#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-05-24 15:51:14 +0300 (Thu, 24 May 2018) $ #$Revision: 831 $ #$URL: svn://172.16.1.111/rod/cif/1/00/03/1000320.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_1000320 loop_ _publ_author_name 'Orlandi, P.' 'Demartin, F.' 'Pasero, M.' 'Leverett, P.' 'Williams, P. A.' 'Hibbs, D. E.' _publ_section_title ; Gelosaite, BiMo6+(2-5x)Mo5+6xO7(OH)*H2O (0<=x<=0.4), a new mineral from Su Senargiu (CA), Sardinia, Italy, and a second occurrence from Kingsgate, New England, Australia ; _journal_name_full 'American Mineralogist' _journal_page_first 268 _journal_page_last 273 _journal_paper_doi 10.2138/am.2011.3597 _journal_volume 96 _journal_year 2011 _chemical_compound_source 'Su Senargiu, Sardinia, Italy' _chemical_formula_sum 'Bi H3 Mo2.102 O9' _chemical_name_mineral Gelosaite _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90 _cell_angle_beta 100.42 _cell_angle_gamma 90 _cell_length_a 5.8505 _cell_length_b 9.0421 _cell_length_c 13.9173 _cell_volume 724.095 _exptl_crystal_density_diffrn 5.115 _cod_original_formula_sum 'Bi Mo2.102 O9 H3' _cod_database_code 9015598 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type other _raman_measurement_device.excitation_laser_wavelength 532 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 15 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R120031.rod _rod_data_source.block 3500000 _rod_database.code 1000320 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9015598 COD http://www.crystallography.net/cod/9015598.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 192.7009 0.0000000E+00 193.1830 0.6442870 193.6652 0.2546690 194.1473 0.2290040 194.6294 2.246307 195.1115 5.524353 195.5936 8.769318 196.0757 11.65912 196.5579 14.65714 197.0400 18.83737 197.5221 24.24487 198.0042 29.81506 198.4863 34.75143 198.9684 38.99429 199.4506 44.43710 199.9327 51.45465 200.4148 59.37720 200.8969 66.76096 201.3790 73.69427 201.8611 80.03955 202.3433 85.57626 202.8254 90.23273 203.3075 95.16656 203.7896 100.8216 204.2717 106.4351 204.7538 109.9299 205.2360 111.0975 205.7181 110.9381 206.2002 109.9789 206.6823 108.4932 207.1644 106.4256 207.6465 103.2297 208.1287 98.88281 208.6108 94.12152 209.0929 88.90298 209.5750 83.47983 210.0571 77.85989 210.5392 71.76996 211.0214 66.74106 211.5035 63.37424 211.9856 61.02216 212.4677 57.12515 212.9498 51.06635 213.4319 44.85049 213.9140 39.68216 214.3962 35.84467 214.8783 32.01852 215.3604 28.04318 215.8425 24.01074 216.3246 20.53284 216.8067 17.82990 217.2889 15.18451 217.7710 12.00693 218.2531 7.881805 218.7352 4.405151 219.2173 1.720459 219.6994 0.2619630 220.1816 1.838409 220.6637 3.099152 221.1458 3.876312 221.6279 4.072876 222.1100 3.709778 222.5921 2.714050 223.0743 0.8423160 223.5564 1.677643 224.0385 3.822479 224.5206 5.311615 225.0027 6.813538 225.4848 8.799683 225.9670 11.59094 226.4491 14.10269 226.9312 16.39938 227.4133 18.38010 227.8954 19.52670 228.3775 19.34430 228.8597 19.03094 229.3418 