#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 16:00:55 +0300 (Thu, 24 May 2018) $
#$Revision: 868 $
#$URL: svn://172.16.1.111/rod/cif/1/00/03/1000352.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000352
loop_
_publ_author_name
'Zoppi, M.'
'Pratesi, G.'
_publ_section_title
;
 The dual behavior of the beta-As4S4 altered by light
;
_journal_name_full               'American Mineralogist'
_journal_page_first              890
_journal_page_last               896
_journal_paper_doi               10.2138/am.2012.3968
_journal_volume                  97
_journal_year                    2012
_chemical_compound_source        Synthetic
_chemical_formula_sum            'As8 S9'
_chemical_name_mineral           Alacranite
_space_group_IT_number           13
_symmetry_space_group_name_Hall  '-P 2yc'
_symmetry_space_group_name_H-M   'P 1 2/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 102.397
_cell_angle_gamma                90
_cell_length_a                   9.9342
_cell_length_b                   9.5566
_cell_length_c                   9.1104
_cell_volume                     844.749
_exptl_crystal_density_diffrn    3.491
_cod_database_code               9016439
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R150030.rod
_rod_data_source.block           3500000
_rod_database.code               1000352
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9016439 COD http://www.crystallography.net/cod/9016439.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
106.6573 0.0000000E+00
107.1394 5.519043
107.6215 4.765137
108.1036 2.092285
108.5858 4.319336
109.0679 2.468750
109.5500 24.42090
110.0321 49.48975
110.5142 70.98730
110.9963 84.55029
111.4785 99.15039
111.9606 116.4272
112.4427 136.1929
112.9248 154.0449
113.4069 168.4541
113.8890 181.1118
114.3712 193.5674
114.8533 208.6514
115.3354 221.0767
115.8175 227.9590
116.2996 228.8052
116.7817 230.1831
117.2639 235.8979
117.7460 243.1084
118.2281 248.1963
118.7102 248.3975
119.1923 247.0049
119.6744 245.6675
120.1566 244.3628
120.6387 243.3784
121.1208 242.4067
121.6029 241.6533
122.0850 241.7402
122.5671 241.6680
123.0493 242.8247
123.5314 247.2183
124.0135 256.1289
124.4956 265.2427
124.9777 269.9795
125.4598 271.0054
125.9420 271.2412
126.4241 272.3433
126.9062 273.8311
127.3883 275.0762
127.8704 276.3120
128.3525 276.6309
128.8347 273.3960
129.3168 266.7954
129.7989 261.3286
130.2810 260.8569
130.7631 264.6177
131.2452 269.5464
131.7274 276.0635
132.2095 282.7573
132.6916 285.0479
133.1737 282.4536
133.6558 278.8823
134.1379 278.3545
134.6201 280.8506
135.1022 282.5107
135.5843 281.2144
136.0664 277.7041
136.5485 279.0068
137.0306 286.4795
137.5128 295.5610
137.9949 299.7534
138.4770 297.6274
138.9591 297.5625
139.4412 303.0845
139.9233 314.7261
140.4055 323.7705
140.8876 329.4707
141.3697 333.0972
141.8518 336.8501
142.3339 341.1455
142.8160 344.4751
143.2982 345.8101
143.7803 343.8989
144.2624 344.3286
144.7445 348.2715
145.2266 354.2720
145.7087 359.2295
146.1909 363.5713
146.6730 366.5010
147.1551 367.4204
147.6372 363.7871
148.1193 362.8457
148.6014 366.4575
149.0836 373.1177
149.5657 377.2788
150.0478 376.9507
150.5299 375.8291
151.0120 375.4224
151.4941 375.1206
151.9763 376.1831
152.4584 379.1138
152.9405 383.5234
153.4226 387.5132
153.9047 390.8716
154.3868 393.7002
154.8690 396.0391
155.3511 396.8965
155.8332 398.2456
156.3153 401.1758
156.7974 405.3369
157.2795 407.9390
157.7617 407.4624
158.2438 405.7783
158.7259 404.2646
159.2080 401.6079
159.6901 400.8623
