#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-05-24 16:00:03 +0300 (Thu, 24 May 2018) $ #$Revision: 855 $ #$URL: svn://172.16.1.111/rod/cif/1/00/03/1000342.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_1000342 loop_ _publ_author_name 'Cooper, M. A.' 'Hawthorne, F. C.' _publ_section_title ; Boleite: Resolution of the formula, KPb26Ag9Cu24Cl62(OH)48 ; _journal_name_full 'The Canadian Mineralogist' _journal_page_first 801 _journal_page_last 808 _journal_paper_doi 10.2113/gscanmin.38.4.801 _journal_volume 38 _journal_year 2000 _chemical_compound_source R130099 _chemical_formula_sum 'Ag9 Cl62 Cu24 H48 K O48 Pb26' _chemical_name_mineral Boleite _space_group_IT_number 221 _symmetry_space_group_name_Hall '-P 4 2 3' _symmetry_space_group_name_H-M 'P m -3 m' _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_length_a 15.288 _cell_length_b 15.288 _cell_length_c 15.288 _cell_volume 3573.156 _exptl_crystal_density_diffrn 5.083 _cod_original_formula_sum 'K Pb26 Ag9 Cu24 Cl62 O48 H48' _cod_database_code 9004592 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type other _raman_measurement_device.excitation_laser_wavelength 532 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 15 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R130099.rod _rod_data_source.block 3500000 _rod_database.code 1000342 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9004592 COD http://www.crystallography.net/cod/9004592.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 90.80798 0.0000000E+00 91.29010 0.5681610 91.77222 0.5542910 92.25433 0.4839780 92.73645 0.1450350 93.21857 3.5324000E-02 93.70068 0.3315660 94.18280 0.9056630 94.66492 1.121521 95.14703 0.8856660 95.62915 0.4327240 96.11127 0.1464840 96.59338 7.5424001E-02 97.07550 0.2174990 97.55762 0.6761320 98.03973 1.448944 98.52185 2.031143 99.00397 2.103401 99.48608 1.657166 99.96820 1.538536 100.4503 1.819687 100.9324 2.327637 101.4146 2.704750 101.8967 2.899292 102.3788 3.066704 102.8609 3.238121 103.3430 3.356697 103.8251 3.456108 104.3073 3.611237 104.7894 3.844231 105.2715 4.057632 105.7536 4.315285 106.2357 4.519615 106.7178 4.579849 107.2000 4.444000 107.6821 4.329559 108.1642 4.268112 108.6463 4.255608 109.1284 4.180054 109.6105 4.031792 110.0927 3.913246 110.5748 3.862335 111.0569 3.894814 111.5390 3.990135 112.0211 4.215652 112.5032 4.663467 112.9854 4.840515 113.4675 4.445412 113.9496 3.841049 114.4317 3.512871 114.9138 3.655052 115.3959 4.016022 115.8781 4.528107 116.3602 5.316231 116.8423 5.907158 117.3244 5.951576 117.8065 5.685921 118.2886 5.932854 118.7708 6.511902 119.2529 7.067757 119.7350 7.631767 120.2171 7.980919 120.6992 8.363167 121.1813 8.858311 121.6635 9.230080 122.1456 9.477905 122.6277 9.194778 123.1098 8.684593 123.5919 8.429111 124.0740 8.222332 124.5562 7.997967 125.0383 7.695663 125.5204 7.317181 126.0025 7.083740 126.4846 7.483532 126.9667 8.283855 127.4489 8.649490 127.9310 8.068420 128.4131 7.051926 128.8952 6.577766 