#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-05-24 16:00:43 +0300 (Thu, 24 May 2018) $ #$Revision: 865 $ #$URL: svn://172.16.1.111/rod/cif/1/00/03/1000349.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_1000349 loop_ _publ_author_name 'Balassone, G.' 'Franco, E.' 'Mattia, C. A.' 'Puliti, R.' _publ_section_title ; Indialite in xenolithic rocks from Somma-Vesuvius volcano (Southern Italy): Crystal chemistry and petrogenetic features ; _journal_name_full 'American Mineralogist' _journal_page_first 1 _journal_page_last 6 _journal_volume 89 _journal_year 2004 _chemical_compound_source R140777 _chemical_formula_sum 'Al4.251 Ca0.084 Fe0.06 K0.336 Mg1.94 O18 Si4.749' _chemical_name_mineral Indialite _space_group_IT_number 192 _symmetry_space_group_name_Hall '-P 6 2c' _symmetry_space_group_name_H-M 'P 6/m c c' _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_length_a 9.775 _cell_length_b 9.775 _cell_length_c 9.354 _cell_volume 774.037 _exptl_crystal_density_diffrn 2.588 _cod_original_formula_sum '(Al4.251 Si4.749) (Mg1.94 Fe.06) O18 K.336 Ca.084' _cod_database_code 9003098 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type other _raman_measurement_device.excitation_laser_wavelength 532 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 15 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R140777.rod _rod_data_source.block 3500000 _rod_database.code 1000349 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9003098 COD http://www.crystallography.net/cod/9003098.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 89.78320 0.0000000E+00 90.26532 1.7090000E-03 90.74744 4.309082 91.22955 15.96411 91.71167 28.81775 92.19379 37.26520 92.67590 39.31348 93.15802 37.37646 93.64014 34.88397 94.12225 32.91510 94.60437 27.00851 95.08649 26.52261 95.56860 29.26514 96.05072 25.75403 96.53284 15.92539 97.01495 5.498322 97.49707 0.6492000 97.97919 2.717560 98.46130 2.253784 98.94342 1.066315 99.42554 6.935577 99.90765 11.23962 100.3898 13.93964 100.8719 15.45157 101.3540 16.04178 101.8361 15.31082 102.3182 15.14871 102.8004 16.36462 103.2825 19.24075 103.7646 21.93643 104.2467 23.43872 104.7288 25.19040 105.2109 30.78394 105.6931 41.59326 106.1752 54.03281 106.6573 66.96875 107.1394 82.70483 107.6215 95.15359 108.1036 104.2384 108.5858 110.1353 109.0679 113.1202 109.5500 110.4769 110.0321 107.0454 110.5142 105.4135 110.9963 104.9306 111.4785 106.8442 111.9606 111.5089 112.4427 118.8398 112.9248 127.6468 113.4069 137.4984 113.8890 148.7845 114.3712 161.9530 114.8533 177.6967 115.3354 194.6420 115.8175 212.7968 116.2996 232.5488 116.7817 251.5943 117.2639 271.6503 117.7460 290.1771 118.2281 303.9284 118.7102 313.2241 119.1923 316.5050 119.6744 311.9330 120.1566 298.5247 120.6387 281.0615 121.1208 258.9294 121.6029 234.8158 122.0850 214.4005 122.5671 201.2383 123.0493 192.8346 123.5314 187.6711 124.0135 187.0341 124.4956 185.6730 124.9777 177.6647 125.4598 164.2637 125.9420 150.3467 126.4241 138.7153 126.9062 