#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 16:00:23 +0300 (Thu, 24 May 2018) $
#$Revision: 860 $
#$URL: svn://172.16.1.111/rod/cif/1/00/03/1000345.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000345
loop_
_publ_author_name
'Xu, K.'
'Xue, J.'
'Ding, Y.'
'Lu, G.'
_publ_section_title
;
 Discovery of stolzite in China and refinement of its crystal structure
;
_journal_name_full               'Acta Geologica Sinica'
_journal_page_first              111
_journal_page_last               116
_journal_paper_doi               10.1111/j.1755-6724.1995.mp8001009.x
_journal_volume                  8
_journal_year                    1995
_chemical_compound_source        'Yaogangxian, Hunan Province, China'
_chemical_formula_sum            'O4 Pb W'
_chemical_name_mineral           Stolzite
_space_group_IT_number           88
_symmetry_space_group_name_Hall  'I 4bw -1bw'
_symmetry_space_group_name_H-M   'I 41/a :1'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   5.44505
_cell_length_b                   5.44503
_cell_length_c                   12.0495
_cell_volume                     357.249
_exptl_crystal_density_diffrn    8.460
_cod_original_sg_symbol_H-M      'I 41/a'
_cod_original_formula_sum        'Pb W O4'
_cod_database_code               9014025
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R130615.rod
_rod_data_source.block           3500000
_rod_database.code               1000345
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9014025 COD http://www.crystallography.net/cod/9014025.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
200.2485 0.0000000E+00
200.7306 0.1940460
201.2127 0.1440350
201.6948 0.2426760
202.1769 0.6802900
202.6591 1.139763
203.1412 1.115555
203.6233 0.7046660
204.1054 0.4508510
204.5875 0.4611660
205.0696 0.6849290
205.5518 1.121109
206.0339 1.929291
206.5160 2.528610
206.9981 2.666367
207.4802 2.615211
207.9623 2.722038
208.4445 2.694389
208.9266 2.600105
209.4087 2.511292
209.8908 2.446724
210.3729 2.416519
210.8550 2.245949
211.3372 1.770714
211.8193 1.565163
212.3014 1.893875
212.7835 2.754448
213.2656 3.008957
213.7477 2.452141
214.2298 1.589928
214.7120 1.033356
215.1941 0.8936770
215.6762 1.130898
216.1583 1.598404
216.6404 2.270584
217.1225 2.768143
217.6047 2.809998
218.0868 2.843704
218.5689 3.076004
219.0510 3.115715
219.5331 3.206665
220.0152 3.091843
220.4974 2.747795
220.9795 2.726738
221.4616 3.099800
221.9437 3.531349
222.4258 3.651627
222.9079 3.326332
223.3901 3.069435
223.8722 3.103867
224.3543 3.453941
224.8364 3.634857
225.3185 3.738037
225.8006 3.726639
226.2828 3.579727
226.7649 3.321617
227.2470 2.996254
227.7291 2.602615
228.2112 2.184402
228.6933 1.795326
229.1755 1.394279
229.6576 0.9991840
230.1397 0.6383360
230.6218 0.2751850
231.1039 3.5705999E-02
231.5860 8.7130005E-03
232.0682 0.1926120
232.5503 0.2588200
233.0324 0.1082610
233.5145 0.1046300
233.9966 0.1544340
234.4787 0.1427380
234.9609 0.2686390
235.4430 7.8130001E-03
235.9251 0.7399670
236.4072 1.145111
236.8893 1.042252
237.3714 0.7363590
237.8536 0.6287460
238.3357 0.9083710
238.8178 1.046043
239.2999 0.8350370
239.7820 0.1993790
240.2641 0.1470030
240.7463 6.2362999E-02
241.2284 0.1955950
241.7105 0.3169940
242.1926 0.2569660
242.6747 0.1438830
243.1568 2.9594000E-02
243.6390 0.2935100
244.1211 0.3538510
244.6032 9.2133000E-02
245.0853 0.2657170
245.5674 0.4441910
246.0495 0.3210140
