#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-06-07 10:51:56 +0300 (Thu, 07 Jun 2018) $
#$Revision: 972 $
#$URL: svn://172.16.1.111/rod/cif/1/00/04/1000432.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000432
loop_
_publ_author_name
'Antao, S. M.'
_publ_section_title
;
 Structural trends for celestite (SrSO4), anglesite (PbSO4), and barite
 (BaSO4): confirmation of expected variations within SO4 groups
;
_journal_name_full               'American Mineralogist'
_journal_page_first              661
_journal_page_last               665
_journal_paper_doi               10.2138/am.2012.3905
_journal_volume                  97
_journal_year                    2012
_chemical_compound_source        Synthetic
_chemical_formula_sum            'O4 Pb S'
_chemical_name_mineral           Anglesite
_space_group_IT_number           62
_symmetry_space_group_name_Hall  '-P 2c 2ab'
_symmetry_space_group_name_H-M   'P b n m'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   6.95802
_cell_length_b                   8.48024
_cell_length_c                   5.39754
_cell_volume                     318.486
_exptl_crystal_density_diffrn    6.325
_cod_original_formula_sum        'Pb S O4'
_cod_database_code               9015524
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R040004.rod
_rod_data_source.block           3500000
_rod_database.code               1000432
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9015524 COD http://www.crystallography.net/cod/9015524.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
113.1730 0.0000000E+00
113.6551 9.368896
114.1373 5.788330
114.6194 1.480225
115.1015 15.81494
115.5836 39.75830
116.0657 70.43262
116.5478 105.4106
117.0300 144.0974
117.5121 187.2952
117.9942 233.0784
118.4763 282.9343
118.9584 338.8079
119.4405 399.4651
119.9227 468.1216
120.4048 546.6191
120.8869 636.1167
121.3690 731.9294
121.8511 830.8599
122.3332 933.7944
122.8154 1042.776
123.2975 1159.934
123.7796 1282.621
124.2617 1409.948
124.7438 1539.297
125.2259 1673.525
125.7081 1815.665
126.1902 1962.386
126.6723 2086.376
127.1544 2194.386
127.6365 2303.312
128.1186 2411.083
128.6008 2516.329
129.0829 2619.918
129.5650 2724.677
130.0471 2830.326
130.5292 2930.069
131.0113 3019.383
131.4935 3098.611
131.9756 3169.168
132.4577 3233.385
132.9398 3288.742
133.4219 3324.933
133.9040 3341.761
134.3862 3344.760
134.8683 3342.177
135.3504 3333.857
135.8325 3307.426
136.3146 3256.610
136.7967 3183.058
137.2789 3100.684
137.7610 3008.167
138.2431 2908.122
138.7252 2800.650
139.2073 2683.720
139.6894 2566.927
140.1716 2452.407
140.6537 2339.103
141.1358 2227.544
141.6179 2113.430
142.1000 2002.282
142.5821 1906.543
143.0643 1827.002
143.5464 1758.676
144.0285 1698.866
144.5106 1648.821
144.9927 1605.037
145.4748 1567.890
145.9570 1537.223
146.4391 1515.337
146.9212 1504.776
147.4033 1499.321
147.8854 1495.817
148.3675 1493.142
148.8497 1494.344
149.3318 1502.377
149.8139 1515.307
150.2960 1523.741
150.7781 1532.484
151.2602 1533.570
151.7424 1524.582
152.2245 1501.586
152.7066 1471.180
153.1887 1434.686
153.6708 1393.359
154.1529 1340.804
154.6351 1268.066
155.1172 1187.502
155.5993 1108.781
156.0814 1028.729
156.5635 948.5137
157.0456 867.4065
157.5278 786.0811
158.0099 712.0317
158.4920 646.1499
158.9741 587.1406
159.4562 533.6243
159.9383 485.8196
160.4205 443.4392
160.9026 407.9971
161.3847 380.0613
161.8668 353.6746
162.3489 327.0032
162.8310 301.4945
163.3132 277.8564
163.7953 254.4866
164.2774 233.7273
164.7595 218.1379
