#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-06-07 10:41:14 +0300 (Thu, 07 Jun 2018) $
#$Revision: 921 $
#$URL: svn://172.16.1.111/rod/cif/1/00/03/1000394.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000394
loop_
_publ_author_name
'Robinson, K.'
'Gibbs, G. V.'
'Ribbe, P. H.'
_publ_section_title
;
 The crystal structures of the humite minerals. IV. Clinohumite and
 titanclinohumite
;
_journal_name_full               'American Mineralogist'
_journal_page_first              43
_journal_page_last               49
_journal_volume                  58
_journal_year                    1973
_chemical_compound_source        R050183
_chemical_formula_sum            'Fe0.58 H2 Mg8.42 O18 Si4'
_chemical_name_mineral           Hydroxylclinohumite
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2xab'
_symmetry_space_group_name_H-M   'P 21/b 1 1'
_cell_angle_alpha                100.786
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   4.7441
_cell_length_b                   10.2501
_cell_length_c                   13.6635
_cell_volume                     652.684
_exptl_crystal_density_diffrn    3.253
_cod_original_cell_volume        652.683
_cod_original_formula_sum        'Mg8.42 Fe.58 Si4 O18 H2'
_cod_database_code               9000292
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R050183.rod
_rod_data_source.block           3500000
_rod_database.code               1000394
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9000292 COD http://www.crystallography.net/cod/9000292.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
139.0943 0.0000000E+00
139.5765 1.026352
140.0586 1.984772
140.5407 2.394562
141.0228 2.193954
141.5049 1.918716
141.9870 1.884430
142.4692 2.273285
142.9513 1.974304
143.4334 1.710648
143.9155 1.452026
144.3976 1.084198
144.8797 0.2184300
145.3619 0.1656040
145.8440 0.2102510
146.3261 1.165161
146.8082 1.722885
147.2903 1.736160
147.7724 1.533691
148.2546 1.296402
148.7367 0.8641510
149.2188 0.7122500
149.7009 1.515869
150.1830 2.203995
150.6651 2.993546
151.1473 4.010605
151.6294 5.049332
152.1115 5.696609
152.5936 5.667618
153.0757 5.572678
153.5578 5.369995
154.0400 5.037186
154.5221 5.024582
155.0042 6.038300
155.4863 7.061371
155.9684 7.217056
156.4505 5.235168
156.9327 3.502136
157.4148 2.839584
157.8969 3.461685
158.3790 3.582458
158.8611 2.278885
159.3432 0.5111080
159.8254 0.6690980
160.3075 0.6062320
160.7896 0.2761990
161.2717 8.3130002E-02
161.7538 0.1249240
162.2359 8.1940003E-02
162.7181 1.127121
163.2002 2.441040
163.6823 3.231033
164.1644 2.603043
164.6465 1.829559
165.1286 1.634949
165.6108 2.207352
166.0929 2.929733
166.5750 3.814789
167.0571 4.627075
167.5392 4.939362
168.0213 3.864853
168.5035 2.621613
168.9856 2.211243
169.4677 2.995621
169.9498 3.945023
170.4319 4.361267
170.9140 4.411636
171.3962 4.483017
171.8783 4.952271
172.3604 5.470749
172.8425 5.607864
173.3246 5.112259
173.8067 4.651169
174.2889 5.034805
174.7710 6.005783
175.2531 6.728455
175.7352 6.417816
176.2173 5.629868
176.6994 5.113937
177.1816 5.049957
177.6637 5.239258
178.1458 5.504227
178.6279 5.940613
179.1100 6.635132
179.5921 7.340652
180.0743 8.077011
180.5564 9.084015
181.0385 10.57085
181.5206 12.07552
182.0027 13.02800
182.4848 13.53915
182.9670 13.95354
183.4491 14.41063
183.9312 14.96401
184.4133 15.80952
184.8954 17.19409
185.3775 18.68053
185.8597 19.43320
186.3418 19.45732
186.8239 19.32281
187.3060 19.68817
