#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-05-24 16:33:39 +0300 (Thu, 24 May 2018) $ #$Revision: 892 $ #$URL: svn://172.16.1.111/rod/cif/1/00/03/1000370.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_1000370 loop_ _publ_author_name 'Cruciani, G.' 'Gualtieri, A.' _publ_section_title ; Dehydration dynamics of analcime by in situ synchrotron powder diffraction Sample at T = 298 K ; _journal_name_full 'American Mineralogist' _journal_page_first 112 _journal_page_last 119 _journal_volume 84 _journal_year 1999 _chemical_compound_source R060023 _chemical_formula_sum 'Al1.9 H4 Na1.95 O14 Si4.1' _chemical_name_mineral Analcime _space_group_IT_number 142 _symmetry_space_group_name_Hall '-I 4bd 2c' _symmetry_space_group_name_H-M 'I 41/a c d :2' _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 13.7295 _cell_length_b 13.7295 _cell_length_c 13.7036 _cell_volume 2583.117 _diffrn_ambient_temperature 298 _exptl_crystal_density_diffrn 2.259 _cod_original_sg_symbol_H-M 'I 41/a c d' _cod_original_formula_sum '(Si4.1 Al1.9) Na1.95 O14 H4' _cod_database_code 9002000 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type helium-neon _raman_measurement_device.excitation_laser_wavelength 780 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 12 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R060023.rod _rod_data_source.block 3500000 _rod_database.code 1000370 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9002000 COD http://www.crystallography.net/cod/9002000.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 152.3061 0.0000000E+00 152.7882 0.7815630 153.2704 1.504089 153.7525 2.193916 154.2346 2.554825 154.7167 1.285400 155.1988 0.1327060 155.6809 7.1709000E-02 156.1631 0.6843110 156.6452 1.750885 157.1273 2.263359 157.6094 2.170479 158.0915 2.083817 158.5736 1.762352 159.0558 1.418793 159.5379 1.142693 160.0200 1.028175 160.5021 1.450333 160.9842 1.939667 161.4663 2.967262 161.9485 3.642509 162.4306 3.344803 162.9127 2.625710 163.3948 2.065895 163.8769 1.838997 164.3590 1.881432 164.8412 1.789558 165.3233 1.585167 165.8054 1.593185 166.2875 1.922737 166.7696 2.613640 167.2517 2.789810 167.7339 1.604828 168.2160 0.1772610 168.6981 0.2658620 169.1802 0.4711230 169.6623 1.431221 170.1444 1.680527 170.6266 1.050064 171.1087 0.4708940 171.5908 0.3557590 172.0729 0.3827210 172.5550 0.2974400 173.0371 7.0039998E-03 173.5193 0.2906340 174.0014 0.2637710 174.4835 0.2745510 174.9656 0.6853260 175.4477 0.8051380 175.9298 0.8110430 176.4120 0.8893590 176.8941 1.135391 177.3762 1.436188 177.8583 1.372276 178.3404 0.3374710 178.8225 0.2155300 179.3047 0.2047420 179.7868 1.038307 180.2689 1.609863 180.7510 1.552017 181.2331 1.036842 181.7152 0.8248830 182.1974 1.229195 182.6795 1.576912 183.1616 1.753120 183.6437 1.797714 184.1258 1.750061 184.6079 1.601082 185.0900 1.408180 185.5722 1.573051 186.0543 2.604126 186.5364 3.381393 187.0185 3.233284 187.5006 2.429169 187.9827 1.809807 188.4649 1.885971 188.9470 