#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-06-07 10:47:22 +0300 (Thu, 07 Jun 2018) $
#$Revision: 967 $
#$URL: svn://172.16.1.111/rod/cif/1/00/04/1000427.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000427
loop_
_publ_author_name
'Basso, R.'
'Cabella, R.'
'Lucchetti, G.'
'Martinelli, A.'
'Palenzona, A.'
_publ_section_title
;
 Vanadiocarpholite, Mn2+V3+Al(Si2O6)(OH)4, a new mineral from the
 Molinello mine, northern Apennines, Italy Note: sample VrC Locality:
 Molinello mine, northern Apennines, Italy
;
_journal_name_full               'European Journal of Mineralogy'
_journal_page_first              501
_journal_page_last               507
_journal_paper_doi               10.1127/0935-1221/2005/0017-0501
_journal_volume                  17
_journal_year                    2005
_chemical_compound_source        R060608
_chemical_formula_sum
'Al3.02 H8 K0.012 Mg0.26 Mn1.74 O20 Si4 V0.98'
_chemical_name_mineral           Carpholite
_space_group_IT_number           68
_symmetry_space_group_name_Hall  '-C 2a 2ac'
_symmetry_space_group_name_H-M   'C c c a :2'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   13.840
_cell_length_b                   20.452
_cell_length_c                   5.143
_cell_volume                     1455.755
_exptl_crystal_density_diffrn    3.076
_cod_original_sg_symbol_H-M      'C c c a'
_cod_original_formula_sum        'K.012 (Mn1.74 Mg.26) Al3.02 V.98 Si4 O20 H8'
_cod_database_code               9005714
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R060608.rod
_rod_data_source.block           3500000
_rod_database.code               1000427
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9005714 COD http://www.crystallography.net/cod/9005714.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
118.629 0.000
119.112 15.075
119.594 1.707
120.076 3.229
120.558 70.388
121.040 164.361
121.522 263.407
122.004 369.339
122.486 465.591
122.968 540.311
123.451 593.539
123.933 629.110
124.415 634.475
124.897 625.100
125.379 622.865
125.861 620.171
126.343 637.596
126.825 721.753
127.307 873.212
127.790 1021.203
128.272 1107.077
128.754 1135.329
129.236 1124.890
129.718 1073.881
130.200 992.386
130.682 894.177
131.164 771.334
131.646 641.025
132.129 520.016
132.611 408.789
133.093 315.440
133.575 244.926
134.057 196.758
134.539 159.576
135.021 133.298
135.503 114.684
135.986 97.336
136.468 80.891
136.950 66.056
137.432 51.779
137.914 37.085
138.396 31.428
138.878 39.919
139.360 58.631
139.842 65.493
140.325 57.113
140.807 43.352
141.289 24.693
141.771 17.081
142.253 16.313
142.735 15.169
143.217 9.323
143.699 4.843
144.182 1.658
144.664 3.125
145.146 1.180
145.628 6.221
146.110 10.487
146.592 24.147
147.074 72.518
147.556 119.049
148.038 169.762
148.521 219.046
149.003 260.544
149.485 277.064
149.967 306.849
150.449 347.890
150.931 414.839
151.413 478.125
151.895 524.766
152.378 553.277
152.860 597.524
153.342 674.823
153.824 766.862
154.306 864.804
154.788 972.709
155.270 1080.967
155.752 1189.696
156.234 1298.721
156.717 1409.444
157.199 1522.302
157.681 1636.383
158.163 1749.552
158.645 1852.171
159.127 1962.872
159.609 2098.417
160.091 2257.679
160.574 2394.317
161.056 2503.076
161.538 2577.131
162.020 2609.499
162.502 2607.712
162.984 2554.918
163.466 2432.281
163.948 2233.864
164.430 2012.321
164.913 1773.733
165.395 1532.083
165.877 1304.184
166.359 1088.505
166.841 895.121
167.323 734.633
167.805 612.643
168.287 505.741
168.770 393.577
169.252 285.904
169.734 202.216
170.216 174.315
170.698 165.588
171.180 139.132
171.662 80.672
172.144 26.378
172.626 5.343
173.109 12.024
173.591 18.920
174.073 2.121
