#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 16:00:43 +0300 (Thu, 24 May 2018) $
#$Revision: 865 $
#$URL: svn://172.16.1.111/rod/cif/1/00/03/1000349.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000349
loop_
_publ_author_name
'Balassone, G.'
'Franco, E.'
'Mattia, C. A.'
'Puliti, R.'
_publ_section_title
;
 Indialite in xenolithic rocks from Somma-Vesuvius volcano (Southern
 Italy): Crystal chemistry and petrogenetic features
;
_journal_name_full               'American Mineralogist'
_journal_page_first              1
_journal_page_last               6
_journal_volume                  89
_journal_year                    2004
_chemical_compound_source        R140777
_chemical_formula_sum
'Al4.251 Ca0.084 Fe0.06 K0.336 Mg1.94 O18 Si4.749'
_chemical_name_mineral           Indialite
_space_group_IT_number           192
_symmetry_space_group_name_Hall  '-P 6 2c'
_symmetry_space_group_name_H-M   'P 6/m c c'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_length_a                   9.775
_cell_length_b                   9.775
_cell_length_c                   9.354
_cell_volume                     774.037
_exptl_crystal_density_diffrn    2.588
_cod_original_formula_sum
'(Al4.251 Si4.749) (Mg1.94 Fe.06) O18 K.336 Ca.084'
_cod_database_code               9003098
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R140777.rod
_rod_data_source.block           3500000
_rod_database.code               1000349
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9003098 COD http://www.crystallography.net/cod/9003098.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
89.78320 0.0000000E+00
90.26532 1.7090000E-03
90.74744 4.309082
91.22955 15.96411
91.71167 28.81775
92.19379 37.26520
92.67590 39.31348
93.15802 37.37646
93.64014 34.88397
94.12225 32.91510
94.60437 27.00851
95.08649 26.52261
95.56860 29.26514
96.05072 25.75403
96.53284 15.92539
97.01495 5.498322
97.49707 0.6492000
97.97919 2.717560
98.46130 2.253784
98.94342 1.066315
99.42554 6.935577
99.90765 11.23962
100.3898 13.93964
100.8719 15.45157
101.3540 16.04178
101.8361 15.31082
102.3182 15.14871
102.8004 16.36462
103.2825 19.24075
103.7646 21.93643
104.2467 23.43872
104.7288 25.19040
105.2109 30.78394
105.6931 41.59326
106.1752 54.03281
106.6573 66.96875
107.1394 82.70483
107.6215 95.15359
108.1036 104.2384
108.5858 110.1353
109.0679 113.1202
109.5500 110.4769
110.0321 107.0454
110.5142 105.4135
110.9963 104.9306
111.4785 106.8442
111.9606 111.5089
112.4427 118.8398
112.9248 127.6468
113.4069 137.4984
113.8890 148.7845
114.3712 161.9530
114.8533 177.6967
115.3354 194.6420
115.8175 212.7968
116.2996 232.5488
116.7817 251.5943
117.2639 271.6503
117.7460 290.1771
118.2281 303.9284
118.7102 313.2241
119.1923 316.5050
119.6744 311.9330
120.1566 298.5247
120.6387 281.0615
121.1208 258.9294
121.6029 234.8158
122.0850 214.4005
122.5671 201.2383
123.0493 192.8346
123.5314 187.6711
124.0135 187.0341
124.4956 185.6730
124.9777 177.6647
125.4598 164.2637
125.9420 150.3467
126.4241 138.7153
126.9062 128.7519
127.3883 119.2480
127.8704 109.6666
128.3525 100.9111
128.8347 94.83142
