#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-05-24 16:33:07 +0300 (Thu, 24 May 2018) $ #$Revision: 884 $ #$URL: svn://172.16.1.111/rod/cif/1/00/03/1000363.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_1000363 loop_ _publ_author_name 'Cruciani, G.' 'Gualtieri, A.' _publ_section_title ; Dehydration dynamics of analcime by in situ synchrotron powder diffraction Sample at T = 298 K ; _journal_name_full 'American Mineralogist' _journal_page_first 112 _journal_page_last 119 _journal_volume 84 _journal_year 1999 _chemical_compound_source R050094 _chemical_formula_sum 'Al1.9 H4 Na1.95 O14 Si4.1' _chemical_name_mineral Analcime _space_group_IT_number 142 _symmetry_space_group_name_Hall '-I 4bd 2c' _symmetry_space_group_name_H-M 'I 41/a c d :2' _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 13.7295 _cell_length_b 13.7295 _cell_length_c 13.7036 _cell_volume 2583.117 _diffrn_ambient_temperature 298 _exptl_crystal_density_diffrn 2.259 _cod_original_sg_symbol_H-M 'I 41/a c d' _cod_original_formula_sum '(Si4.1 Al1.9) Na1.95 O14 H4' _cod_database_code 9002000 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type helium-neon _raman_measurement_device.excitation_laser_wavelength 780 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 12 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R050094.rod _rod_data_source.block 3500000 _rod_database.code 1000363 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9002000 COD http://www.crystallography.net/cod/9002000.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 130.6121 0.0000000E+00 131.0942 0.9445800 131.5764 0.7336430 132.0585 9.347168 132.5406 22.53735 133.0227 37.30566 133.5048 52.29126 133.9869 68.89233 134.4691 85.18945 134.9512 102.9231 135.4333 126.5781 135.9154 160.6470 136.3975 203.7334 136.8796 230.6570 137.3618 231.7048 137.8439 228.8848 138.3260 230.7954 138.8081 238.1104 139.2902 249.5532 139.7723 266.6814 140.2545 289.4795 140.7366 302.8601 141.2187 302.4521 141.7008 294.4390 142.1829 284.2263 142.6650 269.3345 143.1471 257.3972 143.6293 260.7222 144.1114 276.4531 144.5935 291.7715 145.0756 301.6687 145.5577 306.2278 146.0398 309.0662 146.5220 312.0435 147.0041 310.9465 147.4862 298.4395 147.9683 275.7664 148.4504 255.3359 148.9325 253.2690 149.4147 277.3638 149.8968 284.6438 150.3789 257.7524 150.8610 227.7905 151.3431 211.0151 151.8252 198.9248 152.3074 186.0496 152.7895 175.6431 153.2716 168.4414 153.7537 170.3694 154.2358 181.8843 154.7179 191.9089 155.2001 197.1331 155.6822 195.0938 156.1643 187.9385 156.6464 180.6453 157.1285 169.8486 157.6106 157.6519 158.0928 142.3875 158.5749 126.2314 159.0570 113.7874 159.5391 108.4883 160.0212 109.2827 160.5033 103.4387 160.9855 85.77783 161.4676 68.92969 161.9497 53.21411 162.4318 40.16357 162.9139 34.28638 163.3960 39.73340 163.8782 57.14819 164.3603 72.15381 164.8424 90.07690 165.3245 102.0300 165.8066 100.7324 166.2887 86.01904 166.7709 64.53979 167.2530 37.88672 167.7351 6.610107 168.2172 10.28076 168.6993 2.097656 169.1814 24.94434 169.6636 34.83691 170.1457 27.10107 170.6278 12.01270 171.1099 3.928955 171.5920 20.24878 172.0741 30.12036 172.5563 26.73804 173.0384 14.46973 173.5205 5.814209 