#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-05-24 16:08:58 +0300 (Thu, 24 May 2018) $ #$Revision: 882 $ #$URL: svn://172.16.1.111/rod/cif/1/00/03/1000361.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_1000361 loop_ _publ_author_name 'Basciano, L. C.' _publ_section_title ; Mineralogy and crystal structures of barium silicate minerals from Fresno County, California ; _journal_name_full 'Master s Thesis, University of British Columbia' _journal_page_first 1 _journal_page_last 164 _journal_volume 1999 _journal_year 1999 _chemical_compound_source 'Esquire #7, Big Creek, Fresno County, California, USA' _chemical_formula_sum 'Ba Ca2 O9 Si3' _chemical_name_mineral Walstromite _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 69.64 _cell_angle_beta 102.29 _cell_angle_gamma 96.89 _cell_length_a 6.733 _cell_length_b 9.608 _cell_length_c 6.685 _cell_volume 395.650 _exptl_crystal_density_diffrn 3.741 _cod_original_formula_sum 'Ba Ca2 Si3 O9' _cod_database_code 9016690 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type other _raman_measurement_device.excitation_laser_wavelength 532 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 15 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R150079.rod _rod_data_source.block 3500000 _rod_database.code 1000361 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9016690 COD http://www.crystallography.net/cod/9016690.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 90.74744 0.0000000E+00 91.22955 20.44836 91.71167 26.29248 92.19379 30.27332 92.67590 31.44513 93.15802 26.51038 93.64014 17.38428 94.12225 11.99615 94.60437 6.653625 95.08649 3.083557 95.56860 3.286255 96.05072 2.261841 96.53284 0.6497800 97.01495 1.293457 97.49707 2.880127 97.97919 2.685608 98.46130 6.699009 98.94342 5.095154 99.42554 13.43414 99.90765 18.29340 100.3898 19.13080 100.8719 18.00513 101.3540 17.06396 101.8361 15.40167 102.3182 16.75671 102.8004 23.01685 103.2825 35.23773 103.7646 47.55219 104.2467 61.63629 104.7288 75.16370 105.2109 82.02258 105.6931 79.36920 106.1752 74.89825 106.6573 71.81750 107.1394 69.93079 107.6215 69.69409 108.1036 71.06238 108.5858 74.01703 109.0679 78.61053 109.5500 82.96741 110.0321 90.16205 110.5142 101.7507 110.9963 117.9952 111.4785 138.0776 111.9606 162.5038 112.4427 191.0978 112.9248 221.1246 113.4069 258.8054 113.8890 294.5378 114.3712 321.0110 114.8533 337.2855 115.3354 343.7153 115.8175 337.3117 116.2996 316.9344 116.7817 297.5819 117.2639 281.2942 117.7460 269.6801 118.2281 264.7755 118.7102 266.5797 119.1923 275.5485 119.6744 292.2053 120.1566 316.8130 120.6387 348.0996 121.1208 385.7700 121.6029 429.3385 122.0850 477.6205 122.5671 545.0615 123.0493 610.3518 123.5314 652.8061 124.0135 669.5009 124.4956 661.9216 124.9777 620.2518 125.4598 551.3679 125.9420 481.8577 126.4241 424.1649 126.9062 378.1377 127.3883 343.6785 127.8704 321.1897 128.3525 309.6821 128.8347 308.7209 129.3168 318.2120 129.7989 335.5824 130.2810 359.3245 130.7631 389.4056 131.2452 426.6555 131.7274 472.0847 132.2095 524.8561 132.6916 583.0732 133.1737 647.2603 133.6558 711.9271 134.1379 778.2881 134.6201 846.1445 135.1022 899.7232 135.5843 936.8550 136.0664 956.7106 