174.555 24.789
175.037 32.271
175.519 33.209
176.001 36.100
176.483 36.619
176.965 33.116
177.448 23.373
177.930 11.165
178.412 2.094
178.894 13.421
179.376 20.623
179.858 26.478
180.340 39.163
180.822 58.344
181.305 70.192
181.787 53.356
182.269 17.141
182.751 9.196
183.233 7.564
183.715 8.497
184.197 9.677
184.679 4.550
185.161 28.328
185.644 22.946
186.126 13.061
186.608 49.080
187.090 82.633
187.572 114.028
188.054 142.855
188.536 167.216
189.018 195.876
189.501 241.413
189.983 302.404
190.465 368.937
190.947 434.029
191.429 499.651
191.911 576.905
192.393 668.378
192.875 765.284
193.357 850.522
193.840 922.981
194.322 1006.989
194.804 1124.295
195.286 1272.572
195.768 1406.584
196.250 1520.281
196.732 1624.135
197.214 1741.186
197.697 1872.968
198.179 2007.680
198.661 2136.276
199.143 2258.091
199.625 2397.064
200.107 2564.319
200.589 2745.430
201.071 2899.027
201.553 3018.084
202.036 3139.242
202.518 3284.609
203.000 3454.577
203.482 3649.118
203.964 3875.848
204.446 4124.310
204.928 4357.712
205.410 4574.896
205.893 4780.190
206.375 4976.396
206.857 5167.496
207.339 5341.713
207.821 5496.860
208.303 5631.059
208.785 5734.567
209.267 5818.871
209.749 5845.968
210.232 5780.280
210.714 5608.529
211.196 5399.158
211.678 5160.748
212.160 4893.064
212.642 4604.307
213.124 4290.105
213.606 3953.171
214.089 3595.032
214.571 3195.971
215.053 2824.491
215.535 2491.763
216.017 2196.223
216.499 1923.951
216.981 1675.334
217.463 1446.066
217.945 1228.815
218.428 1022.845
218.910 840.017
219.392 686.827
219.874 563.143
220.356 452.543
220.838 357.042
221.320 273.432
221.802 200.028
222.285 139.050
222.767 83.744
223.249 32.075
223.731 17.131
224.213 5.443
224.695 37.216
225.177 54.363
225.659 42.514
226.141 16.752
226.624 17.151
227.106 47.320
227.588 49.411
228.070 62.560
228.552 88.803
229.034 124.426
229.516 165.776
229.998 221.005
230.480 266.088
230.963 294.820
231.445 305.069
231.927 306.448
232.409 292.333
232.891 271.448
233.373 256.513
233.855 251.211
234.337 246.271
234.820 239.028
235.302 229.466
235.784 218.105
236.266 200.574
236.748 183.353
237.230 178.596
237.712 193.189
238.194 209.466
238.676 220.285
239.159 222.817
239.641 233.265
240.123 244.510
240.605 268.027
241.087 330.136
241.569 464.662
242.051 586.851
242.533 670.231
243.016 714.844
243.498 719.952
243.980 661.655
244.462 574.403
244.944 528.306
245.426 551.811
245.908 571.452
246.390 558.705
246.872 500.026
247.355 451.639
247.837 416.079
248.319 389.629
248.801 365.942
249.283 344.962
249.765 326.733
250.247 312.962
250.729 308.181
251.212 291.751
251.694 255.100
252.176 211.918
252.658 189.016
253.140 194.484
253.622 206.556
254.104 217.434
254.586 224.956
255.068 240.250
255.551 269.078
256.033 302.176
256.515 322.177
256.997 327.912
257.479 322.883
257.961 306.436
258.443 274.159
258.925 245.990
259.408 223.501
259.890 203.429
260.372 179.351
260.854 149.644
261.336 118.716
261.818 86.715
262.300 52.077
262.782 24.398
263.264 7.389
263.746 6.010
264.229 30.728
264.711 65.911
265.193 31.244
265.675 21.650
266.157 43.797
266.639 51.429
267.121 37.774
267.603 16.855
268.086 12.316
268.568 27.967
269.050 48.586
269.532 66.324
270.014 67.163
270.496 37.387
270.978 13.929
271.460 77.026
271.943 139.304
272.425 201.167
272.907 259.035
273.389 307.613
273.871 344.993
274.353 403.046
274.835 483.365
275.317 579.964
275.799 686.647
276.282 803.358
276.764 928.649
277.246 1071.381
277.728 1229.907
278.210 1356.211
278.692 1449.375
279.174 1506.924
279.656 1524.375
280.138 1501.207
280.621 1440.839
281.103 1333.008
281.585 1180.469
282.067 1035.716
282.549 895.207
283.031 770.364
283.513 659.281