174.0026 3.038818 174.4847 4.224609 174.9668 8.506348 175.4490 15.60364 175.9311 21.33826 176.4132 23.40039 176.8953 21.82361 177.3774 16.39185 177.8595 3.708984 178.3417 10.42236 178.8238 22.81384 179.3059 33.10071 179.7880 42.12305 180.2701 51.21069 180.7522 61.58435 181.2344 65.47913 181.7165 50.74622 182.1986 35.09570 182.6807 30.93115 183.1628 41.81885 183.6449 60.30823 184.1271 73.07666 184.6092 73.55896 185.0913 82.26440 185.5734 106.7299 186.0555 135.4584 186.5376 159.6106 187.0198 175.8669 187.5019 185.7672 187.9840 191.9948 188.4661 190.8542 188.9482 193.9574 189.4303 209.1271 189.9125 227.1168 190.3946 236.0457 190.8767 229.3994 191.3588 211.1094 191.8409 199.7897 192.3230 194.0459 192.8052 197.0186 193.2873 216.7449 193.7694 245.4547 194.2515 269.1630 194.7336 279.0780 195.2157 277.2128 195.6979 282.9800 196.1800 305.7250 196.6621 324.9371 197.1442 329.2255 197.6263 323.5693 198.1084 321.9401 198.5906 336.5051 199.0727 365.2783 199.5548 377.8646 200.0369 361.1443 200.5190 341.4236 201.0011 333.9365 201.4833 338.9128 201.9654 348.3118 202.4475 355.8564 202.9296 360.6323 203.4117 364.9939 203.8938 374.0554 204.3760 381.3470 204.8581 378.7018 205.3402 365.2543 205.8223 350.5623 206.3044 341.8394 206.7865 338.0688 207.2687 335.9808 207.7508 336.7991 208.2329 338.3428 208.7150 336.8156 209.1971 331.0721 209.6792 325.8789 210.1614 326.1047 210.6435 329.8762 211.1256 333.2395 211.6077 335.1710 212.0898 335.8766 212.5719 336.7399 213.0541 340.5022 213.5362 338.5571 214.0183 319.8893 214.5004 290.6830 214.9825 266.5630 215.4646 257.3135 215.9468 260.6417 216.4289 267.8014 216.9110 282.8358 217.3931 295.8220 217.8752 298.5964 218.3573 294.4991 218.8395 293.1483 219.3216 304.9694 219.8037 327.6438 220.2858 338.8378 220.7679 331.7761 221.2500 319.9663 221.7322 305.9661 222.2143 291.9318 222.6964 283.1627 223.1785 287.5983 223.6606 306.2070 224.1427 314.4474 224.6249 300.2456 225.1070 285.2213 225.5891 278.0092 226.0712 277.2401 226.5533 278.4601 227.0354 277.0498 227.5176 273.1105 227.9997 261.4585 228.4818 224.8533 228.9639 194.1935 229.4460 188.2378 229.9281 203.2771 230.4103 219.8173 230.8924 214.6548 231.3745 178.5009 231.8566 161.3492 232.3387 176.9569 232.8208 197.6594 233.3030 216.1847 233.7851 229.1732 234.2672 232.2322 234.7493 218.3499 235.2314 180.0580 235.7135 153.6813 236.1957 140.9094 236.6778 135.7153 237.1599 140.6796 237.6420 152.7645 238.1241 161.6421 238.6062 154.1201 239.0884 122.2468 239.5705 99.55469 240.0526 87.46704 240.5347 81.56323 241.0168 82.89368 241.4989 89.73608 241.9811 95.71838 242.4632 93.19861 242.9453 79.02698 243.4274 65.46143 243.9095 48.03760 244.3916 34.32837 244.8738 31.69983 245.3559 39.81226 245.8380 49.77991 246.3201 51.00220 246.8022 39.63037 247.2843 31.35034 247.7665 24.72839 248.2486 21.68127 248.7307 26.85132 249.2128 39.39929 249.6949 50.33337 250.1770 48.15027 250.6592 25.83765 251.1413 15.91113 251.6234 28.94458 252.1055 46.36011 252.5876 56.31006 253.0697 56.63184 253.5519 48.74268 254.0340 32.12732 254.5161 2.023926 254.9982 14.84448 255.4803 10.37939 255.9624 1.641968 256.4445 13.67651 256.9267 23.87671 257.4088 28.92517 257.8909 24.53687 258.3730 8.115967 258.8551 