#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:50:51 +0300 (Thu, 24 May 2018) $
#$Revision: 825 $
#$URL: svn://172.16.1.111/rod/cif/1/00/03/1000314.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000314
loop_
_publ_author_name
'Nomura, S. F.'
'Atencio, D.'
'Chukanov, N. V.'
'Rastsvetaeva, R. K.'
'Coutinho, J. M. V.'
'Karipidis, T. K.'
_publ_section_title
;
 Manganoeudialyte - a new mineral from Pocos de Caldas, Minas Gerais,
 Brazil
;
_journal_name_full
'Zapiski Rossiiskogo Mineralogicheskogo Obshchetstva'
_journal_page_first              35
_journal_page_last               47
_journal_volume                  139
_journal_year                    2010
_chemical_compound_source
'Pocos de Caldas massif, Minas Gerais, Brazil'
_chemical_formula_sum
'C2.64 H40.56 Al0.75 Ca18 Ce0.18 F0.39 Fe3.6 K1.17 Mn5.72 Na47.84 Nb0.87 O254.37 Si75.57 Sr2.43 Ti0.57 Zr9.24'
_chemical_name_mineral           Manganoeudialyte
_space_group_IT_number           160
_symmetry_space_group_name_Hall  'R 3 -2"'
_symmetry_space_group_name_H-M   'R 3 m :H'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_length_a                   14.2418
_cell_length_b                   14.2418
_cell_length_c                   30.1143
_cell_volume                     5289.726
_exptl_crystal_density_diffrn    3.096
_cod_original_sg_symbol_H-M      'R 3 m'
_cod_original_formula_sum
'Zr9.24 Ca18 Si75.57 O254.37 Mn5.72 Fe3.6 Na47.84 Al.75 Nb.87 Ti.57 K1.17 Sr2.43 Ce.18 H40.56 C2.64 F.39'
_cod_database_code               9015914
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R110212.rod
_rod_data_source.block           3500000
_rod_database.code               1000314
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9015914 COD http://www.crystallography.net/cod/9015914.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
172.9341 0.0000000E+00
173.4163 0.8787690
173.8984 0.3867190
174.3805 0.5276790
174.8626 0.2594600
175.3447 1.413025
175.8268 3.986496
176.3090 7.177628
176.7911 10.87851
177.2732 14.56877
177.7553 16.60046
178.2374 17.33058
178.7195 18.50398
179.2017 20.79433
179.6838 23.97020
180.1659 27.93433
180.6480 32.78737
181.1301 37.44487
181.6122 40.41963
182.0944 42.28160
182.5765 44.81418
183.0586 49.58139
183.5407 55.42490
184.0228 60.11617
184.5049 63.49879
184.9871 66.16713
185.4692 68.24078
185.9513 69.93372
186.4334 72.30649
186.9155 76.62990
187.3976 82.11681
187.8798 85.96475
188.3619 87.79095
188.8440 89.04491
189.3261 91.70935
189.8082 95.71661
190.2903 99.92503
190.7725 103.8536
191.2546 107.6049
191.7367 111.2427
192.2188 114.7758
192.7009 118.1709
193.1830 121.2295
193.6652 123.9227
194.1473 126.6475
194.6294 129.6689
195.1115 132.9473
195.5936 135.9624
196.0757 138.6430
196.5579 141.1279
197.0400 143.6617
197.5221 146.2471
198.0042 148.8455
198.4863 151.5017
198.9684 154.2074
199.4506 156.8325
199.9327 159.3692
200.4148 161.7888
200.8969 164.0541
201.3790 166.2350
201.8611 168.0448
202.3433 169.1582
202.8254 169.4975
203.3075 170.2452
203.7896 171.7721
204.2717 173.5028
204.7538 173.7612
205.2360 172.2203
205.7181 170.4106
206.2002 169.3946
206.6823 169.4011
207.1644 168.7236
207.6465 166.9769
208.1287 164.8294
208.6108 163.6869
209.0929 163.5490
209.5750 163.0714
210.0571 161.5388
210.5392 158.4872
211.0214 155.4250
211.5035 152.5887
211.9856 149.4456
212.4677 146.4694
212.9498 143.5614
213.4319 139.9985
213.9140 135.5196
214.3962 129.7962
214.8783 124.3731
215.3604 119.4369
215.8425 114.9377
