#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-06-07 10:42:45 +0300 (Thu, 07 Jun 2018) $ #$Revision: 946 $ #$URL: svn://172.16.1.111/rod/cif/1/00/04/1000415.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_1000415 loop_ _publ_author_name 'Abraham, F.' 'Dion, C.' 'Tancret, N.' 'Saadi, M.' _publ_section_title ; Ag2(UO2)2V2O8: a new compound with the carnotite structure. Synthesis, structure and properties ; _journal_name_full 'Advanced Materials Research' _journal_page_first 511 _journal_page_last 520 _journal_volume 1 _journal_year 1994 _chemical_compound_source R070647 _chemical_formula_structural Ag2(UO2)2V2O8 _chemical_formula_sum 'Ag O6 U V' _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90 _cell_angle_beta 100.56 _cell_angle_gamma 90 _cell_length_a 5.8952 _cell_length_b 8.3541 _cell_length_c 10.4142 _cell_volume 504.203 _exptl_crystal_density_diffrn 6.492 _cod_original_formula_sum 'Ag U V O6' _cod_database_code 9012859 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type other _raman_measurement_device.excitation_laser_wavelength 532 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 15 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R070647.rod _rod_data_source.block 3500000 _rod_database.code 1000415 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9012859 COD http://www.crystallography.net/cod/9012859.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 142.3047 0.0000000E+00 142.7868 10.00098 143.2689 3.210449 143.7510 5.518066 144.2331 21.25342 144.7152 37.74658 145.1974 62.94238 145.6795 76.17090 146.1616 110.7695 146.6437 92.63086 147.1258 99.18994 147.6079 137.8101 148.0901 126.8110 148.5722 105.4990 149.0543 53.94775 149.5364 9.249512 150.0185 12.22412 150.5006 27.65332 150.9828 45.29688 151.4649 18.84668 151.9470 45.57031 152.4291 75.85352 152.9112 43.96680 153.3933 8.547852 153.8755 52.94141 154.3576 93.60254 154.8397 118.2959 155.3218 113.9639 155.8039 72.65430 156.2860 54.64062 156.7682 86.89551 157.2503 143.4541 157.7324 192.5518 158.2145 223.9766 158.6966 248.2266 159.1787 270.9990 159.6609 297.9902 160.1430 312.6094 160.6251 292.0127 161.1072 253.9971 161.5893 239.8994 162.0714 285.0264 162.5536 348.1143 163.0357 401.3115 163.5178 431.4385 163.9999 458.3438 164.4820 488.6309 164.9641 522.5850 165.4463 560.6602 165.9284 608.4453 166.4105 658.6602 166.8926 703.4072 167.3747 730.3311 167.8568 757.2246 168.3390 800.6611 168.8211 861.4150 169.3032 916.5293 169.7853 943.1582 170.2674 953.9609 170.7495 971.1660 171.2317 1005.171 171.7138 1050.593 172.1959 1107.761 172.6780 1183.140 173.1601 1247.778 173.6422 1271.989 174.1244 1263.494 174.6065 1246.643 175.0886 1231.367 175.5707 1217.969 176.0528 1207.251 176.5349 1200.864 177.0171 1194.971 177.4992 1185.513 177.9813 1172.457 178.4634 1156.206 178.9455 1135.853 179.4276 1112.241 179.9098 1087.084 180.3919 1059.129 180.8740 1030.534 181.3561 1002.125 181.8382 973.7275 182.3203 950.8750 182.8025 944.7998 183.2846 951.2637 183.7667 952.7148 184.2488 931.8438 184.7309 900.4053 185.2130 899.2598 185.6951 936.4805 186.1773 976.5420 186.6594 958.1318 187.1415 887.8730 187.6236 835.2559 188.1057 844.3750 188.5878 904.7881 189.0700 968.1416 189.5521 1028.713 190.0342 1089.941 190.5163 1162.719 190.9984 1246.612 191.4805 1325.736 191.9627 1386.109 192.4448 1428.643 192.9269 1467.596 193.4090 1505.311 193.8911 1540.667 194.3732 1571.662 