129.3168 91.33936
129.7989 87.98730
130.2810 82.06064
130.7631 74.41458
131.2452 68.42441
131.7274 65.53656
132.2095 64.57721
132.6916 62.24646
133.1737 58.34940
133.6558 54.34055
134.1379 51.73010
134.6201 50.49908
135.1022 49.10004
135.5843 46.77927
136.0664 43.78973
136.5485 42.22031
137.0306 42.27502
137.5128 43.27072
137.9949 44.21735
138.4770 44.89822
138.9591 46.73068
139.4412 51.27988
139.9233 59.01938
140.4055 61.95850
140.8876 58.59250
141.3697 51.91623
141.8518 46.69360
142.3339 43.22784
142.8160 40.55038
143.2982 38.40894
143.7803 36.97943
144.2624 35.55591
144.7445 33.97818
145.2266 32.46329
145.7087 31.56110
146.1909 31.33755
146.6730 31.62958
147.1551 32.49799
147.6372 35.19379
148.1193 36.58420
148.6014 35.90210
149.0836 33.81888
149.5657 32.62335
150.0478 32.40805
150.5299 33.02734
151.0120 34.44125
151.4941 37.63309
151.9763 40.44739
152.4584 42.35480
152.9405 43.66412
153.4226 45.95078
153.9047 49.71048
154.3868 54.17371
154.8690 58.86383
155.3511 66.30872
155.8332 71.07593
156.3153 71.98892
156.7974 69.44067
157.2795 65.50717
157.7617 59.66544
158.2438 53.05237
158.7259 46.51120
159.2080 39.80084
159.6901 33.59778
160.1722 28.18790
160.6544 23.57422
161.1365 19.30453
161.6186 14.45038
162.1007 10.21597
162.5828 7.585602
163.0649 8.854584
163.5471 10.20685
164.0292 9.707733
164.5113 7.284790
164.9934 4.695435
165.4755 2.347443
165.9576 0.4376220
166.4398 0.7647400
166.9219 0.6281130
167.4040 0.1502080
167.8861 7.1319997E-02
168.3682 0.4596860
168.8503 0.6428830
169.3325 0.2033390
169.8146 0.7351680
170.2967 1.960815
170.7788 3.918213
171.2609 5.842834
171.7430 6.987946
172.2252 7.278473
172.7073 7.162567
173.1894 6.754089
173.6715 6.189178
174.1536 5.786163
174.6357 5.584229
175.1179 5.663147
175.6000 6.191315
176.0821 7.225555
176.5642 8.438263
177.0463 9.587952
177.5284 10.67456
178.0106 11.68008
178.4927 12.77014
178.9748 13.74219
179.4569 14.12759
179.9390 13.78088
180.4211 13.26740
180.9033 13.19165
181.3854 13.51691
181.8675 14.05219
182.3496 14.98407
182.8317 16.03485
183.3138 16.62549
183.7960 16.71881
184.2781 16.25342
184.7602 14.58356
185.2423 11.89581
185.7244 9.901764
186.2065 10.19763
186.6887 12.14383
187.1708 13.34314
187.6529 13.47931
188.1350 12.89145
188.6171 11.80560
189.0992 10.23529
189.5814 9.104767
190.0635 9.306641
190.5456 10.62790
191.0277 11.60098
191.5098 12.07111
191.9919 12.12173
192.4741 11.69495
192.9562 10.76010
193.4383 10.05472
193.9204 10.28198
194.4025 11.37335
194.8846 12.18930
195.3668 12.64545
195.8489 12.69803
196.3310 12.01059
196.8131 10.46307
197.2952 9.081787
197.7773 8.844543
198.2595 9.803467
198.7416 9.926453
199.2237 8.705444
199.7058 6.727936
200.1879 5.581268
200.6700 5.316467
201.1522 5.627045
201.6343 6.504974
202.1164 8.039612
202.5985 9.267151
203.0806 10.06024
203.5627 10.47009
204.0449 10.59824
204.5270 10.39133
205.0091 10.06403
205.4912 9.847076
205.9733 9.831757
206.4554 9.348724
206.9376 8.264191
207.4197 6.675568
207.9018 4.792847
208.3839 2.440430
208.8660 0.2416080
209.3481 1.296265
209.8303 2.045441
210.3124 2.743317
210.7945 3.524658
211.2766 4.294250
211.7587 4.669800
