#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 16:00:39 +0300 (Thu, 24 May 2018) $
#$Revision: 864 $
#$URL: svn://172.16.1.111/rod/cif/1/00/03/1000348.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000348
loop_
_publ_author_name
'Keller, P.'
'Lissner, F.'
'Schleid, T.'
_publ_section_title
;
 The crystal structure of arsendescloizite, PbZn(OH)[AsO4], from Tsumeb
 (Namibia) Locality: Tsumeb, Namibia
;
_journal_name_full               'Neues Jahrbuch fur Mineralogie, Monatshefte'
_journal_page_first              374
_journal_page_last               384
_journal_volume                  2003
_journal_year                    2003
_chemical_compound_source        R140430
_chemical_formula_sum            'As H O5 Pb Zn'
_chemical_name_mineral           Arsendescloizite
_space_group_IT_number           19
_symmetry_space_group_name_Hall  'P 2ac 2ab'
_symmetry_space_group_name_H-M   'P 21 21 21'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   7.646
_cell_length_b                   9.363
_cell_length_c                   6.077
_cell_volume                     435.049
_exptl_crystal_density_diffrn    6.542
_cod_original_formula_sum        'Pb Zn As O5 H'
_cod_database_code               9009424
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R140430.rod
_rod_data_source.block           3500000
_rod_database.code               1000348
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9009424 COD http://www.crystallography.net/cod/9009424.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
89.78320 0.0000000E+00
90.26532 10.20538
90.74744 1.094696
91.22955 1.760559
91.71167 11.10556
92.19379 18.58954
92.67590 24.43604
93.15802 29.32996
93.64014 32.80170
94.12225 35.52347
94.60437 39.42029
95.08649 45.59033
95.56860 52.57306
96.05072 57.12512
96.53284 59.40710
97.01495 62.22577
97.49707 68.06476
97.97919 76.80847
98.46130 87.30444
98.94342 98.84021
99.42554 111.5269
99.90765 127.2766
100.3898 146.2667
100.8719 167.7870
101.3540 191.3710
101.8361 217.7836
102.3182 243.8848
102.8004 269.0749
103.2825 293.4194
103.7646 316.4257
104.2467 339.4055
104.7288 360.5960
105.2109 375.3917
105.6931 382.5520
106.1752 386.2600
106.6573 388.3138
107.1394 388.5355
107.6215 387.5983
108.1036 385.2816
108.5858 381.8332
109.0679 378.3438
109.5500 373.5239
110.0321 369.5855
110.5142 367.7244
110.9963 368.3715
111.4785 370.4918
111.9606 374.8696
112.4427 381.3741
112.9248 386.5093
113.4069 387.5208
113.8890 388.1229
114.3712 391.3098
114.8533 398.2443
115.3354 407.2394
115.8175 418.3738
116.2996 431.9637
116.7817 445.1602
117.2639 459.2673
117.7460 472.0137
118.2281 480.4984
118.7102 484.6485
119.1923 483.6308
119.6744 476.3708
120.1566 462.3325
120.6387 444.7419
121.1208 424.0568
121.6029 401.4261
122.0850 379.4417
122.5671 357.4407
123.0493 334.9089
123.5314 313.2777
124.0135 293.0015
124.4956 273.1206
124.9777 253.2248
125.4598 233.3467
125.9420 213.3505
126.4241 192.3336
126.9062 171.1985
127.3883 151.5736
127.8704 133.7615
128.3525 117.6363
128.8347 102.9551
129.3168 89.67572
129.7989 78.16309
130.2810 69.06592
130.7631 62.06073
131.2452 55.44666
131.7274 48.80573
132.2095 42.29410
132.6916 36.26352
133.1737 30.65436
133.6558 25.69119
134.1379 21.55646
134.6201 18.24524
135.1022 15.20459
135.5843 12.25256
136.0664 9.434845
136.5485 7.216675
137.0306 5.583496
137.5128 4.660034
137.9949 4.588531
138.4770 5.241211
138.9591 5.961853
139.4412 6.683899
139.9233 7.454834
140.4055 7.364594
140.8876 6.111328
141.3697 4.344818