165.2416 208.8010
165.7237 198.8948
166.2059 185.1632
166.6880 168.6830
167.1701 150.6128
167.6522 127.2056
168.1343 105.5836
168.6164 91.08423
169.0985 85.55713
169.5807 82.52429
170.0628 78.79407
170.5449 74.76672
171.0270 67.76941
171.5091 59.73279
171.9912 51.86267
172.4734 45.13794
172.9555 39.37585
173.4376 34.65466
173.9197 30.55383
174.4018 27.36841
174.8839 26.10547
175.3661 28.98608
175.8482 33.62659
176.3303 36.79724
176.8124 37.46655
177.2945 37.75464
177.7766 40.39355
178.2588 44.71753
178.7409 48.48499
179.2230 50.61340
179.7051 51.00549
180.1872 49.31946
180.6693 44.67944
181.1515 39.23010
181.6336 36.33350
182.1157 35.69385
182.5978 35.26306
183.0799 33.16687
183.5620 29.95020
184.0442 27.76184
184.5263 27.75830
185.0084 27.81201
185.4905 22.71790
185.9726 12.77258
186.4547 3.532471
186.9369 0.2504880
187.4190 1.519287
187.9011 2.342407
188.3832 2.078613
188.8653 0.2753910
189.3474 5.188477
189.8296 14.61047
190.3117 23.79382
190.7938 29.30188
191.2759 31.41711
191.7580 32.11218
192.2401 31.27051
192.7223 29.70789
193.2044 30.40820
193.6865 33.78467
194.1686 37.23938
194.6507 38.00500
195.1328 36.23169
195.6150 34.59961
196.0971 33.31665
196.5792 32.67786
197.0613 34.70142
197.5434 40.02759
198.0255 44.85107
198.5077 44.35315
198.9898 38.37280
199.4719 33.08972
199.9540 30.14636
200.4361 29.06128
200.9182 27.30432
201.4004 24.52356
201.8825 21.91760
202.3646 21.14111
202.8467 22.41565
203.3288 22.87695
203.8109 21.82050
204.2931 19.32672
204.7752 15.93506
205.2573 11.40588
205.7394 6.548706
206.2215 2.076965
206.7036 2.123596
207.1858 5.630981
207.6679 8.242554
208.1500 10.00214
208.6321 11.33472
209.1142 11.70453
209.5963 12.60535
210.0785 16.22858
210.5606 23.71674
211.0427 29.74170
211.5248 32.66235
212.0069 32.57153
212.4890 32.92560
212.9712 33.54083
213.4533 34.79724
213.9354 37.31494
214.4175 41.29712
214.8996 45.89636
215.3817 51.16718
215.8639 57.14038
216.3460 62.16370
216.8281 66.15765
217.3102 69.26331
217.7923 71.73956
218.2744 73.67151
218.7565 74.53473
219.2387 73.77808
219.7208 71.24500
220.2029 71.10516
220.6850 74.89758
221.1671 79.31622
221.6492 80.42188
222.1314 76.25635
222.6135 73.20392
223.0956 73.54993
223.5777 77.44653
224.0598 78.62042
224.5419 75.26392
225.0241 71.09601
225.5062 70.37860
225.9883 75.66785
226.4704 79.03882
226.9525 78.00751
227.4346 72.16168
227.9168 69.39502
228.3989 71.03943
228.8810 74.36963
229.3631 76.60999
229.8452 77.01086
230.3273 77.73340
230.8095 79.40833
231.2916 82.08893
231.7737 83.85504
232.2558 84.07709
232.7379 84.06879
233.2200 85.33496
233.7022 88.76788
234.1843 91.70282
234.6664 93.42767
235.1485 93.96771
235.6306 95.09882
236.1127 96.77948
236.5949 98.99072
237.0770 101.8678
237.5591 106.2043
238.0412 109.6753
238.5233 111.8259
239.0054 112.6413
239.4876 112.7459
239.9697 111.0233
240.4518 109.7661
240.9339 111.1769
241.4160 116.7089
241.8981 122.0645
242.3803 126.6865
242.8624 130.5602
243.3445 133.6419
243.8266 135.6694
244.3087 137.2260
244.7908 138.7542
245.2730 140.4093
245.7551 141.7225
246.2372 142.3123
246.7193 142.2658
247.2014 143.0729
247.6835 144.7425
248.1657 146.5751
248.6478 148.5001
249.1299 151.6411
249.6120 153.0806
250.0941 152.0146
250.5762 148.8611
251.0584 146.4221
251.5405 144.7176
252.0226 143.3842
252.5047 142.5177
252.9868 142.7284
253.4689 142.5023
253.9511 141.7994
254.4332 140.5095
254.9153 137.8167
255.3974 132.3633
255.8795 127.1133
256.3616 124.4707
256.8438 125.7702
257.3259 127.4642
257.8080 129.5599
258.2901 131.5663
258.7722 131.9550