2.587090 189.4291 3.350975 189.9112 4.592964 190.3933 5.547188 190.8754 5.485550 191.3576 4.483635 191.8397 3.571472 192.3218 3.447403 192.8039 3.837532 193.2860 4.066170 193.7681 3.990242 194.2503 3.796936 194.7324 3.616150 195.2145 3.421867 195.6966 3.410316 196.1787 4.056084 196.6608 4.865807 197.1430 5.218056 197.6251 4.750618 198.1072 3.919594 198.5893 3.480759 199.0714 3.550636 199.5535 3.783646 200.0357 4.222374 200.5178 4.665253 200.9999 4.785149 201.4820 4.327072 201.9641 3.579727 202.4462 3.405289 202.9284 4.251053 203.4105 4.914246 203.8926 4.990776 204.3747 4.760612 204.8568 4.520271 205.3389 4.417015 205.8211 4.408394 206.3032 4.349915 206.7853 4.199921 207.2674 4.098442 207.7495 3.991646 208.2316 3.971664 208.7138 4.194611 209.1959 4.812881 209.6780 5.733154 210.1601 6.224358 210.6422 5.590256 211.1243 5.118942 211.6065 5.098793 212.0886 5.388947 212.5707 5.728912 213.0528 5.918449 213.5349 5.969543 214.0170 6.265770 214.4992 7.137650 214.9813 7.873207 215.4634 8.193687 215.9455 8.233955 216.4276 8.314766 216.9097 8.659218 217.3919 9.196281 217.8740 9.330032 218.3561 8.712975 218.8382 8.163460 219.3203 7.997589 219.8024 8.151611 220.2845 8.435852 220.7667 8.758514 221.2488 9.093063 221.7309 9.347847 222.2130 9.521385 222.6951 9.647011 223.1772 9.704384 223.6594 9.698929 224.1415 9.699379 224.6236 9.738525 225.1057 9.824249 225.5878 9.953918 226.0699 10.16261 226.5521 10.34572 227.0342 10.47787 227.5163 10.54899 227.9984 10.64600 228.4805 10.90991 228.9626 11.16298 229.4448 11.06411 229.9269 10.38127 230.4090 9.670494 230.8911 9.500511 231.3732 9.863472 231.8553 10.07493 232.3375 9.725342 232.8196 9.111893 233.3017 8.597786 233.7838 8.224869 234.2659 7.973991 234.7480 7.907913 235.2302 8.060623 235.7123 8.061455 236.1944 7.551758 236.6765 6.927658 237.1586 6.622627 237.6407 6.758263 238.1229 6.923004 238.6050 6.521217 239.0871 5.401527 239.5692 4.523270 240.0513 4.374756 240.5334 4.437553 241.0156 4.407372 241.4977 4.214127 241.9798 3.908211 242.4619 3.503380 242.9440 2.925091 243.4261 2.533150 243.9083 2.687019 244.3904 2.849182 244.8725 2.593197 245.3546 1.859161 245.8367 1.025917 246.3188 0.6540300 246.8010 0.9445420 247.2831 1.085281 247.7652 0.8771130 248.2473 0.6078000 248.7294 0.4367180 249.2115 0.3934400 249.6937 0.4192810 250.1758 0.4608150 250.6579 0.5579830 251.1400 0.5634500 251.6221 0.4013440 252.1042 0.2148360 252.5864 7.1312003E-02 253.0685 1.6029000E-02 253.5506 5.4439999E-02 254.0327 4.0470000E-02 254.5148 6.2587999E-02 254.9969 8.8261001E-02 255.4790 2.7851000E-02 255.9612 0.1558490 256.4433 0.2373310 256.9254 0.2603610 257.4075 0.2394710 257.8896 0.1898650 258.3718 0.1175310 258.8539 7.2249998E-03 259.3360 0.3277630 259.8181 0.5640410 260.3002 0.4857250 260.7823 0.1628610 261.2645 0.1080400 261.7466 3.7632000E-02 262.2287 0.4394870 262.7108 0.7560460 263.1929 0.8300020 263.6750 0.8630910 264.1572 0.9797590 264.6393 1.135086 265.1214 1.164436 265.6035 0.9061160 266.0856 0.3457980 