194.8554 1599.139 195.3375 1619.606 195.8196 1630.144 196.3017 1630.951 196.7838 1624.259 197.2659 1611.396 197.7481 1592.221 198.2302 1562.806 198.7123 1522.027 199.1944 1475.511 199.6765 1428.369 200.1586 1376.915 200.6408 1329.128 201.1229 1287.800 201.6050 1253.449 202.0871 1217.169 202.5692 1177.062 203.0513 1137.188 203.5335 1103.739 204.0156 1076.280 204.4977 1055.346 204.9798 1039.370 205.4619 1027.048 205.9440 1028.976 206.4262 1049.053 206.9083 1080.499 207.3904 1104.490 207.8725 1117.449 208.3546 1134.487 208.8367 1162.821 209.3189 1205.886 209.8010 1242.803 210.2831 1267.112 210.7652 1288.945 211.2473 1342.873 211.7294 1442.371 212.2116 1544.275 212.6937 1611.827 213.1758 1633.781 213.6579 1660.767 214.1400 1697.981 214.6221 1746.495 215.1043 1818.562 215.5864 1928.566 216.0685 2043.392 216.5506 2126.298 217.0327 2165.165 217.5148 2204.882 217.9970 2251.384 218.4791 2303.004 218.9612 2383.780 219.4433 2508.489 219.9254 2645.672 220.4075 2752.948 220.8897 2817.595 221.3718 2875.332 221.8539 2931.841 222.3360 2983.906 222.8181 3052.900 223.3002 3146.250 223.7824 3251.196 224.2645 3342.966 224.7466 3419.557 225.2287 3488.260 225.7108 3551.023 226.1929 3605.216 226.6750 3664.943 227.1572 3747.799 227.6393 3832.529 228.1214 3865.274 228.6035 3833.974 229.0856 3770.718 229.5677 3688.888 230.0499 3585.169 230.5320 3471.200 231.0141 3343.438 231.4962 3204.250 231.9783 3065.153 232.4604 2930.466 232.9426 2791.545 233.4247 2636.612 233.9068 2446.443 234.3889 2287.784 234.8710 2175.396 235.3531 2104.352 235.8353 2031.895 236.3174 1953.948 236.7995 1876.715 237.2816 1804.293 237.7637 1734.590 238.2458 1674.945 238.7280 1625.467 239.2101 1586.849 239.6922 1565.427 240.1743 1564.843 240.6564 1577.685 241.1385 1598.192 241.6207 1631.564 242.1028 1663.393 242.5849 1689.727 243.0670 1709.612 243.5491 1733.882 244.0313 1755.409 244.5134 1787.246 244.9955 1849.179 245.4776 1969.546 245.9597 2070.427 246.4418 2123.838 246.9240 2114.949 247.4061 2148.490 247.8882 2247.060 248.3703 2371.457 248.8524 2465.132 249.3345 2519.726 249.8167 2557.776 250.2988 2581.924 250.7809 2584.900 251.2630 2603.345 251.7451 2642.717 252.2272 2693.856 252.7094 2742.894 253.1915 2798.738 253.6736 2837.050 254.1557 2850.989 254.6378 2843.566 255.1199 2798.551 255.6021 2695.372 256.0842 2564.992 256.5663 2478.559 257.0484 2456.353 257.5305 2442.626 258.0126 2413.570 258.4948 2363.427 258.9769 2314.646 259.4590 2270.870 259.9411 2227.557 260.4232 2167.136 260.9053 2075.918 261.3875 1992.763 261.8696 1939.672 262.3517 1929.263 262.8338 1910.919 263.3159 1876.748 263.7980 1834.251 264.2802 1812.867 264.7623 1821.948 265.2444 1832.654 265.7265 1826.270 266.2086 1797.238 266.6907 1771.560 267.1729 1754.051 267.6550 1740.834 268.1371 1712.031 268.6192 1656.208 269.1013 1610.365 269.5834 1612.071 270.0656 1679.980 270.5477 1705.688 271.0298 1662.696 271.5119 1569.863 271.9940 1512.131 272.4761 1504.688 272.9583 1495.212 273.4404 1437.935 273.9225 1322.457 274.4046 1218.934 274.8867 1141.220 275.3688 1082.957 275.8510 1010.077 276.3331 917.5498 276.8152 827.0576 277.2973 760.8887 277.7794 722.3682 278.2615 675.6221 278.7437 610.3350 279.2258 532.0723 279.7079 468.0752 280.1900 421.5098 280.6721 377.1191 281.1542 317.8867 281.6364 242.6143 282.1185 177.1396 282.6006 130.0000 283.0827 95.99023 283.5648 51.36133 284.0469 6.417969 284.5291 61.46094 285.0112 94.10156 