136.5485 947.5085 137.0306 905.1686 137.5128 842.8433 137.9949 770.9338 138.4770 686.3366 138.9591 605.9016 139.4412 533.2549 139.9233 468.9222 140.4055 413.8675 140.8876 368.5339 141.3697 332.0309 141.8518 302.7791 142.3339 281.4703 142.8160 266.2894 143.2982 257.2459 143.7803 255.2877 144.2624 256.4833 144.7445 260.6166 145.2266 267.4206 145.7087 276.0125 146.1909 285.6427 146.6730 297.2155 147.1551 311.6398 147.6372 329.2490 148.1193 349.8159 148.6014 374.7497 149.0836 402.4866 149.5657 433.9295 150.0478 469.9413 150.5299 508.2677 151.0120 548.2477 151.4941 596.5137 151.9763 638.2048 152.4584 676.7678 152.9405 710.0901 153.4226 728.5785 153.9047 725.2435 154.3868 710.8808 154.8690 691.3163 155.3511 659.2879 155.8332 630.7073 156.3153 607.5250 156.7974 589.7507 157.2795 577.8263 157.7617 575.8781 158.2438 577.6138 158.7259 578.4973 159.2080 583.7698 159.6901 582.1109 160.1722 570.6001 160.6544 549.2416 161.1365 519.0531 161.6186 475.1104 162.1007 424.8854 162.5828 374.2069 163.0649 321.3060 163.5471 271.9065 164.0292 228.1437 164.5113 190.0969 164.9934 157.9683 165.4755 133.3969 165.9576 114.3202 166.4398 98.48407 166.9219 86.24371 167.4040 75.81970 167.8861 66.53247 168.3682 58.33868 168.8503 50.39749 169.3325 41.67062 169.8146 32.86200 170.2967 25.24026 170.7788 19.87817 171.2609 15.54761 171.7430 11.07126 172.2252 6.256439 172.7073 2.119629 173.1894 0.5761720 173.6715 2.001190 174.1536 2.462433 174.6357 2.143127 175.1179 0.9776920 175.6000 1.211304 176.0821 4.480957 176.5642 8.444824 177.0463 12.75812 177.5284 17.47864 178.0106 22.70929 178.4927 28.89844 178.9748 35.56677 179.4569 42.12384 179.9390 48.85135 180.4211 54.40195 180.9033 57.10788 181.3854 57.24408 181.8675 56.05234 182.3496 53.63745 182.8317 50.45837 183.3138 47.42667 183.7960 44.66357 184.2781 42.07452 184.7602 39.38104 185.2423 36.63342 185.7244 34.51401 186.2065 33.51978 186.6887 33.49326 187.1708 33.88168 187.6529 34.70026 188.1350 35.73920 188.6171 36.88043 189.0992 38.10965 189.5814 38.76205 190.0635 38.64395 190.5456 37.66898 191.0277 35.26486 191.5098 31.19855 191.9919 25.94489 192.4741 20.12909 192.9562 13.71643 193.4383 7.890625 193.9204 3.700928 194.4025 1.070740 194.8846 1.327637 195.3668 3.627686 195.8489 5.822968 196.3310 8.006561 196.8131 10.23785 197.2952 12.01184 197.7773 12.89331 198.2595 12.85516 198.7416 12.73413 199.2237 12.71548 199.7058 12.60397 200.1879 11.84897 200.6700 10.40674 201.1522 8.488922 201.6343 6.024536 202.1164 2.920258 202.5985 0.2795720 203.0806 1.525238 203.5627 2.890717 204.0449 5.112366 204.5270 8.340454 205.0091 11.93680 205.4912 15.60059 205.9733 19.41110 206.4554 22.78323 206.9376 25.62323 207.4197 27.97736 207.9018 30.04004 208.3839 31.69382 208.8660 33.37521 209.3481 35.26294 209.8303 37.27191 210.3124 39.91528 210.7945 43.19617 211.2766 47.16205 211.7587 52.14612 212.2408 58.24829 212.7230 65.20691 213.2051 73.02261 213.6872 81.88919 214.1693 91.09171 214.6514 100.9460 215.1335 111.0517 215.6157 119.1799 216.0978 125.3162 216.5799 129.5894 217.0620 131.9755 217.5441 132.0757 218.0262 131.3985 218.5084 130.0590 218.9905 128.0270 219.4726 125.1230 219.9547 120.7283 220.4368 116.4499 220.9189 113.4066 