#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-05-24 15:59:56 +0300 (Thu, 24 May 2018) $ #$Revision: 853 $ #$URL: svn://172.16.1.111/rod/cif/1/00/03/1000340.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_1000340 loop_ _publ_author_name 'Dreyer, G.' 'Tillmanns, E.' _publ_section_title ; Dreyerite: ein naturliches, tetragonales wismutvanadat von Hirschhorn/Pfalz Locality: Hirschhorn, Pfalz, Germany ; _journal_name_full 'Neues Jahrbuch fur Mineralogie, Monatshefte' _journal_page_first 151 _journal_page_last 154 _journal_volume 1981 _journal_year 1981 _chemical_compound_source R130060 _chemical_formula_sum 'Bi O4 V' _chemical_name_mineral Dreyerite _space_group_IT_number 141 _symmetry_space_group_name_Hall '-I 4bd 2' _symmetry_space_group_name_H-M 'I 41/a m d :2' _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_length_a 7.303 _cell_length_b 7.303 _cell_length_c 6.584 _cell_volume 351.150 _exptl_crystal_density_diffrn 6.127 _cod_original_sg_symbol_H-M 'I 41/a m d' _cod_original_formula_sum 'Bi V O4' _cod_database_code 9011741 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type other _raman_measurement_device.excitation_laser_wavelength 532 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 15 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R130060.rod _rod_data_source.block 3500000 _rod_database.code 1000340 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9011741 COD http://www.crystallography.net/cod/9011741.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 155.4116 0.0000000E+00 155.8937 0.8338240 156.3759 3.070824 156.8580 5.302681 157.3401 8.207787 157.8222 12.28828 158.3043 17.08613 158.7864 21.63145 159.2686 26.01510 159.7507 30.93139 160.2328 35.34081 160.7149 37.45834 161.1970 39.31218 161.6791 42.10070 162.1613 45.53357 162.6434 49.82007 163.1255 57.10774 163.6076 66.60631 164.0897 74.61385 164.5718 77.71130 165.0540 73.44530 165.5361 64.97339 166.0182 56.43594 166.5003 48.21320 166.9824 40.19613 167.4645 32.67646 167.9467 25.99892 168.4288 20.83026 168.9109 16.19090 169.3930 11.28540 169.8751 6.074791 170.3572 1.262535 170.8394 2.915321 171.3215 6.304001 171.8036 8.715286 172.2857 10.16264 172.7678 10.50740 173.2499 9.696487 173.7321 7.674622 174.2142 4.306488 174.6963 0.5824130 175.1784 7.068939 175.6605 15.40637 176.1426 25.17493 176.6248 36.90295 177.1069 51.24347 177.5890 68.39925 178.0711 88.02344 178.5532 109.9565 179.0353 134.3190 179.5175 160.3911 179.9996 188.4245 180.4817 217.9470 180.9638 248.8188 181.4459 281.2287 181.9280 314.6753 182.4102 349.8865 182.8923 385.9816 183.3744 422.4362 183.8565 458.1766 184.3386 493.7487 184.8207 529.1528 185.3029 564.5410 185.7850 600.2435 186.2671 638.1371 186.7492 677.9523 187.2313 718.0150 187.7134 755.8888 188.1956 792.8132 188.6777 832.5012 189.1598 876.0993 189.6419 922.9016 190.1240 971.2977 190.6061 1021.955 191.0883 1075.564 191.5704 1133.179 192.0525 1195.263 192.5346 1260.712 193.0167 1329.103 193.4988 1399.669 193.9810 1465.775 194.4631 1525.126 194.9452 1585.739 195.4273 1646.541 195.9094 1707.512 196.3915 1770.043 196.8737 1834.872 197.3558 1900.951 197.8379 1966.312 198.3200 2030.669 198.8021 2094.659 199.2842 2158.041 199.7664 2221.213 200.2485 2283.654 200.7306 2346.075 201.2127 2408.198 201.6948 2470.028 202.1769 2532.081 202.6591 2593.073 203.1412 2651.363 203.6233 2707.507 204.1054 2760.335 204.5875 