128.7519 127.3883 119.2480 127.8704 109.6666 128.3525 100.9111 128.8347 94.83142 129.3168 91.33936 129.7989 87.98730 130.2810 82.06064 130.7631 74.41458 131.2452 68.42441 131.7274 65.53656 132.2095 64.57721 132.6916 62.24646 133.1737 58.34940 133.6558 54.34055 134.1379 51.73010 134.6201 50.49908 135.1022 49.10004 135.5843 46.77927 136.0664 43.78973 136.5485 42.22031 137.0306 42.27502 137.5128 43.27072 137.9949 44.21735 138.4770 44.89822 138.9591 46.73068 139.4412 51.27988 139.9233 59.01938 140.4055 61.95850 140.8876 58.59250 141.3697 51.91623 141.8518 46.69360 142.3339 43.22784 142.8160 40.55038 143.2982 38.40894 143.7803 36.97943 144.2624 35.55591 144.7445 33.97818 145.2266 32.46329 145.7087 31.56110 146.1909 31.33755 146.6730 31.62958 147.1551 32.49799 147.6372 35.19379 148.1193 36.58420 148.6014 35.90210 149.0836 33.81888 149.5657 32.62335 150.0478 32.40805 150.5299 33.02734 151.0120 34.44125 151.4941 37.63309 151.9763 40.44739 152.4584 42.35480 152.9405 43.66412 153.4226 45.95078 153.9047 49.71048 154.3868 54.17371 154.8690 58.86383 155.3511 66.30872 155.8332 71.07593 156.3153 71.98892 156.7974 69.44067 157.2795 65.50717 157.7617 59.66544 158.2438 53.05237 158.7259 46.51120 159.2080 39.80084 159.6901 33.59778 160.1722 28.18790 160.6544 23.57422 161.1365 19.30453 161.6186 14.45038 162.1007 10.21597 162.5828 7.585602 163.0649 8.854584 163.5471 10.20685 164.0292 9.707733 164.5113 7.284790 164.9934 4.695435 165.4755 2.347443 165.9576 0.4376220 166.4398 0.7647400 166.9219 0.6281130 167.4040 0.1502080 167.8861 7.1319997E-02 168.3682 0.4596860 168.8503 0.6428830 169.3325 0.2033390 169.8146 0.7351680 170.2967 1.960815 170.7788 3.918213 171.2609 5.842834 171.7430 6.987946 172.2252 7.278473 172.7073 7.162567 173.1894 6.754089 173.6715 6.189178 174.1536 5.786163 174.6357 5.584229 175.1179 5.663147 175.6000 6.191315 176.0821 7.225555 176.5642 8.438263 177.0463 9.587952 177.5284 10.67456 178.0106 11.68008 178.4927 12.77014 178.9748 13.74219 179.4569 14.12759 179.9390 13.78088 180.4211 13.26740 180.9033 13.19165 181.3854 13.51691 181.8675 14.05219 182.3496 14.98407 182.8317 16.03485 183.3138 16.62549 183.7960 16.71881 184.2781 16.25342 184.7602 14.58356 185.2423 11.89581 185.7244 9.901764 186.2065 10.19763 186.6887 12.14383 187.1708 13.34314 187.6529 13.47931 188.1350 12.89145 188.6171 11.80560 189.0992 10.23529 189.5814 9.104767 190.0635 9.306641 190.5456 10.62790 191.0277 11.60098 191.5098 12.07111 191.9919 12.12173 192.4741 11.69495 192.9562 10.76010 193.4383 10.05472 193.9204 10.28198 194.4025 11.37335 194.8846 12.18930 195.3668 12.64545 195.8489 12.69803 196.3310 12.01059 196.8131 10.46307 197.2952 9.081787 197.7773 8.844543 198.2595 9.803467 198.7416 9.926453 199.2237 8.705444 199.7058 6.727936 200.1879 5.581268 200.6700 5.316467 201.1522 5.627045 201.6343 6.504974 202.1164 8.039612 202.5985 9.267151 203.0806 10.06024 203.5627 10.47009 204.0449 10.59824 204.5270 10.39133 205.0091 10.06403 205.4912 9.847076 205.9733 9.831757 