#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-06-07 10:43:13 +0300 (Thu, 07 Jun 2018) $
#$Revision: 953 $
#$URL: svn://172.16.1.111/rod/cif/1/00/04/1000420.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000420
loop_
_publ_author_name
'Zubkova, N. V.'
'Pushcharovsky, D. Y.'
'Giester, G.'
'Tillmanns, E.'
'Pekov, I. V.'
'Kleimenov, D. A.'
_publ_section_title
;
 The crystal structure of arsentsumebite, Pb2Cu[(As,S)O4]2(OH) Locality:
 oxidation zone of the Berezovskoye gold deposit, Middle Urals, Russia
;
_journal_name_full               'Mineralogy and Petrology'
_journal_page_first              79
_journal_page_last               88
_journal_paper_doi               10.1007/s007100200016
_journal_volume                  75
_journal_year                    2002
_chemical_compound_source        R110041
_chemical_formula_sum            'As Cu H O9 Pb2 S'
_chemical_name_mineral           Arsentsumebite
_space_group_IT_number           11
_symmetry_space_group_name_Hall  '-P 2yb'
_symmetry_space_group_name_H-M   'P 1 21/m 1'
_cell_angle_alpha                90
_cell_angle_beta                 112.29
_cell_angle_gamma                90
_cell_length_a                   7.804
_cell_length_b                   5.890
_cell_length_c                   8.964
_cell_volume                     381.246
_exptl_crystal_density_diffrn    6.359
_cod_original_formula_sum        'Pb2 Cu (As S) (O9 H)'
_cod_database_code               9009849
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R110041.rod
_rod_data_source.block           3500000
_rod_database.code               1000420
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9009849 COD http://www.crystallography.net/cod/9009849.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
194.6294 0.0000000E+00
195.1115 0.3747560
195.5936 1.844971
196.0757 3.794556
196.5579 5.959229
197.0400 8.599854
197.5221 11.75403
198.0042 13.96704
198.4863 13.85669
198.9684 11.78125
199.4506 10.90369
199.9327 11.49658
200.4148 13.13452
200.8969 14.95374
201.3790 17.46436
201.8611 19.45459
202.3433 19.68188
202.8254 17.29578
203.3075 15.89148
203.7896 16.37634
204.2717 18.35388
204.7538 19.36401
205.2360 19.44543
205.7181 19.63281
206.2002 20.34558
206.6823 22.27991
207.1644 22.70093
207.6465 21.24536
208.1287 18.91211
208.6108 16.45520
209.0929 13.80127
209.5750 12.99048
210.0571 17.04370
210.5392 20.78796
211.0214 23.78357
211.5035 28.07031
211.9856 32.93030
212.4677 34.22253
212.9498 31.64563
213.4319 29.01562
213.9140 28.03455
214.3962 27.92126
214.8783 26.57996
215.3604 23.48425
215.8425 19.33887
216.3246 16.94653
216.8067 17.02588
217.2889 17.65405
217.7710 17.52930
218.2531 16.11304
218.7352 14.98376
219.2173 14.56873
219.6994 14.56189
220.1816 13.37573
220.6637 10.47449
221.1458 7.778442
221.6279 6.571289
222.1100 7.643799
222.5921 8.208130
223.0743 8.289917
223.5564 7.770142
224.0385 5.423340
224.5206 0.2735600
225.0027 5.351074
225.4848 6.973022
225.9670 3.273926
226.4491 0.8425290
226.9312 0.3809810
227.4133 1.549316
227.8954 2.887085
228.3775 4.808594
228.8597 6.260254
229.3418 6.458252
229.8239 4.695313
230.3060 3.421265
230.7881 2.980835
231.2702 3.215088
231.7524 3.476074
232.2345 4.335205
232.7166 4.483643
233.1987 2.954102
233.6808 1.398071
234.1629 4.815796
234.6451 6.958374
235.1272 7.974976
235.6093 8.550049
236.0914 8.469360
236.5735 8.244263
237.0556 8.206421
237.5378 8.667114
238.0199 8.679199
238.5020 8.099609
238.9841 7.057983
239.4662 6.007690
239.9483 4.700806
240.4305 3.805664
240.9126 3.749634
241.3947 4.992065
241.8768 6.139160