285.4933 105.2451 285.9754 123.4785 286.4575 159.3164 286.9396 206.8232 287.4217 248.2949 287.9038 284.8975 288.3860 308.5791 288.8681 307.3955 289.3502 283.5762 289.8323 255.3643 290.3144 225.7832 290.7965 196.5967 291.2787 172.1885 291.7608 152.3955 292.2429 138.6182 292.7250 138.2627 293.2071 147.3105 293.6892 145.6182 294.1714 122.1719 294.6535 85.53613 295.1356 53.69922 295.6177 26.47070 296.0998 0.1728520 296.5819 29.98242 297.0641 62.92188 297.5462 93.65234 298.0283 114.6572 298.5104 135.6113 298.9925 175.3447 299.4746 234.1816 299.9568 298.0195 300.4389 354.3105 300.9210 406.2295 301.4031 462.8340 301.8852 525.7109 302.3673 594.7393 302.8495 675.5029 303.3316 766.7988 303.8137 853.6494 304.2958 916.5342 304.7779 966.3301 305.2600 1021.229 305.7422 1087.212 306.2243 1161.813 306.7064 1244.390 307.1885 1335.338 307.6706 1428.396 308.1527 1522.918 308.6349 1616.603 309.1170 1704.247 309.5991 1786.164 310.0812 1861.234 310.5633 1928.854 311.0454 1989.897 311.5276 2046.553 312.0097 2094.143 312.4918 2140.162 312.9739 2193.684 313.4560 2277.244 313.9381 2352.956 314.4203 2393.095 314.9024 2400.814 315.3845 2408.723 315.8666 2451.768 316.3487 2493.901 316.8308 2501.077 317.3130 2435.878 317.7951 2358.771 318.2772 2296.298 318.7593 2246.286 319.2414 2184.425 319.7235 2106.152 320.2057 2011.086 320.6878 1898.948 321.1699 1755.945 321.6520 1609.519 322.1341 1460.434 322.6162 1310.252 323.0984 1179.606 323.5805 1078.532 324.0626 994.9326 324.5447 920.6592 325.0268 864.3174 325.5089 806.7891 325.9911 735.5645 326.4732 654.7217 326.9553 601.0244 327.4374 591.3164 327.9195 599.3691 328.4016 609.9043 328.8838 632.9141 329.3659 644.9170 329.8480 634.6768 330.3301 607.9277 330.8122 601.4238 331.2943 624.7646 331.7765 658.4502 332.2586 692.8467 332.7407 733.4805 333.2228 764.3506 333.7049 779.2900 334.1870 783.8398 334.6692 801.0850 335.1513 835.2197 335.6334 876.0381 336.1155 916.4287 336.5976 952.7305 337.0797 1001.369 337.5619 1063.433 338.0440 1138.117 338.5261 1224.089 339.0082 1325.035 339.4903 1424.989 339.9724 1510.603 340.4546 1579.652 340.9367 1660.399 341.4188 1757.913 341.9009 1863.557 342.3830 1959.687 342.8651 2046.414 343.3473 2134.422 343.8294 2229.315 344.3115 2330.153 344.7936 2419.188 345.2757 2492.032 345.7578 2566.276 346.2400 2677.347 346.7221 2823.561 347.2042 2975.865 347.6863 3122.322 348.1684 3263.900 348.6505 3403.687 349.1327 3541.558 349.6148 3681.861 350.0969 3833.824 350.5790 3993.084 351.0611 4146.569 351.5432 4284.859 352.0254 4415.710 352.5075 4553.027 352.9896 4696.556 353.4717 4840.825 353.9538 4977.099 354.4359 5109.617 354.9181 5242.948 355.4002 5390.640 355.8823 5534.182 356.3644 5650.423 356.8465 5739.166 357.3286 5830.698 357.8108 5965.661 358.2929 6110.435 358.7750 6223.848 359.2571 6241.710 359.7392 6265.281 360.2213 6364.432 360.7035 6533.962 361.1856 6689.840 361.6677 6780.938 362.1498 6848.273 362.6319 6928.459 363.1140 7041.843 363.5962 7157.822 364.0783 7262.875 364.5604 7359.902 365.0425 7470.348 365.5246 7608.580 366.0067 7756.081 366.4889 7901.199 366.9710 8058.893 367.4531 8196.778 367.9352 8309.486 368.4173 8399.613 368.8994 8477.880 369.3815 8521.810 369.8636 8574.395 370.3458 8658.742 370.8279 8816.468 371.3100 8927.191 371.7921 8982.606 372.2742 8996.913 372.7563 9002.848 373.2385 9009.223 373.7206 8983.878 374.2027 8911.541 374.6848 8786.056 375.1669 8643.392 375.6490 8485.382 