216.3246 110.7706
216.8067 107.1112
217.2889 103.3929
217.7710 99.10782
218.2531 93.84236
218.7352 89.19827
219.2173 85.38406
219.6994 82.23654
220.1816 79.18518
220.6637 76.15488
221.1458 73.25432
221.6279 70.69788
222.1100 68.84763
222.5921 66.25500
223.0743 62.36578
223.5564 57.62663
224.0385 54.05820
224.5206 52.30533
225.0027 50.82262
225.4848 48.53578
225.9670 44.72485
226.4491 41.96437
226.9312 40.86205
227.4133 40.99962
227.8954 40.22169
228.3775 37.97916
228.8597 35.64432
229.3418 34.12970
229.8239 33.91922
230.3060 33.42519
230.7881 32.48981
231.2702 31.19730
231.7524 29.16077
232.2345 25.77718
232.7166 22.53889
233.1987 20.42151
233.6808 20.10812
234.1629 19.34341
234.6451 17.68832
235.1272 15.44495
235.6093 13.93857
236.0914 13.41498
236.5735 13.28618
237.0556 13.32402
237.5378 13.89291
238.0199 13.85518
238.5020 13.19054
238.9841 11.88556
239.4662 9.749908
239.9483 5.975601
240.4305 2.483246
240.9126 0.3583370
241.3947 0.3715210
241.8768 6.1646000E-02
242.3589 0.7479860
242.8410 1.943985
243.3232 3.206055
243.8053 4.787430
244.2874 6.081329
244.7695 6.736801
245.2516 6.486786
245.7337 6.231323
246.2159 6.082458
246.6980 5.939392
247.1801 5.404877
247.6622 4.047119
248.1443 2.946884
248.6264 2.764557
249.1086 4.236420
249.5907 4.782120
250.0728 3.813507
250.5549 2.047134
251.0370 1.514114
251.5191 3.030411
252.0013 4.476837
252.4834 4.853516
252.9655 3.626190
253.4476 2.716736
253.9297 2.214478
254.4118 1.987091
254.8940 1.747574
255.3761 1.535187
255.8582 1.240509
256.3403 0.8179470
256.8224 0.2515260
257.3046 0.3628540
257.7867 0.9810180
258.2688 1.660706
258.7509 2.588837
259.2330 4.005875
259.7151 5.147202
260.1973 5.627350
260.6794 5.223068
261.1615 5.080902
261.6436 5.156631
262.1257 5.531540
262.6078 6.428650
263.0900 8.069000
263.5721 9.690125
264.0542 10.93938
264.5363 11.72279
265.0184 12.93932
265.5005 14.73088
265.9827 16.81778
266.4648 18.81021
266.9469 20.59581
267.4290 22.59267
267.9111 25.14082
268.3932 28.31039
268.8754 30.57256
269.3575 31.65570
269.8396 32.23914
270.3217 33.16380
270.8038 34.52419
271.2859 35.81383
271.7681 36.82384
272.2502 37.56276
272.7323 38.60680
273.2144 40.08545
273.6965 41.56299
274.1786 42.52332
274.6608 42.89235
275.1429 43.22876
275.6250 43.80325
276.1071 44.50215
276.5892 44.20013
277.0714 42.52144
277.5535 40.92570
278.0356 41.00609
278.5177 42.94667
278.9998 44.65753
279.4819 45.74887
279.9641 46.28378
280.4462 46.44014
280.9283 46.18500
281.4104 45.69031
281.8925 44.77831
282.3746 43.42978
282.8568 43.15158
283.3389 44.53137
283.8210 46.87474
284.3031 48.15695
284.7852 48.28261
285.2673 48.25888
285.7495 49.00543
286.2316 50.42868
286.7137 51.13570
287.1958 50.74635
287.6779 49.87030
288.1600 49.82988
288.6422 50.63731
289.1243 51.48882
289.6064 51.64633
290.0885 51.31598
290.5706 51.69926
291.0527 53.07347
291.5349 54.75658
292.0170 55.56247
292.4991 55.55611
292.9812 55.60309
293.4633 56.36874
293.9454 57.57137
294.4276 58.25235
294.9097 58.28854
295.3918 58.09784
295.8739 58.13753
296.3560 58.38762
296.8381 58.75415
297.3203 59.24359
297.8024 59.80754
298.2845 60.35159
298.7666 60.84116
299.2487 61.33270
299.7308 62.00359
300.2130 62.68942
300.6951 62.94673
301.1772 62.08507
301.6593 60.93341
302.1414 60.98518
302.6235 62.23828
303.1057 63.43057
303.5878 63.22934
304.0699 62.20584
304.5520 61.44421
305.0341 61.67549
305.5162 62.05679
305.9984 61.58153
306.4805 60.29774
306.9626 58.74335
307.4447 57.06006
