#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 16:00:07 +0300 (Thu, 24 May 2018) $
#$Revision: 856 $
#$URL: svn://172.16.1.111/rod/cif/1/00/03/1000343.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000343
loop_
_publ_author_name
'Kampf, A. R.'
'Housley, R. M.'
'Mills, S. J.'
'Marty, J.'
'Thorne, B.'
_publ_section_title
;
 Lead-tellurium oxysalts from Otto Mountain near Baker, California: I.
 Ottoite, Pb2TeO5, a new mineral with chains of tellurate octahedra
;
_journal_name_full               'American Mineralogist'
_journal_page_first              1329
_journal_page_last               1336
_journal_paper_doi               10.2138/am.2010.3510
_journal_volume                  95
_journal_year                    2010
_chemical_compound_source        'Otto Mountain, Baker, California, USA'
_chemical_formula_sum            'O5 Pb2 Te'
_chemical_name_mineral           Ottoite
_space_group_IT_number           15
_symmetry_space_group_name_Hall  '-I 2ya'
_symmetry_space_group_name_H-M   'I 1 2/a 1'
_cell_angle_alpha                90
_cell_angle_beta                 91.330
_cell_angle_gamma                90
_cell_length_a                   7.5353
_cell_length_b                   5.7142
_cell_length_c                   10.8981
_cell_volume                     469.126
_exptl_crystal_density_diffrn    8.807
_cod_original_formula_sum        'Pb2 Te O5'
_cod_database_code               9015570
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R130126.rod
_rod_data_source.block           3500000
_rod_database.code               1000343
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9015570 COD http://www.crystallography.net/cod/9015570.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
225.8007 0.0000000E+00
226.2828 3.0884000E-02
226.7649 7.9650998E-02
227.2470 0.3023070
227.7291 0.7668760
228.2112 1.054108
228.6934 2.429993
229.1755 5.255219
229.6576 8.727509
230.1397 11.76202
230.6218 14.15921
231.1039 16.47781
231.5861 18.67487
232.0682 20.64688
232.5503 23.53748
233.0324 27.81107
233.5145 32.59058
233.9966 36.79184
234.4788 39.97678
234.9609 43.30643
235.4430 47.09589
235.9251 51.39383
236.4072 55.83966
236.8893 60.56796
237.3715 65.36609
237.8536 69.87939
238.3357 73.90399
238.8178 78.10471
239.2999 82.93771
239.7820 88.62054
240.2642 92.74106
240.7463 95.05331
241.2284 95.96771
241.7105 95.94284
242.1926 94.86288
242.6747 93.04755
243.1569 90.51886
243.6390 87.22098
244.1211 83.57449
244.6032 79.61639
245.0853 75.48727
245.5674 70.90302
246.0496 65.48291
246.5317 60.43918
247.0138 56.08185
247.4959 52.24786
247.9780 48.51797
248.4601 45.59174
248.9423 42.35706
249.4244 38.70145
249.9065 34.35825
250.3886 30.34259
250.8707 27.57367
251.3528 26.11823
251.8350 24.79019
252.3171 23.36902
252.7992 21.96185
253.2813 20.75897
253.7634 19.98862
254.2455 19.05725
254.7277 17.64566
255.2098 15.79562
255.6919 14.42316
256.1740 13.83728
256.6561 13.43390
257.1382 12.41974
257.6204 10.45599
258.1025 8.816895
258.5846 7.804962
259.0667 7.386353
259.5488 6.950592
260.0309 6.461945
260.5131 6.018890
260.9952 5.784637
261.4773 5.961487
261.9594 5.773010
262.4415 4.968689
262.9236 3.628021
263.4058 2.563904
263.8879 1.705963
264.3700 1.234009
264.8521 1.444580
265.3342 2.679962
265.8163 3.413422
266.2985 3.293579
266.7806 2.474579
267.2627 1.792297
267.7448 1.217072
268.2269 0.8413390
268.7090 0.8651730
269.1912 1.492737
269.6733 1.567963
270.1554 0.6977840
270.6375 0.7743530
271.1196 1.322113
271.6017 0.6544490
272.0839 0.1211240
272.5660 0.1380920