160.1722 404.0396
160.6544 410.9678
161.1365 417.2202
161.6186 420.4189
162.1007 422.5840
162.5828 425.4316
163.0649 430.2290
163.5471 435.1851
164.0292 439.6060
164.5113 441.4746
164.9934 442.7227
165.4755 442.4111
165.9576 441.5747
166.4398 441.6299
166.9219 443.9463
167.4040 446.5342
167.8861 447.6836
168.3682 447.1694
168.8503 447.5845
169.3325 451.8047
169.8146 457.9609
170.2967 463.0688
170.7788 466.0059
171.2609 467.2646
171.7430 466.6357
172.2252 463.8301
172.7073 461.6680
173.1894 462.9971
173.6715 466.6763
174.1536 470.3213
174.6357 472.0850
175.1179 473.3633
175.6000 476.6108
176.0821 482.6357
176.5642 487.4897
177.0463 486.4346
177.5284 480.7861
178.0106 474.7637
178.4927 471.3853
178.9748 468.9180
179.4569 464.1606
179.9390 456.2056
180.4211 448.3550
180.9033 444.5020
181.3854 444.1919
181.8675 445.2778
182.3496 447.2495
182.8317 449.6406
183.3138 450.5337
183.7960 449.6533
184.2781 448.6655
184.7602 450.1660
185.2423 453.5039
185.7244 456.3462
186.2065 456.6084
186.6887 455.1479
187.1708 454.7935
187.6529 455.9126
188.1350 458.4282
188.6171 462.6040
189.0992 468.1812
189.5814 474.1846
190.0635 480.0059
190.5456 485.6245
191.0277 492.0044
191.5098 499.4233
191.9919 506.9810
192.4741 513.1255
192.9562 517.8521
193.4383 521.7422
193.9204 524.7388
194.4025 526.9658
194.8846 530.4497
195.3668 535.3838
195.8489 541.4326
196.3310 549.0684
196.8131 558.8438
197.2952 566.8125
197.7773 569.3198
198.2595 566.2231
198.7416 563.3696
199.2237 561.4985
199.7058 560.4463
200.1879 559.8521
200.6700 559.4609
201.1522 559.4922
201.6343 560.1377
202.1164 561.4165
202.5985 563.4658
203.0806 567.2739
203.5627 571.9531
204.0449 573.3579
204.5270 570.2173
205.0091 565.4473
205.4912 562.1729
205.9733 561.6045
206.4554 558.1191
206.9376 549.7451
207.4197 538.3936
207.9018 531.1768
208.3839 529.3911
208.8660 528.2744
209.3481 524.3301
209.8303 516.5107
210.3124 510.9746
210.7945 509.3833
211.2766 510.5488
211.7587 509.0205
212.2408 504.1094
212.7230 497.9702
213.2051 491.4282
213.6872 483.7354
214.1693 478.1431
214.6514 475.6787
215.1335 475.4512
215.6157 474.0181
216.0978 471.2954
216.5799 467.1367
217.0620 460.6465
217.5441 449.8833
218.0262 442.5239
218.5084 441.0322
218.9905 443.5005
219.4726 440.2002
219.9547 428.2075
220.4368 415.3970
220.9189 407.7812
221.4011 408.9805
221.8832 405.5908
222.3653 394.6636
222.8474 378.4023
223.3295 365.9658
223.8116 358.8833
224.2938 353.7720
224.7759 348.7075
225.2580 343.4937
225.7401 338.9487
226.2222 335.5596
226.7043 332.8213
227.1865 328.3457
227.6686 321.6460
228.1507 314.0381
228.6328 306.2495
229.1149 298.0898
229.5970 290.3115
230.0792 283.5103
230.5613 277.1650
231.0434 269.3140
231.5255 259.2271
232.0076 249.0586
232.4897 240.4014
232.9719 234.9531
233.4540 227.5029
233.9361 217.8970
234.4182 206.1646
234.9003 191.7930
235.3824 172.7163
235.8646 153.9517
236.3467 138.2012
236.8288 127.4121
237.3109 115.0752
237.7930 100.3120
238.2751 83.83887
238.7573 68.18457
239.2394 52.48877
239.7215 38.63086
240.2036 27.74316
240.6857 22.08984
241.1678 13.80078
241.6500 0.8017580
242.1321 14.29053
242.6142 24.68359
243.0963 27.81592
243.5784 29.92334
244.0605 33.38379
244.5427 38.17773
245.0248 44.48828
245.5069 53.25195
245.9890 63.12305
246.4711 70.98779
246.9532 76.06445
247.4354 80.41650
247.9175 84.84814
248.3996 89.74268
248.8817 93.27197
249.3638 95.04492
249.8459 95.56836
250.3281 95.71973
250.8102 95.17969
251.2923 94.67822
251.7744 94.56445
252.2565 95.15039
252.7386 94.62646
253.2208 92.25146
253.7029 89.30176
254.1850 87.78418
