#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-05-24 16:00:07 +0300 (Thu, 24 May 2018) $ #$Revision: 856 $ #$URL: svn://172.16.1.111/rod/cif/1/00/03/1000343.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_1000343 loop_ _publ_author_name 'Kampf, A. R.' 'Housley, R. M.' 'Mills, S. J.' 'Marty, J.' 'Thorne, B.' _publ_section_title ; Lead-tellurium oxysalts from Otto Mountain near Baker, California: I. Ottoite, Pb2TeO5, a new mineral with chains of tellurate octahedra ; _journal_name_full 'American Mineralogist' _journal_page_first 1329 _journal_page_last 1336 _journal_paper_doi 10.2138/am.2010.3510 _journal_volume 95 _journal_year 2010 _chemical_compound_source 'Otto Mountain, Baker, California, USA' _chemical_formula_sum 'O5 Pb2 Te' _chemical_name_mineral Ottoite _space_group_IT_number 15 _symmetry_space_group_name_Hall '-I 2ya' _symmetry_space_group_name_H-M 'I 1 2/a 1' _cell_angle_alpha 90 _cell_angle_beta 91.330 _cell_angle_gamma 90 _cell_length_a 7.5353 _cell_length_b 5.7142 _cell_length_c 10.8981 _cell_volume 469.126 _exptl_crystal_density_diffrn 8.807 _cod_original_formula_sum 'Pb2 Te O5' _cod_database_code 9015570 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type other _raman_measurement_device.excitation_laser_wavelength 532 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 15 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R130126.rod _rod_data_source.block 3500000 _rod_database.code 1000343 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9015570 COD http://www.crystallography.net/cod/9015570.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 225.8007 0.0000000E+00 226.2828 3.0884000E-02 226.7649 7.9650998E-02 227.2470 0.3023070 227.7291 0.7668760 228.2112 1.054108 228.6934 2.429993 229.1755 5.255219 229.6576 8.727509 230.1397 11.76202 230.6218 14.15921 231.1039 16.47781 231.5861 18.67487 232.0682 20.64688 232.5503 23.53748 233.0324 27.81107 233.5145 32.59058 233.9966 36.79184 234.4788 39.97678 234.9609 43.30643 235.4430 47.09589 235.9251 51.39383 236.4072 55.83966 236.8893 60.56796 237.3715 65.36609 237.8536 69.87939 238.3357 73.90399 238.8178 78.10471 239.2999 82.93771 239.7820 88.62054 240.2642 92.74106 240.7463 95.05331 241.2284 95.96771 241.7105 95.94284 242.1926 94.86288 242.6747 93.04755 243.1569 90.51886 243.6390 87.22098 244.1211 83.57449 244.6032 79.61639 245.0853 75.48727 245.5674 70.90302 246.0496 65.48291 246.5317 60.43918 247.0138 56.08185 247.4959 52.24786 247.9780 48.51797 248.4601 45.59174 248.9423 42.35706 249.4244 38.70145 249.9065 34.35825 250.3886 30.34259 250.8707 27.57367 251.3528 26.11823 251.8350 24.79019 252.3171 23.36902 252.7992 21.96185 253.2813 20.75897 253.7634 19.98862 254.2455 19.05725 254.7277 17.64566 255.2098 15.79562 255.6919 14.42316 256.1740 13.83728 256.6561 13.43390 257.1382 12.41974 257.6204 10.45599 258.1025 8.816895 258.5846 7.804962 259.0667 7.386353 259.5488 6.950592 260.0309 6.461945 260.5131 6.018890 260.9952 5.784637 261.4773 5.961487 261.9594 5.773010 262.4415 4.968689 262.9236 3.628021 263.4058 2.563904 263.8879 1.705963 264.3700 1.234009 264.8521 1.444580 265.3342 2.679962 265.8163 3.413422 266.2985 3.293579 266.7806 2.474579 267.2627 1.792297 267.7448 1.217072 268.2269 0.8413390 268.7090 0.8651730 269.1912 1.492737 269.6733 1.567963 270.1554 0.6977840 270.6375 0.7743530 271.1196 1.322113 271.6017 0.6544490 272.0839 0.1211240 272.5660 0.1380920 273.0481 0.7741390 273.5302 1.258423 274.0123 1.019012 274.4944 0.3756410 274.9766 0.3134160 275.4587 