307.9268 55.58827
308.4089 54.83780
308.8911 55.36479
309.3732 55.70717
309.8553 54.75322
310.3374 52.75871
310.8195 50.45442
311.3016 47.96402
311.7838 45.43593
312.2659 43.00003
312.7480 40.75067
313.2301 38.45859
313.7122 35.79077
314.1943 32.96075
314.6765 30.47058
315.1586 28.84050
315.6407 27.40898
316.1228 25.71945
316.6049 23.65039
317.0870 21.58864
317.5692 19.60074
318.0513 17.75668
318.5334 16.16714
319.0155 14.69315
319.4976 13.64894
319.9797 13.37552
320.4619 13.96584
320.9440 14.37553
321.4261 14.01173
321.9082 13.43974
322.3903 13.19620
322.8724 13.30151
323.3546 13.83449
323.8367 14.96095
324.3188 16.65640
324.8009 18.32738
325.2830 20.07797
325.7651 21.64136
326.2473 22.84068
326.7294 22.87791
327.2115 23.46396
327.6936 25.04878
328.1757 27.41626
328.6578 29.52704
329.1400 30.69769
329.6221 32.18126
330.1042 34.58099
330.5863 38.89830
331.0684 42.48531
331.5505 44.97711
332.0327 46.78508
332.5148 48.74026
332.9969 50.53174
333.4790 52.90695
333.9611 56.53421
334.4432 62.25334
334.9254 65.63321
335.4075 65.44623
335.8896 63.90634
336.3717 64.18677
336.8538 67.11319
337.3359 69.87367
337.8180 71.79358
338.3001 72.87570
338.7823 73.27065
339.2644 72.83850
339.7465 72.01007
340.2286 71.20728
340.7107 70.48827
341.1928 69.51282
341.6750 68.16586
342.1571 66.55202
342.6392 65.18436
343.1213 64.09430
343.6034 63.02663
344.0855 61.86298
344.5677 60.60738
345.0498 58.89055
345.5319 56.46194
346.0140 53.91843
346.4961 52.51834
346.9782 52.22894
347.4604 52.12579
347.9425 51.67186
348.4246 50.98009
348.9067 50.56532
349.3888 50.52066
349.8709 50.42592
350.3531 49.58817
350.8352 48.21223
351.3173 47.06480
351.7994 46.55357
352.2815 46.43672
352.7636 46.38721
353.2458 46.40135
353.7279 46.31982
354.2100 45.75122
354.6921 45.02887
355.1742 44.77267
355.6563 45.55437
356.1385 46.45959
356.6206 46.62030
357.1027 46.12450
357.5848 45.42842
358.0669 44.72075
358.5490 43.97961
359.0312 43.17020
359.5133 42.22437
359.9954 41.33200
360.4775 40.86229
360.9596 40.52408
361.4417 39.71437
361.9239 38.03488
362.4060 35.93407
362.8881 33.48965
363.3702 30.57411
363.8523 28.06676
364.3344 26.61250
364.8166 25.59143
365.2987 24.28210
365.7808 22.39326
366.2629 20.36804
366.7450 18.31779
367.2271 16.24539
367.7093 14.08308
368.1914 11.60095
368.6735 9.160965
369.1556 6.975998
369.6377 4.922180
370.1198 3.358276
370.6020 2.374084
371.0841 1.897522
371.5662 1.713791
372.0483 2.228729
372.5304 2.547256
373.0125 2.261185
373.4947 1.148819
373.9768 1.9012000E-02
374.4589 1.371216
374.9410 2.568848
375.4231 2.779709
375.9052 1.746124
376.3874 0.6469120
376.8695 0.2508850
377.3516 0.9609680
377.8337 1.303650
378.3158 1.125992
378.7979 1.010834
379.2801 1.413605
379.7622 2.326981
380.2443 4.052536
380.7264 6.946274
381.2085 10.46066
381.6906 13.16577
382.1728 15.04469
382.6549 16.57469
383.1370 17.62137
383.6191 18.48187
384.1012 20.44443
384.5833 23.81958
385.0655 27.74321
385.5476 30.96611
386.0297 33.72943
386.5118 36.77020
386.9939 41.00186
387.4760 45.52818
387.9582 49.05115
388.4403 51.56699
388.9224 53.55739
389.4045 55.06210
389.8866 56.36917
390.3687 57.92191
390.8509 60.25026
391.3330 62.44501
391.8151 64.06960
392.2972 65.07910
392.7793 65.33682
393.2614 64.07784
393.7436 62.53963
394.2257 61.64752
394.7078 61.89084
395.1899 61.86272
395.6720 60.82027
396.1541 59.24423
396.6363 57.87122
397.1184 57.44077
397.6005 56.65164
398.0826 54.68141
398.5647 51.24159
399.0468 49.16495
399.5290 50.20088