266.5677 4.4013999E-02 267.0499 0.1435590 267.5320 0.2880860 268.0141 0.3607440 268.4962 0.3542210 268.9783 0.2812080 269.4604 0.1341320 269.9426 7.9937004E-02 270.4247 0.1048660 270.9068 0.2498090 271.3889 0.5411340 271.8710 0.5596310 272.3531 0.3798980 272.8352 0.1778720 273.3174 3.3229999E-02 273.7995 3.8288001E-02 274.2816 5.3745002E-02 274.7637 0.4898070 275.2458 0.8473210 275.7279 0.9756620 276.2101 0.9349140 276.6922 0.8219640 277.1743 0.6543460 277.6564 0.4922410 278.1385 0.5454710 278.6206 0.9746930 279.1028 1.277248 279.5849 1.111584 280.0670 0.7534830 280.5491 0.7393150 281.0312 1.310638 281.5133 2.158108 281.9955 2.655674 282.4776 2.698956 282.9597 2.851784 283.4418 3.306515 283.9239 3.942047 284.4060 4.594276 284.8882 5.234489 285.3703 5.820004 285.8524 6.207893 286.3345 6.354736 286.8166 6.763660 287.2987 7.635654 287.7809 8.786453 288.2630 10.01273 288.7451 11.27782 289.2272 12.56213 289.7093 13.75877 290.1914 14.88957 290.6736 16.30383 291.1557 18.18594 291.6378 20.31161 292.1199 22.50019 292.6020 24.73418 293.0841 26.91044 293.5663 28.83604 294.0484 30.61123 294.5305 32.71463 295.0126 35.70096 295.4947 38.67862 295.9768 40.87514 296.4590 42.28492 296.9411 43.29865 297.4232 44.15433 297.9053 44.73083 298.3874 44.83450 298.8695 44.46540 299.3517 43.60958 299.8338 42.21364 300.3159 40.29848 300.7980 37.97227 301.2801 35.14054 301.7622 32.03643 302.2444 29.14402 302.7265 26.47742 303.2086 23.96015 303.6907 21.49212 304.1728 19.11757 304.6549 17.07044 305.1371 15.50567 305.6192 14.16653 306.1013 12.62870 306.5834 10.84788 307.0655 9.254158 307.5476 8.079922 308.0298 7.221581 308.5119 6.461071 308.9940 5.783436 309.4761 5.116142 309.9582 4.240459 310.4403 3.196857 310.9225 2.540665 311.4046 2.810810 311.8867 3.455402 312.3688 3.567360 312.8509 2.985470 313.3330 2.242489 313.8152 1.752018 314.2973 1.462849 314.7794 1.245457 315.2615 1.099712 315.7436 1.004333 316.2257 0.9762120 316.7079 1.020824 317.1900 0.9874990 317.6721 0.7263530 318.1542 0.3234560 318.6363 3.7610000E-03 319.1184 0.1720430 319.6006 0.3101960 320.0827 0.5228540 320.5648 0.7953190 321.0469 0.9724920 321.5290 0.9564780 322.0111 0.8274460 322.4933 0.7507780 322.9754 0.7477910 323.4575 0.7410700 323.9396 0.6971930 324.4217 0.6213230 324.9038 0.4906500 325.3860 0.2440640 325.8681 5.1456001E-02 326.3502 0.2776450 326.8323 0.9425090 327.3144 1.296398 327.7965 0.8234790 328.2787 6.5425999E-02 328.7608 0.6892700 329.2429 0.9149860 329.7250 0.9304850 330.2071 0.8474660 330.6892 0.6826400 331.1714 0.5436250 331.6535 0.4316020 332.1356 0.3801800 332.6177 0.4586140 333.0998 0.6610870 333.5819 0.8253440 334.0641 0.7246480 334.5462 0.5166780 335.0283 0.7639080 335.5104 2.063545 335.9925 3.256500 336.4746 3.343231 336.9568 2.569515 337.4389 2.104885 337.9210 2.579872 338.4031 3.589157 338.8852 4.146263 339.3673 4.080605 339.8495 4.034607 340.3316 4.311417 340.8137 4.777054 341.2958 5.167679 341.7779 5.400826 342.2600 5.552040 342.7421 5.744095 