212.2408 4.542755
212.7230 4.242279
213.2051 4.037537
213.6872 4.067352
214.1693 3.672913
214.6514 2.609314
215.1335 1.094116
215.6157 0.1774900
216.0978 7.6720998E-02
216.5799 0.1766050
217.0620 5.3344999E-02
217.5441 0.4378660
218.0262 0.7031250
218.5084 0.5526120
218.9905 0.1078800
219.4726 2.9022001E-02
219.9547 0.1867070
220.4368 0.6451420
220.9189 1.339813
221.4011 2.485016
221.8832 3.323792
222.3653 3.648682
222.8474 3.623047
223.3295 4.051758
223.8116 5.203461
224.2938 6.370941
224.7759 7.134155
225.2580 7.295990
225.7401 7.518250
226.2222 7.837677
226.7043 8.239410
227.1865 8.667664
227.6686 8.996063
228.1507 9.505035
228.6328 10.42328
229.1149 12.06067
229.5970 13.31174
230.0792 13.79742
230.5613 13.85263
231.0434 14.79010
231.5255 16.84656
232.0076 19.42737
232.4897 22.31296
232.9719 25.93146
233.4540 28.88202
233.9361 30.93427
234.4182 32.31488
234.9003 33.84619
235.3824 35.66089
235.8646 37.43839
236.3467 38.91742
236.8288 39.56827
237.3109 41.13684
237.7930 44.04880
238.2751 47.84332
238.7573 51.09076
239.2394 53.82391
239.7215 55.93759
240.2036 57.20224
240.6857 56.67249
241.1678 57.48709
241.6500 60.26727
242.1321 64.20267
242.6142 67.26889
243.0963 69.02725
243.5784 70.52985
244.0605 72.12701
244.5427 73.66931
245.0248 75.74359
245.5069 78.54791
245.9890 81.82455
246.4711 84.91492
246.9532 87.56448
247.4354 90.50854
247.9175 93.98145
248.3996 98.02625
248.8817 102.5716
249.3638 107.7968
249.8459 113.4357
250.3281 118.9408
250.8102 124.0248
251.2923 129.5189
251.7744 135.8680
252.2565 143.2539
252.7386 150.5483
253.2208 157.9505
253.7029 165.1122
254.1850 171.4590
254.6671 176.3181
255.1492 181.6956
255.6313 188.3375
256.1135 196.4636
256.5956 204.2534
257.0777 211.9695
257.5598 219.0724
258.0419 225.3019
258.5240 232.1351
259.0062 234.4329
259.4883 230.5737
259.9704 220.4911
260.4525 206.5699
260.9346 187.7438
261.4167 166.4841
261.8989 145.0811
262.3810 122.8216
262.8631 103.0257
263.3452 86.96179
263.8273 74.43768
264.3094 62.83008
264.7916 51.69736
265.2737 41.90732
265.7558 34.29773
266.2379 29.31543
266.7200 25.26312
267.2021 21.93546
267.6843 19.28647
268.1664 16.33881
268.6485 12.83298
269.1306 9.534607
269.6127 7.294525
270.0948 6.420441
270.5770 5.338623
271.0591 3.564392
271.5412 1.373901
272.0233 0.3472290
272.5054 0.8708190
272.9875 1.690399
273.4697 1.795654
273.9518 1.006683
274.4339 0.3357240
274.9160 0.1553650
275.3981 0.3906860
275.8802 7.3334001E-02
276.3624 0.9236450
276.8445 1.960022
277.3266 2.491974
277.8087 2.467804
278.2908 3.094696
278.7729 4.576782
279.2551 6.619415
279.7372 8.695496
280.2193 10.89197
280.7014 12.59323
281.1835 13.16360
281.6656 12.62799
282.1478 12.88763
282.6299 14.24780
283.1120 15.96072
283.5941 16.60464
284.0762 16.12164
284.5583 15.80310
285.0405 16.46906
285.5226 17.96649
286.0047 18.63681
286.4868 18.20538
286.9689 17.84100
287.4510 19.38391
287.9332 22.74359
288.4153 26.11578
288.8974 28.61624
289.3795 30.52060
289.8616 32.84875
290.3438 35.65228
290.8259 38.53439
291.3080 41.31689
291.7901 43.89008
292.2722 45.75790
292.7543 46.73245
293.2365 46.88828
293.7186 45.90396