376.1312 8311.860 376.6133 8114.871 377.0954 7887.923 377.5775 7652.229 378.0596 7417.885 378.5417 7189.216 379.0239 6924.202 379.5060 6619.342 379.9881 6294.240 380.4702 5973.823 380.9523 5655.146 381.4344 5346.170 381.9166 5041.794 382.3987 4751.066 382.8808 4480.323 383.3629 4231.187 383.8450 3996.077 384.3271 3770.213 384.8093 3555.441 385.2914 3361.234 385.7735 3193.178 386.2556 3041.376 386.7377 2909.089 387.2198 2796.124 387.7020 2689.093 388.1841 2581.512 388.6662 2474.503 389.1483 2368.752 389.6304 2260.324 390.1125 2163.926 390.5947 2089.570 391.0768 2034.259 391.5589 1991.675 392.0410 1959.466 392.5231 1939.587 393.0052 1932.038 393.4874 1934.948 393.9695 1954.439 394.4516 2010.346 394.9337 2083.393 395.4158 2137.286 395.8979 2142.052 396.3801 2138.400 396.8622 2141.609 397.3443 2150.117 397.8264 2175.271 398.3085 2227.163 398.7906 2293.124 399.2728 2357.613 399.7549 2404.469 400.2370 2467.734 400.7191 2561.882 401.2012 2690.480 401.6833 2797.967 402.1655 2874.592 402.6476 2939.053 403.1297 3007.187 403.6118 3082.830 404.0939 3153.129 404.5760 3212.453 405.0582 3264.438 405.5403 3328.874 406.0224 3408.493 406.5045 3490.561 406.9866 3574.575 407.4688 3662.716 407.9509 3713.387 408.4330 3719.006 408.9151 3690.059 409.3972 3641.812 409.8793 3574.331 410.3615 3502.955 410.8436 3448.316 411.3257 3397.476 411.8078 3303.478 412.2899 3158.233 412.7720 2991.133 413.2542 2833.347 413.7363 2683.494 414.2184 2534.004 414.7005 2381.697 415.1826 2229.674 415.6647 2082.424 416.1469 1941.305 416.6290 1800.378 417.1111 1659.403 417.5932 1515.182 418.0753 1368.321 418.5574 1185.421 419.0396 1026.322 419.5217 932.8379 420.0038 896.7754 420.4859 857.6123 420.9680 794.8594 421.4501 719.3408 421.9323 639.6309 422.4144 547.8750 422.8965 463.6172 423.3786 388.2695 423.8607 322.7432 424.3428 268.3018 424.8250 236.1279 425.3071 205.0547 425.7892 168.4775 426.2713 124.2490 426.7534 77.82520 427.2355 18.92773 427.7177 36.10742 428.1998 57.99414 428.6819 27.05371 429.1640 8.875000 429.6461 30.07422 430.1282 89.29297 430.6104 114.1602 431.0925 97.60449 431.5746 65.92480 432.0567 40.16992 432.5388 20.24121 433.0209 17.12305 433.5031 40.11133 433.9852 75.62207 434.4673 87.23145 434.9494 75.33496 435.4315 63.00000 435.9136 69.23633 436.3958 87.44043 436.8779 101.4004 437.3600 108.4580 437.8421 110.7461 438.3242 107.3955 438.8063 100.5586 439.2885 96.48047 439.7706 105.0957 440.2527 113.9932 440.7348 109.9443 441.2169 90.79980 441.6990 71.49121 442.1812 68.13867 442.6633 66.89941 443.1454 51.18848 443.6275 16.00586 444.1096 67.39355 444.5917 68.37402 445.0739 22.70410 445.5560 10.53809 446.0381 10.03809 446.5202 0.1455080 447.0023 4.916016 447.4844 1.793945 447.9666 5.231445 448.4487 2.353516 448.9308 3.845703 449.4129 4.769531 449.8950 2.666016 450.3771 10.14160 450.8593 13.98340 451.3413 13.18555 451.8235 16.02832 452.3056 26.91211 452.7877 34.33398 453.2698 18.87012 453.7519 21.65625 454.2340 58.91895 454.7162 83.51172 455.1983 98.79297 455.6804 120.1514 456.1625 148.3096 456.6446 170.6279 457.1267 168.5449 457.6089 151.8555 458.0910 148.4199 458.5731 165.8525 459.0552 195.2480 459.5373 233.7930 460.0194 277.0205 460.5016 310.8457 460.9837 314.9189 461.4658 312.7461 461.9479 327.9980 462.4300 366.8408 462.9121 403.0186 463.3943 412.0117 463.8764 413.4551 464.3585 432.5117 464.8406 503.0566 465.3227 566.6074 465.8048 602.1738 466.2870 609.3047 