129.3773 6.483036 129.8594 6.501045 130.3416 6.371677 130.8237 6.158459 131.3058 5.911636 131.7879 5.640228 132.2700 5.346027 132.7521 5.018131 133.2343 4.618965 133.7164 4.246487 134.1985 4.163837 134.6806 4.403347 135.1627 4.628502 135.6448 4.621571 136.1270 4.380051 136.6091 4.062309 137.0912 3.649517 137.5733 3.193035 138.0554 2.836575 138.5375 2.596146 139.0197 2.405998 139.5018 2.193329 139.9839 1.932590 140.4660 1.787373 140.9481 1.848843 141.4302 2.087360 141.9124 2.092884 142.3945 1.781490 142.8766 1.355629 143.3587 1.036224 143.8408 0.9554060 144.3229 0.7041630 144.8051 8.0109000E-02 145.2872 1.041817 145.7693 1.607777 146.2514 1.274967 146.7335 0.6112710 147.2156 0.3404920 147.6978 0.6681250 148.1799 1.138798 148.6620 1.365658 149.1441 1.741123 149.6262 1.984001 150.1083 2.136185 150.5905 2.142750 151.0726 1.903187 151.5547 0.9877740 152.0368 0.1909900 152.5189 0.2260890 153.0010 1.5903000E-02 153.4832 0.1680790 153.9653 4.2934000E-02 154.4474 0.2135580 154.9295 0.2513730 155.4116 0.3341140 155.8937 0.8836670 156.3759 1.080990 156.8580 0.5872190 157.3401 0.1453820 157.8222 8.2424000E-02 158.3043 0.1439700 158.7864 0.2098960 159.2686 0.3859250 159.7507 0.5446280 160.2328 0.6051250 160.7149 0.5421410 161.1970 0.3847470 161.6791 2.2533000E-02 162.1613 0.4851680 162.6434 0.8008000 163.1255 0.7135120 163.6076 0.3984910 164.0897 1.2035000E-02 164.5718 0.7780110 165.0540 1.310616 165.5361 1.057468 166.0182 5.0586998E-02 166.5003 0.8310320 166.9824 1.084911 167.4645 0.9597590 167.9467 0.7595440 168.4288 0.6231650 168.9109 0.4375760 169.3930 7.9425998E-02 169.8751 0.4646450 170.3572 0.9893420 170.8394 1.288830 171.3215 1.479687 171.8036 1.758236 172.2857 2.231750 172.7678 2.828289 173.2499 3.498882 173.7321 4.255280 174.2142 5.016453 174.6963 5.626873 175.1784 6.186722 175.6605 6.940647 176.1426 8.068184 176.6248 9.440109 177.1069 10.90829 177.5890 12.48526 178.0711 14.06663 178.5532 15.43420 179.0353 16.69068 179.5175 18.14595 179.9996 20.06166 180.4817 22.28533 180.9638 24.61956 181.4459 27.11279 181.9280 29.53294 182.4102 31.59435 182.8923 33.29766 183.3744 34.89311 183.8565 36.48137 184.3386 38.07213 184.8207 39.64969 185.3029 41.24874 185.7850 42.78876 186.2671 44.10429 186.7492 45.20114 187.2313 46.35293 187.7134 47.85942 188.1956 49.63147 188.6777 51.12130 189.1598 52.13673 189.6419 52.97380 190.1240 54.34691 190.6061 56.29818 191.0883 58.28621 191.5704 59.86903 192.0525 61.10772 192.5346 62.40783 193.0167 63.75084 193.4988 65.19001 193.9810 66.80009 194.4631 68.52425 194.9452 70.37134 195.4273 71.93852 195.9094 73.23536 196.3915 74.54257 196.8737 75.93666 197.3558 77.36702 197.8379 78.65750 198.3200 79.77828 198.8021 80.90105 199.2842 82.22450 199.7664 83.77323 200.2485 85.12876 200.7306 86.18314 201.2127 86.98927 201.6948 87.85468 202.1769 88.79483 202.6591 89.71752 203.1412 90.50727 203.6233 91.20402 204.1054 91.86589 204.5875 92.44283 205.0696 92.95216 205.5518 93.82012 206.0339 95.16158 206.5160 96.57549 