283.995 561.794
284.478 542.187
284.960 528.577
285.442 550.480
285.924 563.800
286.406 569.000
286.888 541.671
287.370 556.419
287.852 554.351
288.335 560.662
288.817 576.673
289.299 607.909
289.781 626.083
290.263 630.504
290.745 628.784
291.227 629.795
291.709 632.010
292.191 626.414
292.674 609.108
293.156 583.123
293.638 552.082
294.120 516.060
294.602 483.664
295.084 460.530
295.566 447.056
296.048 446.345
296.530 463.770
297.013 490.174
297.495 510.396
297.977 524.989
298.459 536.906
298.941 544.128
299.423 550.950
299.905 566.862
300.387 595.278
300.870 632.380
301.352 679.717
301.834 735.080
302.316 783.287
302.798 804.575
303.280 813.811
303.762 836.453
304.244 883.135
304.727 933.501
305.209 965.319
305.691 981.901
306.173 996.225
306.655 1015.453
307.137 1036.456
307.619 1055.765
308.101 1073.138
308.583 1087.614
309.065 1098.500
309.548 1105.926
310.030 1109.820
310.512 1109.639
310.994 1107.095
311.476 1101.297
311.958 1089.211
312.440 1084.698
312.922 1112.657
313.405 1152.177
313.887 1165.699
314.369 1115.338
314.851 1050.357
315.333 1000.207
315.815 969.154
316.297 942.542
316.779 921.303
317.262 899.264
317.744 868.116
318.226 805.761
318.708 747.141
319.190 709.677
319.672 696.772
320.154 682.721
320.636 654.086
321.118 623.633
321.601 604.500
322.083 613.311
322.565 616.290
323.047 604.790
323.529 577.618
324.011 553.484
324.493 534.879
324.975 521.979
325.457 514.226
325.940 509.767
326.422 511.756
326.904 521.323
327.386 538.114
327.868 558.224
328.350 584.907
328.832 613.968
329.314 642.049
329.797 663.710
330.279 694.012
330.761 736.115
331.243 787.355
331.725 836.039
332.207 873.345
332.689 918.873
333.171 981.888
333.654 1069.745
334.136 1160.204
334.618 1251.260
335.100 1344.907
335.582 1451.096
336.064 1581.799
336.546 1697.579
337.028 1771.845
337.510 1787.504
337.992 1855.894
338.475 1995.600
338.957 2165.594
339.439 2309.280
339.921 2421.173
340.403 2526.176
340.885 2633.090
341.367 2741.938
341.849 2835.669
342.332 2914.751
342.814 2979.603
343.296 3039.050
343.778 3093.092
344.260 3107.110
344.742 3064.971
345.224 2976.742
345.706 2879.639
346.189 2773.802
346.671 2649.501
347.153 2490.799
347.635 2302.997
348.117 2119.843
348.599 1948.934
349.081 1786.088
349.563 1626.235
350.045 1469.722
350.528 1321.447
351.010 1183.515
351.492 1056.240
351.974 940.493
352.456 834.666
352.938 741.286
353.420 668.600
353.902 611.958
354.384 554.870
354.867 483.087
355.349 409.557
355.831 347.940
356.313 299.751
356.795 263.736
357.277 246.050
357.759 239.211
358.241 230.682
358.724 218.545
359.206 200.571
359.688 169.991
360.170 125.828
360.652 91.643
361.134 68.054
361.616 59.384
362.098 54.897
362.581 49.415
363.063 42.991
363.545 32.756
364.027 27.477
364.509 20.233
364.991 12.920
365.473 7.290
365.955 12.294
366.437 13.362
366.919 11.908
367.402 7.451
367.884 0.479
368.366 7.284
368.848 19.836
369.330 29.560
369.812 33.140
370.294 26.096
370.776 21.805
371.259 20.286
371.741 21.446
372.223 25.635
372.705 35.725
373.187 43.986
373.669 46.208
374.151 40.479
374.633 46.217
375.116 58.700
375.598 31.993
376.080 11.148
376.562 4.324
377.044 12.073
377.526 7.530
378.008 5.525
378.490 1.949
378.973 22.072
379.455 45.453
379.937 47.491
380.419 29.562
380.901 19.310
381.383 24.133
381.865 34.537
382.347 30.738
382.829 13.278
383.311 7.450
383.794 26.166
384.276 43.407
384.758 59.292
385.240 59.695
385.722 42.341
386.204 10.057
386.686 33.439
387.168 78.441
387.651 117.258
388.133 157.072
388.615 205.445
389.097 262.916
389.579 327.954
390.061 402.536
390.543 482.559
391.025 564.850
391.508 642.868
391.990 726.854
392.472 821.230