6.694824 259.3372 26.96936 259.8194 41.07727 260.3015 35.61511 260.7836 10.06885 261.2657 19.76965 261.7478 39.49963 262.2299 47.37830 262.7121 51.20728 263.1942 50.63489 263.6763 47.92944 264.1584 41.02148 264.6405 29.10669 265.1227 18.02893 265.6048 13.47217 266.0869 16.52405 266.5690 19.37903 267.0511 21.20447 267.5332 23.23193 268.0154 27.85645 268.4975 34.94763 268.9796 39.68005 269.4617 37.51660 269.9438 28.26013 270.4259 19.48145 270.9081 9.135498 271.3902 0.8370360 271.8723 1.342896 272.3544 2.448242 272.8365 6.872803 273.3186 8.182373 273.8008 6.379028 274.2829 4.086670 274.7650 0.1907960 275.2471 3.332397 275.7292 6.579468 276.2113 9.120850 276.6935 6.308105 277.1756 8.119019 277.6577 31.34314 278.1398 44.16968 278.6219 39.54431 279.1040 30.27295 279.5862 23.81860 280.0683 20.19739 280.5504 18.28625 281.0325 16.93042 281.5146 17.16956 281.9967 21.55408 282.4789 35.19006 282.9610 48.25513 283.4431 52.50024 283.9252 49.63550 284.4073 49.10181 284.8894 55.22864 285.3716 67.95984 285.8537 85.27832 286.3358 110.7874 286.8179 135.8619 287.3000 154.3882 287.7821 168.1620 288.2643 183.5463 288.7464 203.3358 289.2285 226.7593 289.7106 251.8217 290.1927 279.3108 290.6748 307.1233 291.1570 333.0870 291.6391 358.3490 292.1212 386.7277 292.6033 420.5363 293.0854 457.1118 293.5675 490.6274 294.0497 519.2920 294.5318 550.8890 295.0139 590.9309 295.4960 636.2740 295.9781 681.4362 296.4602 726.7124 296.9424 766.4088 297.4245 787.7115 297.9066 788.9629 298.3887 788.1198 298.8708 795.8694 299.3529 804.2938 299.8351 798.9546 300.3172 775.1980 300.7993 739.7327 301.2814 699.6321 301.7635 655.1337 302.2456 608.1423 302.7278 553.2892 303.2099 498.7034 303.6920 457.8568 304.1741 434.2548 304.6562 415.3019 305.1383 385.8551 305.6205 345.2769 306.1026 308.5275 306.5847 281.1525 307.0668 256.8514 307.5489 226.7701 308.0310 189.6384 308.5132 156.1498 308.9953 138.0555 309.4774 136.5842 309.9595 131.6997 310.4416 118.9598 310.9237 104.9526 311.4059 94.95837 311.8880 89.02087 312.3701 83.28320 312.8522 73.78064 313.3343 62.67126 313.8164 59.04468 314.2986 72.03796 314.7807 83.13818 315.2628 78.07739 315.7449 60.22083 316.2270 45.58240 316.7091 45.26123 317.1913 55.04089 317.6734 53.52539 318.1555 32.29297 318.6376 14.31360 319.1197 11.74463 319.6018 17.35461 320.0840 14.40625 320.5661 6.969727 321.0482 39.04980 321.5303 55.30188 322.0124 51.97034 322.4945 41.47449 322.9767 20.79248 323.4588 4.235718 323.9409 26.26111 324.4230 42.77771 324.9051 52.55249 325.3872 52.48486 325.8694 35.83862 326.3515 21.20740 326.8336 6.740723 327.3157 3.630737 327.7978 3.210693 328.2799 9.179199 328.7621 24.30579 329.2442 29.08569 329.7263 16.92175 330.2084 11.73254 330.6905 17.80359 331.1726 27.17834 331.6548 34.79224 332.1369 39.79932 332.6190 43.67590 333.1011 48.48596 333.5832 55.38965 334.0653 56.11914 334.5475 42.80762 335.0296 32.86743 335.5117 38.05920 335.9938 54.04041 336.4759 66.12146 336.9580 61.75989 337.4402 41.38989 337.9223 33.00598 338.4044 46.06323 338.8865 60.37793 339.3686 72.57922 339.8507 82.31616 340.3329 89.62268 340.8150 94.46338 341.2971 97.17358 341.7792 99.36865 342.2613 101.2362 342.7434 102.2987 343.2256 101.9895 343.7077 101.1432 