2809.452 205.0696 2855.089 205.5518 2899.136 206.0339 2942.406 206.5160 2982.477 206.9981 3017.801 207.4802 3048.787 207.9623 3071.918 208.4445 3086.042 208.9266 3091.373 209.4087 3090.975 209.8908 3085.208 210.3729 3073.389 210.8550 3055.007 211.3372 3030.674 211.8193 2998.482 212.3014 2957.375 212.7835 2907.731 213.2656 2852.925 213.7477 2792.680 214.2299 2727.236 214.7120 2657.004 215.1941 2579.871 215.6762 2502.225 216.1583 2424.958 216.6404 2348.753 217.1226 2271.108 217.6047 2190.928 218.0868 2110.490 218.5689 2031.232 219.0510 1952.174 219.5331 1875.724 220.0153 1801.361 220.4974 1728.718 220.9795 1659.360 221.4616 1592.723 221.9437 1529.358 222.4258 1468.938 222.9080 1412.237 223.3901 1357.579 223.8722 1305.303 224.3543 1254.780 224.8364 1207.846 225.3185 1164.533 225.8007 1125.018 226.2828 1089.221 226.7649 1057.746 227.2470 1029.017 227.7291 1003.475 228.2112 981.1300 228.6934 958.7822 229.1755 936.1160 229.6576 913.7620 230.1397 892.8326 230.6218 873.2288 231.1039 855.2538 231.5861 839.1384 232.0682 824.7819 232.5503 812.5561 233.0324 803.1447 233.5145 794.9560 233.9966 785.8665 234.4788 774.4410 234.9609 764.7006 235.4430 757.9719 235.9251 754.6888 236.4072 751.3585 236.8893 746.6844 237.3715 743.1152 237.8536 743.7418 238.3357 749.7499 238.8178 757.9039 239.2999 767.3855 239.7820 777.8956 240.2642 790.7159 240.7463 805.5834 241.2284 822.9005 241.7105 843.4766 242.1926 868.7900 242.6747 894.5082 243.1569 919.6875 243.6390 944.5447 244.1211 968.2361 244.6032 993.3314 245.0853 1015.250 245.5674 1029.271 246.0496 1037.143 246.5317 1034.033 247.0138 1018.956 247.4959 991.7415 247.9780 953.4211 248.4601 900.9880 248.9423 840.3736 249.4244 777.2045 249.9065 709.0586 250.3886 643.0494 250.8707 579.3435 251.3528 518.1726 251.8350 465.0840 252.3171 422.2404 252.7992 385.6581 253.2813 351.3746 253.7634 318.8557 254.2455 290.4066 254.7277 267.0160 255.2098 248.6593 255.6919 231.5815 256.1740 215.7715 256.6561 201.1993 257.1382 188.0361 257.6204 176.2828 258.1025 165.7355 258.5846 156.5812 259.0667 148.7458 259.5488 141.2815 260.0309 134.2441 260.5131 127.6259 260.9952 121.4606 261.4773 115.6675 261.9594 110.5874 262.4415 106.5493 262.9236 103.4183 263.4058 99.70728 263.8879 95.12549 264.3700 90.47351 264.8521 86.30872 265.3342 82.65283 265.8163 79.46106 266.2985 76.80310 266.7806 74.60413 267.2627 72.52417 267.7448 70.62000 268.2269 68.67188 268.7090 66.58362 269.1912 64.44019 269.6733 61.70251 270.1554 58.04663 270.6375 53.79077 271.1196 50.29932 271.6017 47.73303 272.0839 45.45959 272.5660 43.22864 273.0481 41.15613 273.5302 38.33923 274.0123 34.47534 274.4944 29.96362 274.9766 25.88831 275.4587 22.26355 275.9408 19.06775 276.4229 16.48804 276.9050 14.61072 277.3871 12.36194 277.8693 9.605103 278.3514 6.531128 278.8335 3.453369 279.3156 0.3161620 279.7977 2.516602 280.2798 4.521851 280.7620 5.698608 281.2441 7.991455 281.7262 11.83960 282.2083 16.24609 282.6904 19.48425 283.1725 21.51990 283.6547 23.01135 284.1368 24.21985 284.6189 25.15674 285.1010 25.80884 285.5831 26.19031 286.0652 26.26135 286.5474 25.78723 287.0295 24.78027 287.5116 23.94482 287.9937 23.86841 288.4758 24.30530 288.9579 23.92102 289.4401 22.61719 289.9222 20.88489 290.4043 19.46545 290.8864 18.25684 291.3685 16.41431 291.8506 13.41748 292.3328 9.575562 292.8149 6.069214 293.2970 2.925415 293.7791 0.5103760 294.2612 4.849243 294.7433 10.01257 