#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 16:33:07 +0300 (Thu, 24 May 2018) $
#$Revision: 884 $
#$URL: svn://172.16.1.111/rod/cif/1/00/03/1000363.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000363
loop_
_publ_author_name
'Cruciani, G.'
'Gualtieri, A.'
_publ_section_title
;
 Dehydration dynamics of analcime by in situ synchrotron powder
 diffraction Sample at T = 298 K
;
_journal_name_full               'American Mineralogist'
_journal_page_first              112
_journal_page_last               119
_journal_volume                  84
_journal_year                    1999
_chemical_compound_source        R050094
_chemical_formula_sum            'Al1.9 H4 Na1.95 O14 Si4.1'
_chemical_name_mineral           Analcime
_space_group_IT_number           142
_symmetry_space_group_name_Hall  '-I 4bd 2c'
_symmetry_space_group_name_H-M   'I 41/a c d :2'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   13.7295
_cell_length_b                   13.7295
_cell_length_c                   13.7036
_cell_volume                     2583.117
_diffrn_ambient_temperature      298
_exptl_crystal_density_diffrn    2.259
_cod_original_sg_symbol_H-M      'I 41/a c d'
_cod_original_formula_sum        '(Si4.1 Al1.9) Na1.95 O14 H4'
_cod_database_code               9002000
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R050094.rod
_rod_data_source.block           3500000
_rod_database.code               1000363
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9002000 COD http://www.crystallography.net/cod/9002000.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
130.6121 0.0000000E+00
131.0942 0.9445800
131.5764 0.7336430
132.0585 9.347168
132.5406 22.53735
133.0227 37.30566
133.5048 52.29126
133.9869 68.89233
134.4691 85.18945
134.9512 102.9231
135.4333 126.5781
135.9154 160.6470
136.3975 203.7334
136.8796 230.6570
137.3618 231.7048
137.8439 228.8848
138.3260 230.7954
138.8081 238.1104
139.2902 249.5532
139.7723 266.6814
140.2545 289.4795
140.7366 302.8601
141.2187 302.4521
141.7008 294.4390
142.1829 284.2263
142.6650 269.3345
143.1471 257.3972
143.6293 260.7222
144.1114 276.4531
144.5935 291.7715
145.0756 301.6687
145.5577 306.2278
146.0398 309.0662
146.5220 312.0435
147.0041 310.9465
147.4862 298.4395
147.9683 275.7664
148.4504 255.3359
148.9325 253.2690
149.4147 277.3638
149.8968 284.6438
150.3789 257.7524
150.8610 227.7905
151.3431 211.0151
151.8252 198.9248
152.3074 186.0496
152.7895 175.6431
153.2716 168.4414
153.7537 170.3694
154.2358 181.8843
154.7179 191.9089
155.2001 197.1331
155.6822 195.0938
156.1643 187.9385
156.6464 180.6453
157.1285 169.8486
157.6106 157.6519
158.0928 142.3875
158.5749 126.2314
159.0570 113.7874
159.5391 108.4883
160.0212 109.2827
160.5033 103.4387
160.9855 85.77783
161.4676 68.92969
161.9497 53.21411
162.4318 40.16357
162.9139 34.28638
163.3960 39.73340
163.8782 57.14819
164.3603 72.15381
164.8424 90.07690
165.3245 102.0300
165.8066 100.7324
166.2887 86.01904
166.7709 64.53979
167.2530 37.88672
167.7351 6.610107
168.2172 10.28076
168.6993 2.097656
169.1814 24.94434
169.6636 34.83691
170.1457 27.10107
170.6278 12.01270
171.1099 3.928955
171.5920 20.24878
172.0741 30.12036
172.5563 26.73804
173.0384 14.46973
173.5205 5.814209
174.0026 3.038818
174.4847 4.224609
174.9668 8.506348
175.4490 15.60364
175.9311 21.33826
176.4132 23.40039
176.8953 21.82361
177.3774 16.39185
177.8595 3.708984
178.3417 10.42236
178.8238 22.81384
179.3059 33.10071
179.7880 42.12305
180.2701 51.21069
180.7522 61.58435