206.4554 9.348724 206.9376 8.264191 207.4197 6.675568 207.9018 4.792847 208.3839 2.440430 208.8660 0.2416080 209.3481 1.296265 209.8303 2.045441 210.3124 2.743317 210.7945 3.524658 211.2766 4.294250 211.7587 4.669800 212.2408 4.542755 212.7230 4.242279 213.2051 4.037537 213.6872 4.067352 214.1693 3.672913 214.6514 2.609314 215.1335 1.094116 215.6157 0.1774900 216.0978 7.6720998E-02 216.5799 0.1766050 217.0620 5.3344999E-02 217.5441 0.4378660 218.0262 0.7031250 218.5084 0.5526120 218.9905 0.1078800 219.4726 2.9022001E-02 219.9547 0.1867070 220.4368 0.6451420 220.9189 1.339813 221.4011 2.485016 221.8832 3.323792 222.3653 3.648682 222.8474 3.623047 223.3295 4.051758 223.8116 5.203461 224.2938 6.370941 224.7759 7.134155 225.2580 7.295990 225.7401 7.518250 226.2222 7.837677 226.7043 8.239410 227.1865 8.667664 227.6686 8.996063 228.1507 9.505035 228.6328 10.42328 229.1149 12.06067 229.5970 13.31174 230.0792 13.79742 230.5613 13.85263 231.0434 14.79010 231.5255 16.84656 232.0076 19.42737 232.4897 22.31296 232.9719 25.93146 233.4540 28.88202 233.9361 30.93427 234.4182 32.31488 234.9003 33.84619 235.3824 35.66089 235.8646 37.43839 236.3467 38.91742 236.8288 39.56827 237.3109 41.13684 237.7930 44.04880 238.2751 47.84332 238.7573 51.09076 239.2394 53.82391 239.7215 55.93759 240.2036 57.20224 240.6857 56.67249 241.1678 57.48709 241.6500 60.26727 242.1321 64.20267 242.6142 67.26889 243.0963 69.02725 243.5784 70.52985 244.0605 72.12701 244.5427 73.66931 245.0248 75.74359 245.5069 78.54791 245.9890 81.82455 246.4711 84.91492 246.9532 87.56448 247.4354 90.50854 247.9175 93.98145 248.3996 98.02625 248.8817 102.5716 249.3638 107.7968 249.8459 113.4357 250.3281 118.9408 250.8102 124.0248 251.2923 129.5189 251.7744 135.8680 252.2565 143.2539 252.7386 150.5483 253.2208 157.9505 253.7029 165.1122 254.1850 171.4590 254.6671 176.3181 255.1492 181.6956 255.6313 188.3375 256.1135 196.4636 256.5956 204.2534 257.0777 211.9695 257.5598 219.0724 258.0419 225.3019 258.5240 232.1351 259.0062 234.4329 259.4883 230.5737 259.9704 220.4911 260.4525 206.5699 260.9346 187.7438 261.4167 166.4841 261.8989 145.0811 262.3810 122.8216 262.8631 103.0257 263.3452 86.96179 263.8273 74.43768 264.3094 62.83008 264.7916 51.69736 265.2737 41.90732 265.7558 34.29773 266.2379 29.31543 266.7200 25.26312 267.2021 21.93546 267.6843 19.28647 268.1664 16.33881 268.6485 12.83298 269.1306 9.534607 269.6127 7.294525 270.0948 6.420441 270.5770 5.338623 271.0591 3.564392 271.5412 1.373901 272.0233 0.3472290 272.5054 0.8708190 272.9875 1.690399 273.4697 1.795654 273.9518 1.006683 274.4339 0.3357240 274.9160 0.1553650 275.3981 0.3906860 275.8802 7.3334001E-02 276.3624 0.9236450 276.8445 1.960022 277.3266 2.491974 277.8087 2.467804 278.2908 3.094696 278.7729 4.576782 279.2551 6.619415 279.7372 8.695496 280.2193 10.89197 280.7014 12.59323 281.1835 13.16360 281.6656 12.62799 282.1478 12.88763 282.6299 14.24780 283.1120 15.96072 283.5941 16.60464 284.0762 16.12164 284.5583 15.80310 285.0405 