466.7691 613.2295 467.2512 602.7812 467.7333 599.7148 468.2154 617.4268 468.6975 666.7285 469.1797 719.5322 469.6618 776.0605 470.1439 834.2812 470.6260 890.8125 471.1081 951.7744 471.5902 995.5791 472.0724 1001.515 472.5545 965.0010 473.0366 976.6104 473.5187 1047.972 474.0008 1134.135 474.4829 1176.671 474.9651 1179.221 475.4472 1185.583 475.9293 1214.129 476.4114 1251.577 476.8935 1263.360 477.3756 1252.198 477.8578 1252.159 478.3399 1309.695 478.8220 1388.136 479.3041 1431.690 479.7862 1423.793 480.2683 1394.708 480.7505 1348.771 481.2326 1298.700 481.7147 1270.875 482.1968 1293.617 482.6789 1326.366 483.1610 1355.203 483.6432 1381.048 484.1253 1380.397 484.6074 1313.226 485.0895 1233.138 485.5716 1184.221 486.0537 1222.204 486.5359 1236.448 487.0180 1204.982 487.5001 1136.799 487.9822 1083.512 488.4643 1057.619 488.9464 1035.246 489.4286 1004.337 489.9107 962.8809 490.3928 921.4443 490.8749 876.8271 491.3570 834.0186 491.8391 805.7559 492.3213 793.7158 492.8034 775.2930 493.2855 733.5889 493.7676 682.2422 494.2497 662.3643 494.7318 673.7432 495.2140 688.1885 495.6961 677.4502 496.1782 655.6758 496.6603 648.8008 497.1424 669.3623 497.6245 688.8867 498.1067 676.6221 498.5888 647.0674 499.0709 633.4258 499.5530 664.6035 500.0351 702.1221 500.5172 730.1006 500.9994 748.1318 501.4815 750.9463 501.9636 710.1104 502.4457 660.3584 502.9278 633.3721 503.4099 646.3037 503.8921 663.0713 504.3742 686.7461 504.8563 713.2930 505.3384 726.8594 505.8205 730.2285 506.3026 717.7295 506.7848 679.9287 507.2669 610.0410 507.7490 566.6514 508.2311 557.8379 508.7132 557.7998 509.1953 521.7783 509.6775 454.4902 510.1596 412.9404 510.6417 429.3877 511.1238 475.8496 511.6059 499.9482 512.0880 500.2324 512.5701 485.4170 513.0522 441.7422 513.5344 394.0264 514.0165 377.9102 514.4986 409.4521 514.9807 443.3340 515.4628 447.5039 515.9449 435.7637 516.4271 431.4746 516.9092 441.1445 517.3913 461.3047 517.8734 495.9062 518.3555 545.8867 518.8376 588.0869 519.3198 617.4697 519.8019 640.4033 520.2840 660.5381 520.7661 674.8340 521.2482 691.6025 521.7303 709.6221 522.2125 731.2324 522.6946 760.3164 523.1767 796.2627 523.6588 842.5596 524.1409 907.0215 524.6230 984.6748 525.1052 1044.551 525.5873 1084.749 526.0694 1122.612 526.5515 1171.219 527.0336 1230.487 527.5157 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768.5740 2982.759 769.0562 2841.300 769.5383 2709.595 770.0204 2587.702 770.5025 2477.381 770.9846 2376.025 771.4667 2284.981 771.9489 2207.353 772.4310 2119.648 772.9131 1999.769 773.3952 1868.906 773.8773 1748.541 774.3594 1646.837 774.8416 1546.771 775.3237 1447.243 775.8058 1350.350 776.2879 1251.366 776.7700 1150.293 777.2521 1075.373 777.7343 1043.461 778.2164 1016.182 778.6985 931.3076 779.1806 810.1924 779.6627 698.9512 780.1448 611.2480 780.6270 545.0117 781.1091 513.6572 781.5912 503.8320 782.0733 476.0244 782.5554 414.4209 783.0375 354.4375 783.5197 300.7793 784.0018 255.4824 784.4839 231.8213 784.9660 230.2988 785.4481 222.4336 785.9302 188.3486 786.4124 141.1094 786.8945 102.2715 787.3766 70.60547 787.8587 41.39941 788.3408 15.35547 788.8229 10.79688 789.3051 41.78125 789.7872 78.65137 790.2693 99.31055 790.7514 96.55957 791.2335 87.18359 791.7156 78.34277 792.1978 69.95020 792.6799 63.85449 793.1620 60.18457 793.6441 57.03223 794.1262 66.70996 794.6083 70.41211 795.0905 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