273.0481 0.7741390
273.5302 1.258423
274.0123 1.019012
274.4944 0.3756410
274.9766 0.3134160
275.4587 0.9513240
275.9408 1.691650
276.4229 2.209015
276.9050 2.502075
277.3871 2.574585
277.8693 2.373932
278.3514 2.007324
278.8335 1.699402
279.3156 1.444214
279.7977 1.244934
280.2798 1.120544
280.7620 1.075256
281.2441 1.029541
281.7262 0.9946900
282.2083 0.9360660
282.6904 0.7560420
283.1725 0.4453430
283.6547 9.6923999E-02
284.1368 9.6771002E-02
284.6189 0.1492920
285.1010 0.2840580
285.5831 0.5294490
286.0652 0.7781980
286.5474 0.7661740
287.0295 0.5028080
287.5116 0.4740910
287.9937 1.045532
288.4758 2.096039
288.9579 2.861511
289.4401 3.326477
289.9222 3.650604
290.4043 3.925690
290.8864 4.179871
291.3685 4.643585
291.8506 5.535889
292.3328 6.687592
292.8149 7.524567
293.2970 8.029602
293.7791 8.487152
294.2612 9.217621
294.7433 10.15591
295.2255 11.01227
295.7076 11.49472
296.1897 11.94013
296.6718 13.13669
297.1539 15.05896
297.6360 17.03433
298.1182 18.33069
298.6003 19.22134
299.0824 20.45215
299.5645 22.41068
300.0466 24.60678
300.5287 26.17450
301.0109 27.21912
301.4930 28.56290
301.9751 31.01599
302.4572 34.12170
302.9393 37.01495
303.4214 39.42169
303.9036 41.80579
304.3857 44.79840
304.8678 48.23453
305.3499 51.58289
305.8320 54.44107
306.3141 57.03320
306.7963 59.47787
307.2784 61.68298
307.7605 64.16638
308.2426 67.54984
308.7247 71.56366
309.2068 75.56430
309.6890 78.99011
310.1711 82.38947
310.6532 86.23639
311.1353 90.62469
311.6174 95.12640
312.0995 99.32239
312.5817 103.4076
313.0638 107.7579
313.5459 112.9196
314.0280 118.1471
314.5101 122.9131
314.9922 127.1322
315.4744 131.4982
315.9565 136.6516
316.4386 142.0193
316.9207 146.8802
317.4028 150.7773
317.8849 154.4164
318.3671 158.3740
318.8492 162.6295
319.3313 165.8467
319.8134 167.2997
320.2955 167.6891
320.7776 167.5574
321.2598 167.0846
321.7419 166.0245
322.2240 164.6013
322.7061 162.6764
323.1882 159.4589
323.6703 153.9932
324.1525 147.6706
324.6346 141.3098
325.1167 135.2937
325.5988 128.7659
326.0809 121.3873
326.5630 113.4416
327.0452 105.6493
327.5273 97.57809
328.0094 90.10754
328.4915 83.54156
328.9736 78.41956
329.4557 73.39633
329.9379 68.40057
330.4200 63.46716
330.9021 58.71494
331.3842 53.92697
331.8663 49.66351
332.3484 46.17657
332.8306 43.61774
333.3127 40.83139
333.7948 37.57050
334.2769 34.29062
334.7590 31.55798
335.2411 29.59283
335.7233 27.70041
336.2054 25.69980
336.6875 23.61041
337.1696 22.02567
337.6517 21.12323
338.1339 20.38644
338.6160 19.44357
339.0981 18.29794
339.5802 16.87924
340.0623 15.03766
340.5444 12.98642
341.0266 11.53491
341.5087 10.72470
341.9908 10.19208
342.4729 9.698273
342.9550 9.244202
343.4371 9.066772
343.9193 9.309784
344.4014 9.569733
344.8835 8.986755
345.3656 7.574371
345.8477 6.196014
346.3298 5.273315
346.8120 4.731628
347.2941 4.299652
347.7762 3.981567
348.2583 3.736420
348.7404 3.630249
349.2225 3.596466
349.7047 3.328735
350.1868 2.484528
350.6689 1.436676
351.1510 0.8656620
351.6331 0.7656860
352.1152 0.8178710
352.5974 0.7874150
353.0795 0.7143550
353.5616 0.6894530
354.0437 0.8178710
354.5258 0.8977050
355.0079 0.6013490
355.4901 2.7984999E-02
355.9722 0.3834530
356.4543 0.2407840
356.9364 0.1475520
357.4185 0.4956970
357.9006 0.7849430
358.3828 0.9455870
358.8649 0.7904660
359.3470 0.4820560
359.8291 0.3479610
360.3112 0.4911800
360.7933 0.8803410
361.2755 1.688660
361.7576 3.047241
362.2397 3.927460
362.7218 3.485596
363.2039 2.516174
363.6860 1.906403
364.1682 1.843109
364.6503 2.217316
365.1324 3.313995
365.6145 5.086426