221.4011 111.9665 221.8832 110.7493 222.3653 109.5710 222.8474 108.5376 223.3295 108.1652 223.8116 108.8730 224.2938 109.5998 224.7759 109.8446 225.2580 109.9449 225.7401 108.7100 226.2222 105.9082 226.7043 101.7059 227.1865 96.54355 227.6686 90.21564 228.1507 83.37897 228.6328 76.33792 229.1149 68.65720 229.5970 61.88425 230.0792 56.44904 230.5613 51.97501 231.0434 47.00977 231.5255 41.06000 232.0076 35.55182 232.4897 31.36060 232.9719 28.92496 233.4540 27.09390 233.9361 25.90363 234.4182 25.19083 234.9003 24.36688 235.3824 23.12390 235.8646 22.19226 236.3467 21.92627 236.8288 22.41138 237.3109 23.42230 237.7930 25.29263 238.2751 27.60196 238.7573 29.00061 239.2394 28.77591 239.7215 28.64752 240.2036 29.48923 240.6857 32.02542 241.1678 33.83914 241.6500 34.65683 242.1321 34.80997 242.6142 35.16803 243.0963 35.89081 243.5784 36.57907 244.0605 37.04486 244.5427 37.18512 245.0248 37.43802 245.5069 38.03409 245.9890 38.66342 246.4711 38.68808 246.9532 38.25867 247.4354 36.99628 247.9175 34.67953 248.3996 31.01566 248.8817 27.15497 249.3638 22.73941 249.8459 18.32520 250.3281 15.03378 250.8102 13.44626 251.2923 11.95895 251.7744 9.856812 252.2565 6.743134 252.7386 4.594635 253.2208 3.730774 253.7029 3.606476 254.1850 3.359558 254.6671 2.850433 255.1492 2.499756 255.6313 2.439026 256.1135 2.690491 256.5956 3.428741 257.0777 4.617035 257.5598 6.273132 258.0419 8.522705 258.5240 11.56921 259.0062 14.81244 259.4883 18.14026 259.9704 21.62659 260.4525 25.14783 260.9346 28.98462 261.4167 32.91821 261.8989 36.90265 262.3810 40.89331 262.8631 45.01013 263.3452 49.41083 263.8273 54.15588 264.3094 58.11804 264.7916 61.39545 265.2737 63.87732 265.7558 65.37872 266.2379 65.63654 266.7200 65.78638 267.2021 66.28021 267.6843 67.05487 268.1664 66.73737 268.6485 65.05798 269.1306 62.80090 269.6127 60.57477 270.0948 58.38068 270.5770 55.90027 271.0591 52.85968 271.5412 49.49628 272.0233 46.93121 272.5054 45.16205 272.9875 44.21802 273.4697 44.25598 273.9518 45.40887 274.4339 47.03088 274.9160 49.05841 275.3981 51.48956 275.8802 54.31714 276.3624 57.42706 276.8445 61.23248 277.3266 66.22705 277.8087 72.50812 278.2908 78.57758 278.7729 84.26825 279.2551 89.74329 279.7372 95.06696 280.2193 100.1790 280.7014 105.7032 281.1835 111.9395 281.6656 118.8904 282.1478 126.5623 282.6299 134.7971 283.1120 144.0752 283.5941 155.1669 284.0762 168.1444 284.5583 182.6550 285.0405 198.9008 285.5226 216.7800 286.0047 235.5600 286.4868 255.4215 286.9689 275.5656 287.4510 295.6794 287.9332 315.6530 288.4153 333.4797 288.8974 348.8985 289.3795 361.4164 289.8616 368.9298 290.3438 371.5662 290.8259 368.2545 291.3080 356.5897 291.7901 337.3953 292.2722 314.6232 292.7543 288.0680 293.2365 259.6754 293.7186 233.4620 294.2007 209.6357 294.6828 189.0003 295.1649 172.3303 295.6470 159.6057 296.1292 150.2322 296.6113 144.2968 297.0934 141.5244 297.5755 141.9262 298.0576 145.3978 298.5397 150.6285 299.0219 157.9485 299.5040 166.3069 299.9861 173.6229 300.4682 180.0026 300.9503 184.1963 301.4324 185.6940 301.9146 184.0813 302.3967 177.6478 302.8788 163.0585 303.3609 143.6815 303.8430 124.0074 304.3251 104.2110 304.8073 85.83026 305.2894 69.85840 305.7715 56.31927 306.2536 