242.3589 7.136841
242.8410 8.004395
243.3232 8.749390
243.8053 8.897705
244.2874 9.564941
244.7695 11.61707
245.2516 16.76526
245.7337 19.32898
246.2159 18.13586
246.6980 14.33264
247.1801 11.69019
247.6622 10.79846
248.1443 10.09424
248.6264 8.731323
249.1086 6.017700
249.5907 4.341187
250.0728 4.237793
250.5549 5.063232
251.0370 5.062622
251.5191 3.858643
252.0013 2.466797
252.4834 2.474976
252.9655 2.586914
253.4476 3.214966
253.9297 4.845459
254.4118 6.790039
254.8940 7.329834
255.3761 5.485596
255.8582 3.954712
256.3403 4.011597
256.8224 6.300781
257.3046 7.948975
257.7867 8.749390
258.2688 8.991211
258.7509 9.137939
259.2330 8.900391
259.7151 9.106812
260.1973 10.13281
260.6794 12.09827
261.1615 14.32227
261.6436 17.21899
262.1257 20.02747
262.6078 21.02588
263.0900 18.95203
263.5721 18.15637
264.0542 20.77258
264.5363 27.72717
265.0184 32.26904
265.5005 34.02869
265.9827 33.96533
266.4648 32.95813
266.9469 30.11377
267.4290 29.00964
267.9111 31.43201
268.3932 37.71936
268.8754 41.77063
269.3575 42.73438
269.8396 42.70288
270.3217 44.42969
270.8038 48.37329
271.2859 52.09436
271.7681 54.85950
272.2502 56.70276
272.7323 58.53381
273.2144 60.29492
273.6965 62.00623
274.1786 63.35303
274.6608 64.06323
275.1429 66.30261
275.6250 71.02478
276.1071 77.80701
276.5892 83.86755
277.0714 89.08521
277.5535 93.68091
278.0356 97.50574
278.5177 100.3966
278.9998 103.9218
279.4819 108.6180
279.9641 114.2279
280.4462 119.2399
280.9283 123.6174
281.4104 127.5559
281.8925 130.8098
282.3746 133.1863
282.8568 136.5995
283.3389 141.8807
283.8210 148.7753
284.3031 155.4462
284.7852 161.7405
285.2673 168.4060
285.7495 176.3640
286.2316 185.4919
286.7137 194.1866
287.1958 201.8702
287.6779 209.9307
288.1600 221.9203
288.6422 237.8606
289.1243 253.0371
289.6064 263.0803
290.0885 269.1622
290.5706 277.1196
291.0527 287.6527
291.5349 300.1733
292.0170 314.5317
292.4991 330.2877
292.9812 344.5901
293.4633 353.9003
293.9454 360.2367
294.4276 370.4684
294.9097 385.3967
295.3918 401.8352
295.8739 416.2439
296.3560 428.6808
296.8381 440.1254
297.3203 450.6587
297.8024 460.4387
298.2845 470.1007
298.7666 479.7721
299.2487 488.6378
299.7308 495.2791
300.2130 500.4667
300.6951 506.3157
301.1772 514.5864
301.6593 523.5233
302.1414 530.5544
302.6235 535.6489
303.1057 540.3137
303.5878 546.4613
304.0699 552.9236
304.5520 557.3884
305.0341 558.4390
305.5162 557.8302
305.9984 556.8271
306.4805 555.5507
306.9626 554.7976
307.4447 556.2728
307.9268 558.2579
308.4089 558.6241
308.8911 557.1797
309.3732 553.4216
309.8553 545.8671
310.3374 535.4086
310.8195 524.8859
311.3016 515.2969
311.7838 506.8149
312.2659 499.7830
312.7480 494.9996
313.2301 489.9445
313.7122 482.1611
314.1943 472.9401
314.6765 465.1660
315.1586 462.3971
315.6407 459.8994
316.1228 454.5027
316.6049 445.1481
317.0870 435.7617
317.5692 428.1019
318.0513 421.4601
318.5334 414.8947
319.0155 407.2876
319.4976 400.4222
319.9797 395.5382
320.4619 392.8136
320.9440 389.5298
321.4261 383.8597
321.9082 377.8152
322.3903 373.2965
322.8724 371.9395
323.3546 370.9380
323.8367 369.6915
324.3188 368.1815
324.8009 366.5958
325.2830 364.6621
325.7651 362.6716
326.2473 360.8280
326.7294 358.8912
327.2115 357.7542
327.6936 358.0240
328.1757 359.2916
328.6578 360.0011
329.1400 358.9719
329.6221 358.5322
330.1042 359.7012
330.5863 363.2775
331.0684 367.2035
331.5505 371.6594
332.0327 376.3804
332.5148 380.7197
332.9969 384.3323
333.4790 387.9229
333.9611 391.6289
334.4432 395.2043
334.9254 399.8517
335.4075 406.4120
335.8896 413.1882
336.3717 417.6355
336.8538 418.7534