344.1898 99.97485 344.6719 98.60938 345.1540 98.32214 345.6361 102.3743 346.1183 115.2782 346.6004 123.6177 347.0825 121.3174 347.5646 118.3468 348.0467 123.7646 348.5288 138.5078 349.0110 154.3776 349.4931 159.2324 349.9752 148.5172 350.4573 145.0630 350.9394 154.6002 351.4215 167.2686 351.9037 181.7775 352.3858 196.2039 352.8679 205.9398 353.3500 204.0665 353.8321 191.1707 354.3142 187.8593 354.7964 202.7885 355.2785 217.2383 355.7606 220.6144 356.2427 218.2507 356.7248 221.5366 357.2069 239.5819 357.6891 265.9485 358.1712 282.2806 358.6533 286.7239 359.1354 285.0020 359.6175 272.2483 360.0996 257.6300 360.5818 252.8507 361.0639 263.7130 361.5460 280.3815 362.0281 287.6714 362.5102 283.8191 362.9923 287.1510 363.4745 310.4667 363.9566 339.3026 364.4387 359.0033 364.9208 367.3203 365.4029 372.8464 365.8850 380.7235 366.3672 390.9520 366.8493 403.6682 367.3314 418.8574 367.8135 437.9326 368.2956 464.5411 368.7777 496.8364 369.2599 522.1064 369.7420 530.2565 370.2241 530.9431 370.7062 538.5002 371.1883 553.4249 371.6704 572.6675 372.1526 598.0649 372.6347 628.5632 373.1168 654.4585 373.5989 676.2914 374.0810 692.5870 374.5631 696.3903 375.0453 689.6254 375.5274 690.1382 376.0095 710.5626 376.4916 746.2195 376.9737 774.3855 377.4558 785.9812 377.9380 801.4636 378.4201 834.8026 378.9022 875.1133 379.3843 902.8555 379.8664 910.3796 380.3485 907.5322 380.8307 913.8867 381.3128 933.4573 381.7949 953.4138 382.2770 972.8328 382.7591 992.4709 383.2412 1014.468 383.7234 1038.640 384.2055 1060.173 384.6876 1072.672 385.1697 1073.001 385.6518 1077.445 386.1339 1088.201 386.6161 1100.306 387.0982 1113.827 387.5803 1126.926 388.0624 1134.938 388.5445 1133.518 389.0266 1124.117 389.5088 1122.633 389.9909 1143.676 390.4730 1155.877 390.9551 1146.808 391.4372 1128.329 391.9193 1116.141 392.4015 1117.209 392.8836 1124.557 393.3657 1124.287 393.8478 1115.036 394.3299 1101.072 394.8120 1081.533 395.2942 1058.862 395.7763 1035.363 396.2584 1011.014 396.7405 982.8451 397.2226 945.7356 397.7047 899.7515 398.1869 856.1733 398.6690 811.6260 399.1511 775.2441 399.6332 755.5071 400.1153 747.8921 400.5974 739.2705 401.0796 722.9797 401.5617 700.9921 402.0438 678.0157 402.5259 654.8046 403.0080 627.5677 403.4901 588.6820 403.9723 545.9258 404.4544 511.4778 404.9365 488.4733 405.4186 472.2900 405.9007 464.5854 406.3828 462.6963 406.8650 450.8029 407.3471 420.4625 407.8292 381.2241 408.3113 346.9744 408.7934 316.8582 409.2755 293.7687 409.7577 284.7458 410.2398 281.0929 410.7219 271.3766 411.2040 253.5591 411.6861 230.6475 412.1682 203.0465 412.6504 169.3735 413.1325 150.4535 413.6146 161.2600 414.0967 172.4697 414.5788 166.6501 415.0609 146.9565 415.5431 125.4049 416.0252 109.0820 416.5073 97.11914 416.9894 85.11426 417.4715 74.62427 417.9536 62.07605 418.4358 41.66809 418.9179 21.58179 419.4000 11.65149 419.8821 14.46118 420.3642 23.10474 420.8463 27.48022 421.3285 26.71680 421.8106 23.88989 422.2927 17.43408 422.7748 10.42908 423.2569 5.343018 423.7390 1.289551 424.2212 5.407593 424.7033 19.84131 425.1854 39.50537 425.6675 47.47998 426.1496 34.20142 426.6317 25.45312 427.1139 39.58142 427.5960 60.48035 428.0781 65.78674 428.5602 44.43677 429.0423 14.82239 