141.8518 3.037292
142.3339 2.151886
142.8160 1.806152
143.2982 2.161957
143.7803 3.532684
144.2624 4.575531
144.7445 5.043793
145.2266 5.255829
145.7087 6.017517
146.1909 7.917206
146.6730 9.622620
147.1551 10.66171
147.6372 10.89099
148.1193 10.01987
148.6014 7.489197
149.0836 4.046082
149.5657 1.260773
150.0478 0.5303340
150.5299 1.877502
151.0120 3.031952
151.4941 3.698486
151.9763 4.516327
152.4584 5.566315
152.9405 6.815247
153.4226 8.105225
153.9047 10.45618
154.3868 12.18625
154.8690 12.38086
155.3511 9.094269
155.8332 6.236877
156.3153 4.539063
156.7974 3.896179
157.2795 3.413147
157.7617 3.139740
158.2438 2.822937
158.7259 2.278748
159.2080 1.117706
159.6901 4.5563001E-02
160.1722 0.5473330
160.6544 0.7023010
161.1365 1.229187
161.6186 3.240021
162.1007 5.409668
162.5828 6.541992
163.0649 5.051239
163.5471 3.419495
164.0292 2.747070
164.5113 3.071045
164.9934 3.813629
165.4755 4.871887
165.9576 6.132507
166.4398 7.449982
166.9219 9.019196
167.4040 10.45245
167.8861 11.24036
168.3682 11.30487
168.8503 11.76807
169.3325 13.63022
169.8146 16.34726
170.2967 19.01620
170.7788 21.24759
171.2609 23.28421
171.7430 25.25562
172.2252 27.15796
172.7073 29.20004
173.1894 31.90808
173.6715 34.92294
174.1536 37.37631
174.6357 38.56323
175.1179 39.12012
175.6000 39.87650
176.0821 40.96423
176.5642 41.87610
177.0463 42.32977
177.5284 42.24573
178.0106 41.39307
178.4927 39.39127
178.9748 36.59879
179.4569 33.60275
179.9390 30.38986
180.4211 27.16022
180.9033 24.00101
181.3854 20.94461
181.8675 18.20578
182.3496 15.73492
182.8317 13.65894
183.3138 12.21097
183.7960 11.60876
184.2781 11.37927
184.7602 10.54605
185.2423 9.179230
185.7244 8.386383
186.2065 9.301056
186.6887 11.55246
187.1708 13.56683
187.6529 15.07327
188.1350 16.41913
188.6171 18.14233
189.0992 20.25146
189.5814 22.72617
190.0635 25.58228
190.5456 28.78107
191.0277 32.18378
191.5098 35.92798
191.9919 39.59048
192.4741 42.00613
192.9562 43.12988
193.4383 44.46393
193.9204 47.15710
194.4025 51.11429
194.8846 54.89090
195.3668 58.18631
195.8489 61.32928
196.3310 65.29315
196.8131 70.20572
197.2952 75.14362
197.7773 79.20908
198.2595 82.30280
198.7416 86.14594
199.2237 91.03412
199.7058 96.65317
200.1879 102.0245
200.6700 107.0732
201.1522 112.7215
201.6343 119.8362
202.1164 128.5677
202.5985 136.8752
203.0806 144.2737
203.5627 151.1745
204.0449 158.7603
204.5270 167.0783
205.0091 175.7699
205.4912 184.5576
205.9733 193.3912
206.4554 203.0981
206.9376 213.7942
207.4197 225.2972
207.9018 237.7848
208.3839 251.8304
208.8660 265.4819
209.3481 277.2142
209.8303 286.8210
210.3124 295.8617
210.7945 305.0835
211.2766 313.7231
211.7587 318.9334
212.2408 320.5089
212.7230 319.2984
213.2051 315.7539
213.6872 309.3912
214.1693 302.0899
214.6514 294.0862
215.1335 285.2068
215.6157 274.8514
216.0978 262.1466
216.5799 249.3974
217.0620 238.0765
217.5441 228.5966
218.0262 219.1497
218.5084 209.2460
218.9905 199.0941
219.4726 190.2663
219.9547 182.9009
220.4368 176.3902
220.9189 170.5422
221.4011 165.6096
221.8832 160.5327
222.3653 154.9433
222.8474 149.1442
223.3295 144.2948
223.8116 140.8591
224.2938 137.8062
224.7759 134.5630
225.2580 131.1232
225.7401 127.5439
226.2222 123.7335
226.7043 119.7791
227.1865 115.8869
227.6686 112.1526
228.1507 108.4365
228.6328 104.7552
229.1149 101.3316
229.5970 97.39899
230.0792 92.67340
230.5613 87.40967
231.0434 82.76160
231.5255 78.98752
232.0076 75.53934
232.4897 72.25607
232.9719 69.46335
233.4540 66.11334
233.9361 61.95810