295.2255 15.56140 295.7076 20.72266 296.1897 26.48938 296.6718 35.20947 297.1539 46.76685 297.6360 58.82483 298.1182 69.26123 298.6003 78.56738 299.0824 88.25537 299.5645 98.72314 300.0466 109.8134 300.5287 121.0400 301.0109 132.4873 301.4930 145.2998 301.9751 160.1497 302.4572 176.8741 302.9393 194.9880 303.4214 215.0129 303.9036 235.7156 304.3857 255.3711 304.8678 274.4059 305.3499 294.8813 305.8320 317.6499 306.3141 342.5787 306.7963 369.2671 307.2784 398.2358 307.7605 428.1396 308.2426 457.8473 308.7247 487.6765 309.2068 518.3960 309.6890 549.8480 310.1711 582.6824 310.6532 617.3800 311.1353 654.0884 311.6174 691.3363 312.0995 727.1509 312.5817 762.5117 313.0638 799.4995 313.5459 839.8644 314.0280 881.8235 314.5101 924.5957 314.9922 967.9695 315.4744 1012.017 315.9565 1056.186 316.4386 1101.100 316.9207 1146.869 317.4028 1194.842 317.8849 1243.070 318.3671 1290.375 318.8492 1337.236 319.3313 1384.828 319.8134 1434.604 320.2955 1485.009 320.7776 1534.215 321.2598 1583.611 321.7419 1630.370 322.2240 1673.693 322.7061 1713.722 323.1882 1751.341 323.6703 1788.387 324.1525 1821.992 324.6346 1850.288 325.1167 1874.044 325.5988 1891.577 326.0809 1903.473 326.5630 1909.148 327.0452 1906.949 327.5273 1892.621 328.0094 1874.043 328.4915 1854.269 328.9736 1836.291 329.4557 1811.016 329.9379 1776.262 330.4200 1734.712 330.9021 1691.021 331.3842 1642.902 331.8663 1595.172 332.3484 1548.826 332.8306 1504.934 333.3127 1460.570 333.7948 1414.548 334.2769 1368.911 334.7590 1326.277 335.2411 1286.108 335.7233 1249.502 336.2054 1217.569 336.6875 1189.858 337.1696 1162.893 337.6517 1135.918 338.1339 1111.194 338.6160 1091.033 339.0981 1075.614 339.5802 1062.982 340.0623 1053.022 340.5444 1045.621 341.0266 1040.605 341.5087 1037.679 341.9908 1038.048 342.4729 1042.998 342.9550 1052.447 343.4371 1063.198 343.9193 1074.665 344.4014 1087.769 344.8835 1103.653 345.3656 1122.311 345.8477 1144.141 346.3298 1170.184 346.8120 1199.937 347.2941 1229.584 347.7762 1259.066 348.2583 1290.041 348.7404 1324.297 349.2225 1361.819 349.7047 1402.459 350.1868 1447.171 350.6689 1494.324 351.1510 1541.791 351.6331 1589.364 352.1152 1637.642 352.5974 1686.657 353.0795 1736.782 353.5616 1788.784 354.0437 1843.209 354.5258 1898.904 355.0079 1955.622 355.4901 2013.123 355.9722 2071.279 356.4543 2129.359 356.9364 2188.404 357.4185 2250.745 357.9006 2318.038 358.3828 2385.039 358.8649 2449.191 359.3470 2510.984 359.8291 2572.072 360.3112 2634.712 360.7933 2695.838 361.2755 2754.392 361.7576 2810.179 362.2397 2862.500 362.7218 2913.500 363.2039 2960.167 363.6860 2998.997 364.1682 3029.256 364.6503 3051.325 365.1324 3065.472 365.6145 3071.793 366.0966 3068.062 366.5787 3054.009 367.0609 3029.888 367.5430 2995.809 368.0251 2951.155 368.5072 2896.700 368.9893 2831.398 369.4714 2756.519 369.9536 2677.566 370.4357 2592.649 370.9178 2505.438 371.3999 2418.053 371.8820 2329.789 372.3641 2241.176 372.8463 2152.578 373.3284 2064.526 373.8105 1976.082 374.2926 1884.659 374.7747 1798.097 375.2568 1718.396 375.7390 1645.262 376.2211 1574.837 376.7032 1506.153 377.1853 1440.545 377.6674 1377.702 378.1495 1317.451 378.6317 1259.587 379.1138 1203.743 379.5959 1150.002 380.0780 1096.607 380.5601 1043.771 381.0422 992.1223 381.5244 941.7997 382.0065 892.6514 382.4886 846.6130 382.9707 803.4476 383.4528 763.4147 383.9349 726.6816 384.4171 692.9128 384.8992 660.6127 