246.5317 0.2456590
247.0138 0.3375020
247.4959 0.6272890
247.9780 0.6887970
248.4601 0.3520430
248.9422 5.1628001E-02
249.4244 0.1269300
249.9065 0.3435060
250.3886 0.7002790
250.8707 0.7388760
251.3528 0.4377290
251.8349 0.3592450
252.3171 0.6442790
252.7992 1.002716
253.2813 1.139824
253.7634 1.000755
254.2455 0.7550810
254.7276 0.3569030
255.2098 0.2018050
255.6919 0.4084320
256.1740 8.8684000E-02
256.6561 0.3687590
257.1382 0.5923770
257.6204 0.5034640
258.1025 0.3429790
258.5846 0.2215190
259.0667 0.1320040
259.5488 0.1051180
260.0309 0.5920870
260.5131 1.068047
260.9952 1.256088
261.4773 1.013077
261.9594 0.8978120
262.4415 1.056839
262.9236 1.458031
263.4058 1.677963
263.8879 1.628769
264.3700 1.555359
264.8521 1.635445
265.3342 1.852325
265.8163 2.287109
266.2985 3.047081
266.7806 4.040779
267.2627 4.756187
267.7448 5.127899
268.2269 5.342033
268.7090 5.522293
269.1912 5.674004
269.6733 5.746498
270.1554 5.661095
270.6375 5.519760
271.1196 5.747536
271.6017 6.424660
272.0839 7.221909
272.5660 7.954315
273.0481 8.655815
273.5302 9.129623
274.0123 9.296631
274.4944 9.285263
274.9766 9.416763
275.4587 9.665703
275.9408 10.13315
276.4229 10.96514
276.9050 12.21099
277.3871 13.25448
277.8693 14.00256
278.3514 14.58366
278.8335 15.26620
279.3156 16.07018
279.7977 16.96863
280.2798 17.93142
280.7620 18.94783
281.2441 20.15094
281.7262 21.60232
282.2083 23.13922
282.6904 24.42259
283.1725 25.42813
283.6547 26.50645
284.1368 27.81223
284.6189 29.32859
285.1010 31.05252
285.5831 33.01859
286.0652 35.09349
286.5474 37.07675
287.0295 38.96541
287.5116 40.87896
287.9937 42.85653
288.4758 44.91571
288.9579 46.96861
289.4401 49.00403
289.9222 51.27095
290.4043 54.06848
290.8864 57.35716
291.3685 60.92762
291.8506 64.83054
292.3328 68.96355
292.8149 72.71570
293.2970 76.04736
293.7791 79.45352
294.2612 83.42060
294.7433 87.92963
295.2255 92.74774
295.7076 97.58398
296.1897 102.7297
296.6718 108.8283
297.1539 115.8523
297.6360 123.2483
298.1182 130.1383
298.6003 136.9241
299.0824 144.8231
299.5645 154.2526
300.0466 164.9107
300.5287 176.5584
301.0109 189.1046
301.4930 202.3868
301.9751 215.6645
302.4572 229.6341
302.9393 245.2046
303.4214 262.9200
303.9036 282.0390
304.3857 301.8400
304.8678 322.3246
305.3499 344.0060
305.8320 366.9509
306.3141 391.2332
306.7963 416.5268
307.2784 443.0754
307.7605 470.5804
308.2426 499.1001
308.7247 528.4783
309.2068 558.3289
309.6890 588.6362
310.1711 619.2396
310.6532 649.3602
311.1353 678.5344
311.6174 708.7253
312.0995 740.7826
312.5817 774.3341
313.0638 809.1940
313.5459 845.3779
314.0280 883.1266
314.5101 922.7128
314.9922 963.9916
315.4744 1006.999
315.9565 1050.688
316.4386 1096.312
316.9207 1144.697
317.4028 1198.279
317.8849 1253.216
318.3671 1308.225
318.8492 1363.710
319.3313 1418.764
319.8134 1474.867
320.2955 1529.814
320.7776 1581.203
321.2598 1631.834
321.7419 1675.931
322.2240 1714.111
322.7061 1745.412
323.1882 1764.954
323.6703 1773.495
324.1525 1768.807
324.6346 1749.693
325.1167 1715.687
325.5988 1667.808
326.0809 1604.003
326.5630 1526.216
327.0452 1439.399
327.5273 1336.830
328.0094 1232.334
328.4915 1129.642
328.9736 1028.130
329.4557 932.1841
329.9379 840.4925
330.4200 754.4340
330.9021 677.4846
331.3842 610.6060
331.8663 550.7267
332.3484 497.0422
332.8306 450.7201
333.3127 409.0096
333.7948 372.1584
334.2769 339.5818
334.7590 311.3360
335.2411 288.2768
335.7233 267.0799
336.2054 247.1551