0.9513240 275.9408 1.691650 276.4229 2.209015 276.9050 2.502075 277.3871 2.574585 277.8693 2.373932 278.3514 2.007324 278.8335 1.699402 279.3156 1.444214 279.7977 1.244934 280.2798 1.120544 280.7620 1.075256 281.2441 1.029541 281.7262 0.9946900 282.2083 0.9360660 282.6904 0.7560420 283.1725 0.4453430 283.6547 9.6923999E-02 284.1368 9.6771002E-02 284.6189 0.1492920 285.1010 0.2840580 285.5831 0.5294490 286.0652 0.7781980 286.5474 0.7661740 287.0295 0.5028080 287.5116 0.4740910 287.9937 1.045532 288.4758 2.096039 288.9579 2.861511 289.4401 3.326477 289.9222 3.650604 290.4043 3.925690 290.8864 4.179871 291.3685 4.643585 291.8506 5.535889 292.3328 6.687592 292.8149 7.524567 293.2970 8.029602 293.7791 8.487152 294.2612 9.217621 294.7433 10.15591 295.2255 11.01227 295.7076 11.49472 296.1897 11.94013 296.6718 13.13669 297.1539 15.05896 297.6360 17.03433 298.1182 18.33069 298.6003 19.22134 299.0824 20.45215 299.5645 22.41068 300.0466 24.60678 300.5287 26.17450 301.0109 27.21912 301.4930 28.56290 301.9751 31.01599 302.4572 34.12170 302.9393 37.01495 303.4214 39.42169 303.9036 41.80579 304.3857 44.79840 304.8678 48.23453 305.3499 51.58289 305.8320 54.44107 306.3141 57.03320 306.7963 59.47787 307.2784 61.68298 307.7605 64.16638 308.2426 67.54984 308.7247 71.56366 309.2068 75.56430 309.6890 78.99011 310.1711 82.38947 310.6532 86.23639 311.1353 90.62469 311.6174 95.12640 312.0995 99.32239 312.5817 103.4076 313.0638 107.7579 313.5459 112.9196 314.0280 118.1471 314.5101 122.9131 314.9922 127.1322 315.4744 131.4982 315.9565 136.6516 316.4386 142.0193 316.9207 146.8802 317.4028 150.7773 317.8849 154.4164 318.3671 158.3740 318.8492 162.6295 319.3313 165.8467 319.8134 167.2997 320.2955 167.6891 320.7776 167.5574 321.2598 167.0846 321.7419 166.0245 322.2240 164.6013 322.7061 162.6764 323.1882 159.4589 323.6703 153.9932 324.1525 147.6706 324.6346 141.3098 325.1167 135.2937 325.5988 128.7659 326.0809 121.3873 326.5630 113.4416 327.0452 105.6493 327.5273 97.57809 328.0094 90.10754 328.4915 83.54156 328.9736 78.41956 329.4557 73.39633 329.9379 68.40057 330.4200 63.46716 330.9021 58.71494 331.3842 53.92697 331.8663 49.66351 332.3484 46.17657 332.8306 43.61774 333.3127 40.83139 333.7948 37.57050 334.2769 34.29062 334.7590 31.55798 335.2411 29.59283 335.7233 27.70041 336.2054 25.69980 336.6875 23.61041 337.1696 22.02567 337.6517 21.12323 338.1339 20.38644 338.6160 19.44357 339.0981 18.29794 339.5802 16.87924 340.0623 15.03766 340.5444 12.98642 341.0266 11.53491 341.5087 10.72470 341.9908 10.19208 342.4729 9.698273 342.9550 9.244202 343.4371 9.066772 343.9193 9.309784 344.4014 9.569733 344.8835 8.986755 345.3656 7.574371 345.8477 6.196014 346.3298 5.273315 346.8120 4.731628 347.2941 4.299652 347.7762 3.981567 348.2583 3.736420 348.7404 3.630249 349.2225 3.596466 349.7047 3.328735 350.1868 2.484528 350.6689 1.436676 351.1510 0.8656620 351.6331 0.7656860 352.1152 0.8178710 352.5974 0.7874150 353.0795 0.7143550 353.5616 0.6894530 354.0437 0.8178710 354.5258 0.8977050 355.0079 0.6013490 355.4901 2.7984999E-02 355.9722 0.3834530 356.4543 0.2407840 356.9364 0.1475520 357.4185 0.4956970 357.9006 0.7849430 358.3828 0.9455870 358.8649 0.7904660 359.3470 0.4820560 359.8291 0.3479610 360.3112 0.4911800 360.7933 0.8803410 361.2755 1.688660 361.7576 3.047241 362.2397 3.927460 362.7218 3.485596 363.2039 2.516174 363.6860 1.906403 364.1682 1.843109 364.6503 2.217316 365.1324 3.313995 365.6145 5.086426 366.0966 6.257080 366.5787 6.019989 367.0609 5.491394 367.5430 5.387390 368.0251 6.196381 