#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:58:56 +0300 (Thu, 24 May 2018) $
#$Revision: 838 $
#$URL: svn://172.16.1.111/rod/cif/1/00/03/1000325.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000325
loop_
_publ_author_name
'Sokolova, E.'
'Camara, F.'
_publ_section_title
;
 From structure topology to chemical composition. III. Titanium silicates:
 The crystal chemistry of barytolamprophyllite Locality: Mt. Yuksporr,
 Khibina alkaline massif, Kola Peninsula, Russia
;
_journal_name_full               'The Canadian Mineralogist'
_journal_page_first              403
_journal_page_last               412
_journal_paper_doi               10.3749/canmin.46.2.403
_journal_volume                  46
_journal_year                    2008
_chemical_compound_source        R120087
_chemical_formula_sum
'Al0.03 Ba0.88 Ca0.13 Fe0.35 K0.61 Mg0.05 Mn0.28 Na2.09 Nb0.01 O18 Si4 Sr0.33 Ti2.91'
_chemical_name_mineral           Barytolamprophyllite
_space_group_IT_number           12
_symmetry_space_group_name_Hall  '-C 2y'
_symmetry_space_group_name_H-M   'C 1 2/m 1'
_cell_angle_alpha                90
_cell_angle_beta                 96.676
_cell_angle_gamma                90
_cell_length_a                   19.8971
_cell_length_b                   7.1165
_cell_length_c                   5.4108
_cell_volume                     760.962
_exptl_crystal_density_diffrn    3.511
_cod_original_formula_sum
;Al0.03 Ba0.88 Ca0.13 Fe0.35 K0.61 Mg0.05 Mn0.28 Na2.09 Nb0.01 O18 Si4 Sr0.33
 Ti2.91
;
_cod_database_code               9010662
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R120087.rod
_rod_data_source.block           3500000
_rod_database.code               1000325
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9010662 COD http://www.crystallography.net/cod/9010662.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
180.6480 0.0000000E+00
181.1301 0.1474460
181.6122 0.2576330
182.0944 0.5824240
182.5765 0.6040990
183.0586 0.2124440
183.5407 0.1684000
184.0228 0.2528990
184.5049 3.6495000E-02
184.9871 0.3645590
185.4692 0.8772200
185.9513 1.478424
186.4334 2.002804
186.9155 2.276104
187.3976 2.403942
187.8798 2.772648
188.3619 3.410011
188.8440 4.196095
189.3261 4.980572
189.8082 5.770000
190.2903 6.530266
190.7725 7.162464
191.2546 7.728607
191.7367 8.575737
192.2188 9.807220
192.7009 11.11251
193.1830 11.83955
193.6652 11.98038
194.1473 12.21263
194.6294 12.94331
195.1115 14.13261
195.5936 15.31454
196.0757 16.47063
196.5579 17.59261
197.0400 18.60392
197.5221 19.48084
198.0042 20.48168
198.4863 21.80918
198.9684 23.46025
199.4506 25.12627
199.9327 26.79574
200.4148 28.43222
200.8969 29.87824
201.3790 31.10563
201.8611 32.40456
202.3433 34.01556
202.8254 35.98053
203.3075 37.75060
203.7896 39.13795
204.2717 40.40152
204.7538 42.28397
205.2360 44.93390
205.7181 47.61496
206.2002 49.81038
206.6823 51.40357
207.1644 53.30551
207.6465 55.73949
208.1287 58.43746
208.6108 60.65886
209.0929 62.31705
209.5750 63.74830
210.0571 65.12724
210.5392 66.47246
211.0214 67.71646
211.5035 68.83857
211.9856 69.86054
212.4677 70.94238
212.9498 72.20544
213.4319 73.27541
213.9140 73.86658
214.3962 73.80619
214.8783 73.92673
215.3604 74.40838
215.8425 75.10934
216.3246 75.45141
216.8067 75.43162
217.2889 75.07176
217.7710 74.29289
218.2531 72.85936
218.7352 71.72400
219.2173 71.12505
219.6994 70.87382
220.1816 70.06636
220.6637 68.41016
221.1458 66.68574
221.6279 65.45209
222.1100 65.00029
222.5921 64.42891
223.0743 63.63771
223.5564 62.70195