366.0966 6.257080
366.5787 6.019989
367.0609 5.491394
367.5430 5.387390
368.0251 6.196381
368.5072 6.936371
368.9893 7.576691
369.4714 8.104980
369.9536 8.426666
370.4357 8.159363
370.9178 8.094177
371.3999 8.568085
371.8820 9.796417
372.3641 11.03610
372.8463 12.34253
373.3284 13.60632
373.8105 14.64297
374.2926 15.33365
374.7747 16.05573
375.2568 16.86060
375.7390 17.74847
376.2211 19.16071
376.7032 21.46344
377.1853 23.54700
377.6674 24.14218
378.1495 23.04053
378.6317 22.34509
379.1138 22.59241
379.5959 23.42746
380.0780 23.75604
380.5601 23.54584
381.0422 23.18008
381.5244 22.96298
382.0065 22.84216
382.4886 22.49524
382.9707 21.86807
383.4528 21.08649
383.9349 20.40652
384.4171 19.76572
384.8992 18.83310
385.3813 17.10559
385.8634 15.07913
386.3455 13.61298
386.8276 12.75143
387.3098 12.08588
387.7919 11.41992
388.2740 10.67026
388.7561 9.674774
389.2382 7.985138
389.7203 6.395844
390.2025 5.623016
390.6846 5.564423
391.1667 5.745209
391.6488 6.439789
392.1309 6.959106
392.6130 6.618927
393.0952 4.887268
393.5773 3.191559
394.0594 2.146759
394.5415 1.562531
395.0236 1.083496
395.5057 0.4328610
395.9879 2.3071000E-02
396.4700 0.1351930
396.9521 0.8978580
397.4342 1.475464
397.9163 1.703766
398.3984 1.711426
398.8806 1.615082
399.3627 1.298065
399.8448 1.014343
400.3269 0.6444400
400.8090 0.2597350
401.2911 0.4286500
401.7733 1.539673
402.2554 2.743500
402.7375 3.603638
403.2196 4.015045
403.7017 4.332367
404.1838 4.498077
404.6660 4.619263
405.1481 4.919067
405.6302 5.461151
406.1123 5.946808
406.5944 6.136230
407.0765 6.071869
407.5587 6.798767
408.0408 8.526367
408.5229 10.25430
409.0050 10.63400
409.4871 9.788269
409.9692 9.626892
410.4514 10.71606
410.9335 12.54910
411.4156 14.23514
411.8977 15.76181
412.3798 17.11099
412.8619 18.23752
413.3441 19.14688
413.8262 19.67590
414.3083 19.69647
414.7904 19.93774
415.2725 21.58588
415.7546 23.97690
416.2368 25.75626
416.7189 26.02365
417.2010 25.63889
417.6831 25.11203
418.1652 24.47940
418.6473 23.97971
419.1295 24.12375
419.6116 24.26984
420.0937 23.84204
420.5758 22.49307
421.0579 20.85751
421.5400 18.93045
422.0222 16.85715
422.5043 14.94250
422.9864 13.22083
423.4685 11.73312
423.9506 10.56757
424.4327 9.915619
424.9149 8.984283
425.3970 7.379669
425.8791 5.711578
426.3612 4.524750
426.8433 4.056030
427.3254 3.861359
427.8076 4.078918
428.2897 4.617401
428.7718 4.347992
429.2539 2.729065
429.7360 1.387787
430.2181 1.627258
430.7003 3.854950
431.1824 4.765656
431.6645 3.865295
432.1466 2.269440
432.6287 1.927551
433.1108 2.847992
433.5930 3.710571
434.0751 4.023712
434.5572 3.924805
435.0393 3.512543
435.5214 2.784241
436.0035 2.397614
436.4857 3.280151
436.9678 4.964172
437.4499 6.310547
437.9320 7.006470
438.4141 7.402313
438.8962 7.936798
439.3784 8.513580
439.8605 8.809387
440.3426 8.296692
440.8247 7.798615
441.3068 8.099030
441.7889 9.347412
442.2711 10.57977
442.7532 11.45142
443.2353 12.05707
443.7174 12.48123
444.1995 12.80417
444.6816 12.90015
445.1638 12.35440
445.6459 11.41779
446.1280 11.22943
446.6101 12.96826
447.0922 14.68887
447.5743 15.51193
448.0565 14.96838
448.5386 14.73291
449.0207 15.10489
449.5028 15.55133
449.9849 15.30511
450.4670 13.95981
450.9492 12.94635
451.4313 12.67490
451.9134 13.01331
452.3955 13.24545
452.8776 13.47601
453.3597 13.33643
453.8419 12.35046
454.3240 10.49982
454.8061 9.013672
455.2882 8.088867
455.7703 7.457672
456.2524 6.696960
456.7346 5.847900
457.2167 5.226776
457.6988 5.020020
458.1809 5.085297
458.6630 5.340851
459.1451 5.750244
459.6273 5.846558
460.1094 4.928955