16.46906 285.5226 17.96649 286.0047 18.63681 286.4868 18.20538 286.9689 17.84100 287.4510 19.38391 287.9332 22.74359 288.4153 26.11578 288.8974 28.61624 289.3795 30.52060 289.8616 32.84875 290.3438 35.65228 290.8259 38.53439 291.3080 41.31689 291.7901 43.89008 292.2722 45.75790 292.7543 46.73245 293.2365 46.88828 293.7186 45.90396 294.2007 43.76279 294.6828 42.01651 295.1649 42.69473 295.6470 45.02078 296.1292 46.43985 296.6113 46.13669 297.0934 44.75363 297.5755 42.91364 298.0576 40.68427 298.5397 38.85638 299.0219 38.37363 299.5040 38.67429 299.9861 38.49332 300.4682 37.42252 300.9503 36.14966 301.4324 35.51791 301.9146 35.42157 302.3967 35.37610 302.8788 35.19171 303.3609 34.84451 303.8430 34.32437 304.3251 33.65262 304.8073 32.72028 305.2894 31.38556 305.7715 29.70178 306.2536 27.76373 306.7357 25.52600 307.2178 23.10587 307.7000 20.71051 308.1821 18.37628 308.6642 15.77408 309.1463 12.10922 309.6284 8.110016 310.1105 4.864594 310.5927 3.059296 311.0748 2.056519 311.5569 1.653351 312.0390 1.828522 312.5211 1.873840 313.0032 1.368866 313.4854 0.5406190 313.9675 0.3639220 314.4496 1.732727 314.9317 2.720245 315.4138 2.595001 315.8959 1.552246 316.3781 0.8393550 316.8602 1.502289 317.3423 2.410156 317.8244 2.730774 318.3065 2.051025 318.7886 1.096771 319.2708 6.7230001E-02 319.7529 1.059937 320.2350 2.351318 320.7171 4.221344 321.1992 5.945618 321.6813 7.059174 322.1635 7.053711 322.6456 7.433228 323.1277 8.819946 323.6098 10.71173 324.0919 12.27576 324.5740 12.61984 325.0562 13.28458 325.5383 14.97574 326.0204 18.16580 326.5025 20.57349 326.9846 21.54446 327.4667 21.87424 327.9489 22.42737 328.4310 24.16095 328.9131 25.07455 329.3952 24.71844 329.8773 23.07419 330.3594 21.22733 330.8416 18.98886 331.3237 16.73956 331.8058 14.72815 332.2879 12.79834 332.7700 11.39795 333.2521 10.91739 333.7343 11.06128 334.2164 10.11279 334.6985 7.164246 335.1806 4.413971 335.6627 3.240570 336.1448 4.347870 336.6270 4.978699 337.1091 4.893707 337.5912 4.479645 338.0733 4.461304 338.5554 4.804352 339.0375 5.438416 339.5197 6.656128 340.0018 8.561951 340.4839 9.219299 340.9660 8.257782 341.4481 6.978882 341.9302 7.019196 342.4124 8.360413 342.8945 9.450623 343.3766 9.965179 343.8587 10.03043 344.3408 10.04700 344.8229 9.973297 345.3051 10.03494 345.7872 10.40015 346.2693 11.04498 346.7514 12.12296 347.2335 13.93698 347.7156 15.85187 348.1978 16.45413 348.6799 15.85858 349.1620 15.22845 349.6441 15.28458 350.1262 15.79834 350.6083 16.35052 351.0905 16.95810 351.5726 17.46716 352.0547 17.67984 352.5368 17.64206 353.0189 17.48575 353.5010 16.71011 353.9832 16.12198 354.4653 17.04498 354.9474 19.59604 355.4295 22.05353 355.9116 23.00037 356.3937 23.01004 356.8759 22.92398 357.3580 22.79840 357.8401 22.87625 358.3222 23.46216 358.8043 24.48340 359.2864 25.43958 359.7686 25.68375 360.2507 25.95334 360.7328 26.89325 361.2149 28.88712 361.6970 31.16498 362.1791 33.50000 362.6613 35.88907 363.1434 38.32993 363.6255 41.40967 364.1076 44.06082 