224.0385 61.76518
224.5206 60.70227
225.0027 59.54507
225.4848 58.38561
225.9670 57.12925
226.4491 55.92653
226.9312 54.80632
227.4133 53.71120
227.8954 52.53796
228.3775 51.07185
228.8597 49.52615
229.3418 48.21715
229.8239 47.31268
230.3060 46.29745
230.7881 45.09476
231.2702 43.74402
231.7524 42.44659
232.2345 41.08369
232.7166 39.95219
233.1987 39.31656
233.6808 39.57857
234.1629 39.41965
234.6451 38.56171
235.1272 37.20398
235.6093 36.24316
236.0914 35.95007
236.5735 35.68264
237.0556 35.04578
237.5378 33.75029
238.0199 32.72682
238.5020 32.06567
238.9841 31.71478
239.4662 31.36110
239.9483 31.00585
240.4305 30.65228
240.9126 30.30750
241.3947 29.99477
241.8768 29.63145
242.3589 29.23734
242.8410 28.79101
243.3232 28.21155
243.8053 27.37863
244.2874 26.57883
244.7695 25.96712
245.2516 25.61130
245.7337 25.29453
246.2159 25.11265
246.6980 24.94773
247.1801 24.38329
247.6622 23.12376
248.1443 21.90095
248.6264 21.11490
249.1086 21.05389
249.5907 20.71805
250.0728 20.00654
250.5549 19.03648
251.0370 18.12108
251.5191 17.31114
252.0013 16.47681
252.4834 15.51441
252.9655 14.27799
253.4476 13.34378
253.9297 12.86292
254.4118 12.61933
254.8940 12.10489
255.3761 11.19227
255.8582 10.22972
256.3403 9.348434
256.8224 8.542152
257.3046 7.856155
257.7867 7.376488
258.2688 6.965088
258.7509 6.359146
259.2330 5.537277
259.7151 4.569824
260.1973 3.383842
260.6794 1.849312
261.1615 0.7891920
261.6436 0.3602520
262.1257 0.2792510
262.6078 7.9117000E-02
263.0900 0.2889180
263.5721 0.6517790
264.0542 0.9333800
264.5363 1.112709
265.0184 1.359291
265.5005 1.690582
265.9827 2.067513
266.4648 2.476723
266.9469 2.985504
267.4290 3.317993
267.9111 3.332085
268.3932 3.000298
268.8754 2.837891
269.3575 2.915039
269.8396 3.056625
270.3217 3.022179
270.8038 2.760010
271.2859 2.535538
271.7681 2.454865
272.2502 2.511185
272.7323 2.413452
273.2144 2.097450
273.6965 1.765762
274.1786 1.715317
274.6608 2.041290
275.1429 2.111755
275.6250 1.708885
276.1071 0.9031520
276.5892 0.1856540
277.0714 0.4292220
277.5535 0.9609910
278.0356 1.397858
278.5177 1.727753
278.9998 2.094673
279.4819 2.569160
279.9641 3.095657
280.4462 3.362434
280.9283 3.312943
281.4104 3.247574
281.8925 3.472046
282.3746 3.992836
282.8568 4.328125
283.3389 4.297585
283.8210 4.114983
284.3031 4.452545
284.7852 5.370712
285.2673 6.332878
285.7495 6.934418
286.2316 7.207840
286.7137 7.535408
287.1958 7.940063
287.6779 8.461769
288.1600 9.225677
288.6422 10.23476
289.1243 11.30129
289.6064 12.35728
290.0885 13.38074
290.5706 14.16982
291.0527 14.66003
291.5349 15.01865
292.0170 15.44567
292.4991 15.94337
292.9812 16.60922
293.4633 17.62790
293.9454 18.86301
294.4276 19.79372
294.9097 20.31420
295.3918 20.83694
295.8739 21.97324
296.3560 23.60156
296.8381 25.20380
297.3203 26.46460
297.8024 27.52591
298.2845 28.72261
298.7666 30.08150
299.2487 31.41709
299.7308 32.49929
300.2130 33.41733
300.6951 34.40751
301.1772 35.55702
301.6593 36.83217
302.1414 38.25813
302.6235 39.81802
303.1057 41.36251
303.5878 42.78812
304.0699 44.09844
304.5520 45.25546
305.0341 46.09879
305.5162 46.91983
305.9984 48.10374
306.4805 49.59166
306.9626 51.05929
307.4447 52.23280
307.9268 53.25972
308.4089 54.31932
308.8911 55.50653
309.3732 56.66583
309.8553 57.72333
310.3374 58.65872
310.8195 59.42371
311.3016 60.02341
311.7838 60.41020
312.2659 60.47897
312.7480 60.04005
313.2301 59.68414
313.7122 59.91884
314.1943 60.49263
314.6765 60.87051
315.1586 60.75092
315.6407 60.40552
316.1228 60.00163
316.6049 59.57605
317.0870 59.03016