385.3813 628.0240 385.8634 596.2178 386.3455 565.9175 386.8276 537.2539 387.3098 511.1318 387.7919 488.5505 388.2740 468.6758 388.7561 450.2634 389.2382 433.7828 389.7203 417.4097 390.2025 399.0438 390.6846 379.3815 391.1667 361.1914 391.6488 346.9678 392.1309 334.6022 392.6130 322.2948 393.0952 309.7783 393.5773 297.5574 394.0594 285.5659 394.5415 274.1877 395.0236 264.1331 395.5057 257.2820 395.9879 250.3656 396.4700 241.8540 396.9521 231.3315 397.4342 221.3215 397.9163 212.3657 398.3984 204.0344 398.8806 195.9322 399.3627 188.6186 399.8448 180.8502 400.3269 172.0160 400.8090 162.3312 401.2911 153.9678 401.7733 148.0105 402.2554 141.9785 402.7375 134.3931 403.2196 124.1082 403.7017 115.1833 404.1838 108.2626 404.6660 102.3426 405.1481 95.68579 405.6302 87.99487 406.1123 80.49329 406.5944 73.64075 407.0765 67.37292 407.5587 61.16602 408.0408 54.90839 408.5229 48.91345 409.0050 43.43549 409.4871 38.49799 409.9692 34.04877 410.4514 30.02075 410.9335 26.42914 411.4156 23.35327 411.8977 20.81982 412.3798 18.56293 412.8619 17.13007 413.3441 15.79773 413.8262 12.81989 414.3083 7.720947 414.7904 2.322021 415.2725 2.085876 415.7546 5.509399 416.2368 8.148621 416.7189 9.256409 417.2010 10.11292 417.6831 12.14423 418.1652 15.21783 418.6473 17.59467 419.1295 17.54510 419.6116 16.72632 420.0937 16.60925 420.5758 18.34863 421.0579 19.72101 421.5400 20.01624 422.0222 19.44531 422.5043 18.61707 422.9864 17.14014 423.4685 15.84314 423.9506 15.17468 424.4327 15.46851 424.9149 15.27350 425.3970 14.47925 425.8791 13.20728 426.3612 11.53766 426.8433 8.940735 427.3254 6.820251 427.8076 5.616699 428.2897 5.161560 428.7718 4.040710 429.2539 1.897461 429.7360 0.1837160 430.2181 1.422607 430.7003 1.619324 431.1824 2.257690 431.6645 3.439697 432.1466 5.016357 432.6287 6.788269 433.1108 8.767517 433.5930 10.95892 434.0751 13.43542 434.5572 16.15881 435.0393 18.80371 435.5214 21.35858 436.0035 24.39642 436.4857 28.92975 436.9678 34.32739 437.4499 39.11401 437.9320 42.94684 438.4141 46.07642 438.8962 48.33966 439.3784 50.03809 439.8605 52.07385 440.3426 55.27124 440.8247 58.78040 441.3068 61.99664 441.7889 64.86993 442.2711 67.31219 442.7532 68.89868 443.2353 70.16138 443.7174 71.61639 444.1995 74.29999 444.6816 76.39838 445.1638 77.11285 445.6459 76.73877 446.1280 76.56128 446.6101 77.21277 447.0922 77.71387 447.5743 77.60034 448.0565 76.73041 448.5386 75.71124 449.0207 74.44073 449.5028 73.07849 449.9849 71.93933 450.4670 71.19183 450.9492 70.21722 451.4313 68.80597 451.9134 67.05658 452.3955 65.67194 452.8776 64.70239 453.3597 64.22614 453.8419 64.59497 454.3240 65.80133 454.8061 66.33118 455.2882 65.89209 455.7703 65.15570 456.2524 65.16901 456.7346 65.85321 457.2167 66.90686 457.6988 68.46240 458.1809 70.18616 458.6630 71.40100 459.1451 72.12897 459.6273 72.73761 460.1094 73.35522 460.5915 74.07507 461.0736 75.07172 461.5557 76.50006 462.0378 77.92065 462.5200 78.96301 463.0021 79.81635 463.4842 80.85791 463.9663 82.23199 464.4484 83.84027 464.9305 85.80554 465.4127 88.16687 465.8948 90.21063 466.3769 91.45026 466.8590 92.52917 467.3411 93.91119 467.8232 95.34827 468.3054 97.47797 468.7875 100.7796 469.2696 104.6942 469.7517 107.8298 470.2338 109.8787 470.7159 111.6758 471.1981 113.5381 471.6802 115.4373 472.1623 116.7287 472.6444 117.1876 473.1265 117.3922 473.6086 118.0323 474.0908 119.1285 474.5729 120.3270 475.0550 121.7217 475.5371 