259.2543 130.0715
259.7365 127.7808
260.2186 125.9406
260.7007 124.6030
261.1828 123.1500
261.6649 121.5905
262.1470 120.0842
262.6292 118.9460
263.1113 118.5440
263.5934 118.0165
264.0755 116.7697
264.5576 114.4316
265.0397 112.4189
265.5219 110.5655
266.0040 109.0527
266.4861 108.4621
266.9682 109.1298
267.4503 109.7754
267.9324 110.1180
268.4146 110.4593
268.8967 109.4723
269.3788 106.1724
269.8609 102.2738
270.3430 101.7833
270.8251 105.8499
271.3073 109.5282
271.7894 110.6755
272.2715 109.1140
272.7536 107.4489
273.2357 105.4261
273.7178 103.7481
274.2000 103.6086
274.6821 105.2834
275.1642 107.1238
275.6463 108.7267
276.1284 110.0837
276.6105 110.5385
277.0927 109.7798
277.5748 108.6660
278.0569 108.4016
278.5390 109.1535
279.0211 110.1152
279.5032 111.4490
279.9854 112.8615
280.4675 111.8289
280.9496 107.8268
281.4317 103.4286
281.9138 101.5882
282.3959 102.3435
282.8781 102.5186
283.3602 100.9341
283.8423 98.36078
284.3244 98.00491
284.8065 100.1130
285.2886 102.2642
285.7708 102.3010
286.2529 100.4019
286.7350 98.19907
287.2171 95.60245
287.6992 93.12231
288.1813 92.84714
288.6635 94.91840
289.1456 96.80243
289.6277 96.06335
290.1098 93.08359
290.5919 90.83908
291.0740 90.20798
291.5562 89.98627
292.0383 87.14331
292.5204 81.78577
293.0025 77.10382
293.4846 75.53726
293.9667 76.39236
294.4489 77.42041
294.9310 78.54556
295.4131 79.32101
295.8952 79.17075
296.3773 78.07547
296.8594 76.01266
297.3416 72.07062
297.8237 67.19839
298.3058 63.61331
298.7879 61.61765
299.2700 61.00238
299.7521 62.52448
300.2343 65.35645
300.7164 66.84576
301.1985 64.49722
301.6806 60.49683
302.1627 58.31064
302.6448 58.05655
303.1270 58.62689
303.6091 59.27219
304.0912 59.90948
304.5733 60.41260
305.0554 61.04205
305.5375 61.38678
306.0197 60.82965
306.5018 59.46310
306.9839 58.07602
307.4660 57.43307
307.9481 57.01321
308.4302 55.97867
308.9124 53.33621
309.3945 50.79010
309.8766 49.96155
310.3587 50.62650
310.8408 51.50851
311.3229 51.43271
311.8051 51.32718
312.2872 52.34607
312.7693 55.70242
313.2514 58.38974
313.7335 58.33859
314.2156 56.18796
314.6978 53.74771
315.1799 50.76663
315.6620 48.53992
316.1441 48.37915
316.6262 51.10974
317.1083 53.62460
317.5905 54.49600
318.0726 54.33829
318.5547 54.20248
319.0368 54.97562
319.5189 55.40524
320.0010 54.35699
320.4832 51.14523
320.9653 49.47397
321.4474 52.32617
321.9295 56.59683
322.4116 58.65210
322.8937 55.67984
323.3759 52.37134
323.8580 49.68372
324.3401 47.69318
324.8222 47.16223
325.3043 50.54242
325.7864 54.15482
326.2686 55.17325
326.7507 49.92938
327.2328 45.82211
327.7149 44.27493
328.1970 45.07352
328.6791 45.52457
329.1613 45.68253
329.6434 45.39084
330.1255 44.49622
330.6076 41.43747
331.0897 40.08786
331.5718 41.86417
332.0540 45.36127
332.5361 46.43484
333.0182 43.19916
333.5003 40.04227
333.9824 38.88367
334.4645 40.67761
334.9467 41.51974
335.4288 41.20166
335.9109 40.07324
336.3930 38.49091
336.8751 35.89905
337.3572 34.17990
337.8394 34.25748
338.3215 36.24091
338.8036 36.93539
339.2857 35.88071
339.7678 34.34476
340.2499 34.07681
340.7320 35.51389
341.2141 35.39178
341.6963 32.28616
342.1784 27.12387
342.6605 24.47665
343.1426 24.71127
343.6247 25.79510
344.1068 26.46567
344.5890 26.68716
345.0711 25.75980
345.5532 23.07587
346.0353 19.90588
346.5174 19.26547
346.9995 21.11902
347.4817 23.07928
347.9638 23.80087
348.4459 23.46439
348.9280 22.55090
349.4101 20.97787
349.8922 19.33652
350.3744 18.56863
350.8565 18.45270
351.3386 18.12875
351.8207 16.94595
352.3028 15.38849
352.7849 14.24677
353.2671 13.53189