19.38391 229.8239 20.88748 230.3060 21.90897 230.7881 22.15738 231.2702 21.80557 231.7524 21.65207 232.2345 21.69049 232.7166 21.92087 233.1987 22.38657 233.6808 23.27594 234.1629 23.94153 234.6451 24.20007 235.1272 24.18832 235.6093 24.47192 236.0914 24.86951 236.5735 25.79971 237.0556 27.67786 237.5378 31.43210 238.0199 34.09204 238.5020 35.20694 238.9841 35.12158 239.4662 35.06119 239.9483 34.49872 240.4305 34.69498 240.9126 36.60168 241.3947 41.78647 241.8768 45.19144 242.3589 46.01651 242.8410 44.95407 243.3232 44.42389 243.8053 44.64777 244.2874 45.10217 244.7695 45.50421 245.2516 45.69183 245.7337 46.19556 246.2159 47.22836 246.6980 48.55276 247.1801 49.35818 247.6622 49.29282 248.1443 49.23398 248.6264 49.60791 249.1086 50.58133 249.5907 51.58011 250.0728 52.58551 250.5549 53.36789 251.0370 54.23483 251.5191 55.18408 252.0013 56.25763 252.4834 57.53552 252.9655 59.24252 253.4476 60.53720 253.9297 61.33163 254.4118 61.75558 254.8940 62.09659 255.3761 62.34116 255.8582 62.52133 256.3403 62.66043 256.8224 62.79105 257.3046 62.72900 257.7867 62.35297 258.2688 61.85162 258.7509 61.63510 259.2330 61.87067 259.7151 62.04230 260.1973 61.88474 260.6794 61.26102 261.1615 60.95596 261.6436 61.04077 262.1257 61.39120 262.6078 61.76746 263.0900 62.04883 263.5721 62.65939 264.0542 63.73962 264.5363 65.32281 265.0184 67.32941 265.5005 69.97113 265.9827 72.85065 266.4648 75.34283 266.9469 77.19260 267.4290 79.35968 267.9111 82.23178 268.3932 85.87311 268.8754 89.27841 269.3575 92.61478 269.8396 95.79315 270.3217 98.33472 270.8038 99.81100 271.2859 101.9227 271.7681 105.5848 272.2502 110.6947 272.7323 114.2120 273.2144 115.6012 273.6965 116.2985 274.1786 117.7667 274.6608 120.0972 275.1429 122.6818 275.6250 125.4812 276.1071 128.4585 276.5892 131.4118 277.0714 134.2120 277.5535 137.1136 278.0356 140.3040 278.5177 143.7794 278.9998 147.5991 279.4819 151.8813 279.9641 156.5163 280.4462 160.8357 280.9283 164.8326 281.4104 168.6366 281.8925 172.4995 282.3746 176.4371 282.8568 179.8880 283.3389 182.6545 283.8210 184.9731 284.3031 187.5504 284.7852 190.4155 285.2673 193.2171 285.7495 195.7683 286.2316 198.0888 286.7137 200.2541 287.1958 202.2679 287.6779 204.1664 288.1600 206.0761 288.6422 208.0023 289.1243 209.6804 289.6064 210.7614 290.0885 211.3708 290.5706 212.1875 291.0527 213.3316 291.5349 214.5203 292.0170 215.2134 292.4991 215.4465 292.9812 215.7355 293.4633 216.3208 293.9454 217.1739 294.4276 218.2399 294.9097 219.5256 295.3918 220.9528 295.8739 222.3024 296.3560 223.6508 296.8381 225.4061 297.3203 228.3828 297.8024 231.7728 298.2845 233.7750 298.7666 234.2718 299.2487 234.2923 299.7308 235.2310 300.2130 236.5951 300.6951 236.9702 301.1772 235.8675 301.6593 233.4299 302.1414 229.5853 302.6235 224.3834 303.1057 218.4935 303.5878 212.6851 304.0699 206.5908 304.5520 199.6475 305.0341 191.5649 305.5162 182.6878 305.9984 172.8978 306.4805 162.4107 306.9626 152.0306 307.4447 142.4452 307.9268 133.3334 308.4089 124.4118 308.8911 115.4751 