#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-06-07 10:53:21 +0300 (Thu, 07 Jun 2018) $ #$Revision: 991 $ #$URL: svn://172.16.1.111/rod/cif/1/00/04/1000448.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_1000448 loop_ _publ_author_name 'Giuseppetti, G.' 'Mazzi, F.' 'Tadini, C.' _publ_section_title ; The crystal structure of synthetic burkeite Na4SO4(CO3)t(SO4)1-t Sample A Note sign of y-coordinate for O3 and O5 altered to reproduce reported bond lengths Locality: synthetic ; _journal_name_full 'Neues Jahrbuch fur Mineralogie, Monatshefte' _journal_page_first 203 _journal_page_last 221 _journal_volume 1988 _journal_year 1988 _chemical_compound_source R060112 _chemical_formula_sum 'C0.61 Na3 O3.5 S0.89' _chemical_name_mineral Burkeite _space_group_IT_number 59 _symmetry_space_group_name_Hall 'P 2ac 2ac -1ac' _symmetry_space_group_name_H-M 'P m n m :1' _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_length_a 5.170 _cell_length_b 9.217 _cell_length_c 7.058 _cell_volume 336.327 _exptl_crystal_density_diffrn 6.353 _cod_original_sg_symbol_H-M 'P m n m' _cod_original_formula_sum 'Na3 C.61 S.89 O3.5' _cod_database_code 9009345 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type other _raman_measurement_device.excitation_laser_wavelength 532 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 15 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R060112.rod _rod_data_source.block 3500000 _rod_database.code 1000448 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9009345 COD http://www.crystallography.net/cod/9009345.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 150.5283 0.0000000E+00 151.0105 27.56659 151.4926 34.25360 151.9747 37.77319 152.4568 42.16492 152.9389 47.61829 153.4210 52.87372 153.9032 56.63501 154.3853 59.10071 154.8674 59.33704 155.3495 56.69342 155.8316 49.98688 156.3137 43.06427 156.7959 35.59241 157.2780 28.22064 157.7601 22.26489 158.2422 18.49335 158.7243 15.74615 159.2065 13.42004 159.6886 11.31519 160.1707 9.545776 160.6528 6.736450 161.1349 3.971741 161.6170 4.278412 162.0992 12.09531 162.5813 21.19528 163.0634 27.25259 163.5455 26.49396 164.0276 26.42224 164.5097 30.90045 164.9919 39.06628 165.4740 47.52576 165.9561 55.49316 166.4382 62.46176 166.9203 68.17584 167.4024 71.60135 167.8846 74.66742 168.3667 78.48846 168.8488 83.01645 169.3309 87.87585 169.8130 93.42157 170.2952 98.99728 170.7773 103.6879 171.2594 106.0406 171.7415 108.2776 172.2236 112.5781 172.7057 118.7975 173.1879 125.1797 173.6700 131.3782 174.1521 136.6821 174.6342 140.1177 175.1163 140.3054 175.5984 139.2663 176.0806 138.9800 176.5627 139.4149 177.0448 139.7621 177.5269 139.5028 178.0090 138.4568 178.4911 136.9468 178.9733 135.8468 179.4554 135.3677 179.9375 134.3055 180.4196 133.7411 180.9017 135.0184 181.3838 137.9766 181.8660 142.7347 182.3481 146.7810 182.8302 147.4362 183.3123 144.5536 183.7944 143.3917 184.2766 144.1568 184.7587 144.2411 185.2408 140.9119 185.7229 135.1276 186.2050 129.7626 186.6871 126.3825 187.1693 124.0348 187.6514 121.4431 188.1335 118.2644 188.6156 114.5420 189.0977 110.7754 189.5798 106.9500 190.0620 102.8802 190.5441 97.62997 191.0262 91.90199 191.5083 89.26035 