122.8597 476.0192 122.7455 476.5013 121.5500 476.9835 120.4576 477.4656 120.5874 477.9477 120.9976 478.4298 119.9883 478.9119 117.4881 479.3940 114.5772 479.8762 112.1077 480.3583 109.7793 480.8404 107.2369 481.3225 104.5504 481.8046 101.3028 482.2867 97.18182 482.7689 92.33826 483.2510 87.09900 483.7331 80.66980 484.2152 74.70862 484.6973 70.22205 485.1794 67.57129 485.6616 64.52716 486.1437 60.59686 486.6258 56.35919 487.1079 52.19696 487.5900 47.79602 488.0721 43.94592 488.5543 40.93646 489.0364 38.39923 489.5185 35.17780 490.0006 31.08905 490.4827 26.97083 490.9648 23.03943 491.4470 19.30811 491.9291 16.70630 492.4112 15.39307 492.8933 14.50909 493.3754 13.38062 493.8575 11.98322 494.3397 10.13763 494.8218 7.576294 495.3039 5.019470 495.7860 3.626953 496.2681 3.180908 496.7502 2.954590 497.2324 2.613892 497.7145 2.252747 498.1966 2.060364 498.6787 2.031006 499.1608 1.719543 499.6429 1.1353000E-02 500.1251 1.682861 500.6072 1.975220 501.0893 1.115051 501.5714 3.261780 502.0535 3.058167 502.5356 1.263977 503.0178 0.3663940 503.4999 1.826233 503.9820 3.003723 504.4641 3.731812 504.9462 3.972229 505.4283 4.532532 505.9105 5.660400 506.3926 6.685486 506.8747 7.043579 507.3568 6.630859 507.8389 6.208923 508.3210 5.809509 508.8032 5.460266 509.2853 5.191162 509.7674 5.005188 510.2495 4.939880 510.7316 5.072083 511.2137 5.333130 511.6959 5.736267 512.1780 6.242371 512.6601 6.407837 513.1422 5.653198 513.6243 4.476074 514.1064 3.412415 514.5886 2.454712 515.0707 1.978577 515.5528 2.610779 516.0349 3.754089 516.5170 4.580750 516.9991 4.763672 517.4813 4.602600 517.9634 4.124146 518.4455 3.361389 518.9276 2.513794 519.4097 1.369446 519.8918 0.3433230 520.3740 0.3829960 520.8561 0.7310790 521.3382 1.005554 521.8203 1.151672 522.3024 1.264709 522.7845 1.424316 523.2667 1.607422 523.7488 1.947815 524.2309 2.516846 524.7130 3.208130 525.1951 3.763916 525.6772 4.185852 526.1594 4.566528 526.6415 4.974182 527.1236 5.376160 527.6057 5.640137 528.0878 5.769958 528.5699 6.029480 529.0521 6.996033 529.5342 8.108276 530.0163 8.528687 530.4984 7.562744 530.9805 6.759888 531.4626 6.989380 531.9448 7.994873 532.4269 9.274780 532.9090 11.19379 533.3911 12.86884 533.8732 13.87860 534.3553 14.17316 534.8375 14.66815 535.3196 15.50458 535.8017 16.41418 536.2838 17.26471 536.7659 18.09113 537.2480 18.67712 537.7302 18.86908 538.2123 19.01385 538.6944 19.72705 539.1765 21.06268 539.6586 22.24188 540.1407 23.00873 540.6229 23.53070 541.1050 24.24347 541.5871 25.12500 542.0692 25.85907 542.5513 26.08105 543.0334 26.11371 543.5156 26.38489 543.9977 26.92303 544.4798 27.81146 544.9619 29.58618 545.4440 31.53723 545.9261 32.82550 546.4083 32.37518 546.8904 32.44336 547.3725 34.18341 547.8546 36.93195 548.3367 39.30145 548.8188 40.95435 549.3010 42.29218 549.7831 43.21954 550.2652 43.75623 550.7473 44.87683 551.2294 46.87494 551.7115 48.96130 552.1937 50.74292 552.6758 52.24139 553.1579 53.11749 553.6400 53.20508 554.1221 53.16364 554.6042 53.89581 555.0864 55.31207 555.5685 56.82278 556.0506 58.21271 556.5327 59.65192 557.0148 61.62015 557.4969 63.88348 557.9791 65.63815 558.4612 65.80450 558.9433 65.82391 559.4254 66.83487 559.9075 68.90778 560.3896 71.03064 560.8718 73.21918 561.3539 75.00024 561.8360 76.00555 562.3181 75.63507 562.8002 75.36481 563.2823 75.10999 563.7645 75.05145 564.2466 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