181.2344 65.47913
181.7165 50.74622
182.1986 35.09570
182.6807 30.93115
183.1628 41.81885
183.6449 60.30823
184.1271 73.07666
184.6092 73.55896
185.0913 82.26440
185.5734 106.7299
186.0555 135.4584
186.5376 159.6106
187.0198 175.8669
187.5019 185.7672
187.9840 191.9948
188.4661 190.8542
188.9482 193.9574
189.4303 209.1271
189.9125 227.1168
190.3946 236.0457
190.8767 229.3994
191.3588 211.1094
191.8409 199.7897
192.3230 194.0459
192.8052 197.0186
193.2873 216.7449
193.7694 245.4547
194.2515 269.1630
194.7336 279.0780
195.2157 277.2128
195.6979 282.9800
196.1800 305.7250
196.6621 324.9371
197.1442 329.2255
197.6263 323.5693
198.1084 321.9401
198.5906 336.5051
199.0727 365.2783
199.5548 377.8646
200.0369 361.1443
200.5190 341.4236
201.0011 333.9365
201.4833 338.9128
201.9654 348.3118
202.4475 355.8564
202.9296 360.6323
203.4117 364.9939
203.8938 374.0554
204.3760 381.3470
204.8581 378.7018
205.3402 365.2543
205.8223 350.5623
206.3044 341.8394
206.7865 338.0688
207.2687 335.9808
207.7508 336.7991
208.2329 338.3428
208.7150 336.8156
209.1971 331.0721
209.6792 325.8789
210.1614 326.1047
210.6435 329.8762
211.1256 333.2395
211.6077 335.1710
212.0898 335.8766
212.5719 336.7399
213.0541 340.5022
213.5362 338.5571
214.0183 319.8893
214.5004 290.6830
214.9825 266.5630
215.4646 257.3135
215.9468 260.6417
216.4289 267.8014
216.9110 282.8358
217.3931 295.8220
217.8752 298.5964
218.3573 294.4991
218.8395 293.1483
219.3216 304.9694
219.8037 327.6438
220.2858 338.8378
220.7679 331.7761
221.2500 319.9663
221.7322 305.9661
222.2143 291.9318
222.6964 283.1627
223.1785 287.5983
223.6606 306.2070
224.1427 314.4474
224.6249 300.2456
225.1070 285.2213
225.5891 278.0092
226.0712 277.2401
226.5533 278.4601
227.0354 277.0498
227.5176 273.1105
227.9997 261.4585
228.4818 224.8533
228.9639 194.1935
229.4460 188.2378
229.9281 203.2771
230.4103 219.8173
230.8924 214.6548
231.3745 178.5009
231.8566 161.3492
232.3387 176.9569
232.8208 197.6594
233.3030 216.1847
233.7851 229.1732
234.2672 232.2322
234.7493 218.3499
235.2314 180.0580
235.7135 153.6813
236.1957 140.9094
236.6778 135.7153
237.1599 140.6796
237.6420 152.7645
238.1241 161.6421
238.6062 154.1201
239.0884 122.2468
239.5705 99.55469
240.0526 87.46704
240.5347 81.56323
241.0168 82.89368
241.4989 89.73608
241.9811 95.71838
242.4632 93.19861
242.9453 79.02698
243.4274 65.46143
243.9095 48.03760
244.3916 34.32837
244.8738 31.69983
245.3559 39.81226
245.8380 49.77991
246.3201 51.00220
246.8022 39.63037
247.2843 31.35034
247.7665 24.72839
248.2486 21.68127
248.7307 26.85132
249.2128 39.39929
249.6949 50.33337
250.1770 48.15027
250.6592 25.83765
251.1413 15.91113
251.6234 28.94458
252.1055 46.36011
252.5876 56.31006
253.0697 56.63184
253.5519 48.74268
254.0340 32.12732
254.5161 2.023926
254.9982 14.84448
255.4803 10.37939
255.9624 1.641968
256.4445 13.67651
256.9267 23.87671
257.4088 28.92517
257.8909 24.53687
258.3730 8.115967
258.8551 6.694824
259.3372 26.96936
259.8194 41.07727
260.3015 35.61511
260.7836 10.06885
261.2657 19.76965
261.7478 39.49963
262.2299 47.37830
262.7121 51.20728
263.1942 50.63489
263.6763 47.92944
264.1584 41.02148
264.6405 29.10669
265.1227 18.02893
265.6048 13.47217
266.0869 16.52405
266.5690 19.37903
267.0511 21.20447
267.5332 23.23193
268.0154 27.85645
268.4975 34.94763
268.9796 39.68005
269.4617 37.51660
269.9438 28.26013
270.4259 19.48145
270.9081 9.135498
271.3902 0.8370360
271.8723 1.342896
272.3544 2.448242
272.8365 6.872803
273.3186 8.182373
273.8008 6.379028
274.2829 4.086670