309.3732 106.8934 309.8553 99.06686 310.3374 91.90399 310.8195 84.92014 311.3016 77.58995 311.7838 70.55646 312.2659 64.38919 312.7480 59.46170 313.2301 54.86441 313.7122 49.91217 314.1943 44.82645 314.6765 40.19151 315.1586 36.38254 315.6407 33.03352 316.1228 29.92188 316.6049 27.07544 317.0870 24.31642 317.5692 21.48970 318.0513 18.74365 318.5334 16.30594 319.0155 14.47733 319.4976 12.77576 319.9797 10.95386 320.4619 8.964264 320.9440 7.232620 321.4261 5.994171 321.9082 5.039200 322.3903 4.176224 322.8724 3.299225 323.3546 2.570175 323.8367 1.992966 324.3188 1.572037 324.8009 1.411209 325.2830 2.330307 325.7651 3.029419 326.2473 2.665863 326.7294 0.5300140 327.2115 2.828018 327.6936 3.368668 328.1757 2.534378 328.6578 2.296585 329.1400 3.247711 329.6221 4.314865 330.1042 5.068634 330.5863 5.496979 331.0684 5.615494 331.5505 5.172302 332.0327 4.468597 332.5148 4.204803 332.9969 4.812668 333.4790 5.297623 333.9611 5.291016 334.4432 4.636246 334.9254 4.159973 335.4075 3.973694 335.8896 3.887115 336.3717 3.623749 336.8538 3.108475 337.3359 2.602890 337.8180 2.152847 338.3001 1.758789 338.7823 1.516144 339.2644 1.447220 339.7465 1.474869 340.2286 1.618774 340.7107 1.953033 341.1928 1.887756 341.6750 1.187515 342.1571 3.5110001E-02 342.6392 0.7947850 343.1213 1.261398 343.6034 1.673370 344.0855 2.301407 344.5677 3.128998 345.0498 3.813370 345.5319 4.279846 346.0140 4.635223 346.4961 4.989059 346.9782 5.348053 347.4604 5.956238 347.9425 7.131531 348.4246 8.697418 348.9067 9.899933 349.3888 10.63326 349.8709 11.33551 350.3531 12.62967 350.8352 14.37160 351.3173 16.02008 351.7994 17.27670 352.2815 18.32639 352.7636 19.41435 353.2458 20.53918 353.7279 21.84720 354.2100 23.51521 354.6921 25.43925 355.1742 27.44600 355.6563 29.59119 356.1385 31.70387 356.6206 33.60760 357.1027 35.33702 357.5848 37.01799 358.0669 38.76469 358.5490 40.49911 359.0312 42.14040 359.5133 43.67963 359.9954 45.15631 360.4775 46.60474 360.9596 48.02019 361.4417 49.36597 361.9239 50.56270 362.4060 51.75624 362.8881 53.10242 363.3702 54.69666 363.8523 56.01855 364.3344 56.83379 364.8166 57.31146 365.2987 57.64719 365.7808 57.63776 366.2629 57.73154 366.7450 58.19722 367.2271 59.03018 367.7093 59.48067 368.1914 59.24200 368.6735 58.72861 369.1556 58.20175 369.6377 57.65579 370.1198 57.13181 370.6020 56.76811 371.0841 56.44339 371.5662 55.70018 372.0483 54.27071 372.5304 52.75522 373.0125 51.42216 373.4947 50.43184 373.9768 49.15126 374.4589 47.37814 374.9410 45.46176 375.4231 44.08456 375.9052 43.54587 376.3874 42.68294 376.8695 41.06161 377.3516 38.68811 377.8337 36.56860 378.3158 34.68555 378.7979 33.03751 379.2801 31.79893 379.7622 30.99550 380.2443 29.78433 380.7264 27.78255 381.2085 25.42152 381.6906 23.96635 382.1728 23.43472 382.6549 22.99809 383.1370 22.10875 383.6191 20.85413 384.1012 19.62900 384.5833 18.28819 385.0655 16.93884 385.5476 15.86493 386.0297 15.10123 386.5118 14.47325 386.9939 13.91599 387.4760 13.33926 387.9582 12.58029 388.4403 11.65388 