.3781 6.827629 316.8602 7.926750 317.3423 9.122803 317.8244 10.10368 318.3065 10.46745 318.7886 11.07742 319.2708 12.36544 319.7529 14.13312 320.2350 15.82916 320.7171 17.17947 321.1992 18.48381 321.6813 19.89275 322.1635 21.48230 322.6456 23.03796 323.1277 24.37689 323.6098 25.67494 324.0919 27.22767 324.5740 29.07788 325.0562 31.18652 325.5383 33.56637 326.0204 36.23772 326.5025 39.04968 326.9846 42.10287 327.4667 45.24055 327.9489 48.33447 328.4310 51.25623 328.9131 54.28635 329.3952 57.47414 329.8773 60.81970 330.3594 64.36908 330.8416 68.32177 331.3237 72.27042 331.8058 75.90307 332.2879 79.03912 332.7700 82.17206 333.2521 85.29815 333.7343 88.47101 334.2164 92.01637 334.6985 96.16357 335.1806 100.2613 335.6627 103.8633 336.1448 106.5616 336.6270 109.9261 337.1091 114.0781 337.5912 118.8010 338.0733 123.7368 338.5554 128.8152 339.0375 134.1989 339.5197 139.9761 340.0018 146.0966 340.4839 152.5197 340.9660 158.9745 341.4481 166.0464 341.9302 174.3770 342.4124 184.0808 342.8945 194.4446 343.3766 205.4757 343.8587 217.0084 344.3408 228.7793 344.8229 240.7163 345.3051 252.9707 345.7872 266.0612 346.2693 279.7289 346.7514 292.7490 347.2335 304.8651 347.7156 316.0548 348.1978 326.4817 348.6799 336.0364 349.1620 343.3407 349.6441 347.8235 350.1262 349.3634 350.6083 347.6209 351.0905 342.4772 351.5726 334.2972 352.0547 322.7670 352.5368 308.3977 353.0189 292.7810 353.5010 275.9520 353.9832 258.6683 354.4653 241.6191 354.9474 224.6480 355.4295 208.6111 355.9116 193.9026 356.3937 180.5172 356.8759 168.6335 357.3580 158.4771 357.8401 149.5579 358.3222 141.6591 358.8043 134.7072 359.2864 128.6800 359.7686 123.8508 360.2507 119.7533 360.7328 116.0215 361.2149 112.2877 361.6970 109.3253 362.1791 107.5340 362.6613 106.7358 363.1434 106.5275 363.6255 106.4466 364.1076 107.1904 364.5897 109.1534 365.0718 112.4982 365.5540 116.5197 366.0361 120.8975 366.5182 125.9500 367.0003 132.0594 367.4824 139.5165 367.9645 147.7802 368.4467 157.0688 368.9288 167.2827 369.4109 177.3616 369.8930 187.7845 370.3751 197.7146 370.8572 206.7732 371.3394 216.1516 371.8215 222.5997 372.3036 226.4504 372.7857 227.1682 373.2678 222.6445 373.7499 211.2718 374.2321 197.4099 374.7142 182.5651 375.1963 165.8732 375.6784 151.4242 376.1605 139.3732 376.6426 129.4972 377.1248 122.0987 377.6069 117.3300 378.0890 113.5857 378.5711 110.4814 379.0532 107.9889 379.5353 106.3832 380.0175 105.8562 380.4996 105.1759 380.9817 103.4896 381.4638 100.7594 381.9459 96.36492 382.4280 89.86620 382.9102 82.10848 383.3923 74.40941 383.8744 66.77479 384.3565 59.94238 384.8386 54.48731 385.3207 50.16286 385.8029 46.66843 386.2850 43.93814 386.7671 42.03660 387.2492 41.27127 387.7313 41.37605 388.2134 41.76766 388.6956 42.02638 389.1777 42.54529 389.6598 43.75588 390.1419 45.63977 390.6240 47.80197 391.1061 50.06834 391.5883 52.47458 392.0704 55.07559 392.5525 57.97955 393.0346 60.95578 393.5167 63.91203 393.9988 66.89009 394.4810 70.03745 394.9631 73.39863 395.4452 76.94581 395.9273 80.60921 396.4094 84.25884 396.8915 88.43129 397.3737 93.15394 397.8558 98.46633 398.3379 104.4201 398.8200 110.7595 399.3021 118.0206 399.7842 126.4184 400.2664 135.9428 400.7485 145.9772 401.2306 156.4582 401.7127 167.3926 402.1948 178.7881 402.6769 190.8657 403.1591 203.0164 403.6412 215.7679 404.1233 228.3136 404.6054 239.1087 405.0875 248.1549 405.5696 255.1328 406.0518 260.3987 406.5339 264.0443 407.0160 262.9148 407.4981 256.7474 407.9802 246.6869 408.4623 233.3604 408.9445 216.7406 409.4266 198.9491 409.9087 180.0654 410.3908 160.7757 410.8729 142.5029 411.3550 125.2028 411.8372 109.6687 412.3193 96.49357 412.8014 85.33890 413.2835 75.32555 413.7656 66.28730 414.2477 58.30669 414.7299 51.81786 415.2120 46.50609 415.6941 41.79793 416.1762 37.23347 416.6583 33.19807 417.1404 30.21284 417.6226 28.22868 418.1047 26.45490 418.5868 24.39584 419.0689 22.32150 419.5510 20.46777 420.0331 19.02045 420.5153 17.65144 420.9974 16.20898 421.4795 14.75865 421.9616 13.52723 422.4437 12.60733 422.9258 11.87624 423.4080 11.34460 423.8901 11.10802 424.3722 10.69897 424.8543 9.853638 425.3364 8.932945 425.8185 8.301933 426.3007 8.207008 426.7828 8.032509 427.2649 7.669456 427.7470 7.149803 428.2291 6.644409 428.7112 6.101723 429.1934 5.670052 429.6755 5.452362 430.1576 5.503571 430.6397 5.500336 431.1218 5.437248 431.6039 5.312073 432.0861 5.088997 432.5682 4.759529 433.0503 4.457886 433.5324 4.185745 434.0145 3.982262 434.4966 4.046631 434.9788 4.387886 435.4609 4.739525 435.9430 4.827347 436.4251 4.748581 436.9072 4.802704 437.3893 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