#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 16:33:39 +0300 (Thu, 24 May 2018) $
#$Revision: 892 $
#$URL: svn://172.16.1.111/rod/cif/1/00/03/1000370.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000370
loop_
_publ_author_name
'Cruciani, G.'
'Gualtieri, A.'
_publ_section_title
;
 Dehydration dynamics of analcime by in situ synchrotron powder
 diffraction Sample at T = 298 K
;
_journal_name_full               'American Mineralogist'
_journal_page_first              112
_journal_page_last               119
_journal_volume                  84
_journal_year                    1999
_chemical_compound_source        R060023
_chemical_formula_sum            'Al1.9 H4 Na1.95 O14 Si4.1'
_chemical_name_mineral           Analcime
_space_group_IT_number           142
_symmetry_space_group_name_Hall  '-I 4bd 2c'
_symmetry_space_group_name_H-M   'I 41/a c d :2'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   13.7295
_cell_length_b                   13.7295
_cell_length_c                   13.7036
_cell_volume                     2583.117
_diffrn_ambient_temperature      298
_exptl_crystal_density_diffrn    2.259
_cod_original_sg_symbol_H-M      'I 41/a c d'
_cod_original_formula_sum        '(Si4.1 Al1.9) Na1.95 O14 H4'
_cod_database_code               9002000
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R060023.rod
_rod_data_source.block           3500000
_rod_database.code               1000370
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9002000 COD http://www.crystallography.net/cod/9002000.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
152.3061 0.0000000E+00
152.7882 0.7815630
153.2704 1.504089
153.7525 2.193916
154.2346 2.554825
154.7167 1.285400
155.1988 0.1327060
155.6809 7.1709000E-02
156.1631 0.6843110
156.6452 1.750885
157.1273 2.263359
157.6094 2.170479
158.0915 2.083817
158.5736 1.762352
159.0558 1.418793
159.5379 1.142693
160.0200 1.028175
160.5021 1.450333
160.9842 1.939667
161.4663 2.967262
161.9485 3.642509
162.4306 3.344803
162.9127 2.625710
163.3948 2.065895
163.8769 1.838997
164.3590 1.881432
164.8412 1.789558
165.3233 1.585167
165.8054 1.593185
166.2875 1.922737
166.7696 2.613640
167.2517 2.789810
167.7339 1.604828
168.2160 0.1772610
168.6981 0.2658620
169.1802 0.4711230
169.6623 1.431221
170.1444 1.680527
170.6266 1.050064
171.1087 0.4708940
171.5908 0.3557590
172.0729 0.3827210
172.5550 0.2974400
173.0371 7.0039998E-03
173.5193 0.2906340
174.0014 0.2637710
174.4835 0.2745510
174.9656 0.6853260
175.4477 0.8051380
175.9298 0.8110430
176.4120 0.8893590
176.8941 1.135391
177.3762 1.436188
177.8583 1.372276
178.3404 0.3374710
178.8225 0.2155300
179.3047 0.2047420
179.7868 1.038307
180.2689 1.609863
180.7510 1.552017
181.2331 1.036842
181.7152 0.8248830
182.1974 1.229195
182.6795 1.576912
183.1616 1.753120
183.6437 1.797714
184.1258 1.750061
184.6079 1.601082
185.0900 1.408180
185.5722 1.573051
186.0543 2.604126
186.5364 3.381393
187.0185 3.233284
187.5006 2.429169
187.9827 1.809807
188.4649 1.885971
188.9470 2.587090
189.4291 3.350975
189.9112 4.592964
190.3933 5.547188
190.8754 5.485550
191.3576 4.483635
191.8397 3.571472
192.3218 3.447403
192.8039 3.837532
193.2860 4.066170
193.7681 3.990242
194.2503 3.796936
194.7324 3.616150
195.2145 3.421867
195.6966 3.410316
196.1787 4.056084
196.6608 4.865807
197.1430 5.218056
197.6251 4.750618
198.1072 3.919594
198.5893 3.480759
199.0714 3.550636
199.5535 3.783646
200.0357 4.222374