187.7881 20.36389
188.2702 20.50156
188.7523 19.90448
189.2345 18.65494
189.7166 16.72375
190.1987 14.05925
190.6808 11.42018
191.1629 9.497406
191.6451 8.232529
192.1272 7.134750
192.6093 6.058105
193.0914 5.074249
193.5735 4.367844
194.0556 3.932877
194.5378 3.796875
195.0199 4.128021
195.5020 4.901199
195.9841 5.504593
196.4662 5.645538
196.9483 5.536621
197.4305 5.998154
197.9126 7.110825
198.3947 8.387299
198.8768 9.325699
199.3589 9.917770
199.8410 10.35893
200.3232 10.63547
200.8053 10.78537
201.2874 11.07945
201.7695 11.55814
202.2516 12.04237
202.7337 12.29178
203.2159 12.25208
203.6980 12.37727
204.1801 12.86609
204.6622 13.64685
205.1443 14.02463
205.6264 13.89284
206.1086 13.62402
206.5907 13.57045
207.0728 13.73190
207.5549 14.14388
208.0370 14.96249
208.5191 16.13882
209.0013 16.75426
209.4834 16.65837
209.9655 16.28998
210.4476 16.12688
210.9297 16.24258
211.4118 16.31905
211.8940 16.43451
212.3761 16.57225
212.8582 15.80438
213.3403 13.87349
213.8224 11.44176
214.3045 9.162323
214.7867 6.942764
215.2688 5.117081
215.7509 3.837006
216.2330 3.106567
216.7151 2.239838
217.1972 1.126862
217.6794 6.1797999E-02
218.1615 1.029037
218.6436 1.763702
219.1257 2.280853
219.6078 2.570404
220.0899 2.621292
220.5721 2.559021
221.0542 2.402313
221.5363 2.181747
222.0184 1.942123
222.5005 1.713516
222.9826 1.380722
223.4648 0.8867340
223.9469 0.2186430
224.4290 0.2974090
224.9111 0.5397190
225.3932 0.7814030
225.8753 1.346024
226.3575 2.443466
226.8396 3.409866
227.3217 4.096771
227.8038 4.514465
228.2859 4.798721
228.7680 4.921402
229.2502 4.945877
229.7323 4.882874
230.2144 4.545364
230.6965 4.520782
231.1786 5.048035
231.6607 6.126816
232.1429 6.854324
232.6250 7.189377
233.1071 7.222687
233.5892 7.002029
234.0713 6.419312
234.5534 5.795074
235.0356 5.128799
235.5177 4.431458
235.9998 3.940323
236.4819 3.695297
236.9640 3.602524
237.4461 3.594299
237.9283 3.708084
238.4104 3.831772
238.8925 3.988220
239.3746 4.167694
239.8567 4.152863
240.3388 3.854019
240.8210 3.464966
241.3031 3.109940
241.7852 2.703674
242.2673 2.509598
242.7494 2.634232
243.2315 3.044846
243.7137 3.357574
244.1958 3.622696
244.6779 3.735947
245.1600 3.558762
245.6421 2.763290
246.1242 2.396240
246.6064 2.845779
247.0885 3.912933
247.5706 4.130005
248.0527 2.941574
248.5348 1.637161
249.0169 1.049057
249.4990 1.375488
249.9812 1.997330
250.4633 3.068085
250.9454 4.422363
251.4275 5.191864
251.9096 4.960495
252.3917 4.742645
252.8739 5.242615
253.3560 7.076126
253.8381 8.093765
254.3202 7.863434
254.8023 6.751602
255.2844 6.104248
255.7666 6.050415
256.2487 6.238693
256.7308 6.518295
257.2129 6.956818
257.6950 7.305984
258.1772 7.582520
258.6593 7.751846
259.1414 7.729736
259.6235 7.494400
260.1056 7.102951
260.5877 6.492859
261.0699 5.459991
261.5520 4.892059
262.0341 4.927750
262.5162 5.350479
262.9983 5.779892
263.4804 6.362747
263.9626 6.617142
264.4447 6.254776
264.9268 5.084076
265.4089 4.122543
265.8910 3.304977
266.3731 2.753494
266.8553 2.625977
267.3374 2.858017
267.8195 3.725052
268.3016 5.579056
268.7837 8.663269
269.2658 10.75883
269.7480 11.62918
270.2301 11.83922
270.7122 12.42413
271.1943 13.83269
271.6764 13.89137
272.1585 11.27786
272.6407 5.985153
273.1228 2.670837
273.6049 1.751831
274.0870 2.072189
274.5691 2.437302
275.0512 2.878860
275.5334 3.137192
276.0155 2.987961
276.4976 2.507584
276.9797 2.596237
277.4618 3.472000
277.9439 4.379745
278.4261 4.411057
278.9081 3.460571