392.954 926.586
393.436 1041.731
393.918 1168.874
394.400 1304.082
394.882 1446.965
395.364 1604.206
395.847 1757.145
396.329 1893.810
396.811 2024.233
397.293 2171.285
397.775 2348.024
398.257 2534.675
398.739 2726.684
399.221 2932.067
399.703 3118.860
400.186 3285.077
400.668 3433.249
401.150 3567.644
401.632 3702.919
402.114 3802.186
402.596 3862.623
403.078 3883.760
403.560 3844.437
404.043 3731.241
404.525 3579.233
405.007 3412.122
405.489 3231.969
405.971 3022.369
406.453 2766.811
406.935 2493.642
407.417 2266.442
407.900 2090.054
408.382 1935.808
408.864 1789.370
409.346 1651.234
409.828 1528.293
410.310 1417.158
410.792 1331.217
411.274 1297.762
411.756 1307.740
412.238 1317.196
412.721 1303.911
413.203 1282.129
413.685 1274.123
414.167 1279.845
414.649 1295.590
415.131 1323.811
415.613 1359.024
416.095 1392.751
416.578 1422.819
417.060 1451.244
417.542 1497.574
418.024 1546.673
418.506 1554.933
418.988 1449.683
419.470 1332.266
419.952 1278.312
420.435 1314.456
420.917 1340.673
421.399 1312.572
421.881 1258.252
422.363 1214.068
422.845 1195.116
423.327 1179.903
423.809 1160.963
424.291 1137.935
424.774 1126.124
425.256 1125.286
425.738 1136.514
426.220 1160.719
426.702 1201.406
427.184 1247.281
427.666 1291.394
428.148 1343.047
428.630 1431.437
429.113 1569.240
429.595 1713.915
430.077 1845.479
430.559 1960.440
431.041 2078.959
431.523 2199.321
432.005 2331.170
432.487 2487.909
432.970 2668.487
433.452 2861.318
433.934 3064.665
434.416 3275.597
434.898 3486.865
435.380 3701.149
435.862 3931.688
436.344 4208.428
436.827 4507.554
437.309 4782.792
437.791 5038.077
438.273 5243.323
438.755 5366.863
439.237 5415.471
439.719 5408.520
440.201 5363.326
440.683 5264.784
441.165 5088.449
441.648 4827.239
442.130 4538.120
442.612 4240.948
443.094 3938.136
443.576 3636.090
444.058 3321.947
444.540 3027.678
445.022 2760.584
445.505 2516.320
445.987 2287.474
446.469 2053.407
446.951 1845.787
447.433 1675.236
447.915 1528.755
448.397 1454.687
448.879 1361.894
449.362 1294.515
449.844 1220.925
450.326 1141.444
450.808 1038.552
451.290 965.795
451.772 881.857
452.254 803.478
452.736 726.249
453.218 681.753
453.701 667.469
454.183 683.477
454.665 699.887
455.147 713.013
455.629 724.030
456.111 733.055
456.593 740.160
457.075 748.875
457.557 760.969
458.040 776.334
458.522 794.396
459.004 815.190
459.486 839.735
459.968 875.382
460.450 914.172
460.932 942.599
461.414 947.406
461.897 950.456
462.379 962.476
462.861 983.033
463.343 1015.314
463.825 1075.917
464.307 1134.773
464.789 1168.916
465.271 1165.647
465.754 1170.257
466.236 1207.934
466.718 1253.000
467.200 1272.491
467.682 1235.172
468.164 1205.406
468.646 1197.771
469.128 1210.517
469.610 1213.470
470.093 1207.860
470.575 1190.563
471.057 1156.842
471.539 1102.180
472.021 1051.668
472.503 1007.115
472.985 965.857
473.467 923.890
473.949 881.712
474.432 835.084
474.914 780.824
475.396 720.995
475.878 659.148
476.360 595.006
476.842 539.039
477.324 505.535
477.806 486.879
478.289 469.325
478.771 452.673
479.253 430.536
479.735 387.914
480.217 334.237
480.699 293.651
481.181 281.466
481.663 284.009
482.146 299.493
482.628 329.868
483.110 343.380
483.592 312.307
484.074 267.494
484.556 236.459
485.038 237.336
485.520 235.785
486.002 221.832
486.484 201.494
486.967 195.061
487.449 218.474
487.931 234.177
488.413 224.990
488.895 185.264
489.377 155.337
489.859 137.558
490.341 126.686
490.824 118.424
491.306 113.168
491.788 107.474
492.270 101.848
492.752 94.438
493.234 78.256
493.716 54.134
494.198 31.448
494.681 14.005
495.163 2.774
495.645 3.257
496.127 17.443
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