234.4182 57.22107
234.9003 52.57877
235.3824 47.88831
235.8646 43.49539
236.3467 39.59189
236.8288 36.33847
237.3109 33.21042
237.7930 30.22812
238.2751 27.33749
238.7573 24.40918
239.2394 21.13843
239.7215 18.24924
240.2036 16.20151
240.6857 15.83298
241.1678 14.23758
241.6500 10.53040
242.1321 5.850372
242.6142 3.206116
243.0963 3.913116
243.5784 4.698517
244.0605 4.164246
244.5427 1.695007
245.0248 0.4148250
245.5069 2.044739
245.9890 3.385864
246.4711 4.863678
246.9532 6.691254
247.4354 8.307892
247.9175 9.489777
248.3996 10.17505
248.8817 10.60043
249.3638 10.60181
249.8459 10.43933
250.3281 10.62509
250.8102 11.36676
251.2923 12.08246
251.7744 12.57269
252.2565 12.80557
252.7386 12.93188
253.2208 12.85056
253.7029 12.73572
254.1850 12.91888
254.6671 13.73395
255.1492 14.19849
255.6313 13.97537
256.1135 12.99191
256.5956 11.83475
257.0777 10.31335
257.5598 8.841156
258.0419 8.062225
258.5240 8.348145
259.0062 8.541412
259.4883 8.287720
259.9704 7.579834
260.4525 6.950104
260.9346 6.504486
261.4167 6.028473
261.8989 5.162323
262.3810 3.601318
262.8631 2.521484
263.3452 2.422791
263.8273 3.273468
264.3094 3.395660
264.7916 2.582489
265.2737 1.331055
265.7558 3.6773998E-02
266.2379 1.322235
266.7200 2.628418
267.2021 3.940826
267.6843 5.218384
268.1664 6.034302
268.6485 6.089508
269.1306 6.287964
269.6127 7.430359
270.0948 9.667419
270.5770 12.09845
271.0591 14.53702
271.5412 17.01190
272.0233 19.82092
272.5054 22.92502
272.9875 26.27527
273.4697 29.83466
273.9518 33.66495
274.4339 37.52090
274.9160 41.22470
275.3981 45.00220
275.8802 49.79303
276.3624 55.68475
276.8445 61.91318
277.3266 67.75836
277.8087 73.12250
278.2908 79.72412
278.7729 87.92520
279.2551 97.17590
279.7372 105.8947
280.2193 113.9819
280.7014 122.4559
281.1835 131.9019
281.6656 142.3176
282.1478 153.4757
282.6299 165.3719
283.1120 178.0014
283.5941 191.2623
284.0762 205.2055
284.5583 220.0918
285.0405 236.4711
285.5226 254.1956
286.0047 271.6803
286.4868 288.6832
286.9689 306.2271
287.4510 325.5924
287.9332 346.7593
288.4153 369.5403
288.8974 393.4604
289.3795 418.6646
289.8616 444.7453
290.3438 471.5949
290.8259 500.0511
291.3080 531.9803
291.7901 566.5892
292.2722 601.1229
292.7543 634.3361
293.2365 666.6603
293.7186 699.5732
294.2007 732.8199
294.6828 764.0433
295.1649 791.3141
295.6470 814.6354
296.1292 835.1909
296.6113 853.7516
297.0934 868.7725
297.5755 878.2976
298.0576 882.3613
298.5397 881.0225
299.0219 872.1246
299.5040 857.8919
299.9861 843.1049
300.4682 828.5061
300.9503 814.4717
301.4324 800.5142
301.9146 787.0109
302.3967 775.1647
302.8788 765.6880
303.3609 758.5317
303.8430 753.6530
304.3251 750.9384
304.8073 750.8053
305.2894 752.9827
305.7715 758.0123
306.2536 767.3450
306.7357 782.6783
307.2178 802.1548
307.7000 823.4767
308.1821 846.3051
308.6642 872.1960
309.1463 902.9845
309.6284 937.3386
310.1105 973.7281
310.5927 1009.813
311.0748 1048.342
311.5569 1091.811
312.0390 1140.284
312.5211 1191.891
313.0032 1247.266
313.4854 1305.335
313.9675 1364.207
314.4496 1425.220
314.9317 1485.015
315.4138 1542.339
315.8959 1597.208
316.3781 1651.650
316.8602 1710.229
317.3423 1766.109
317.8244 1814.218
318.3065 1853.193
318.7886 1884.584
319.2708 1908.341
319.7529 1924.601
320.2350 1933.755
320.7171 1935.886
321.1992 1930.651
321.6813 1917.540
322.1635 1895.508
322.6456 1867.922
323.1277 1833.709
323.6098 1794.533
324.0919 1753.036
324.5740 1708.547
325.0562 1663.259
325.5383 1617.538
326.0204 1571.018
326.5025 1525.750
326.9846 1480.605