274.7650 0.1907960
275.2471 3.332397
275.7292 6.579468
276.2113 9.120850
276.6935 6.308105
277.1756 8.119019
277.6577 31.34314
278.1398 44.16968
278.6219 39.54431
279.1040 30.27295
279.5862 23.81860
280.0683 20.19739
280.5504 18.28625
281.0325 16.93042
281.5146 17.16956
281.9967 21.55408
282.4789 35.19006
282.9610 48.25513
283.4431 52.50024
283.9252 49.63550
284.4073 49.10181
284.8894 55.22864
285.3716 67.95984
285.8537 85.27832
286.3358 110.7874
286.8179 135.8619
287.3000 154.3882
287.7821 168.1620
288.2643 183.5463
288.7464 203.3358
289.2285 226.7593
289.7106 251.8217
290.1927 279.3108
290.6748 307.1233
291.1570 333.0870
291.6391 358.3490
292.1212 386.7277
292.6033 420.5363
293.0854 457.1118
293.5675 490.6274
294.0497 519.2920
294.5318 550.8890
295.0139 590.9309
295.4960 636.2740
295.9781 681.4362
296.4602 726.7124
296.9424 766.4088
297.4245 787.7115
297.9066 788.9629
298.3887 788.1198
298.8708 795.8694
299.3529 804.2938
299.8351 798.9546
300.3172 775.1980
300.7993 739.7327
301.2814 699.6321
301.7635 655.1337
302.2456 608.1423
302.7278 553.2892
303.2099 498.7034
303.6920 457.8568
304.1741 434.2548
304.6562 415.3019
305.1383 385.8551
305.6205 345.2769
306.1026 308.5275
306.5847 281.1525
307.0668 256.8514
307.5489 226.7701
308.0310 189.6384
308.5132 156.1498
308.9953 138.0555
309.4774 136.5842
309.9595 131.6997
310.4416 118.9598
310.9237 104.9526
311.4059 94.95837
311.8880 89.02087
312.3701 83.28320
312.8522 73.78064
313.3343 62.67126
313.8164 59.04468
314.2986 72.03796
314.7807 83.13818
315.2628 78.07739
315.7449 60.22083
316.2270 45.58240
316.7091 45.26123
317.1913 55.04089
317.6734 53.52539
318.1555 32.29297
318.6376 14.31360
319.1197 11.74463
319.6018 17.35461
320.0840 14.40625
320.5661 6.969727
321.0482 39.04980
321.5303 55.30188
322.0124 51.97034
322.4945 41.47449
322.9767 20.79248
323.4588 4.235718
323.9409 26.26111
324.4230 42.77771
324.9051 52.55249
325.3872 52.48486
325.8694 35.83862
326.3515 21.20740
326.8336 6.740723
327.3157 3.630737
327.7978 3.210693
328.2799 9.179199
328.7621 24.30579
329.2442 29.08569
329.7263 16.92175
330.2084 11.73254
330.6905 17.80359
331.1726 27.17834
331.6548 34.79224
332.1369 39.79932
332.6190 43.67590
333.1011 48.48596
333.5832 55.38965
334.0653 56.11914
334.5475 42.80762
335.0296 32.86743
335.5117 38.05920
335.9938 54.04041
336.4759 66.12146
336.9580 61.75989
337.4402 41.38989
337.9223 33.00598
338.4044 46.06323
338.8865 60.37793
339.3686 72.57922
339.8507 82.31616
340.3329 89.62268
340.8150 94.46338
341.2971 97.17358
341.7792 99.36865
342.2613 101.2362
342.7434 102.2987
343.2256 101.9895
343.7077 101.1432
344.1898 99.97485
344.6719 98.60938
345.1540 98.32214
345.6361 102.3743
346.1183 115.2782
346.6004 123.6177
347.0825 121.3174
347.5646 118.3468
348.0467 123.7646
348.5288 138.5078
349.0110 154.3776
349.4931 159.2324
349.9752 148.5172
350.4573 145.0630
350.9394 154.6002
351.4215 167.2686
351.9037 181.7775
352.3858 196.2039
352.8679 205.9398
353.3500 204.0665
353.8321 191.1707
354.3142 187.8593
354.7964 202.7885
355.2785 217.2383
355.7606 220.6144
356.2427 218.2507
356.7248 221.5366
357.2069 239.5819
357.6891 265.9485
358.1712 282.2806
358.6533 286.7239
359.1354 285.0020
359.6175 272.2483
360.0996 257.6300
360.5818 252.8507
361.0639 263.7130
361.5460 280.3815
362.0281 287.6714
362.5102 283.8191
362.9923 287.1510
363.4745 310.4667
363.9566 339.3026
364.4387 359.0033
364.9208 367.3203
365.4029 372.8464
365.8850 380.7235
366.3672 390.9520
366.8493 403.6682
367.3314 418.8574