353.7492 12.99780
354.2313 13.14178
354.7134 13.22418
355.1955 11.82550
355.6776 6.925018
356.1598 1.834717
356.6419 2.4110000E-03
357.1240 0.9377750
357.6061 1.993195
358.0882 1.939270
358.5703 1.044250
359.0525 0.6395570
359.5346 3.687561
360.0167 6.334045
360.4988 7.593140
360.9809 7.687866
361.4630 7.093445
361.9452 5.421173
362.4273 3.561127
362.9094 1.768188
363.3915 0.1443180
363.8736 0.9253540
364.3557 0.9608760
364.8379 3.848969
365.3200 5.785583
365.8021 5.380341
366.2842 4.910706
366.7663 4.832855
367.2484 5.155884
367.7306 6.214539
368.2127 8.774323
368.6948 11.61172
369.1769 13.93384
369.6590 16.09869
370.1411 17.24243
370.6233 16.79041
371.1054 15.19415
371.5875 14.14175
372.0696 13.68634
372.5517 13.76230
373.0338 14.57358
373.5160 16.91122
373.9981 17.56210
374.4802 15.70859
374.9623 12.79510
375.4444 11.23752
375.9265 11.45450
376.4087 11.82468
376.8908 11.94672
377.3729 11.81998
377.8550 11.45093
378.3371 10.87430
378.8192 10.02155
379.3014 8.781647
379.7835 7.113068
380.2656 5.326416
380.7477 3.358704
381.2298 1.466797
381.7119 0.4740910
382.1941 0.4197080
382.6762 0.1981200
383.1583 0.9839480
383.6404 2.967102
384.1225 4.971191
384.6046 6.816010
385.0868 8.924988
385.5689 12.51151
386.0510 17.04980
386.5331 20.59406
387.0152 20.90714
387.4973 20.27219
387.9795 22.20099
388.4616 26.72745
388.9437 31.91031
389.4258 36.52072
389.9079 40.81244
390.3900 44.99655
390.8722 48.81186
391.3543 52.91544
391.8364 57.98364
392.3185 63.75641
392.8006 69.42654
393.2827 74.09897
393.7649 78.83777
394.2470 84.29138
394.7291 90.57474
395.2112 97.52585
395.6933 105.1689
396.1754 113.4301
396.6576 122.1857
397.1397 131.8033
397.6218 141.5051
398.1039 150.9366
398.5860 160.0287
399.0681 169.5769
399.5503 181.2260
400.0324 192.4239
400.5145 201.1442
400.9966 204.4210
401.4787 209.5008
401.9608 217.1183
402.4430 226.9164
402.9251 237.8751
403.4072 251.9413
403.8893 264.2213
404.3714 271.3387
404.8535 270.8278
405.3357 276.0302
405.8178 288.3401
406.2999 304.3639
406.7820 319.6241
407.2641 334.1352
407.7462 347.6287
408.2284 359.3600
408.7105 369.8928
409.1926 383.8726
409.6747 401.7267
410.1568 419.8617
410.6389 434.2406
411.1211 445.7025
411.6032 459.9338
412.0853 478.3683
412.5674 499.1241
413.0495 519.1677
413.5316 539.2422
414.0138 562.4360
414.4959 591.5803
414.9780 625.1944
415.4601 659.0193
415.9422 692.7386
416.4243 732.3132
416.9065 781.2162
417.3886 839.5182
417.8707 906.3815
418.3528 982.1962
418.8349 1066.701
419.3170 1163.223
419.7992 1270.948
420.2813 1380.054
420.7634 1490.972
421.2455 1601.099
421.7276 1708.515
422.2097 1813.546
422.6919 1916.191
423.1740 2014.317
423.6561 2111.086
424.1382 2213.685
424.6203 2316.379
425.1024 2429.056
425.5846 2553.120
426.0667 2687.649
426.5488 2839.864
427.0309 3007.966
427.5130 3197.222
427.9951 3410.592
428.4773 3643.258
428.9594 3910.638
429.4415 4213.854
429.9236 4550.681
430.4057 4922.841
430.8878 5329.637
431.3700 5768.057
431.8521 6240.218
432.3342 6746.298
432.8163 7271.505
433.2984 7818.551
433.7805 8375.367
434.2627 8927.587
434.7448 9476.389
435.2269 10032.20
435.7090 10609.35
436.1911 11193.50
436.6732 11775.71
437.1554 12350.85
437.6375 12855.06
438.1196 13277.62
438.6017 13592.27
439.0838 13740.17
439.5659 13700.95
440.0480 13569.75
440.5302 13349.48
441.0123 13103.44
441.4944 12937.99
441.9765 12857.74
442.4586 12903.77
442.9407 13101.73
443.4229 13448.88
443.9050 13933.36
444.3871 14588.67
444.8692 15348.98
445.3513 16176.45
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