327.4667 1437.447
327.9489 1397.693
328.4310 1361.876
328.9131 1328.833
329.3952 1298.021
329.8773 1269.425
330.3594 1244.161
330.8416 1222.576
331.3237 1204.289
331.8058 1189.273
332.2879 1178.829
332.7700 1169.348
333.2521 1160.189
333.7343 1151.598
334.2164 1145.062
334.6985 1141.988
335.1806 1138.834
335.6627 1133.854
336.1448 1127.074
336.6270 1118.406
337.1091 1107.692
337.5912 1095.307
338.0733 1081.588
338.5554 1066.339
339.0375 1050.853
339.5197 1035.766
340.0018 1021.285
340.4839 1005.625
340.9660 988.8140
341.4481 971.3867
341.9302 954.4886
342.4124 938.0321
342.8945 921.2704
343.3766 903.4890
343.8587 885.1960
344.3408 868.0900
344.8229 852.3754
345.3051 837.0031
345.7872 821.6970
346.2693 806.2716
346.7514 788.7094
347.2335 768.4279
347.7156 746.2780
348.1978 724.5753
348.6799 703.1984
349.1620 680.5068
349.6441 655.3545
350.1262 628.0919
350.6083 599.5609
351.0905 569.5443
351.5726 538.3960
352.0547 505.5573
352.5368 471.6361
353.0189 438.4922
353.5010 407.5101
353.9832 377.5920
354.4653 347.3292
354.9474 316.3535
355.4295 286.0819
355.9116 256.7361
356.3937 228.7834
356.8759 203.3320
357.3580 180.9620
357.8401 160.7583
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358.8043 125.6727
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359.7686 96.35156
360.2507 83.55304
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365.5540 28.15778
366.0361 28.73004
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367.0003 33.33759
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367.9645 45.77203
368.4467 54.74072
368.9288 65.46680
369.4109 76.94513
369.8930 88.82849
370.3751 101.7365
370.8572 116.0342
371.3394 130.5718
371.8215 148.3011
372.3036 170.2174
372.7857 195.4118
373.2678 220.9224
373.7499 246.5259
374.2321 273.1898
374.7142 300.9382
375.1963 329.6969
375.6784 360.5258
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377.6069 497.8604
378.0890 534.0037
378.5711 571.4861
379.0532 610.9034
379.5353 653.8608
380.0175 700.6849
380.4996 751.4286
380.9817 805.7964
381.4638 863.7432
381.9459 927.3774
382.4280 996.2437
382.9102 1071.354
383.3923 1152.735
383.8744 1241.074
384.3565 1336.668
384.8386 1438.991
385.3207 1548.555
385.8029 1663.853
386.2850 1786.310
386.7671 1911.963
387.2492 2041.535
387.7313 2172.266
388.2134 2295.353
388.6956 2416.153
389.1777 2519.992
389.6598 2599.658
390.1419 2653.656
390.6240 2669.832
391.1061 2637.780
391.5883 2565.522
392.0704 2460.226
392.5525 2311.600
393.0346 2147.708
393.5167 1968.039
393.9988 1779.859
394.4810 1601.476
394.9631 1436.448
395.4452 1284.880
395.9273 1146.905
396.4094 1022.721
396.8915 911.4448
397.3737 814.8050
397.8558 730.3561
398.3379 655.1002
398.8200 591.7727
399.3021 534.5566
399.7842 482.6692
400.2664 436.0999
400.7485 393.7147
401.2306 356.5048
401.7127 322.9869
402.1948 292.4797
402.6769 265.2880
403.1591 240.5845
403.6412 218.5518
404.1233 198.8838
404.6054 180.0876
405.0875 162.0845
405.5696 145.8215
406.0518 131.9371
406.5339 120.4789
407.0160 109.9158
407.4981 100.4352
407.9802 91.66263
408.4623 82.86557
408.9445 74.04254
409.4266 67.01538
409.9087 62.74445
410.3908 60.24701
410.8729 57.68237
411.3550 54.98706
411.8372 51.69647
412.3193 46.64948
412.8014 40.77313
413.2835 36.23779
413.7656 33.38971
414.2477 31.44220
414.7299 29.92484
415.2120 28.68411
415.6941 27.46909
416.1762 26.18481
416.6583 24.78027
417.1404 23.37659
417.6226 21.90851
418.1047 19.83640
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