367.8135 437.9326
368.2956 464.5411
368.7777 496.8364
369.2599 522.1064
369.7420 530.2565
370.2241 530.9431
370.7062 538.5002
371.1883 553.4249
371.6704 572.6675
372.1526 598.0649
372.6347 628.5632
373.1168 654.4585
373.5989 676.2914
374.0810 692.5870
374.5631 696.3903
375.0453 689.6254
375.5274 690.1382
376.0095 710.5626
376.4916 746.2195
376.9737 774.3855
377.4558 785.9812
377.9380 801.4636
378.4201 834.8026
378.9022 875.1133
379.3843 902.8555
379.8664 910.3796
380.3485 907.5322
380.8307 913.8867
381.3128 933.4573
381.7949 953.4138
382.2770 972.8328
382.7591 992.4709
383.2412 1014.468
383.7234 1038.640
384.2055 1060.173
384.6876 1072.672
385.1697 1073.001
385.6518 1077.445
386.1339 1088.201
386.6161 1100.306
387.0982 1113.827
387.5803 1126.926
388.0624 1134.938
388.5445 1133.518
389.0266 1124.117
389.5088 1122.633
389.9909 1143.676
390.4730 1155.877
390.9551 1146.808
391.4372 1128.329
391.9193 1116.141
392.4015 1117.209
392.8836 1124.557
393.3657 1124.287
393.8478 1115.036
394.3299 1101.072
394.8120 1081.533
395.2942 1058.862
395.7763 1035.363
396.2584 1011.014
396.7405 982.8451
397.2226 945.7356
397.7047 899.7515
398.1869 856.1733
398.6690 811.6260
399.1511 775.2441
399.6332 755.5071
400.1153 747.8921
400.5974 739.2705
401.0796 722.9797
401.5617 700.9921
402.0438 678.0157
402.5259 654.8046
403.0080 627.5677
403.4901 588.6820
403.9723 545.9258
404.4544 511.4778
404.9365 488.4733
405.4186 472.2900
405.9007 464.5854
406.3828 462.6963
406.8650 450.8029
407.3471 420.4625
407.8292 381.2241
408.3113 346.9744
408.7934 316.8582
409.2755 293.7687
409.7577 284.7458
410.2398 281.0929
410.7219 271.3766
411.2040 253.5591
411.6861 230.6475
412.1682 203.0465
412.6504 169.3735
413.1325 150.4535
413.6146 161.2600
414.0967 172.4697
414.5788 166.6501
415.0609 146.9565
415.5431 125.4049
416.0252 109.0820
416.5073 97.11914
416.9894 85.11426
417.4715 74.62427
417.9536 62.07605
418.4358 41.66809
418.9179 21.58179
419.4000 11.65149
419.8821 14.46118
420.3642 23.10474
420.8463 27.48022
421.3285 26.71680
421.8106 23.88989
422.2927 17.43408
422.7748 10.42908
423.2569 5.343018
423.7390 1.289551
424.2212 5.407593
424.7033 19.84131
425.1854 39.50537
425.6675 47.47998
426.1496 34.20142
426.6317 25.45312
427.1139 39.58142
427.5960 60.48035
428.0781 65.78674
428.5602 44.43677
429.0423 14.82239
429.5244 1.103271
430.0066 3.162476
430.4887 0.3758540
430.9708 11.84888
431.4529 23.66833
431.9350 27.89014
432.4171 24.33569
432.8993 16.99585
433.3814 3.572632
433.8635 11.34058
434.3456 18.52808
434.8277 16.17395
435.3098 10.94495
435.7920 7.048950
436.2741 4.876465
436.7562 6.468872
437.2383 15.51501
437.7204 25.02063
438.2025 30.04749
438.6847 32.04858
439.1668 35.45154
439.6489 42.39709
440.1310 52.18628
440.6131 63.00537
441.0952 77.43201
441.5774 89.29565
442.0595 96.93042
442.5416 102.7412
443.0237 106.4651
443.5058 109.3042
443.9879 117.0139
444.4701 137.9856
444.9522 175.6440
445.4343 201.5327
445.9164 197.9280
446.3985 200.3134
446.8806 227.6183
447.3628 268.1171
447.8449 298.7673
448.3270 305.8546
448.8091 298.9285
449.2912 301.6943
449.7733 316.7399
450.2555 334.3699
450.7375 354.9469
451.2197 375.3633
451.7018 391.1161
452.1839 401.5349
452.6660 416.4479
453.1481 443.4169
453.6302 481.5820
454.1124 528.8861
454.5945 590.6144
455.0766 650.1743
455.5587 686.9944
456.0408 709.2748
456.5229 741.0192
457.0051 793.8010
457.4872 853.8533
457.9693 909.2120
458.4514 960.9695
458.9335 1013.558
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1276.121 0.0000000E+00