317.5692 58.41828
318.0513 57.64413
318.5334 56.57361
319.0155 54.69916
319.4976 52.91451
319.9797 51.75467
320.4619 51.31496
320.9440 50.62802
321.4261 49.24780
321.9082 47.56680
322.3903 45.96189
322.8724 44.31403
323.3546 42.93521
323.8367 42.06422
324.3188 41.67326
324.8009 41.04984
325.2830 40.00311
325.7651 38.77557
326.2473 37.53348
326.7294 35.96490
327.2115 34.73264
327.6936 33.99991
328.1757 33.70442
328.6578 33.46506
329.1400 33.19695
329.6221 33.04282
330.1042 33.07443
330.5863 33.51696
331.0684 33.80287
331.5505 33.82370
332.0327 33.69083
332.5148 33.65690
332.9969 33.72559
333.4790 33.93091
333.9611 34.25957
334.4432 34.63268
334.9254 35.42000
335.4075 36.83555
335.8896 38.44733
336.3717 39.61646
336.8538 40.11593
337.3359 40.71110
337.8180 41.73921
338.3001 43.18213
338.7823 43.86403
339.2644 43.47911
339.7465 42.93145
340.2286 43.23979
340.7107 44.61127
341.1928 45.58144
341.6750 45.74144
342.1571 45.33057
342.6392 45.31348
343.1213 45.76591
343.6034 46.21119
344.0855 46.26705
344.5677 45.95111
345.0498 45.67230
345.5319 45.48380
346.0140 45.34978
346.4961 45.25298
346.9782 45.18867
347.4604 45.00694
347.9425 44.56790
348.4246 43.93326
348.9067 43.35188
349.3888 42.84667
349.8709 42.34484
350.3531 41.67567
350.8352 40.91036
351.3173 40.31631
351.7994 40.11531
352.2815 40.11465
352.7636 40.01104
353.2458 39.80275
353.7279 39.51952
354.2100 39.24981
354.6921 38.91131
355.1742 38.35621
355.6563 37.43733
356.1385 36.38007
356.6206 35.22880
357.1027 34.05011
357.5848 33.20652
358.0669 33.30160
358.5490 33.62906
359.0312 33.47369
359.5133 32.50248
359.9954 31.47024
360.4775 30.81343
360.9596 30.41097
361.4417 30.01626
361.9239 29.57528
362.4060 29.07543
362.8881 28.53600
363.3702 27.98338
363.8523 27.26128
364.3344 26.10768
364.8166 24.83118
365.2987 23.77418
365.7808 23.33885
366.2629 22.84031
366.7450 22.05724
367.2271 20.98714
367.7093 19.96939
368.1914 19.03063
368.6735 18.16240
369.1556 17.34977
369.6377 16.34119
370.1198 15.73860
370.6020 15.89795
371.0841 16.52625
371.5662 16.54519
372.0483 15.61382
372.5304 14.48831
373.0125 13.42558
373.4947 12.34867
373.9768 11.59421
374.4589 11.24366
374.9410 11.13974
375.4231 11.05480
375.9052 10.99953
376.3874 10.93027
376.8695 10.81767
377.3516 10.66325
377.8337 10.60923
378.3158 10.66132
378.7979 10.80403
379.2801 11.03929
379.7622 11.38445
380.2443 11.80837
380.7264 12.31663
381.2085 12.86182
381.6906 13.36366
382.1728 13.82636
382.6549 14.21331
383.1370 14.33031
383.6191 14.32112
384.1012 14.78526
384.5833 15.81880
385.0655 17.09692
385.5476 18.34177
386.0297 19.51293
386.5118 20.42358
386.9939 20.87953
387.4760 21.09938
387.9582 21.38081
388.4403 21.71764
388.9224 22.03008
389.4045 22.28981
389.8866 22.48283
390.3687 22.57664
390.8509 22.48422
391.3330 22.37283
391.8151 22.42400
392.2972 22.56682
392.7793 22.54684
393.2614 22.21173
393.7436 21.70013
394.2257 21.09164
394.7078 20.41036
395.1899 19.61890
395.6720 18.58562
396.1541 17.45025
396.6363 16.44067
397.1184 15.67212
397.6005 14.98756
398.0826 14.35938
398.5647 13.79556
399.0468 13.20998
399.5290 12.54761
400.0111 11.88916
400.4932 11.29548
400.9753 10.73709
401.4574 10.28606
401.9395 10.01057
402.4217 9.862740
402.9038 9.609753
403.3859 9.136055
403.8680 8.727112
404.3501 8.521717
404.8322 8.558208
405.3144 8.696228
405.7965 8.990284
406.2786 9.321861
406.7607 9.481422
407.2428 9.435806
407.7249 9.393486
408.2071 9.403282
408.6892 9.471104
409.1713 9.643867
409.6534 9.923077
410.1355 10.29957
410.6176 10.88511