368.5072 6.936371 368.9893 7.576691 369.4714 8.104980 369.9536 8.426666 370.4357 8.159363 370.9178 8.094177 371.3999 8.568085 371.8820 9.796417 372.3641 11.03610 372.8463 12.34253 373.3284 13.60632 373.8105 14.64297 374.2926 15.33365 374.7747 16.05573 375.2568 16.86060 375.7390 17.74847 376.2211 19.16071 376.7032 21.46344 377.1853 23.54700 377.6674 24.14218 378.1495 23.04053 378.6317 22.34509 379.1138 22.59241 379.5959 23.42746 380.0780 23.75604 380.5601 23.54584 381.0422 23.18008 381.5244 22.96298 382.0065 22.84216 382.4886 22.49524 382.9707 21.86807 383.4528 21.08649 383.9349 20.40652 384.4171 19.76572 384.8992 18.83310 385.3813 17.10559 385.8634 15.07913 386.3455 13.61298 386.8276 12.75143 387.3098 12.08588 387.7919 11.41992 388.2740 10.67026 388.7561 9.674774 389.2382 7.985138 389.7203 6.395844 390.2025 5.623016 390.6846 5.564423 391.1667 5.745209 391.6488 6.439789 392.1309 6.959106 392.6130 6.618927 393.0952 4.887268 393.5773 3.191559 394.0594 2.146759 394.5415 1.562531 395.0236 1.083496 395.5057 0.4328610 395.9879 2.3071000E-02 396.4700 0.1351930 396.9521 0.8978580 397.4342 1.475464 397.9163 1.703766 398.3984 1.711426 398.8806 1.615082 399.3627 1.298065 399.8448 1.014343 400.3269 0.6444400 400.8090 0.2597350 401.2911 0.4286500 401.7733 1.539673 402.2554 2.743500 402.7375 3.603638 403.2196 4.015045 403.7017 4.332367 404.1838 4.498077 404.6660 4.619263 405.1481 4.919067 405.6302 5.461151 406.1123 5.946808 406.5944 6.136230 407.0765 6.071869 407.5587 6.798767 408.0408 8.526367 408.5229 10.25430 409.0050 10.63400 409.4871 9.788269 409.9692 9.626892 410.4514 10.71606 410.9335 12.54910 411.4156 14.23514 411.8977 15.76181 412.3798 17.11099 412.8619 18.23752 413.3441 19.14688 413.8262 19.67590 414.3083 19.69647 414.7904 19.93774 415.2725 21.58588 415.7546 23.97690 416.2368 25.75626 416.7189 26.02365 417.2010 25.63889 417.6831 25.11203 418.1652 24.47940 418.6473 23.97971 419.1295 24.12375 419.6116 24.26984 420.0937 23.84204 420.5758 22.49307 421.0579 20.85751 421.5400 18.93045 422.0222 16.85715 422.5043 14.94250 422.9864 13.22083 423.4685 11.73312 423.9506 10.56757 424.4327 9.915619 424.9149 8.984283 425.3970 7.379669 425.8791 5.711578 426.3612 4.524750 426.8433 4.056030 427.3254 3.861359 427.8076 4.078918 428.2897 4.617401 428.7718 4.347992 429.2539 2.729065 429.7360 1.387787 430.2181 1.627258 430.7003 3.854950 431.1824 4.765656 431.6645 3.865295 432.1466 2.269440 432.6287 1.927551 433.1108 2.847992 433.5930 3.710571 434.0751 4.023712 434.5572 3.924805 435.0393 3.512543 435.5214 2.784241 436.0035 2.397614 436.4857 3.280151 436.9678 4.964172 437.4499 6.310547 437.9320 7.006470 438.4141 7.402313 438.8962 7.936798 439.3784 8.513580 439.8605 8.809387 440.3426 8.296692 440.8247 7.798615 441.3068 8.099030 441.7889 9.347412 442.2711 10.57977 442.7532 11.45142 443.2353 12.05707 443.7174 12.48123 444.1995 12.80417 444.6816 12.90015 445.1638 12.35440 445.6459 11.41779 446.1280 11.22943 446.6101 12.96826 447.0922 14.68887 447.5743 15.51193 448.0565 14.96838 448.5386 14.73291 449.0207 15.10489 449.5028 15.55133 449.9849 15.30511 450.4670 13.95981 450.9492 12.94635 451.4313 12.67490 451.9134 13.01331 452.3955 13.24545 452.8776 13.47601 453.3597 13.33643 453.8419 12.35046 454.3240 10.49982 454.8061 9.013672 455.2882 8.088867 455.7703 7.457672 456.2524 6.696960 456.7346 5.847900 457.2167 5.226776 457.6988 5.020020 458.1809 5.085297 458.6630 5.340851 459.1451 5.750244 459.6273 5.846558 460.1094 4.928955 460.5915 3.605286 461.0736 2.672302 461.5557 2.371033 