294.2007 43.76279
294.6828 42.01651
295.1649 42.69473
295.6470 45.02078
296.1292 46.43985
296.6113 46.13669
297.0934 44.75363
297.5755 42.91364
298.0576 40.68427
298.5397 38.85638
299.0219 38.37363
299.5040 38.67429
299.9861 38.49332
300.4682 37.42252
300.9503 36.14966
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301.9146 35.42157
302.3967 35.37610
302.8788 35.19171
303.3609 34.84451
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304.3251 33.65262
304.8073 32.72028
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305.7715 29.70178
306.2536 27.76373
306.7357 25.52600
307.2178 23.10587
307.7000 20.71051
308.1821 18.37628
308.6642 15.77408
309.1463 12.10922
309.6284 8.110016
310.1105 4.864594
310.5927 3.059296
311.0748 2.056519
311.5569 1.653351
312.0390 1.828522
312.5211 1.873840
313.0032 1.368866
313.4854 0.5406190
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314.9317 2.720245
315.4138 2.595001
315.8959 1.552246
316.3781 0.8393550
316.8602 1.502289
317.3423 2.410156
317.8244 2.730774
318.3065 2.051025
318.7886 1.096771
319.2708 6.7230001E-02
319.7529 1.059937
320.2350 2.351318
320.7171 4.221344
321.1992 5.945618
321.6813 7.059174
322.1635 7.053711
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328.9131 25.07455
329.3952 24.71844
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330.3594 21.22733
330.8416 18.98886
331.3237 16.73956
331.8058 14.72815
332.2879 12.79834
332.7700 11.39795
333.2521 10.91739
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334.2164 10.11279
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340.4839 9.219299
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343.3766 9.965179
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368.4467 36.98471
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380.9817 7.322968
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382.4280 6.013367
382.9102 6.269775
383.3923 6.208374
383.8744 5.853668
384.3565 5.476044
384.8386 5.234833
385.3207 5.092529
385.8029 4.954407
386.2850 4.793213
386.7671 4.728607
387.2492 5.167999
387.7313 5.811371
388.2134 5.959930
388.6956 4.871399
389.1777 3.430359
389.6598 2.421082
390.1419 1.846252
390.6240 1.375671
391.1061 0.6031490
391.5883 7.6141000E-02
392.0704 0.1926270
392.5525 1.014771
393.0346 1.922485
393.5167 1.610016
393.9988 0.4258730
394.4810 0.6778560
394.9631 1.691132
395.4452 2.301361
395.9273 2.231232
396.4094 1.173615
396.8915 0.3160400
397.3737 0.2080080
397.8558 0.3884580
398.3379 0.2035220
398.8200 1.478912
399.3021 2.349152
399.7842 1.375671
400.2664 1.430054
400.7485 2.675934
401.2306 1.304443
401.7127 0.6326290
402.1948 1.879791
402.6769 2.282532
403.1591 2.318146
403.6412 1.892365
404.1233 1.169983
404.6054 0.4639890
405.0875 0.3244020
405.5696 0.7708130
406.0518 0.5246580
406.5339 0.4440310
407.0160 0.8298950
407.4981 0.5498050
407.9802 0.1023560
408.4623 0.8294070
408.9445 1.642944
409.4266 2.560303
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410.8729 5.886353
411.3550 6.990784
411.8372 8.108032
412.3193 9.560242
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