200.5178 4.665253
200.9999 4.785149
201.4820 4.327072
201.9641 3.579727
202.4462 3.405289
202.9284 4.251053
203.4105 4.914246
203.8926 4.990776
204.3747 4.760612
204.8568 4.520271
205.3389 4.417015
205.8211 4.408394
206.3032 4.349915
206.7853 4.199921
207.2674 4.098442
207.7495 3.991646
208.2316 3.971664
208.7138 4.194611
209.1959 4.812881
209.6780 5.733154
210.1601 6.224358
210.6422 5.590256
211.1243 5.118942
211.6065 5.098793
212.0886 5.388947
212.5707 5.728912
213.0528 5.918449
213.5349 5.969543
214.0170 6.265770
214.4992 7.137650
214.9813 7.873207
215.4634 8.193687
215.9455 8.233955
216.4276 8.314766
216.9097 8.659218
217.3919 9.196281
217.8740 9.330032
218.3561 8.712975
218.8382 8.163460
219.3203 7.997589
219.8024 8.151611
220.2845 8.435852
220.7667 8.758514
221.2488 9.093063
221.7309 9.347847
222.2130 9.521385
222.6951 9.647011
223.1772 9.704384
223.6594 9.698929
224.1415 9.699379
224.6236 9.738525
225.1057 9.824249
225.5878 9.953918
226.0699 10.16261
226.5521 10.34572
227.0342 10.47787
227.5163 10.54899
227.9984 10.64600
228.4805 10.90991
228.9626 11.16298
229.4448 11.06411
229.9269 10.38127
230.4090 9.670494
230.8911 9.500511
231.3732 9.863472
231.8553 10.07493
232.3375 9.725342
232.8196 9.111893
233.3017 8.597786
233.7838 8.224869
234.2659 7.973991
234.7480 7.907913
235.2302 8.060623
235.7123 8.061455
236.1944 7.551758
236.6765 6.927658
237.1586 6.622627
237.6407 6.758263
238.1229 6.923004
238.6050 6.521217
239.0871 5.401527
239.5692 4.523270
240.0513 4.374756
240.5334 4.437553
241.0156 4.407372
241.4977 4.214127
241.9798 3.908211
242.4619 3.503380
242.9440 2.925091
243.4261 2.533150
243.9083 2.687019
244.3904 2.849182
244.8725 2.593197
245.3546 1.859161
245.8367 1.025917
246.3188 0.6540300
246.8010 0.9445420
247.2831 1.085281
247.7652 0.8771130
248.2473 0.6078000
248.7294 0.4367180
249.2115 0.3934400
249.6937 0.4192810
250.1758 0.4608150
250.6579 0.5579830
251.1400 0.5634500
251.6221 0.4013440
252.1042 0.2148360
252.5864 7.1312003E-02
253.0685 1.6029000E-02
253.5506 5.4439999E-02
254.0327 4.0470000E-02
254.5148 6.2587999E-02
254.9969 8.8261001E-02
255.4790 2.7851000E-02
255.9612 0.1558490
256.4433 0.2373310
256.9254 0.2603610
257.4075 0.2394710
257.8896 0.1898650
258.3718 0.1175310
258.8539 7.2249998E-03
259.3360 0.3277630
259.8181 0.5640410
260.3002 0.4857250
260.7823 0.1628610
261.2645 0.1080400
261.7466 3.7632000E-02
262.2287 0.4394870
262.7108 0.7560460
263.1929 0.8300020
263.6750 0.8630910
264.1572 0.9797590
264.6393 1.135086
265.1214 1.164436
265.6035 0.9061160
266.0856 0.3457980
266.5677 4.4013999E-02
267.0499 0.1435590
267.5320 0.2880860
268.0141 0.3607440
268.4962 0.3542210
268.9783 0.2812080
269.4604 0.1341320
269.9426 7.9937004E-02
270.4247 0.1048660
270.9068 0.2498090
271.3889 0.5411340
271.8710 0.5596310
272.3531 0.3798980
272.8352 0.1778720
273.3174 3.3229999E-02
273.7995 3.8288001E-02
274.2816 5.3745002E-02
274.7637 0.4898070
275.2458 0.8473210
275.7279 0.9756620
276.2101 0.9349140
276.6922 0.8219640
277.1743 0.6543460
277.6564 0.4922410
278.1385 0.5454710
278.6206 0.9746930
279.1028 1.277248
279.5849 1.111584
280.0670 0.7534830
280.5491 0.7393150
281.0312 1.310638
281.5133 2.158108
281.9955 2.655674
282.4776 2.698956
282.9597 2.851784
283.4418 3.306515
283.9239 3.942047
284.4060 4.594276
284.8882 5.234489
285.3703 5.820004
285.8524 6.207893
286.3345 6.354736
286.8166 6.763660
287.2987 7.635654
287.7809 8.786453
288.2630 10.01273