462.0378 2.325073 462.5200 2.484650 463.0021 2.718353 463.4842 2.761749 463.9663 2.443726 464.4484 1.976563 464.9305 1.380585 465.4127 0.6447450 465.8948 0.1254580 466.3769 9.2345998E-02 466.8590 6.6161998E-02 467.3411 0.1682430 467.8232 1.226715 468.3054 1.658691 468.7875 0.9334410 469.2696 0.3664250 469.7517 0.7142640 470.2338 0.4757080 470.7159 1.524994 471.1981 1.789215 471.6802 1.232147 472.1623 0.7053220 472.6444 0.1198120 473.1265 0.1879580 473.6086 0.4261470 474.0908 1.934998 474.5729 2.671326 475.0550 2.142822 475.5371 0.9890440 476.0192 0.2322080 476.5013 0.1266780 476.9835 5.2917000E-02 477.4656 0.9951170 477.9477 2.301605 478.4298 2.511688 478.9119 1.539154 479.3940 0.5318910 479.8762 0.5187070 480.3583 0.9754640 480.8404 1.208527 481.3225 0.9397580 481.8046 0.5231320 482.2867 9.3993999E-02 482.7689 0.7272950 483.2510 0.9110720 483.7331 0.2489930 484.2152 1.273132 484.6973 1.347809 485.1794 0.1492920 485.6616 0.5673830 486.1437 0.2781680 486.6258 0.3251650 487.1079 0.7377010 487.5900 0.9776000 488.0721 0.9707030 488.5543 0.6246030 489.0364 4.6599999E-02 489.5185 0.5178830 490.0006 1.172791 490.4827 1.489502 490.9648 1.066711 491.4470 3.0944999E-02 491.9291 0.3269650 492.4112 0.3263850 492.8933 1.077362 493.3754 0.9478150 493.8575 0.1276860 494.3397 0.5719300 494.8218 1.033264 495.3039 1.190308 495.7860 0.5859990 496.2681 0.4928590 496.7502 1.072357 497.2324 3.8605001E-02 497.7145 1.466522 498.1966 1.726807 498.6787 0.7395020 499.1608 2.4994001E-02 499.6429 0.5448610 500.1251 1.499481 500.6072 2.001465 501.0893 1.497070 501.5714 1.006531 502.0535 0.6550600 502.5356 0.4667970 503.0178 0.5001530 503.4999 1.232239 503.9820 1.671936 504.4641 1.471130 504.9462 0.6026000 505.4283 3.7994001E-02 505.9105 0.4458310 506.3926 0.6100770 506.8747 0.4220890 507.3568 0.2109990 507.8389 0.5482790 508.3210 0.4255070 508.8032 0.1417240 509.2853 0.3102720 509.7674 0.8923340 510.2495 1.256226 510.7316 0.8153690 511.2137 0.1188660 511.6959 0.6479800 512.1780 2.287445 512.6601 3.659485 513.1422 3.426514 513.6243 2.454681 514.1064 1.859863 514.5886 1.907410 515.0707 2.085480 515.5528 2.085449 516.0349 2.026489 516.5170 2.075409 516.9991 2.450745 517.4813 2.778442 517.9634 2.957703 518.4455 2.994385 518.9276 2.932251 519.4097 2.648010 519.8918 2.447968 520.3740 2.394043 520.8561 2.411835 521.3382 2.632813 521.8203 3.195282 522.3024 3.822510 522.7845 4.129395 523.2667 4.020599 523.7488 4.125122 524.2309 4.632477 524.7130 5.418213 525.1951 6.102264 525.6772 6.656830 526.1594 7.095947 526.6415 7.424103 527.1236 7.642883 527.6057 7.751129 528.0878 7.809143 528.5699 7.836304 529.0521 7.688171 529.5342 7.552155 530.0163 7.674316 530.4984 8.272522 530.9805 8.847809 531.4626 8.935852 531.9448 8.843964 532.4269 9.115417 532.9090 10.29822 533.3911 11.47952 533.8732 12.34631 534.3553 12.88773 534.8375 13.44785 535.3196 14.18930 535.8017 14.67834 536.2838 14.57648 536.7659 13.51611 537.2480 13.04626 537.7302 13.40991 538.2123 14.16653 538.6944 14.58365 539.1765 14.63861 539.6586 14.67627 540.1407 14.82001 540.6229 14.92758 541.1050 14.68658 541.5871 14.21326 542.0692 13.72778 542.5513 13.20029 543.0334 12.81665 543.5156 12.91061 543.9977 13.58896 544.4798 14.14374 544.9619 13.84009 545.4440 13.26819 545.9261 12.96393 546.4083 13.30954 546.8904 13.58514 547.3725 13.37112 547.8546 12.87012 548.3367 12.56091 548.8188 12.39581 549.3010 12.68646 549.7831 13.62317 550.2652 15.14255 550.7473 16.15259 551.2294 16.59094 551.7115 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