191.9904 90.26477 192.4725 92.20453 192.9547 90.28040 193.4368 81.39285 193.9189 72.69354 194.4010 66.52301 194.8831 62.69061 195.3652 58.83067 195.8474 54.38719 196.3295 50.30098 196.8116 49.08093 197.2937 51.06535 197.7758 53.29797 198.2579 54.51610 198.7401 54.59386 199.2222 51.60425 199.7043 44.60330 200.1864 35.76331 200.6685 29.93573 201.1507 27.59839 201.6328 25.99341 202.1149 23.51527 202.5970 20.10510 203.0791 16.72823 203.5612 13.29398 204.0434 10.08203 204.5255 8.126740 205.0076 7.901215 205.4897 7.327011 205.9718 4.990723 206.4539 0.6143950 206.9361 3.497086 207.4182 7.353043 207.9003 10.73238 208.3824 11.89238 208.8645 10.85686 209.3466 10.05075 209.8288 11.64690 210.3109 16.88226 210.7930 18.97916 211.2751 16.30734 211.7572 10.33043 212.2393 6.192833 212.7215 4.135918 213.2036 3.407364 213.6857 4.106522 214.1678 7.286942 214.6499 8.609070 215.1320 6.918625 215.6142 3.113869 216.0963 1.391365 216.5784 2.644821 217.0605 4.212654 217.5426 4.440941 218.0247 3.064987 218.5069 1.414597 218.9890 0.7007830 219.4711 3.165100 219.9532 5.108444 220.4353 6.486763 220.9175 7.139839 221.3996 6.832176 221.8817 4.839172 222.3638 4.251884 222.8459 6.087929 223.3280 9.641930 223.8102 10.96704 224.2923 8.791378 224.7744 6.511784 225.2565 6.307434 225.7386 9.027302 226.2207 11.42948 226.7029 13.11862 227.1850 14.22714 227.6671 15.41655 228.1492 16.79633 228.6313 18.09678 229.1134 19.28986 229.5956 21.08228 230.0777 20.88246 230.5598 17.74277 231.0419 12.55619 231.5240 9.141874 232.0062 7.756130 232.4883 7.827745 232.9704 9.095211 233.4525 11.81446 233.9346 15.18261 234.4167 19.82149 234.8989 25.27214 235.3810 29.04958 235.8631 30.78220 236.3452 31.14636 236.8273 30.38778 237.3094 27.70963 237.7916 25.58556 238.2737 24.13883 238.7558 23.28369 239.2379 22.66149 239.7200 21.87437 240.2021 21.38296 240.6843 21.76833 241.1664 23.97607 241.6485 25.36180 242.1306 25.80236 242.6127 25.37006 243.0948 24.15728 243.5770 21.69586 244.0591 19.13482 244.5412 16.97820 245.0233 14.81545 245.5054 14.22784 245.9876 15.85749 246.4697 19.19074 246.9518 22.70108 247.4339 27.45741 247.9160 30.52734 248.3981 29.98537 248.8803 23.15772 249.3624 19.20590 249.8445 20.61394 250.3266 21.69483 250.8087 23.69011 251.2908 24.59526 251.7730 25.63759 252.2551 27.46994 252.7372 30.71630 253.2193 32.96412 253.7014 33.77322 254.1835 33.73391 254.6657 33.89766 255.1478 34.45716 255.6299 34.93288 256.1120 35.23178 256.5941 35.49393 257.0763 35.06761 257.5584 33.50473 258.0405 36.82736 258.5226 38.92488 259.0047 39.14803 259.4868 39.30606 259.9690 40.27040 260.4511 42.36737 260.9332 43.87335 261.4153 44.81665 261.8974 44.99420 262.3795 43.84942 262.8617 40.57958 263.3438 41.78251 263.8259 42.92295 264.3080 41.40516 264.7901 40.50274 265.2722 40.49190 265.7544 40.72589 266.2365 40.23107 266.7186 38.79421 267.2007 37.88974 267.6828 38.27102 268.1649 39.94017 268.6471 39.03469 269.1292 35.21259 269.6113 36.27373 270.0934 39.41557 270.5755 42.29152 271.0576 43.78783 271.5398 43.10156 272.0219 40.15051 272.5040 38.06892 272.9861 37.18806 273.4682 37.26750 273.9503 38.13804 274.4325 39.89576 274.9146 40.63786 275.3967 39.62983 275.8788 37.29433 276.3610 36.62635 276.8431 