411.0998 11.61159
411.5819 12.03336
412.0640 11.97601
412.5461 11.72383
413.0282 11.78039
413.5103 12.08793
413.9925 12.30365
414.4746 12.03490
414.9567 11.60850
415.4388 11.64872
415.9209 12.26241
416.4030 12.79043
416.8852 12.47766
417.3673 11.74437
417.8494 11.27462
418.3315 11.58999
418.8136 12.03646
419.2957 12.18321
419.7779 12.07213
420.2600 11.98505
420.7421 12.15677
421.2242 12.33848
421.7063 12.33774
422.1884 12.00097
422.6706 11.70364
423.1527 11.59196
423.6348 11.57195
424.1169 11.46539
424.5990 11.16811
425.0811 10.85015
425.5633 10.57754
426.0454 10.36899
426.5275 10.06711
427.0096 9.594379
427.4917 9.081509
427.9738 8.631603
428.4560 8.262474
428.9381 7.929710
429.4202 7.685181
429.9023 7.468975
430.3844 7.015785
430.8665 6.254017
431.3487 5.469101
431.8308 4.831398
432.3129 4.357563
432.7950 3.734509
433.2771 2.910721
433.7592 2.077187
434.2414 1.471836
434.7235 1.082481
435.2056 0.7666360
435.6877 0.5163310
436.1698 0.2884330
436.6519 5.5916000E-02
437.1341 0.5074310
437.6162 0.9010850
438.0983 1.069344
438.5804 1.114540
439.0625 1.206284
439.5446 1.369881
440.0268 1.592129
440.5089 1.972427
440.9910 2.402039
441.4731 2.650272
441.9552 2.504715
442.4373 2.236671
442.9195 1.960377
443.4016 1.687214
443.8837 1.545498
444.3658 1.721149
444.8479 1.977642
445.3300 2.125542
445.8122 2.059132
446.2943 1.977325
446.7764 1.926491
447.2585 1.885910
447.7406 1.802399
448.2227 1.690609
448.7049 1.515282
449.1870 1.237801
449.6691 0.8274270
450.1512 0.5069240
450.6333 0.3139720
451.1154 0.1697200
451.5976 1.9112000E-02
452.0797 0.1090580
452.5618 0.3473210
453.0439 0.7484780
453.5260 1.257481
454.0081 1.737804
454.4903 2.207886
454.9724 2.625526
455.4545 2.900940
455.9366 3.044758
456.4187 3.313446
456.9008 3.734955
457.3830 4.200768
457.8651 4.582623
458.3472 4.891430
458.8293 5.143581
459.3114 5.269550
459.7935 5.430969
460.2757 5.851227
460.7578 6.485271
461.2399 7.141365
461.7220 7.776962
462.2041 8.368065
462.6862 8.856304
463.1684 9.205997
463.6505 9.581768
464.1326 10.12005
464.6147 10.71528
465.0968 11.23751
465.5789 11.57056
466.0611 11.89223
466.5432 12.26819
467.0253 12.69324
467.5074 13.08834
467.9895 13.38684
468.4716 13.70141
468.9538 14.09547
469.4359 14.65275
469.9180 15.09220
470.4001 15.35162
470.8822 15.53817
471.3643 15.85631
471.8465 16.42844
472.3286 16.75850
472.8107 16.63092
473.2928 16.14912
473.7749 15.90063
474.2570 15.91075
474.7392 16.03255
475.2213 16.29597
475.7034 16.63558
476.1855 16.51276
476.6676 15.76908
477.1497 14.90626
477.6319 14.68999
478.1140 14.94232
478.5961 15.08754
479.0782 14.68406
479.5603 14.16130
480.0424 14.09802
480.5246 14.43502
481.0067 14.69627
481.4888 14.48291
481.9709 14.11593
482.4530 13.88667
482.9352 13.90209
483.4173 13.92898
483.8994 13.83642
484.3815 13.70495
484.8636 13.65924
485.3457 13.78135
485.8279 13.93586
486.3100 14.12049
486.7921 14.33325
487.2742 14.44963
487.7563 14.35938
488.2384 14.28638
488.7206 14.35141
489.2027 14.56937
489.6848 14.92123
490.1669 15.53686
490.6490 16.14676
491.1311 16.28111
491.6133 15.87786
492.0954 15.41658
492.5775 14.99511
493.0596 14.63968
493.5417 14.46701
494.0238 14.47732
494.5060 14.52594
494.9881 14.57563
495.4702 14.57010
495.9523 14.35541
496.4344 13.89527
496.9165 13.33298
497.3987 12.81440
497.8808 12.28804
498.3629 11.66320
498.8450 10.70241
499.3271 9.809158
499.8092 9.403053
500.2914 9.387367
500.7735 9.207512
501.2556 8.464287
501.7377 7.616371
502.2198 6.931297
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