254.6671 88.39014
255.1492 89.19043
255.6313 89.77197
256.1135 90.24219
256.5956 90.42773
257.0777 90.87744
257.5598 90.72705
258.0419 88.62891
258.5240 84.00244
259.0062 79.01123
259.4883 73.78320
259.9704 68.35303
260.4525 65.40576
260.9346 67.11475
261.4167 68.69678
261.8989 63.67188
262.3810 48.84375
262.8631 36.01221
263.3452 28.48682
263.8273 26.01562
264.3094 23.00146
264.7916 19.99268
265.2737 15.16309
265.7558 5.715332
266.2379 10.25342
266.7200 24.40527
267.2021 34.83057
267.6843 41.89502
268.1664 49.45117
268.6485 56.73633
269.1306 65.93457
269.6127 79.16504
270.0948 97.08398
270.5770 115.4634
271.0591 133.4692
271.5412 151.0718
272.0233 168.9043
272.5054 186.2593
272.9875 204.5371
273.4697 224.6714
273.9518 247.0488
274.4339 270.1816
274.9160 294.0220
275.3981 318.3394
275.8802 342.7969
276.3624 366.5806
276.8445 392.1123
277.3266 420.9722
277.8087 453.2969
278.2908 487.4634
278.7729 523.3828
279.2551 561.0762
279.7372 599.3999
280.2193 638.4312
280.7014 678.8828
281.1835 721.8735
281.6656 767.3818
282.1478 813.0293
282.6299 858.1831
283.1120 904.5439
283.5941 954.5801
284.0762 1008.554
284.5583 1066.128
285.0405 1129.732
285.5226 1198.438
286.0047 1262.430
286.4868 1320.286
286.9689 1377.971
287.4510 1443.677
287.9332 1517.150
288.4153 1594.154
288.8974 1672.040
289.3795 1751.196
289.8616 1830.236
290.3438 1908.967
290.8259 1988.828
291.3080 2071.552
291.7901 2156.309
292.2722 2243.645
292.7543 2333.276
293.2365 2424.697
293.7186 2516.106
294.2007 2606.674
294.6828 2697.953
295.1649 2791.235
295.6470 2885.493
296.1292 2981.026
296.6113 3077.131
297.0934 3173.530
297.5755 3271.882
298.0576 3372.461
298.5397 3471.948
299.0219 3567.302
299.5040 3660.749
299.9861 3756.692
300.4682 3857.658
300.9503 3959.359
301.4324 4058.812
301.9146 4154.989
302.3967 4248.481
302.8788 4335.966
303.3609 4421.161
303.8430 4507.760
304.3251 4596.508
304.8073 4686.396
305.2894 4780.533
305.7715 4875.489
306.2536 4966.102
306.7357 5044.902
307.2178 5119.542
307.7000 5196.733
308.1821 5277.155
308.6642 5357.186
309.1463 5433.712
309.6284 5507.529
310.1105 5581.332
310.5927 5658.036
311.0748 5732.607
311.5569 5802.525
312.0390 5867.563
312.5211 5928.587
313.0032 5985.722
313.4854 6040.471
313.9675 6093.485
314.4496 6142.835
314.9317 6192.634
315.4138 6247.074
315.8959 6305.186
316.3781 6361.802
316.8602 6412.186
317.3423 6461.135
317.8244 6512.283
318.3065 6569.953
318.7886 6624.216
319.2708 6667.232
319.7529 6703.824
320.2350 6747.289
320.7171 6809.353
321.1992 6871.759
321.6813 6924.357
322.1635 6960.938
322.6456 6998.556
323.1277 7039.258
323.6098 7083.054
324.0919 7130.170
324.5740 7187.452
325.0562 7240.724
325.5383 7284.792
326.0204 7317.458
326.5025 7348.976
326.9846 7377.470
327.4667 7406.236
327.9489 7439.286
328.4310 7484.739
328.9131 7525.958
329.3952 7562.099
329.8773 7593.367
330.3594 7615.337
330.8416 7618.926
331.3237 7620.777
331.8058 7633.245
332.2879 7666.179
332.7700 7692.680
333.2521 7707.518
333.7343 7713.811
334.2164 7728.192
334.6985 7757.682
335.1806 7783.738
335.6627 7794.960
336.1448 7785.064
336.6270 7779.204
337.1091 7779.452
337.5912 7783.000
338.0733 7784.616
338.5554 7784.572
339.0375 7781.938
339.5197 7776.533
340.0018 7768.445
340.4839 7756.369
340.9660 7739.564
341.4481 7720.748
341.9302 7705.333
342.4124 7693.819
342.8945 7676.025
343.3766 7645.925
343.8587 7607.154
344.3408 7577.117
344.8229 7557.291
345.3051 7536.737
345.7872 7505.115
346.2693 7463.697
346.7514 7419.021
347.2335 7371.049
347.7156 7323.012
348.1978 7283.836