429.5244 1.103271 430.0066 3.162476 430.4887 0.3758540 430.9708 11.84888 431.4529 23.66833 431.9350 27.89014 432.4171 24.33569 432.8993 16.99585 433.3814 3.572632 433.8635 11.34058 434.3456 18.52808 434.8277 16.17395 435.3098 10.94495 435.7920 7.048950 436.2741 4.876465 436.7562 6.468872 437.2383 15.51501 437.7204 25.02063 438.2025 30.04749 438.6847 32.04858 439.1668 35.45154 439.6489 42.39709 440.1310 52.18628 440.6131 63.00537 441.0952 77.43201 441.5774 89.29565 442.0595 96.93042 442.5416 102.7412 443.0237 106.4651 443.5058 109.3042 443.9879 117.0139 444.4701 137.9856 444.9522 175.6440 445.4343 201.5327 445.9164 197.9280 446.3985 200.3134 446.8806 227.6183 447.3628 268.1171 447.8449 298.7673 448.3270 305.8546 448.8091 298.9285 449.2912 301.6943 449.7733 316.7399 450.2555 334.3699 450.7375 354.9469 451.2197 375.3633 451.7018 391.1161 452.1839 401.5349 452.6660 416.4479 453.1481 443.4169 453.6302 481.5820 454.1124 528.8861 454.5945 590.6144 455.0766 650.1743 455.5587 686.9944 456.0408 709.2748 456.5229 741.0192 457.0051 793.8010 457.4872 853.8533 457.9693 909.2120 458.4514 960.9695 458.9335 1013.558 459.4156 1066.930 459.8978 1125.115 460.3799 1201.023 460.8620 1304.090 461.3441 1403.457 461.8262 1490.585 462.3083 1573.219 462.7905 1656.826 463.2726 1743.464 463.7547 1835.198 464.2368 1934.216 464.7189 2039.877 465.2010 2157.462 465.6832 2285.746 466.1653 2425.342 466.6474 2579.612 467.1295 2744.270 467.6116 2913.937 468.0938 3083.873 468.5759 3260.341 469.0580 3457.659 469.5401 3684.420 470.0222 3909.337 470.5043 4115.892 470.9865 4326.156 471.4686 4557.663 471.9507 4809.690 472.4328 5068.117 472.9149 5315.329 473.3970 5558.799 473.8792 5829.116 474.3613 6134.677 474.8434 6445.306 475.3255 6745.463 475.8076 7036.889 476.2897 7326.708 476.7719 7621.934 477.2540 7908.051 477.7361 8173.689 478.2182 8422.023 478.7003 8664.779 479.1824 8906.552 479.6646 9138.851 480.1467 9348.833 480.6288 9542.662 481.1109 9691.797 481.5930 9796.077 482.0751 9853.134 482.5573 9853.779 483.0394 9803.208 483.5215 9720.966 484.0036 9621.707 484.4857 9503.479 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657.1264 511.9664 628.1274 512.4485 592.1224 512.9306 560.1976 513.4127 534.8497 513.8948 514.7636 514.3770 503.8154 514.8591 499.7930 515.3412 488.2570 515.8233 457.3989 516.3054 411.0985 516.7875 376.0444 517.2697 359.2227 517.7518 346.1573 518.2339 338.5269 518.7160 332.4982 519.1981 322.8507 519.6802 309.1846 520.1624 296.8922 520.6445 294.1161 521.1266 301.3109 521.6087 298.7510 522.0908 281.1116 522.5729 261.4041 523.0551 244.1456 523.5372 229.1001 524.0193 215.7624 524.5014 203.5328 524.9835 194.2151 525.4656 192.9034 525.9478 197.2520 526.4299 192.9135 526.9120 173.0809 527.3941 151.8489 527.8762 148.9951 528.3583 165.6114 528.8405 171.7839 529.3226 155.9374 529.8047 136.6454 530.2868 123.8251 530.7689 117.5921 531.2510 116.8123 531.7332 121.3440 532.2153 128.6573 532.6974 132.7756 533.1795 134.9034 533.6616 130.9981 534.1437 115.3367 534.6259 99.32056 535.1080 91.06567 535.5901 89.36182 536.0722 87.34918 536.5543 79.32751 537.0364 67.88458 537.5186 61.75464 538.0007 62.29614 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