400.0111 51.83244
400.4932 51.98227
400.9753 48.84937
401.4574 46.63528
401.9395 46.15659
402.4217 47.07892
402.9038 47.72284
403.3859 48.08540
403.8680 48.02347
404.3501 47.39572
404.8322 46.18596
405.3144 44.64059
405.7965 42.66502
406.2786 40.63177
406.7607 39.02087
407.2428 37.81227
407.7249 36.94693
408.2071 36.53125
408.6892 36.45660
409.1713 36.20004
409.6534 35.80312
410.1355 35.03856
410.6176 33.48096
411.0998 31.30122
411.5819 29.36525
412.0640 27.76324
412.5461 26.54521
413.0282 25.86955
413.5103 25.65822
413.9925 25.54259
414.4746 25.49373
414.9567 25.36089
415.4388 24.89777
415.9209 24.05502
416.4030 22.99229
416.8852 21.66170
417.3673 20.21265
417.8494 18.91330
418.3315 17.99026
418.8136 17.14139
419.2957 16.05153
419.7779 14.77138
420.2600 13.66013
420.7421 13.09895
421.2242 12.66794
421.7063 12.02788
422.1884 10.92961
422.6706 9.961655
423.1527 9.536713
423.6348 9.319473
424.1169 8.697723
424.5990 6.565018
425.0811 4.913620
425.5633 4.511307
426.0454 5.594986
426.5275 6.173752
427.0096 6.180603
427.4917 5.774643
427.9738 5.026840
428.4560 3.657501
428.9381 2.527451
429.4202 1.730988
429.9023 1.254791
430.3844 1.116684
430.8665 1.530731
431.3487 1.694809
431.8308 0.9729460
432.3129 0.7160640
432.7950 1.626831
433.2771 1.593994
433.7592 1.094498
434.2414 0.7573850
434.7235 0.5662540
435.2056 0.2644650
435.6877 0.2099150
436.1698 0.8616490
436.6519 1.972000
437.1341 3.489319
437.6162 4.527023
438.0983 3.839691
438.5804 2.375977
439.0625 1.852692
439.5446 2.720123
440.0268 3.983551
440.5089 5.037567
440.9910 5.826355
441.4731 6.230087
441.9552 5.814148
442.4373 5.298157
442.9195 5.234268
443.4016 5.620659
443.8837 5.800674
444.3658 5.407631
444.8479 4.745750
445.3300 4.050629
445.8122 3.098930
446.2943 2.454544
446.7764 2.389763
447.2585 2.699951
447.7406 2.863304
448.2227 2.676414
448.7049 2.510040
449.1870 2.569962
449.6691 2.993736
450.1512 2.793694
450.6333 1.631180
451.1154 0.2253800
451.5976 0.7293170
452.0797 1.088142
452.5618 1.456299
453.0439 2.008621
453.5260 2.580719
454.0081 2.584648
454.4903 1.913994
454.9724 1.370369
455.4545 1.546791
455.9366 2.313278
456.4187 2.808662
456.9008 3.010231
457.3830 2.895515
457.8651 2.047356
458.3472 0.7855450
458.8293 0.2288130
459.3114 1.194221
459.7935 2.571472
460.2757 3.087906
460.7578 2.806114
461.2399 2.069954
461.7220 0.3508680
462.2041 1.317947
462.6862 1.772102
463.1684 0.5957030
463.6505 0.6435090
464.1326 1.246788
464.6147 1.397522
465.0968 1.341019
465.5789 1.145844
466.0611 0.7460780
466.5432 0.1937640
467.0253 1.562401
467.5074 2.186401
467.9895 1.329376
468.4716 0.1802750
468.9538 0.7429350
469.4359 1.522331
469.9180 1.846924
470.4001 1.470764
470.8822 0.8157500
471.3643 0.5365370
471.8465 0.7694550
472.3286 0.9936140
472.8107 1.108032
473.2928 1.106354
473.7749 0.8647690
474.2570 0.3091430
474.7392 8.6815000E-02
475.2213 0.2618790
475.7034 1.193184
476.1855 1.494186
476.6676 0.9116520
477.1497 0.1144410
477.6319 0.1320500
478.1140 0.7157440
478.5961 1.054443
479.0782 0.4868930
479.5603 0.3206790
480.0424 0.6326520
480.5246 0.4767460
481.0067 8.0092996E-02
481.4888 0.8560560
481.9709 1.725983
482.4530 1.939041
482.9352 1.181107
483.4173 0.2685780
483.8994 0.5947490
484.3815 1.387161
484.8636 2.067047
485.3457 2.523491
485.8279 2.968979
486.3100 3.388832
486.7921 3.791641
487.2742 4.452126
487.7563 5.527435
488.2384 6.712082
488.7206 7.844513
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1303.016 0.0000000E+00