348.6799 7252.967
349.1620 7222.061
349.6441 7186.770
350.1262 7147.424
350.6083 7103.863
351.0905 7054.766
351.5726 7004.917
352.0547 6959.595
352.5368 6917.944
353.0189 6877.564
353.5010 6838.646
353.9832 6799.515
354.4653 6758.767
354.9474 6715.794
355.4295 6669.845
355.9116 6616.285
356.3937 6560.235
356.8759 6509.836
357.3580 6473.093
357.8401 6437.320
358.3222 6394.006
358.8043 6343.720
359.2864 6291.871
359.7686 6239.827
360.2507 6187.557
360.7328 6136.080
361.2149 6086.869
361.6970 6035.610
362.1791 5979.580
362.6613 5920.078
363.1434 5860.157
363.6255 5797.812
364.1076 5737.249
364.5897 5681.354
365.0718 5634.608
365.5540 5583.277
366.0361 5520.536
366.5182 5453.309
367.0003 5390.033
367.4824 5339.633
367.9645 5285.195
368.4467 5219.856
368.9288 5144.004
369.4109 5074.718
369.8930 5016.743
370.3751 4962.367
370.8572 4906.198
371.3394 4848.274
371.8215 4789.606
372.3036 4728.949
372.7857 4667.351
373.2678 4608.844
373.7499 4555.000
374.2321 4500.595
374.7142 4442.715
375.1963 4378.809
375.6784 4320.050
376.1605 4268.297
376.6426 4219.707
377.1248 4171.593
377.6069 4124.228
378.0890 4072.304
378.5711 4012.513
379.0532 3946.129
379.5353 3887.796
380.0175 3838.247
380.4996 3790.348
380.9817 3737.082
381.4638 3679.230
381.9459 3620.628
382.4280 3562.797
382.9102 3504.428
383.3923 3444.248
383.8744 3381.803
384.3565 3318.632
384.8386 3257.278
385.3207 3195.746
385.8029 3132.167
386.2850 3065.593
386.7671 2997.349
387.2492 2928.757
387.7313 2859.025
388.2134 2787.750
388.6956 2714.922
389.1777 2641.541
389.6598 2567.803
390.1419 2494.118
390.6240 2420.729
391.1061 2347.218
391.5883 2273.668
392.0704 2199.750
392.5525 2124.470
393.0346 2050.442
393.5167 1976.935
393.9988 1904.559
394.4810 1834.029
394.9631 1768.783
395.4452 1702.944
395.9273 1632.650
396.4094 1555.075
396.8915 1480.589
397.3737 1413.886
397.8558 1350.242
398.3379 1283.841
398.8200 1211.363
399.3021 1138.804
399.7842 1066.333
400.2664 993.9409
400.7485 924.0601
401.2306 858.3452
401.7127 794.3145
402.1948 730.3213
402.6769 664.5371
403.1591 602.9404
403.6412 547.1714
404.1233 495.3418
404.6054 440.2803
405.0875 380.6587
405.5696 323.5728
406.0518 272.1074
406.5339 226.3945
407.0160 183.1826
407.4981 142.6768
407.9802 105.7227
408.4623 74.63818
408.9445 49.23438
409.4266 24.08252
409.9087 3.235840
410.3908 30.21045
410.8729 50.44043
411.3550 64.06787
411.8372 73.77100
412.3193 79.64502
412.8014 83.34180
413.2835 89.52588
413.7656 99.69824
414.2477 109.3516
414.7299 113.0688
415.2120 112.4805
415.6941 111.1382
416.1762 111.5420
416.6583 111.6636
417.1404 109.3755
417.6226 104.8291
418.1047 100.1797
418.5868 96.70850
419.0689 93.85400
419.5510 91.15137
420.0331 88.79834
420.5153 86.15576
420.9974 81.94873
421.4795 77.11279
421.9616 73.99512
422.4437 74.97217
422.9258 76.15381
423.4080 75.86963
423.8901 73.69824
424.3722 70.96680
424.8543 67.87354
425.3364 64.05078
425.8185 59.04297
426.3007 51.14697
426.7828 44.49609
427.2649 40.17578
427.7470 37.74805
428.2291 34.45459
428.7112 30.48145
429.1934 25.38623
429.6755 18.50391
430.1576 9.260742
430.6397 1.789063
431.1218 3.085449
431.6039 7.211426
432.0861 13.60791
432.5682 22.38916
433.0503 31.82471
433.5324 41.65771
434.0145 51.68994
434.4966 61.20312
434.9788 70.24072
435.4609 78.92090
435.9430 86.26465
436.4251 93.38379
436.9072 103.4868
437.3893 117.7109
437.8715 133.7607
438.3536 149.5186
438.8357 165.0317
439.3178 180.4233
439.7999 194.9912
440.2820 209.9126
440.7642 225.9829
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