343.2242 5.993683 343.7064 6.153053 344.1885 5.981140 344.6706 5.812325 345.1527 6.114075 345.6348 6.950050 346.1169 7.837837 346.5991 8.330711 347.0812 8.398865 347.5633 8.533211 348.0454 8.681999 348.5275 8.943047 349.0096 9.455063 349.4918 10.16818 349.9739 10.82639 350.4560 11.24783 350.9381 11.50685 351.4202 11.97964 351.9023 13.01981 352.3845 13.82932 352.8666 13.99497 353.3487 13.79020 353.8308 13.70889 354.3129 13.94871 354.7950 14.36310 355.2772 14.66322 355.7593 14.73827 356.2414 14.94281 356.7235 15.37462 357.2056 15.91458 357.6877 16.43221 358.1699 16.90932 358.6520 17.43968 359.1341 18.16904 359.6162 19.18659 360.0983 19.85430 360.5804 19.74767 361.0626 19.71265 361.5447 20.36241 362.0268 21.53236 362.5089 22.56210 362.9910 22.96088 363.4731 22.82542 363.9553 23.03671 364.4374 23.60317 364.9195 24.49915 365.4016 26.00262 365.8837 27.73129 366.3658 29.17403 366.8480 30.12796 367.3301 30.76020 367.8122 31.41253 368.2943 32.08986 368.7764 32.76793 369.2585 33.33720 369.7407 33.98717 370.2228 34.99456 370.7049 36.31606 371.1870 37.52572 371.6691 38.08180 372.1512 37.80167 372.6334 37.96602 373.1155 39.10257 373.5976 40.16154 374.0797 40.55091 374.5618 40.56069 375.0439 40.89943 375.5261 42.08727 376.0082 43.89664 376.4903 45.11787 376.9724 45.16436 377.4545 45.45055 377.9366 46.53986 378.4188 47.79440 378.9009 48.49615 379.3830 48.42431 379.8651 48.05297 380.3472 48.09789 380.8293 48.62233 381.3115 49.34571 381.7936 50.62559 382.2757 51.79371 382.7578 52.39603 383.2399 52.50250 383.7220 52.58173 384.2042 53.06812 384.6863 53.89664 385.1684 54.42571 385.6505 54.54108 386.1326 54.64763 386.6147 54.85917 387.0969 55.12831 387.5790 55.37811 388.0611 55.55394 388.5432 55.73828 389.0253 56.16264 389.5074 56.94154 389.9896 57.46117 390.4717 57.41476 390.9538 57.06521 391.4359 56.52268 391.9180 55.79180 392.4001 55.13797 392.8823 54.89782 393.3644 54.97876 393.8465 54.76800 394.3286 54.03651 394.8107 53.22045 395.2928 52.75436 395.7750 52.53128 396.2571 52.15218 396.7392 51.28204 397.2213 50.25445 397.7034 49.66018 398.1855 49.55915 398.6677 49.22765 399.1498 48.14840 399.6319 46.56796 400.1140 45.10984 400.5961 43.82296 401.0782 42.62351 401.5604 41.40660 402.0425 40.22743 402.5246 39.29519 403.0067 38.75151 403.4888 38.27269 403.9709 37.34452 404.4531 35.93781 404.9352 34.47345 405.4173 32.94025 405.8994 31.43015 406.3815 30.13667 406.8636 29.03902 407.3458 27.76689 407.8279 25.95604 408.3100 23.66424 408.7921 21.89060 409.2742 20.93676 409.7563 20.09689 410.2385 19.17548 410.7206 18.18928 411.2027 17.21365 411.6848 16.28510 412.1669 15.32797 412.6490 14.17107 413.1311 12.49480 413.6133 11.19270 414.0954 10.57625 414.5775 10.09317 415.0596 9.326439 415.5417 8.257805 416.0238 7.141495 416.5060 6.221130 416.9881 5.507851 417.4702 4.694672 417.9523 3.456512 418.4344 2.466713 418.9165 2.016975 419.3987 1.878716 419.8808 1.736458 420.3629 1.450035 420.8450 1.054237 421.3271 0.5926900 421.8092 2.9785000E-02 422.2914 