337.3359 419.8694
337.8180 422.3871
338.3001 426.2446
338.7823 427.2805
339.2644 425.3156
339.7465 420.9689
340.2286 414.1765
340.7107 404.4939
341.1928 395.6719
341.6750 389.1110
342.1571 383.8694
342.6392 376.7019
343.1213 367.5009
343.6034 356.7612
344.0855 344.1799
344.5677 329.9469
345.0498 315.9286
345.5319 302.3081
346.0140 289.2362
346.4961 277.1360
346.9782 266.0271
347.4604 255.2189
347.9425 244.1162
348.4246 232.9854
348.9067 223.5518
349.3888 216.1906
349.8709 209.0841
350.3531 199.6028
350.8352 188.3702
351.3173 177.7605
351.7994 168.6648
352.2815 160.7717
352.7636 153.7437
353.2458 147.5643
353.7279 141.5537
354.2100 134.8700
354.6921 127.9821
355.1742 121.7899
355.6563 117.0017
356.1385 112.4475
356.6206 106.6443
357.1027 99.87964
357.5848 93.75598
358.0669 90.12708
358.5490 87.08752
359.0312 82.68787
359.5133 75.90283
359.9954 69.11926
360.4775 63.61731
360.9596 59.11108
361.4417 55.05603
361.9239 51.17053
362.4060 47.69666
362.8881 45.03699
363.3702 43.49805
363.8523 41.35388
364.3344 36.14307
364.8166 30.69299
365.2987 28.21460
365.7808 34.64758
366.2629 38.99622
366.7450 37.38257
367.2271 29.78040
367.7093 22.91296
368.1914 16.76294
368.6735 12.05957
369.1556 9.280884
369.6377 10.81995
370.1198 11.32959
370.6020 10.08179
371.0841 7.570557
371.5662 5.663208
372.0483 5.294312
372.5304 4.381226
373.0125 1.807861
373.4947 3.486084
373.9768 7.360107
374.4589 9.556885
374.9410 10.58875
375.4231 11.14502
375.9052 11.05188
376.3874 10.93738
376.8695 11.15454
377.3516 11.64648
377.8337 10.84766
378.3158 8.323608
378.7979 5.589111
379.2801 4.129883
379.7622 3.953491
380.2443 4.347778
380.7264 5.339111
381.2085 6.675659
381.6906 8.026001
382.1728 9.423950
382.6549 9.868164
383.1370 7.937744
383.6191 4.345825
384.1012 2.209717
384.5833 2.184570
385.0655 2.502441
385.5476 0.4932860
386.0297 3.276367
386.5118 6.672729
386.9939 9.035522
387.4760 10.30176
387.9582 9.577759
388.4403 6.838989
388.9224 5.140747
389.4045 8.504150
389.8866 14.08606
390.3687 17.87048
390.8509 17.78845
391.3330 16.29370
391.8151 14.33069
392.2972 12.19507
392.7793 11.02002
393.2614 12.26147
393.7436 14.10229
394.2257 15.36877
394.7078 15.93872
395.1899 15.64307
395.6720 13.05591
396.1541 9.782349
396.6363 8.410034
397.1184 11.32849
397.6005 14.58630
398.0826 16.90161
398.5647 18.10938
399.0468 19.14551
399.5290 20.25732
400.0111 21.13647
400.4932 21.51929
400.9753 20.45728
401.4574 20.20032
401.9395 21.26538
402.4217 23.36328
402.9038 24.99622
403.3859 25.53210
403.8680 26.54504
404.3501 29.08423
404.8322 33.94177
405.3144 37.37573
405.7965 38.93774
406.2786 39.55981
406.7607 40.72461
407.2428 42.55457
407.7249 44.24780
408.2071 45.42053
408.6892 46.19482
409.1713 47.15308
409.6534 48.20740
410.1355 49.98486
410.6176 54.04053
411.0998 59.74719
411.5819 63.07617
412.0640 62.58911
412.5461 60.48132
413.0282 60.19275
413.5103 61.51233
413.9925 63.18298
414.4746 64.75989
414.9567 66.13586
415.4388 66.92810
415.9209 67.02747
416.4030 67.36365
416.8852 69.30664
417.3673 71.92896
417.8494 73.72363
418.3315 73.97888
418.8136 73.37842
419.2957 71.68665
419.7779 69.21631
420.2600 67.81519
420.7421 69.77734
421.2242 72.28638
421.7063 73.05579
422.1884 70.17908
422.6706 68.46936
423.1527 69.25000
423.6348 71.96606
424.1169 75.53760
424.5990 79.82751
425.0811 84.95520
425.5633 91.02112
426.0454 98.06543
426.5275 105.5791
427.0096 113.4790
427.4917 121.9528
427.9738 131.2797
428.4560 141.9634
428.9381 152.2112
429.4202 161.1259
429.9023 169.4557
430.3844 180.5984
430.8665 195.2102
431.3487 210.4121
431.8308 224.8434