460.5915 3.605286
461.0736 2.672302
461.5557 2.371033
462.0378 2.325073
462.5200 2.484650
463.0021 2.718353
463.4842 2.761749
463.9663 2.443726
464.4484 1.976563
464.9305 1.380585
465.4127 0.6447450
465.8948 0.1254580
466.3769 9.2345998E-02
466.8590 6.6161998E-02
467.3411 0.1682430
467.8232 1.226715
468.3054 1.658691
468.7875 0.9334410
469.2696 0.3664250
469.7517 0.7142640
470.2338 0.4757080
470.7159 1.524994
471.1981 1.789215
471.6802 1.232147
472.1623 0.7053220
472.6444 0.1198120
473.1265 0.1879580
473.6086 0.4261470
474.0908 1.934998
474.5729 2.671326
475.0550 2.142822
475.5371 0.9890440
476.0192 0.2322080
476.5013 0.1266780
476.9835 5.2917000E-02
477.4656 0.9951170
477.9477 2.301605
478.4298 2.511688
478.9119 1.539154
479.3940 0.5318910
479.8762 0.5187070
480.3583 0.9754640
480.8404 1.208527
481.3225 0.9397580
481.8046 0.5231320
482.2867 9.3993999E-02
482.7689 0.7272950
483.2510 0.9110720
483.7331 0.2489930
484.2152 1.273132
484.6973 1.347809
485.1794 0.1492920
485.6616 0.5673830
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487.1079 0.7377010
487.5900 0.9776000
488.0721 0.9707030
488.5543 0.6246030
489.0364 4.6599999E-02
489.5185 0.5178830
490.0006 1.172791
490.4827 1.489502
490.9648 1.066711
491.4470 3.0944999E-02
491.9291 0.3269650
492.4112 0.3263850
492.8933 1.077362
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493.8575 0.1276860
494.3397 0.5719300
494.8218 1.033264
495.3039 1.190308
495.7860 0.5859990
496.2681 0.4928590
496.7502 1.072357
497.2324 3.8605001E-02
497.7145 1.466522
498.1966 1.726807
498.6787 0.7395020
499.1608 2.4994001E-02
499.6429 0.5448610
500.1251 1.499481
500.6072 2.001465
501.0893 1.497070
501.5714 1.006531
502.0535 0.6550600
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503.0178 0.5001530
503.4999 1.232239
503.9820 1.671936
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504.9462 0.6026000
505.4283 3.7994001E-02
505.9105 0.4458310
506.3926 0.6100770
506.8747 0.4220890
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507.8389 0.5482790
508.3210 0.4255070
508.8032 0.1417240
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509.7674 0.8923340
510.2495 1.256226
510.7316 0.8153690
511.2137 0.1188660
511.6959 0.6479800
512.1780 2.287445
512.6601 3.659485
513.1422 3.426514
513.6243 2.454681
514.1064 1.859863
514.5886 1.907410
515.0707 2.085480
515.5528 2.085449
516.0349 2.026489
516.5170 2.075409
516.9991 2.450745
517.4813 2.778442
517.9634 2.957703
518.4455 2.994385
518.9276 2.932251
519.4097 2.648010
519.8918 2.447968
520.3740 2.394043
520.8561 2.411835
521.3382 2.632813
521.8203 3.195282
522.3024 3.822510
522.7845 4.129395
523.2667 4.020599
523.7488 4.125122
524.2309 4.632477
524.7130 5.418213
525.1951 6.102264
525.6772 6.656830
526.1594 7.095947
526.6415 7.424103
527.1236 7.642883
527.6057 7.751129
528.0878 7.809143
528.5699 7.836304
529.0521 7.688171
529.5342 7.552155
530.0163 7.674316
530.4984 8.272522
530.9805 8.847809
531.4626 8.935852
531.9448 8.843964
532.4269 9.115417
532.9090 10.29822
533.3911 11.47952
533.8732 12.34631
534.3553 12.88773
534.8375 13.44785
535.3196 14.18930
535.8017 14.67834
536.2838 14.57648
536.7659 13.51611
537.2480 13.04626
537.7302 13.40991
538.2123 14.16653
538.6944 14.58365
539.1765 14.63861
539.6586 14.67627
540.1407 14.82001
540.6229 14.92758
541.1050 14.68658
541.5871 14.21326
542.0692 13.72778
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1299.957 1.0620000E-02
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1301.403 0.5730590
1301.885 0.0000000E+00