288.7451 11.27782
289.2272 12.56213
289.7093 13.75877
290.1914 14.88957
290.6736 16.30383
291.1557 18.18594
291.6378 20.31161
292.1199 22.50019
292.6020 24.73418
293.0841 26.91044
293.5663 28.83604
294.0484 30.61123
294.5305 32.71463
295.0126 35.70096
295.4947 38.67862
295.9768 40.87514
296.4590 42.28492
296.9411 43.29865
297.4232 44.15433
297.9053 44.73083
298.3874 44.83450
298.8695 44.46540
299.3517 43.60958
299.8338 42.21364
300.3159 40.29848
300.7980 37.97227
301.2801 35.14054
301.7622 32.03643
302.2444 29.14402
302.7265 26.47742
303.2086 23.96015
303.6907 21.49212
304.1728 19.11757
304.6549 17.07044
305.1371 15.50567
305.6192 14.16653
306.1013 12.62870
306.5834 10.84788
307.0655 9.254158
307.5476 8.079922
308.0298 7.221581
308.5119 6.461071
308.9940 5.783436
309.4761 5.116142
309.9582 4.240459
310.4403 3.196857
310.9225 2.540665
311.4046 2.810810
311.8867 3.455402
312.3688 3.567360
312.8509 2.985470
313.3330 2.242489
313.8152 1.752018
314.2973 1.462849
314.7794 1.245457
315.2615 1.099712
315.7436 1.004333
316.2257 0.9762120
316.7079 1.020824
317.1900 0.9874990
317.6721 0.7263530
318.1542 0.3234560
318.6363 3.7610000E-03
319.1184 0.1720430
319.6006 0.3101960
320.0827 0.5228540
320.5648 0.7953190
321.0469 0.9724920
321.5290 0.9564780
322.0111 0.8274460
322.4933 0.7507780
322.9754 0.7477910
323.4575 0.7410700
323.9396 0.6971930
324.4217 0.6213230
324.9038 0.4906500
325.3860 0.2440640
325.8681 5.1456001E-02
326.3502 0.2776450
326.8323 0.9425090
327.3144 1.296398
327.7965 0.8234790
328.2787 6.5425999E-02
328.7608 0.6892700
329.2429 0.9149860
329.7250 0.9304850
330.2071 0.8474660
330.6892 0.6826400
331.1714 0.5436250
331.6535 0.4316020
332.1356 0.3801800
332.6177 0.4586140
333.0998 0.6610870
333.5819 0.8253440
334.0641 0.7246480
334.5462 0.5166780
335.0283 0.7639080
335.5104 2.063545
335.9925 3.256500
336.4746 3.343231
336.9568 2.569515
337.4389 2.104885
337.9210 2.579872
338.4031 3.589157
338.8852 4.146263
339.3673 4.080605
339.8495 4.034607
340.3316 4.311417
340.8137 4.777054
341.2958 5.167679
341.7779 5.400826
342.2600 5.552040
342.7421 5.744095
343.2242 5.993683
343.7064 6.153053
344.1885 5.981140
344.6706 5.812325
345.1527 6.114075
345.6348 6.950050
346.1169 7.837837
346.5991 8.330711
347.0812 8.398865
347.5633 8.533211
348.0454 8.681999
348.5275 8.943047
349.0096 9.455063
349.4918 10.16818
349.9739 10.82639
350.4560 11.24783
350.9381 11.50685
351.4202 11.97964
351.9023 13.01981
352.3845 13.82932
352.8666 13.99497
353.3487 13.79020
353.8308 13.70889
354.3129 13.94871
354.7950 14.36310
355.2772 14.66322
355.7593 14.73827
356.2414 14.94281
356.7235 15.37462
357.2056 15.91458
357.6877 16.43221
358.1699 16.90932
358.6520 17.43968
359.1341 18.16904
359.6162 19.18659
360.0983 19.85430
360.5804 19.74767
361.0626 19.71265
361.5447 20.36241
362.0268 21.53236
362.5089 22.56210
362.9910 22.96088
363.4731 22.82542
363.9553 23.03671
364.4374 23.60317
364.9195 24.49915
365.4016 26.00262
365.8837 27.73129
366.3658 29.17403
366.8480 30.12796
367.3301 30.76020
367.8122 31.41253
368.2943 32.08986
368.7764 32.76793
369.2585 33.33720
369.7407 33.98717
370.2228 34.99456
370.7049 36.31606
371.1870 37.52572
371.6691 38.08180
372.1512 37.80167
372.6334 37.96602
373.1155 39.10257
373.5976 40.16154
374.0797 40.55091
374.5618 40.56069
375.0439 40.89943
375.5261 42.08727
376.0082 43.89664
376.4903 45.11787
376.9724 45.16436
377.4545 45.45055
377.9366 46.53986
378.4188 47.79440
378.9009 48.49615