336.6875 228.4386
337.1696 212.6170
337.6517 200.2857
338.1338 189.7571
338.6159 179.9197
339.0981 170.6885
339.5802 162.2002
340.0623 154.5420
340.5444 147.6315
341.0265 141.6709
341.5086 136.6407
341.9908 132.2749
342.4729 128.2636
342.9550 124.6106
343.4371 121.6750
343.9192 119.6287
344.4013 118.1229
344.8835 116.4552
345.3656 114.6288
345.8477 113.3250
346.3298 113.0770
346.8119 113.6912
347.2940 114.2554
347.7762 114.7016
348.2583 115.4794
348.7404 117.2762
349.2225 119.8961
349.7046 122.5736
350.1867 125.0310
350.6689 127.3834
351.1510 130.0201
351.6331 132.9244
352.1152 135.5373
352.5973 137.4097
353.0794 138.6199
353.5616 139.3861
354.0437 139.8744
354.5258 139.8033
355.0079 139.3394
355.4900 138.2498
355.9721 135.4810
356.4543 129.6393
356.9364 122.1199
357.4185 114.1307
357.9006 105.6515
358.3827 97.47754
358.8648 90.07114
359.3470 83.24544
359.8291 76.59710
360.3112 69.56511
360.7933 62.94958
361.2754 57.20670
361.7575 52.43854
362.2397 48.15984
362.7218 44.26907
363.2039 40.72633
363.6860 37.49552
364.1681 34.53796
364.6502 31.88190
365.1324 29.67000
365.6145 27.90089
366.0966 26.27663
366.5787 24.90109
367.0608 23.45226
367.5429 21.79182
368.0251 19.34096
368.5072 17.38586
368.9893 16.30280
369.4714 15.83017
369.9535 15.14099
370.4356 13.92572
370.9178 12.80182
371.3999 12.07127
371.8820 11.96632
372.3641 11.62791
372.8462 10.91650
373.3283 10.06800
373.8105 9.443909
374.2926 9.110252
374.7747 8.854614
375.2568 8.655319
375.7389 8.511879
376.2210 8.170303
376.7032 7.534348
377.1853 6.887550
377.6674 6.514771
378.1495 6.446327
378.6316 6.373672
379.1137 6.255775
379.5959 6.082985
380.0780 5.767601
380.5601 5.294548
381.0422 4.877411
381.5243 4.756065
382.0064 4.854019
382.4886 4.733047
382.9707 4.312843
383.4528 3.769203
383.9349 3.307304
384.4170 2.923851
384.8991 2.600227
385.3813 2.381325
385.8634 2.192963
386.3455 1.849815
386.8276 1.339378
387.3097 0.8881450
387.7918 0.7846070
388.2740 0.8569790
388.7561 0.7924500
389.2382 0.3096850
389.7203 0.1823040
390.2024 0.2380680
390.6845 4.4884000E-02
391.1667 0.2038350
391.6488 0.2163850
392.1309 0.7651600
392.6130 1.035141
393.0951 0.7991560
393.5772 0.5959010
394.0594 0.6750790
394.5415 0.9386290
395.0236 1.205338
395.5057 1.505547
395.9878 1.721260
396.4699 1.765617
396.9521 1.597023
397.4342 1.493080
397.9163 1.469284
398.3984 1.540833
398.8805 1.721741
399.3626 2.385544
399.8448 2.719711
400.3269 2.523399
400.8090 1.871567
401.2911 1.330833
401.7732 0.9582370
402.2553 0.6249850
402.7375 0.2364960
403.2196 0.3397900
403.7017 0.6217580
404.1838 0.5131150
404.6659 0.1771390
405.1480 0.1179200
405.6302 0.4168320
406.1123 0.5112530
406.5944 0.2242430
407.0765 0.4145200
407.5586 0.7170030
408.0407 0.6368790
408.5229 0.4029540
409.0050 0.1528700
409.4871 9.5367000E-02
409.9692 6.0081001E-02
410.4513 0.4590450
410.9334 1.145821
411.4156 1.289291
411.8977 0.9228130
412.3798 0.4797590
412.8619 0.1590880
413.3440 1.1848000E-02
413.8261 0.1089940
414.3083 0.6139070
414.7904 1.039467
415.2725 0.7661360
415.7546 8.5899003E-02
416.2367 0.4095150
416.7188 0.3876420
417.2010 0.1172490
417.6831 0.3322980
418.1652 0.9305190
418.6473 1.295067
419.1294 1.010460
419.6115 0.4978940
420.0937 0.1378630
420.5758 6.1127000E-02
421.0579 7.6468997E-02
421.5400 0.2362210
422.0221 0.4426120
422.5042 0.4540020
422.9864 0.2249910
423.4685 0.7167740
423.9506 0.5893400
424.4327 0.4734040
424.9148 1.163918