388.9224 10.85007 389.4045 10.62033 389.8866 10.65849 390.3687 10.45802 390.8509 9.458298 391.3330 8.508698 391.8151 8.346176 392.2972 8.855255 392.7793 9.381454 393.2614 9.496857 393.7436 9.539978 394.2257 9.807037 394.7078 10.47237 395.1899 11.09213 395.6720 11.36351 396.1541 11.50407 396.6363 11.86075 397.1184 12.60603 397.6005 13.47018 398.0826 14.36505 398.5647 15.27083 399.0468 16.24503 399.5290 17.52879 400.0111 18.83839 400.4932 19.89041 400.9753 20.23064 401.4574 20.85539 401.9395 21.88007 402.4217 23.26106 402.9038 24.84531 403.3859 27.00339 403.8680 28.81094 404.3501 29.65869 404.8322 29.04974 405.3144 29.27414 405.7965 30.64700 406.2786 32.47336 406.7607 33.53766 407.2428 33.66119 407.7249 34.02330 408.2071 35.21078 408.6892 37.01064 409.1713 37.91978 409.6534 37.82474 410.1355 37.50125 410.6176 37.68143 411.0998 38.27661 411.5819 38.77437 412.0640 39.06480 412.5461 39.22969 413.0282 39.40005 413.5103 39.56723 413.9925 39.68727 414.4746 39.77390 414.9567 39.78342 415.4388 39.59525 415.9209 39.17345 416.4030 38.78329 416.8852 38.59763 417.3673 38.59863 417.8494 38.75279 418.3315 39.20888 418.8136 39.68533 419.2957 39.96399 419.7779 40.08185 420.2600 40.28362 420.7421 40.78154 421.2242 41.35033 421.7063 41.81357 422.1884 42.09814 422.6706 42.37657 423.1527 42.60155 423.6348 42.86137 424.1169 43.31874 424.5990 44.10870 425.0811 44.99371 425.5633 45.96149 426.0454 47.04826 426.5275 47.91881 427.0096 48.41435 427.4917 48.81705 427.9738 49.41499 428.4560 50.55315 428.9381 51.09059 429.4202 50.54153 429.9023 49.37241 430.3844 49.35829 430.8665 50.97952 431.3487 52.39035 431.8308 52.52927 432.3129 51.32878 432.7950 50.31705 433.2771 49.51990 433.7592 48.89865 434.2414 48.42699 434.7235 48.09799 435.2056 47.81573 435.6877 47.59990 436.1698 47.38419 436.6519 46.97809 437.1341 46.39355 437.6162 45.82416 438.0983 45.43799 438.5804 45.15286 439.0625 44.76709 439.5446 44.16391 440.0268 43.74434 440.5089 43.83591 440.9910 44.37630 441.4731 45.23196 441.9552 46.59729 442.4373 48.05878 442.9195 49.30142 443.4016 50.32358 443.8837 51.51427 444.3658 52.95966 444.8479 54.71472 445.3300 56.78662 445.8122 59.39340 446.2943 62.06097 446.7764 64.57869 447.2585 67.11032 447.7406 70.08023 448.2227 74.05542 448.7049 77.88931 449.1870 81.15233 449.6691 83.65140 450.1512 86.81241 450.6333 90.71721 451.1154 95.12065 451.5976 99.87076 452.0797 105.0725 452.5618 110.2047 453.0439 115.1768 453.5260 119.9724 454.0081 124.8906 454.4903 129.9846 454.9724 135.1806 455.4545 140.4412 455.9366 145.7550 456.4187 151.4849 456.9008 157.6421 457.3830 163.9208 457.8651 169.7878 458.3472 175.3845 458.8293 180.9146 459.3114 186.5346 459.7935 192.1018 460.2757 197.5620 460.7578 202.8636 461.2399 207.9196 461.7220 213.0952 462.2041 217.8346 462.6862 221.4277 463.1684 223.6014 463.6505 225.4072 464.1326 227.6598 464.6147 229.7612 465.0968 230.9606 465.5789 230.7143 466.0611 229.8455 466.5432 228.5625 467.0253 226.8731 467.5074 224.7027 467.9895 222.0433 468.4716 