432.3129 238.4760
432.7950 252.1398
433.2771 265.3654
433.7592 279.9880
434.2414 299.3253
434.7235 323.0167
435.2056 346.9324
435.6877 370.3132
436.1698 392.8800
436.6519 413.8778
437.1341 433.3149
437.6162 452.3214
438.0983 474.1262
438.5804 495.7311
439.0625 511.5300
439.5446 519.8112
440.0268 524.9083
440.5089 531.4189
440.9910 537.7686
441.4731 540.4845
441.9552 537.4139
442.4373 530.4209
442.9195 520.5614
443.4016 507.9763
443.8837 492.5088
444.3658 472.0100
444.8479 449.5474
445.3300 427.6924
445.8122 405.5070
446.2943 385.5308
446.7764 369.5212
447.2585 355.9609
447.7406 340.9843
448.2227 321.1193
448.7049 303.0184
449.1870 289.0004
449.6691 280.1287
450.1512 269.5793
450.6333 256.2323
451.1154 242.6097
451.5976 230.9403
452.0797 221.3263
452.5618 213.8497
453.0439 208.8622
453.5260 205.9131
454.0081 203.4713
454.4903 201.5891
454.9724 199.9282
455.4545 197.8915
455.9366 195.7280
456.4187 195.6257
456.9008 198.0221
457.3830 200.5773
457.8651 199.5735
458.3472 196.3125
458.8293 195.2759
459.3114 199.4800
459.7935 204.8525
460.2757 206.5316
460.7578 204.8840
461.2399 201.8933
461.7220 196.8290
462.2041 191.9935
462.6862 190.2678
463.1684 192.9147
463.6505 194.7438
464.1326 192.9592
464.6147 188.9966
465.0968 184.6265
465.5789 180.3021
466.0611 175.6277
466.5432 169.9596
467.0253 163.5717
467.5074 158.4830
467.9895 155.6375
468.4716 153.3003
468.9538 151.0151
469.4359 149.2954
469.9180 146.5426
470.4001 142.5026
470.8822 137.5422
471.3643 131.9388
471.8465 125.1218
472.3286 119.3008
472.8107 115.2733
473.2928 112.7787
473.7749 109.9816
474.2570 106.9045
474.7392 103.5391
475.2213 99.52869
475.7034 94.96179
476.1855 90.93274
476.6676 87.58423
477.1497 84.65515
477.6319 81.87048
478.1140 79.39087
478.5961 77.64197
479.0782 77.77063
479.5603 78.11841
480.0424 76.22546
480.5246 72.41150
481.0067 69.36890
481.4888 69.54700
481.9709 70.52002
482.4530 70.20984
482.9352 67.63953
483.4173 65.26855
483.8994 64.79919
484.3815 64.79102
484.8636 63.37720
485.3457 57.91174
485.8279 53.28870
486.3100 51.31506
486.7921 52.01770
487.2742 51.75061
487.7563 50.04700
488.2384 47.88953
488.7206 45.85474
489.2027 44.03955
489.6848 41.97791
490.1669 39.58496
490.6490 37.06665
491.1311 34.64844
491.6133 32.33411
492.0954 30.21729
492.5775 28.19751
493.0596 26.40161
493.5417 25.76929
494.0238 26.31628
494.5060 26.34790
494.9881 23.42114
495.4702 19.05457
495.9523 17.46973
496.4344 19.71094
496.9165 22.36597
497.3987 21.77417
497.8808 19.18677
498.3629 16.97559
498.8450 16.40271
499.3271 16.24231
499.8092 16.03003
500.2914 15.69958
500.7735 14.85205
501.2556 12.13000
501.7377 9.749146
502.2198 9.396362
502.7019 12.74854
503.1841 14.30188
503.6662 11.50354
504.1483 7.319214
504.6304 5.296997
505.1125 7.153564
505.5946 8.541260
506.0768 8.723145
506.5589 7.762451
507.0410 6.456299
507.5231 4.458130
508.0052 3.114136
508.4873 3.491089
508.9695 5.598022
509.4516 6.824463
509.9337 7.138550
510.4158 6.589478
510.8979 4.405273
511.3800 1.150024
511.8622 0.3319090
512.3443 1.564941
512.8264 4.239258
513.3085 3.868286
513.7906 1.209351
514.2728 1.034546
514.7549 0.6433110
515.2370 0.4219970
515.7191 0.2404790
516.2012 1.427002
516.6833 2.832275
517.1655 2.847412
517.6476 2.395264
518.1297 2.263550
518.6118 3.013184
519.0939 3.583862
519.5760 3.825684
520.0582 3.769775
520.5403 3.484619
521.0224 2.482422
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1282.767 4.401611
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1301.087 3.472412
1301.569 3.233765
1302.051 2.428833
1302.533 1.388916
1303.016 0.0000000E+00