206.9981 97.65089 207.4802 98.36658 207.9623 98.85812 208.4445 99.14474 208.9266 99.24778 209.4087 99.28068 209.8908 99.19402 210.3729 99.08241 210.8550 98.96473 211.3372 98.73585 211.8193 98.91257 212.3014 99.79137 212.7835 101.3525 213.2656 102.3369 213.7477 102.5693 214.2299 102.5019 214.7120 102.6669 215.1941 103.1126 215.6762 103.6435 216.1583 104.3222 216.6404 105.1800 217.1226 105.4018 217.6047 104.6800 218.0868 103.6849 218.5689 103.2417 219.0510 103.5499 219.5331 103.9385 220.0153 104.3163 220.4974 104.7409 220.9795 104.6976 221.4616 104.0435 221.9437 103.1174 222.4258 102.3531 222.9080 101.9642 223.3901 101.2564 223.8722 99.99125 224.3543 98.05158 224.8364 96.15321 225.3185 94.28808 225.8007 92.53661 226.2828 91.00994 226.7649 89.89891 227.2470 88.64998 227.7291 87.05232 228.2112 84.99167 228.6934 83.29301 229.1755 82.20793 229.6576 81.26086 230.1397 79.79871 230.6218 77.39888 231.1039 75.23785 231.5861 73.74059 232.0682 73.03437 232.5503 71.93182 233.0324 70.16642 233.5145 68.24216 233.9966 66.81210 234.4788 66.21122 234.9609 65.51796 235.4430 64.42516 235.9251 62.82899 236.4072 61.59227 236.8893 60.91920 237.3715 60.43391 237.8536 59.65239 238.3357 58.35969 238.8178 57.13061 239.2999 56.14240 239.7820 55.45425 240.2642 54.59811 240.7463 53.48761 241.2284 52.27799 241.7105 51.16227 242.1926 50.20247 242.6747 49.21936 243.1569 48.13753 243.6390 46.91668 244.1211 45.91206 244.6032 45.23080 245.0853 44.66153 245.5674 43.97051 246.0496 43.15644 246.5317 42.22083 247.0138 41.13481 247.4959 39.88024 247.9780 38.63300 248.4601 37.30915 248.9423 36.06636 249.4244 35.09005 249.9065 34.47216 250.3886 33.95221 250.8707 33.55550 251.3528 33.30669 251.8350 32.68922 252.3171 31.52914 252.7992 30.19908 253.2813 29.03452 253.7634 27.95941 254.2455 27.24938 254.7277 27.08877 255.2098 27.48997 255.6919 27.55450 256.1740 27.15133 256.6561 26.57409 257.1382 26.12104 257.6204 25.88602 258.1025 25.52431 258.5846 24.89305 259.0667 24.01431 259.5488 23.49419 260.0309 23.57588 260.5131 23.67729 260.9952 23.22620 261.4773 21.95549 261.9594 20.89468 262.4415 20.31125 262.9236 20.13942 263.4058 19.73833 263.8879 19.04623 264.3700 18.17933 264.8521 17.12243 265.3342 15.72719 265.8163 14.71740 266.2985 14.34408 266.7806 14.47367 267.2627 14.29737 267.7448 13.70016 268.2269 13.00481 268.7090 12.49681 269.1912 12.26263 269.6733 11.79023 270.1554 10.84158 270.6375 9.607533 271.1196 8.965046 271.6017 9.092072 272.0839 9.380116 272.5660 9.407116 273.0481 9.119938 273.5302 8.960590 274.0123 9.059383 274.4944 9.255833 274.9766 9.021416 275.4587 8.241863 275.9408 7.426880 276.4229 6.910419 276.9050 6.713604 277.3871 6.568275 277.8693 6.486000 278.3514 6.417706 278.8335 6.234077 279.3156 5.916477 279.7977 5.626904 280.2798 5.473484 280.7620 5.458736 281.2441 5.372570 281.7262 5.170380 282.2083 4.954803 282.6904 4.944851 283.1725 5.155952 283.6547 5.345531 284.1368 5.337231 284.6189 5.159184 285.1010 5.168201 285.5831 5.403904 286.0652 5.736065 