218.8977 468.9538 215.3002 469.4359 211.4004 469.9180 206.7993 470.4001 201.2136 470.8822 195.0618 471.3643 188.9113 471.8465 182.7636 472.3286 176.5837 472.8107 170.2872 473.2928 163.9946 473.7749 157.9246 474.2570 152.1477 474.7392 146.3761 475.2213 140.4152 475.7034 134.2764 476.1855 127.9547 476.6676 121.3709 477.1497 114.8612 477.6319 108.9769 478.1140 103.6055 478.5961 98.46533 479.0782 93.51654 479.5603 88.68640 480.0424 83.82599 480.5246 78.94402 481.0067 74.30038 481.4888 70.23230 481.9709 66.37105 482.4530 62.34857 482.9352 57.89438 483.4173 53.77182 483.8994 50.38651 484.3815 47.48149 484.8636 44.70343 485.3457 41.77608 485.8279 39.17252 486.3100 37.24467 486.7921 35.98433 487.2742 34.23395 487.7563 31.71684 488.2384 28.97574 488.7206 26.25948 489.2027 23.38628 489.6848 21.11154 490.1669 19.63614 490.6490 18.55856 491.1311 17.19965 491.6133 15.52933 492.0954 13.86665 492.5775 12.23677 493.0596 10.70680 493.5417 9.532135 494.0238 8.718048 494.5060 8.064972 494.9881 7.490479 495.4702 6.962433 495.9523 6.380081 496.4344 5.727982 496.9165 5.039429 497.3987 4.195023 497.8808 3.347641 498.3629 2.808411 498.8450 3.154373 499.3271 3.472580 499.8092 3.112671 500.2914 2.166046 500.7735 1.197525 501.2556 0.2387700 501.7377 0.5541690 502.2198 1.056992 502.7019 1.140076 503.1841 1.249680 503.6662 1.419052 504.1483 1.651184 504.6304 1.958847 505.1125 2.487427 505.5946 2.832870 506.0768 2.826370 506.5589 2.581207 507.0410 2.731949 507.5231 3.450119 508.0052 4.088547 508.4873 4.256882 508.9695 3.947189 509.4516 3.814529 509.9337 3.924835 510.4158 3.960632 510.8979 3.379837 511.3800 2.349701 511.8622 1.653214 512.3443 1.589615 512.8264 1.819534 513.3085 1.981705 513.7906 2.069504 514.2728 2.060333 514.7549 1.895844 515.2370 1.655502 515.7191 1.379974 516.2012 1.066895 516.6833 0.8026280 517.1655 0.7557370 517.6476 0.7025600 518.1297 0.4490360 518.6118 0.2543790 519.0939 0.9022220 519.5760 1.439331 520.0582 1.865417 520.5403 2.188950 521.0224 2.288193 521.5045 2.448471 521.9866 2.729858 522.4688 3.132553 522.9509 3.694763 523.4330 4.473862 523.9151 5.277466 524.3972 5.966263 524.8793 6.534866 525.3615 6.962738 525.8436 7.141037 526.3257 7.484634 526.8078 8.879990 527.2899 11.06454 527.7720 12.81227 528.2542 13.24576 528.7363 13.27933 529.2184 14.18393 529.7005 15.83400 530.1826 17.58151 530.6647 19.37785 531.1469 20.88382 531.6290 21.60004 532.1111 21.18929 532.5932 21.32535 533.0753 23.10095 533.5574 25.57216 534.0396 27.73259 534.5217 29.05226 535.0038 30.49472 535.4859 32.26479 535.9680 34.26808 536.4501 36.23334 536.9323 38.13930 537.4144 40.03865 537.8965 41.92282 538.3786 43.78160 538.8607 45.71548 539.3428 47.71019 539.8250 49.77098 540.3071 51.84178 540.7892 53.91620 541.2713 56.27950 541.7534 59.05882 542.2355 61.85657 542.7177 64.08214 543.1998 65.86501 543.6819 67.56181 544.1640 69.25946 544.6461 70.97931 545.1282 72.76254 545.6104 74.59807 546.0925 76.45367 546.5746 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