279.3903 2.798630
279.8724 2.799606
280.3545 3.311172
280.8366 3.727051
281.3187 4.106201
281.8008 4.195892
282.2830 3.501297
282.7651 1.988937
283.2472 1.023666
283.7293 0.9074550
284.2114 1.451172
284.6935 2.263931
285.1757 3.400909
285.6578 4.319031
286.1399 4.563400
286.6220 4.170319
287.1041 3.551392
287.5862 2.586197
288.0684 1.667007
288.5505 1.694717
289.0326 2.668045
289.5147 3.945007
289.9968 5.444733
290.4789 7.028183
290.9611 7.739960
291.4432 7.342911
291.9253 6.496964
292.4074 6.208771
292.8895 6.434647
293.3716 6.753082
293.8538 6.781708
294.3359 6.718948
294.8180 7.358826
295.3001 8.849670
295.7822 10.43340
296.2643 11.19202
296.7465 11.22867
297.2286 11.03516
297.7107 10.50238
298.1928 9.950134
298.6749 10.18002
299.1570 11.22816
299.6392 12.47794
300.1213 13.22707
300.6034 13.68071
301.0855 14.33263
301.5676 15.42752
302.0497 16.78828
302.5319 18.15221
303.0140 19.53461
303.4961 20.98630
303.9782 22.55571
304.4603 24.22226
304.9424 26.02020
305.4246 27.94798
305.9067 29.99380
306.3888 32.57158
306.8709 35.42569
307.3530 37.37331
307.8351 37.21999
308.3173 35.84836
308.7994 34.30440
309.2815 32.81462
309.7636 31.14641
310.2457 28.92592
310.7278 26.34172
311.2100 23.94955
311.6921 21.88266
312.1742 20.21954
312.6563 19.12459
313.1384 18.68085
313.6205 18.52660
314.1027 18.35951
314.5848 18.35043
315.0669 18.78934
315.5490 20.09502
316.0311 21.67067
316.5132 23.21294
316.9954 24.71933
317.4775 26.03322
317.9596 26.87126
318.4417 27.54399
318.9238 28.41425
319.4059 29.98563
319.8881 31.40469
320.3702 32.34674
320.8523 32.80943
321.3344 32.94806
321.8165 32.90948
322.2986 32.50412
322.7808 31.58908
323.2629 29.20636
323.7450 27.31651
324.2271 26.85745
324.7092 27.44801
325.1913 27.09703
325.6735 24.36137
326.1556 21.45573
326.6377 19.51164
327.1198 19.34177
327.6019 19.09755
328.0840 18.66113
328.5662 18.08199
329.0483 17.46649
329.5304 16.83060
330.0125 16.15326
330.4946 15.30923
330.9767 13.91493
331.4589 13.45270
331.9410 14.72792
332.4231 16.56210
332.9052 17.27983
333.3873 16.13390
333.8694 15.00273
334.3516 14.27124
334.8337 13.93399
335.3158 13.99216
335.7979 14.59233
336.2800 15.41202
336.7621 16.17535
337.2443 16.92918
337.7264 17.51297
338.2085 17.90901
338.6906 18.11710
339.1727 18.08588
339.6548 17.69507
340.1370 17.44482
340.6191 17.65501
341.1012 18.32774
341.5833 19.13345
342.0654 20.15028
342.5475 21.21324
343.0297 21.73557
343.5118 21.60306
343.9939 21.61026
344.4760 22.39745
344.9581 23.89148
345.4402 24.90155
345.9224 25.29323
346.4045 25.41183
346.8866 25.80620
347.3687 26.46129
347.8508 26.98911
348.3329 27.26826
348.8151 27.26155
349.2972 26.83327
349.7793 25.98418
350.2614 25.05829
350.7435 24.44179
351.2256 24.02870
351.7078 23.50446
352.1899 22.79358
352.6720 21.92120
353.1541 20.75662
353.6362 19.36218
354.1183 18.18456
354.6005 17.86307
355.0826 17.84142
355.5647 17.25980
356.0468 15.80145
356.5289 14.21097
357.0110 13.04469
357.4932 12.22371
357.9753 11.56445
358.4574 11.14285
358.9395 10.73663
359.4216 10.18974
359.9037 9.488388
360.3859 8.644104
360.8680 7.484970
361.3501 6.249069
361.8322 5.231598
362.3143 4.817902
362.7964 4.382385
363.2786 3.514160
363.7607 2.270386
364.2428 1.313751
364.7249 0.9884640
365.2070 0.9629060
365.6891 1.024200
366.1713 1.393631
366.6534 1.518890
367.1355 1.020798
367.6176 0.1756440
368.0997 0.2311710
368.5818 0.3872680
369.0640 1.040756
369.5461 1.305786
370.0282 0.8393400
370.5103 0.8152470
370.9924 1.621841