286.5474 5.987865 287.0295 6.160595 287.5116 6.307159 287.9937 6.477409 288.4758 6.651104 288.9579 6.678108 289.4401 6.535267 289.9222 6.366676 290.4043 6.340805 290.8864 6.447899 291.3685 6.610561 291.8506 6.806473 292.3328 7.035568 292.8149 7.318516 293.2970 7.663048 293.7791 7.979496 294.2612 8.032677 294.7433 7.933914 295.2255 8.156269 295.7076 9.065338 296.1897 10.27377 296.6718 10.91727 297.1539 11.00871 297.6360 11.10375 298.1182 11.85793 298.6003 12.98596 299.0824 13.76298 299.5645 13.84221 300.0466 13.64435 300.5287 13.77787 301.0109 14.20241 301.4930 14.63655 301.9751 14.98304 302.4572 15.18186 302.9393 15.08797 303.4214 14.56180 303.9036 13.93254 304.3857 13.61862 304.8678 13.52787 305.3499 13.31061 305.8320 12.66661 306.3141 11.81199 306.7963 11.01890 307.2784 10.33743 307.7605 9.675690 308.2426 8.965801 308.7247 8.214691 309.2068 7.439487 309.6890 6.600769 310.1711 5.766491 310.6532 4.972752 311.1353 4.202774 311.6174 3.593933 312.0995 3.387718 312.5817 3.388615 313.0638 3.276733 313.5459 2.859634 314.0280 2.333080 314.5101 1.748287 314.9922 1.099285 315.4744 0.6130640 315.9565 0.5492590 316.4386 0.6629710 316.9207 0.6773300 317.4028 0.4088750 317.8849 0.1130750 318.3671 9.3921997E-02 318.8492 0.2176400 319.3313 0.3723030 319.8134 0.7086070 320.2955 1.035000 320.7776 1.194763 321.2598 0.9866260 321.7419 0.7915040 322.2240 0.6672550 322.7061 0.6188890 323.1882 0.6672630 323.6703 0.9402010 324.1525 1.227741 324.6346 1.407673 325.1167 1.338066 325.5988 1.340893 326.0809 1.593876 326.5630 1.953354 327.0452 2.025890 327.5273 1.432564 328.0094 0.8531530 328.4915 0.5270840 328.9736 0.5590060 329.4557 0.6162490 329.9379 0.7133900 330.4200 0.8322720 330.9021 0.9483300 331.3842 1.148460 331.8663 1.233170 332.3484 1.111519 332.8306 0.7383580 333.3127 0.4544220 333.7948 0.2795450 334.2769 0.1814380 334.7590 0.1364250 335.2411 0.2174220 335.7233 0.1639400 336.2054 0.1330340 336.6875 0.6378250 337.1696 0.9809760 337.6517 1.117992 338.1339 1.211960 338.6160 1.396210 339.0981 1.682144 339.5802 1.939604 340.0623 2.133156 340.5444 2.319292 341.0266 2.673098 341.5087 3.231504 341.9908 3.715765 342.4729 3.907982 342.9550 3.810061 343.4371 3.866179 343.9193 4.184498 344.4014 4.586115 344.8835 4.625805 345.3656 4.283051 345.8477 3.958496 346.3298 3.888981 346.8120 4.044552 347.2941 4.264771 347.7762 4.547350 348.2583 4.858168 348.7404 5.165789 349.2225 5.481291 349.7047 5.835873 350.1868 6.253662 350.6689 6.687307 351.1510 7.098783 351.6331 7.489679 352.1152 7.815840 352.5974 7.939730 353.0795 7.981544 353.5616 8.175739 354.0437 8.651558 354.5258 9.221462 355.0079 9.702671 355.4901 10.11205 355.9722 10.53756 356.4543 11.04642 356.9364 11.59541 357.4185 12.14064 357.9006 12.66090 358.3828 13.19840 358.8649 13.81344 359.3470 14.46994 359.8291 15.09740 360.3112 15.64364 360.7933 16.16703 361.2755 16.70849 361.7576 17.27609 362.2397 17.84023 362.7218 18.53758 363.2039 19.16611 363.6860 19.50440 364.1682 19.35511 364.6503 