379.3830 48.42431
379.8651 48.05297
380.3472 48.09789
380.8293 48.62233
381.3115 49.34571
381.7936 50.62559
382.2757 51.79371
382.7578 52.39603
383.2399 52.50250
383.7220 52.58173
384.2042 53.06812
384.6863 53.89664
385.1684 54.42571
385.6505 54.54108
386.1326 54.64763
386.6147 54.85917
387.0969 55.12831
387.5790 55.37811
388.0611 55.55394
388.5432 55.73828
389.0253 56.16264
389.5074 56.94154
389.9896 57.46117
390.4717 57.41476
390.9538 57.06521
391.4359 56.52268
391.9180 55.79180
392.4001 55.13797
392.8823 54.89782
393.3644 54.97876
393.8465 54.76800
394.3286 54.03651
394.8107 53.22045
395.2928 52.75436
395.7750 52.53128
396.2571 52.15218
396.7392 51.28204
397.2213 50.25445
397.7034 49.66018
398.1855 49.55915
398.6677 49.22765
399.1498 48.14840
399.6319 46.56796
400.1140 45.10984
400.5961 43.82296
401.0782 42.62351
401.5604 41.40660
402.0425 40.22743
402.5246 39.29519
403.0067 38.75151
403.4888 38.27269
403.9709 37.34452
404.4531 35.93781
404.9352 34.47345
405.4173 32.94025
405.8994 31.43015
406.3815 30.13667
406.8636 29.03902
407.3458 27.76689
407.8279 25.95604
408.3100 23.66424
408.7921 21.89060
409.2742 20.93676
409.7563 20.09689
410.2385 19.17548
410.7206 18.18928
411.2027 17.21365
411.6848 16.28510
412.1669 15.32797
412.6490 14.17107
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413.6133 11.19270
414.0954 10.57625
414.5775 10.09317
415.0596 9.326439
415.5417 8.257805
416.0238 7.141495
416.5060 6.221130
416.9881 5.507851
417.4702 4.694672
417.9523 3.456512
418.4344 2.466713
418.9165 2.016975
419.3987 1.878716
419.8808 1.736458
420.3629 1.450035
420.8450 1.054237
421.3271 0.5926900
421.8092 2.9785000E-02
422.2914 0.4667210
422.7735 0.5136340
423.2556 0.5052030
423.7377 0.6597370
424.2198 0.9791790
424.7019 1.307922
425.1841 1.498703
425.6662 1.567642
426.1483 1.690079
426.6304 1.919991
427.1125 2.112961
427.5946 2.292145
428.0768 2.377594
428.5589 2.199707
429.0410 1.609230
429.5231 0.9345470
430.0052 0.6146010
430.4873 0.6559980
430.9695 0.7435910
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431.9337 0.9221120
432.4158 0.7122730
432.8979 0.2449040
433.3800 0.2125170
433.8622 0.5371930
434.3443 0.7673110
434.8264 0.9264760
435.3085 0.9977800
435.7906 1.170746
436.2727 1.620636
436.7549 2.305550
437.2370 2.965157
437.7191 3.522270
438.2012 4.120216
438.6833 4.934845
439.1654 5.851273
439.6476 6.570099
440.1297 6.963631
440.6118 7.181343
441.0939 7.452065
441.5760 7.727570
442.0581 8.212471
442.5403 9.019989
443.0224 9.966599
443.5045 10.98466
443.9866 12.02496
444.4687 12.93109
444.9508 13.53503
445.4330 13.89684
445.9151 14.72661
446.3972 16.42825
446.8793 18.12488
447.3614 19.77097
447.8435 21.31045
448.3257 22.57915
448.8078 23.56171
449.2899 24.60090
449.7720 26.27845
450.2541 28.86059
450.7362 31.14214
451.2184 32.62218
451.7005 34.26485
452.1826 36.44373
452.6647 39.10649
453.1468 42.10378
453.6289 45.41489
454.1111 48.92076
454.5932 52.20255
455.0753 55.11686
455.5574 58.31145
456.0395 62.04803
456.5216 66.13538
457.0038 70.40148
457.4859 74.85496
457.9680 79.61562
458.4501 84.81836
458.9322 90.42725
459.4143 96.24895
459.8965 102.2770
460.3786 108.4423
460.8607 114.5873
461.3428 120.8194
461.8249 127.4872
462.3070 134.5242
462.7892 142.1421
463.2713 150.6964
463.7534 160.0102
464.2355 169.2715
464.7176 178.1354
465.1997 186.9912
465.6819 196.6477
466.1640 207.2176
466.6461 217.8803
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