44.83246 306.7357 35.61755 307.2178 28.26031 307.7000 22.67749 308.1821 18.94055 308.6642 16.17371 309.1463 13.69153 309.6284 11.75537 310.1105 10.75586 310.5927 11.45221 311.0748 12.74438 311.5569 13.62506 312.0390 14.09680 312.5211 15.46405 313.0032 18.99188 313.4854 23.63000 313.9675 28.21460 314.4496 32.44360 314.9317 36.45941 315.4138 40.46136 315.8959 44.39044 316.3781 47.97260 316.8602 51.69086 317.3423 54.62970 317.8244 56.08435 318.3065 55.55750 318.7886 54.02728 319.2708 51.73016 319.7529 48.65607 320.2350 44.76190 320.7171 39.65466 321.1992 34.04193 321.6813 28.15485 322.1635 21.65942 322.6456 15.70459 323.1277 10.45996 323.6098 5.890137 324.0919 4.227143 324.5740 1.197632 325.0562 3.903320 325.5383 6.421387 326.0204 8.936890 326.5025 10.54187 326.9846 10.78204 327.4667 10.23535 327.9489 9.517273 328.4310 8.844971 328.9131 7.746826 329.3952 5.996216 329.8773 3.568909 330.3594 1.298218 330.8416 0.4141850 331.3237 2.289001 331.8058 4.865906 332.2879 8.673767 332.7700 12.30646 333.2521 15.60046 333.7343 18.70221 334.2164 22.09576 334.6985 25.78339 335.1806 29.69604 335.6627 33.68781 336.1448 37.43365 336.6270 41.58282 337.1091 46.24927 337.5912 51.36017 338.0733 56.63995 338.5554 61.96277 339.0375 67.51105 339.5197 73.36823 340.0018 79.48425 340.4839 86.10327 340.9660 93.13867 341.4481 100.5876 341.9302 108.4196 342.4124 116.7460 342.8945 124.8448 343.3766 132.7646 343.8587 140.2939 344.3408 147.0773 344.8229 153.1830 345.3051 157.7697 345.7872 160.6465 346.2693 161.5968 346.7514 158.9207 347.2335 151.7734 347.7156 141.4915 348.1978 130.1420 348.6799 117.8073 349.1620 105.4554 349.6441 93.26849 350.1262 81.57861 350.6083 71.25641 351.0905 62.38812 351.5726 54.58997 352.0547 47.21667 352.5368 40.46802 353.0189 34.95422 353.5010 31.38086 353.9832 29.01801 354.4653 26.99939 354.9474 25.26062 355.4295 24.09778 355.9116 23.88446 356.3937 24.36139 356.8759 25.13660 357.3580 26.15833 357.8401 27.35645 358.3222 28.46881 358.8043 29.61322 359.2864 31.42896 359.7686 34.27826 360.2507 37.95221 360.7328 42.26025 361.2149 47.32581 361.6970 52.78308 362.1791 58.41254 362.6613 64.31555 363.1434 70.73315 363.6255 78.34399 364.1076 85.99200 364.5897 93.09875 365.0718 99.20776 365.5540 105.6315 366.0361 113.2950 366.5182 121.1633 367.0003 127.9802 367.4824 133.6144 367.9645 138.1732 368.4467 141.6252 368.9288 143.9102 369.4109 145.4514 369.8930 145.9536 370.3751 145.9399 370.8572 145.6989 371.3394 144.6426 371.8215 144.3550 372.3036 144.8083 372.7857 146.1203 373.2678 148.7174 373.7499 152.7703 374.2321 157.9625 374.7142 164.2166 375.1963 171.7907 375.6784 179.4316 376.1605 187.3110 376.6426 194.7536 377.1248 200.9358 377.6069 206.1418 378.0890 209.0422 378.5711 209.4871 379.0532 207.3182 379.5353 201.1103 380.0175 190.5514 380.4996 177.2060 380.9817 161.5637 381.4638 144.0076 381.9459 126.9090 382.4280 110.5870 382.9102 95.27289 383.3923 82.11523 383.8744 70.89496 384.3565 60.67102 384.8386 50.94458 385.3207 41.87793 385.8029 34.11102 386.2850 27.69843 386.7671 22.23816 387.2492 17.40472 387.7313 13.20917 388.2134 9.681152 388.6956 6.948303 389.1777 4.763489 389.6598 3.112305 390.1419 2.003906 390.6240 1.507600 391.1061 