19.03838 365.1324 18.58518 365.6145 18.00570 366.0966 17.52061 366.5787 17.39010 367.0609 17.23152 367.5430 16.79381 368.0251 15.74568 368.5072 14.75975 368.9893 13.96774 369.4714 13.29485 369.9536 12.50384 370.4357 11.36007 370.9178 10.34330 371.3999 9.701561 371.8820 9.693100 372.3641 9.358879 372.8463 8.534122 373.3284 7.498621 373.8105 6.661566 374.2926 6.038752 374.7747 5.579338 375.2568 5.288206 375.7390 5.165621 376.2211 5.094246 376.7032 5.117355 377.1853 5.092358 377.6674 4.823261 378.1495 4.269772 378.6317 3.808847 379.1138 3.519604 379.5959 3.386944 380.0780 3.434263 380.5601 3.684334 381.0422 3.817610 381.5244 3.493071 382.0065 2.806700 382.4886 2.307697 382.9707 2.057751 383.4528 2.018927 383.9349 2.279398 384.4171 2.756067 384.8992 3.041883 385.3813 2.842878 385.8634 2.395079 386.3455 2.075768 386.8276 1.883707 387.3098 1.739532 387.7919 1.555790 388.2740 1.369791 388.7561 1.257238 389.2382 1.340883 389.7203 1.406713 390.2025 1.205532 390.6846 0.8158840 391.1667 0.5401290 391.6488 0.7172870 392.1309 0.9815790 392.6130 0.9895690 393.0952 0.5169530 393.5773 0.1255280 394.0594 0.1853450 394.5415 0.4842680 395.0236 0.6318110 395.5057 0.3277130 395.9879 1.2054000E-02 396.4700 0.1090470 396.9521 2.0884000E-02 397.4342 7.0271000E-02 397.9163 0.1373580 398.3984 0.3878770 398.8806 0.4859830 399.3627 0.2660430 399.8448 6.5430000E-02 400.3269 0.1392520 400.8090 0.3218920 401.2911 0.2631380 401.7733 0.2931250 402.2554 0.7896670 402.7375 0.9055630 403.2196 0.4279560 403.7017 0.1087570 404.1838 9.7850002E-03 404.6660 3.3333000E-02 405.1481 1.6868999E-02 405.6302 0.1763130 406.1123 0.2759900 406.5944 0.2153470 407.0765 7.2920001E-03 407.5587 3.8495999E-02 408.0408 0.1064300 408.5229 0.3013080 409.0050 0.3967900 409.4871 0.3996120 409.9692 0.4150660 410.4514 0.4704440 410.9335 0.5459920 411.4156 0.5981270 411.8977 0.6289420 412.3798 0.6648480 412.8619 0.7608180 413.3441 0.8675610 413.8262 0.8635160 414.3083 0.7118070 414.7904 0.5660320 415.2725 0.5905670 415.7546 0.7308060 416.2368 0.8731420 416.7189 0.9828530 417.2010 1.062359 417.6831 1.142563 418.1652 1.216623 418.6473 1.184896 419.1295 0.8638020 419.6116 0.4772130 420.0937 0.2301690 420.5758 0.2196160 421.0579 0.2796860 421.5400 0.4119490 422.0222 0.5759470 422.5043 0.6744980 422.9864 0.6712460 423.4685 0.6108040 423.9506 0.4676530 424.4327 0.1586700 424.9149 5.7055000E-02 425.3970 0.3649540 425.8791 0.7793600 426.3612 0.9984130 426.8433 0.8869920 427.3254 0.7887780 427.8076 0.7343940 428.2897 0.7285250 428.7718 0.8282200 429.2539 1.086246 429.7360 1.339949 430.2181 1.472502 430.7003 1.457287 431.1824 1.502567 431.6645 1.632053 432.1466 1.798693 432.6287 1.944151 433.1108 2.068836 433.5930 2.107841 434.0751 1.922522 434.5572 1.647560 435.0393 1.833549 435.5214 2.491983 436.0035 3.138760 436.4857 3.245974 436.9678 3.008766 437.4499 2.891203 437.9320 2.986073 438.4141 3.252819 438.8962 3.783213 439.3784 4.473207 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