425.3969 1.220291
425.8791 1.009758
426.3612 0.8777620
426.8433 0.7617720
427.3254 0.8377760
427.8075 1.208466
428.2896 1.811768
428.7718 2.229637
429.2539 2.414101
429.7360 2.532906
430.2181 2.692268
430.7002 2.902687
431.1823 3.067764
431.6645 3.153076
432.1466 3.220924
432.6287 3.391121
433.1108 3.668999
433.5929 3.930023
434.0750 4.134674
434.5572 4.291962
435.0393 4.406509
435.5214 4.482193
436.0035 4.582130
436.4856 4.782639
436.9677 5.045097
437.4499 5.307312
437.9320 5.495613
438.4141 5.571075
438.8962 5.593285
439.3783 5.580643
439.8604 5.588745
440.3426 5.534874
440.8247 5.584633
441.3068 5.991211
441.7889 6.815117
442.2710 7.440430
442.7531 7.378731
443.2353 7.037521
443.7174 6.821037
444.1995 7.053696
444.6816 7.210381
445.1637 7.025192
445.6458 6.602859
446.1280 6.414246
446.6101 7.016296
447.0922 7.465683
447.5743 7.273430
448.0564 6.021690
448.5385 5.187958
449.0207 4.958527
449.5028 5.031113
449.9849 5.029289
450.4670 4.943100
450.9491 4.832756
451.4312 4.719948
451.9134 4.587303
452.3955 4.302460
452.8776 3.808289
453.3597 3.378242
453.8418 3.253044
454.3239 3.433990
454.8061 3.624855
455.2882 3.839333
455.7703 3.941841
456.2524 3.554970
456.7345 2.763535
457.2166 2.191223
457.6988 2.333771
458.1809 2.823875
458.6630 2.974480
459.1451 2.796799
459.6272 2.588013
460.1093 2.548897
460.5915 2.654564
461.0736 2.903267
461.5557 3.383530
462.0378 3.752892
462.5199 3.647003
463.0020 3.268517
463.4842 3.036049
463.9663 3.258682
464.4484 3.590279
464.9305 3.958778
465.4126 4.355988
465.8947 4.472672
466.3769 4.031204
466.8590 3.409096
467.3411 2.876030
467.8232 2.330513
468.3053 2.037621
468.7874 2.114105
469.2696 2.421898
469.7517 2.630669
470.2338 2.712608
470.7159 2.700371
471.1980 2.603539
471.6801 2.449982
472.1623 2.278137
472.6444 2.042747
473.1265 1.861511
473.6086 1.910011
474.0907 2.179588
474.5728 2.299835
475.0550 2.174789
475.5371 1.938896
476.0192 1.836365
476.5013 1.839851
476.9834 1.844032
477.4655 1.653206
477.9477 1.396584
478.4298 1.446526
478.9119 1.845581
479.3940 2.185555
479.8761 2.043716
480.3582 1.670105
480.8404 1.372940
481.3225 1.307983
481.8046 1.308922
482.2867 1.376930
482.7688 1.450371
483.2509 1.442062
483.7331 1.242531
484.2152 1.026772
484.6973 0.8330460
485.1794 0.6334460
485.6615 0.6882320
486.1436 1.415092
486.6258 2.122673
487.1079 2.265800
487.5900 1.337761
488.0721 0.7804180
488.5542 0.8186110
489.0363 1.268967
489.5185 1.655403
490.0006 1.995651
490.4827 2.176064
490.9648 2.127205
491.4469 1.860809
491.9290 1.487839
492.4112 0.9782030
492.8933 0.5188830
493.3754 0.2705610
493.8575 0.2294010
494.3396 0.1807250
494.8217 0.3826520
495.3039 8.7592997E-02
495.7860 4.248192
496.2681 11.37020
496.7502 16.96955
497.2323 18.27980
497.7144 17.34538
498.1966 15.83662
498.6787 13.84341
499.1608 11.47158
499.6429 7.834435
500.1250 4.319801
500.6071 2.103859
501.0893 2.408188
501.5714 2.749062
502.0535 2.517395
502.5356 1.950172
503.0177 1.590744
503.4998 1.696060
503.9820 1.768631
504.4641 1.636940
504.9462 1.286285
505.4283 1.187393
505.9104 1.502151
506.3925 1.823662
506.8747 1.776955
507.3568 1.273239
507.8389 1.044518
508.3210 1.242477
508.8031 1.611908
509.2852 1.659462
509.7674 1.397141
510.2495 1.172821
510.7316 1.140594
511.2137 1.239151
511.6958 1.403732
512.1780 1.618561
512.6601 1.708611
513.1422 1.389671
513.6243 0.9305420
514.1064 0.7117610
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