0.5307010 391.5883 2.167969 392.0704 3.658325 392.5525 5.403442 393.0346 6.273682 393.5167 5.196838 393.9988 2.820618 394.4810 0.8969730 394.9631 0.7592160 395.4452 0.6452030 395.9273 0.3679200 396.4094 2.603149 396.8915 5.089294 397.3737 7.713806 397.8558 10.46295 398.3379 13.32166 398.8200 16.38379 399.3021 19.44275 399.7842 22.36786 400.2664 25.15295 400.7485 28.30035 401.2306 32.11890 401.7127 35.94104 402.1948 39.25470 402.6769 41.52197 403.1591 44.43384 403.6412 48.16278 404.1233 52.54291 404.6054 57.34607 405.0875 62.61560 405.5696 68.02881 406.0518 73.31232 406.5339 78.44464 407.0160 84.42969 407.4981 91.25464 407.9802 98.82257 408.4623 107.2858 408.9445 116.6666 409.4266 125.7695 409.9087 134.2396 410.3908 142.2811 410.8729 150.5611 411.3550 159.0829 411.8372 166.6706 412.3193 173.1027 412.8014 178.0027 413.2835 180.8792 413.7656 181.9784 414.2477 179.8969 414.7299 172.0894 415.2120 159.8114 415.6941 146.3268 416.1762 132.0085 416.6583 117.7241 417.1404 104.1793 417.6226 91.26923 418.1047 78.99896 418.5868 66.03870 419.0689 54.22198 419.5510 45.24518 420.0331 41.62317 420.5153 38.25238 420.9974 33.02173 421.4795 26.61255 421.9616 20.94336 422.4437 16.73248 422.9258 13.11731 423.4080 9.665222 423.8901 6.111694 424.3722 3.512146 424.8543 2.474609 425.3364 2.196838 425.8185 1.905640 426.3007 1.449829 426.7828 1.220703 427.2649 1.372131 427.7470 1.826111 428.2291 2.091248 428.7112 2.128113 429.1934 2.024536 429.6755 1.859070 430.1576 1.672058 430.6397 1.104614 431.1218 1.584474 431.6039 1.265137 432.0861 2.165100 432.5682 2.731995 433.0503 2.495422 433.5324 0.9774780 434.0145 1.414490 434.4966 3.295227 434.9788 4.663818 435.4609 5.725952 435.9430 6.351013 436.4251 6.813354 436.9072 7.846313 437.3893 9.604797 437.8715 11.93481 438.3536 15.22607 438.8357 19.02869 439.3178 22.08716 439.7999 22.71301 440.2820 22.95374 440.7642 25.29718 441.2463 29.89825 441.7284 33.18256 442.2105 32.74677 442.6926 30.27521 443.1747 27.36353 443.6569 24.12195 444.1390 20.85278 444.6211 17.59283 445.1032 14.36664 445.5853 11.34503 446.0674 8.528442 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473.0660 96.51837 473.5481 97.57416 474.0302 96.29523 474.5123 92.29663 474.9944 86.55994 475.4766 80.11316 475.9587 72.92383 476.4408 65.23798 476.9229 56.49097 477.4050 47.94446 477.8871 41.93195 478.3693 38.30920 478.8514 35.68292 479.3335 33.04266 479.8156 30.74298 480.2977 29.39453 480.7798 29.31958 481.2620 29.71222 481.7441 29.74146 482.2262 29.84308 482.7083 30.74750 483.1904 33.38037 483.6725 36.33899 484.1547 38.93933 484.6368 41.16797 485.1189 43.86536 485.6010 47.20819 486.0831 51.08929 486.5652 55.41815 487.0474 60.37054 487.5295 65.45544 488.0116 70.46991 488.4937 75.67767 488.9758 81.47424 489.4579 87.88037 489.9401 94.79749 490.4222 102.3097 490.9043 110.3741 491.3864 119.0334 491.8685 128.3592 492.3506 138.2267 492.8328 148.6630 493.3149 159.5904 493.7970 171.0896 494.2791 183.3345 494.7612 195.4919 495.2433 207.9490 495.7255 219.7665 496.2076 228.7277 496.6897 234.0559 497.1718 236.1896 497.6539 234.3293 498.1360 229.2388 498.6182 223.7794 499.1003 218.3597 499.5824 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