364.5897 45.66849 365.0718 45.81415 365.5540 46.00781 366.0361 47.37347 366.5182 48.63699 367.0003 48.27124 367.4824 45.09558 367.9645 41.32138 368.4467 36.98471 368.9288 32.11154 369.4109 28.20294 369.8930 25.77600 370.3751 23.93509 370.8572 22.08649 371.3394 20.16586 371.8215 18.36990 372.3036 16.64954 372.7857 15.02066 373.2678 13.54965 373.7499 12.23123 374.2321 11.17490 374.7142 10.36237 375.1963 9.751434 375.6784 9.509247 376.1605 9.851532 376.6426 10.43066 377.1248 10.71976 377.6069 10.69119 378.0890 10.27264 378.5711 9.227020 379.0532 7.705750 379.5353 6.990051 380.0175 7.197540 380.4996 7.579132 380.9817 7.322968 381.4638 6.524231 381.9459 6.003113 382.4280 6.013367 382.9102 6.269775 383.3923 6.208374 383.8744 5.853668 384.3565 5.476044 384.8386 5.234833 385.3207 5.092529 385.8029 4.954407 386.2850 4.793213 386.7671 4.728607 387.2492 5.167999 387.7313 5.811371 388.2134 5.959930 388.6956 4.871399 389.1777 3.430359 389.6598 2.421082 390.1419 1.846252 390.6240 1.375671 391.1061 0.6031490 391.5883 7.6141000E-02 392.0704 0.1926270 392.5525 1.014771 393.0346 1.922485 393.5167 1.610016 393.9988 0.4258730 394.4810 0.6778560 394.9631 1.691132 395.4452 2.301361 395.9273 2.231232 396.4094 1.173615 396.8915 0.3160400 397.3737 0.2080080 397.8558 0.3884580 398.3379 0.2035220 398.8200 1.478912 399.3021 2.349152 399.7842 1.375671 400.2664 1.430054 400.7485 2.675934 401.2306 1.304443 401.7127 0.6326290 402.1948 1.879791 402.6769 2.282532 403.1591 2.318146 403.6412 1.892365 404.1233 1.169983 404.6054 0.4639890 405.0875 0.3244020 405.5696 0.7708130 406.0518 0.5246580 406.5339 0.4440310 407.0160 0.8298950 407.4981 0.5498050 407.9802 0.1023560 408.4623 0.8294070 408.9445 1.642944 409.4266 2.560303 409.9087 3.615784 410.3908 4.765564 410.8729 5.886353 411.3550 6.990784 411.8372 8.108032 412.3193 9.560242 412.8014 11.03290 413.2835 11.60803 413.7656 10.95752 414.2477 10.25452 414.7299 10.87292 415.2120 12.42487 415.6941 13.95630 416.1762 14.57330 416.6583 15.26532 417.1404 17.22876 417.6226 20.43176 418.1047 23.26880 418.5868 24.35950 419.0689 24.86035 419.5510 25.93433 420.0331 28.42462 420.5153 30.79102 420.9974 32.25299 421.4795 33.12579 421.9616 34.12622 422.4437 35.49011 422.9258 37.01239 423.4080 38.86255 423.8901 41.52936 424.3722 42.89099 424.8543 41.58197 425.3364 39.49158 425.8185 38.49731 426.3007 39.74152 426.7828 40.43793 427.2649 40.26825 427.7470 39.25287 428.2291 37.34961 428.7112 34.03271 429.1934 30.74896 429.6755 28.19806 430.1576 26.43140 430.6397 25.32574 431.1218 25.18024 431.6039 25.18530 432.0861 23.72369 432.5682 20.65753 433.0503 18.27911 433.5324 17.63867 434.0145 18.23828 434.4966 18.30072 434.9788 17.81183 435.4609 17.32135 435.9430 17.34650 436.4251 17.74194 436.9072 18.11023 437.3893 18.41278 437.8715 18.62543 438.3536 18.56799 438.8357 18.36902 439.3178 18.39069 439.7999 18.72028 440.2820 19.41864 440.7642 20.82758 441.2463 22.97321 441.7284 24.57977 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