0.4667210 422.7735 0.5136340 423.2556 0.5052030 423.7377 0.6597370 424.2198 0.9791790 424.7019 1.307922 425.1841 1.498703 425.6662 1.567642 426.1483 1.690079 426.6304 1.919991 427.1125 2.112961 427.5946 2.292145 428.0768 2.377594 428.5589 2.199707 429.0410 1.609230 429.5231 0.9345470 430.0052 0.6146010 430.4873 0.6559980 430.9695 0.7435910 431.4516 0.8772510 431.9337 0.9221120 432.4158 0.7122730 432.8979 0.2449040 433.3800 0.2125170 433.8622 0.5371930 434.3443 0.7673110 434.8264 0.9264760 435.3085 0.9977800 435.7906 1.170746 436.2727 1.620636 436.7549 2.305550 437.2370 2.965157 437.7191 3.522270 438.2012 4.120216 438.6833 4.934845 439.1654 5.851273 439.6476 6.570099 440.1297 6.963631 440.6118 7.181343 441.0939 7.452065 441.5760 7.727570 442.0581 8.212471 442.5403 9.019989 443.0224 9.966599 443.5045 10.98466 443.9866 12.02496 444.4687 12.93109 444.9508 13.53503 445.4330 13.89684 445.9151 14.72661 446.3972 16.42825 446.8793 18.12488 447.3614 19.77097 447.8435 21.31045 448.3257 22.57915 448.8078 23.56171 449.2899 24.60090 449.7720 26.27845 450.2541 28.86059 450.7362 31.14214 451.2184 32.62218 451.7005 34.26485 452.1826 36.44373 452.6647 39.10649 453.1468 42.10378 453.6289 45.41489 454.1111 48.92076 454.5932 52.20255 455.0753 55.11686 455.5574 58.31145 456.0395 62.04803 456.5216 66.13538 457.0038 70.40148 457.4859 74.85496 457.9680 79.61562 458.4501 84.81836 458.9322 90.42725 459.4143 96.24895 459.8965 102.2770 460.3786 108.4423 460.8607 114.5873 461.3428 120.8194 461.8249 127.4872 462.3070 134.5242 462.7892 142.1421 463.2713 150.6964 463.7534 160.0102 464.2355 169.2715 464.7176 178.1354 465.1997 186.9912 465.6819 196.6477 466.1640 207.2176 466.6461 217.8803 467.1282 228.0685 467.6103 238.6582 468.0924 250.5697 468.5746 263.6551 469.0567 277.0494 469.5388 289.9922 470.0209 302.6394 470.5030 316.5571 470.9851 332.5311 471.4673 348.7678 471.9494 364.8070 472.4315 381.1410 472.9136 398.3419 473.3957 416.4769 473.8778 435.1278 474.3600 453.5997 474.8421 471.6437 475.3242 491.3557 475.8063 515.1840 476.2884 538.2414 476.7705 558.9525 477.2527 577.8706 477.7348 596.1466 478.2169 614.4171 478.6990 631.8834 479.1811 647.5389 479.6632 661.6183 480.1454 672.2897 480.6275 678.6981 481.1096 681.7318 481.5917 682.7314 482.0738 681.5562 482.5559 676.9964 483.0380 668.0807 483.5201 655.5778 484.0023 640.2689 484.4844 622.1370 484.9665 602.8159 485.4486 583.4097 485.9307 563.2838 486.4128 540.6485 486.8950 514.5956 487.3771 488.3796 487.8592 462.4252 488.3413 437.2334 488.8234 413.3833 489.3055 390.8866 489.7877 369.4458 490.2698 348.8429 490.7519 329.0078 491.2340 310.4637 491.7161 292.9455 492.1982 276.5427 492.6804 261.6084 493.1625 247.6199 493.6446 233.6799 494.1267 219.4517 494.6088 205.6630 495.0909 193.6988 495.5731 184.0647 496.0552 174.6752 496.5373 165.3073 497.0194 156.4138 497.5015 148.3278 497.9836 140.9095 498.4658 133.8356 498.9479 126.9642 499.4300 120.2862 499.9121 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