371.4745 2.707001
371.9567 3.342957
372.4388 3.336548
372.9209 3.141556
373.4030 2.674576
373.8851 1.913681
374.3672 1.920502
374.8494 3.051270
375.3315 4.461716
375.8136 5.450928
376.2957 5.916748
376.7778 6.301987
377.2599 6.631943
377.7421 6.921463
378.2242 7.255386
378.7063 7.665588
379.1884 7.962097
379.6705 8.039490
380.1526 7.895981
380.6348 7.562271
381.1169 7.006073
381.5990 6.353561
382.0811 5.813644
382.5632 5.380539
383.0453 4.823883
383.5275 3.935196
384.0096 2.884079
384.4917 2.195023
384.9738 1.876923
385.4559 1.747879
385.9380 1.728958
386.4202 1.775970
386.9023 1.780014
387.3844 1.736359
387.8665 1.605087
388.3486 1.193542
388.8307 0.6000060
389.3129 0.2199710
389.7950 0.4986270
390.2771 1.013474
390.7592 1.277130
391.2413 1.178360
391.7234 1.053055
392.2056 1.221252
392.6877 1.496750
393.1698 1.591522
393.6519 1.212830
394.1340 0.7760620
394.6161 0.5133210
395.0983 0.4271850
395.5804 0.3309780
396.0625 0.2702030
396.5446 0.1105960
397.0267 0.2551120
397.5089 1.286499
397.9910 1.999527
398.4731 2.033752
398.9552 1.597931
399.4373 1.317078
399.9194 1.490356
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401.8479 0.6090240
402.3300 0.7024080
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403.2942 0.8932800
403.7763 0.4381710
404.2585 9.9854000E-02
404.7406 6.6863999E-02
405.2227 0.2865910
405.7048 0.1928860
406.1869 0.2923280
406.6690 0.9582520
407.1512 1.676773
407.6333 2.447647
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410.5260 6.417740
411.0081 6.105453
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412.4544 5.120895
412.9366 5.709244
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414.8650 9.517731
415.3471 9.824982
415.8293 10.17834
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417.2756 10.53180
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418.2398 10.25632
418.7220 10.87790
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421.1325 13.18956
421.6147 13.09393
422.0968 13.51976
422.5789 14.46066
423.0610 15.42389
423.5431 16.11960
424.0252 16.90994
424.5074 18.05219
424.9895 19.75375
425.4716 21.53334
425.9537 23.51399
426.4358 25.55043
426.9179 27.30428
427.4001 28.67653
427.8822 29.89671
428.3643 30.96484
428.8464 31.81172
429.3285 33.01591
429.8106 34.74007
430.2928 36.59726
430.7749 38.36522
431.2570 40.21227
431.7391 41.18434
432.2212 41.02121
432.7033 40.00874
433.1855 39.11029
433.6676 38.33752
434.1497 37.42081
434.6318 36.21021
435.1139 34.74040
435.5960 32.97690
436.0782 30.81049
436.5603 28.75734
437.0424 27.56252
437.5245 27.07130
438.0066 26.68852
438.4887 26.25557
438.9709 25.76691
439.4530 25.13338
439.9351 24.38934
440.4172 23.79054
440.8993 23.58295
441.3814 23.56506
441.8636 23.54468
442.3457 23.51180
442.8278 23.40030
443.3099 23.01323
443.7920 22.55054
444.2741 22.32925
444.7563 22.71092
445.2384 23.12563
445.7205 23.50169
446.2026 23.82825
446.6847 23.67261
447.1668 22.37964
447.6490 20.95248
448.1311 20.02617
448.6132 20.52809
449.0953 20.32677
449.5774 18.97403
450.0595 17.01723
450.5417 15.65614
451.0238 15.21220
451.5059 14.81926
451.9880 14.22777
452.4701 13.42499
452.9522 12.52798
453.4344 11.47052
453.9165 10.45984
454.3986 9.751556
454.8807 9.327728
455.3628 8.519501
455.8449 7.059814
456.3271 5.481445
456.8092 5.003082
457.2913 5.530060
457.7734 6.001709
458.2555 5.905212
458.7376 5.499237
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1265.801 0.0000000E+00