38.21025 277.3252 39.84616 277.8073 38.97692 278.2894 35.25318 278.7715 32.47501 279.2537 31.45302 279.7358 31.78551 280.2179 32.00223 280.7000 32.07091 281.1821 32.49914 281.6642 33.96426 282.1464 36.40624 282.6285 37.91557 283.1106 38.11832 283.5927 37.42908 284.0748 36.75239 284.5569 36.09271 285.0391 35.31109 285.5212 34.58496 286.0033 33.86458 286.4854 32.03780 286.9675 28.54656 287.4496 26.38618 287.9318 28.10955 288.4139 27.71577 288.8960 26.74234 289.3781 25.94114 289.8602 25.36681 290.3423 25.33417 290.8245 26.14266 291.3066 27.02695 291.7887 26.44680 292.2708 24.58592 292.7529 23.55328 293.2350 23.78852 293.7172 23.21942 294.1993 23.19133 294.6814 23.82952 295.1635 24.62720 295.6456 25.55118 296.1277 26.33598 296.6099 25.75554 297.0920 21.94092 297.5741 26.43147 298.0562 28.86308 298.5383 28.75666 299.0204 27.76096 299.5026 26.98423 299.9847 26.51032 300.4668 26.58305 300.9489 27.73970 301.4311 29.32024 301.9132 30.70653 302.3953 31.93550 302.8774 32.20022 303.3595 29.92088 303.8416 26.49216 304.3238 24.35891 304.8059 24.99618 305.2880 26.58323 305.7701 27.20096 306.2522 26.99915 306.7343 26.78749 307.2165 27.16069 307.6986 27.88122 308.1807 28.59491 308.6628 29.06798 309.1449 29.67345 309.6270 29.79520 310.1092 26.91700 310.5913 31.14581 311.0734 33.65986 311.5555 34.54604 312.0376 28.92264 312.5197 31.69899 313.0019 31.10754 313.4840 30.37693 313.9661 34.33234 314.4482 29.64782 314.9303 33.52251 315.4124 33.96954 315.8946 35.99271 316.3767 34.63442 316.8588 34.32131 317.3409 35.32825 317.8230 37.85888 318.3051 38.95944 318.7873 35.94181 319.2694 32.99603 319.7515 32.09129 320.2336 33.50620 320.7157 34.85815 321.1978 34.96111 321.6800 34.83810 322.1621 35.39367 322.6442 38.05289 323.1263 40.09371 323.6084 40.38272 324.0905 39.06941 324.5727 38.59828 325.0548 39.99896 325.5369 41.82182 326.0190 43.23210 326.5012 44.49818 326.9833 45.17770 327.4654 44.86198 327.9475 43.74277 328.4296 42.90200 328.9117 42.21892 329.3939 42.23150 329.8760 43.32451 330.3581 46.26878 330.8402 48.00415 331.3223 47.79419 331.8044 46.58888 332.2866 46.24203 332.7687 47.40603 333.2508 48.43511 333.7329 48.83898 334.2150 48.38787 334.6971 47.47196 335.1793 46.05790 335.6614 44.38474 336.1435 42.60050 336.6256 40.40461 337.1077 39.08070 337.5898 39.32572 338.0720 41.02718 338.5541 41.24135 339.0362 39.70355 339.5183 37.61902 340.0004 36.23137 340.4825 35.85410 340.9647 34.57745 341.4468 31.46194 341.9289 27.56408 342.4110 26.98298 342.8931 30.15340 343.3752 33.58171 343.8574 34.22389 344.3395 32.35448 344.8216 32.26449 345.3037 34.69994 345.7858 38.09255 346.2679 39.80558 346.7501 39.91452 347.2322 39.77897 347.7143 39.99561 348.1964 40.56996 348.6785 41.75414 349.1607 43.73487 349.6428 45.40209 350.1249 45.64013 350.6070 44.63190 351.0891 42.94255 351.5713 40.36794 352.0534 37.32582 352.5355 34.22052 353.0176 31.13046 353.4997 28.96891 353.9818 29.86261 354.4640 31.94016 354.9461 32.32099 355.4282 29.34810 355.9103 25.31244 356.3924 21.55181 356.8745 18.24800 357.3567 16.23743 357.8388 18.08432 358.3209 20.32579 358.8030 19.37088 359.2851 12.96527 359.7672 7.757522 360.2494 8.579017 360.7315 12.98092 361.2136 16.40235 361.6957 16.02950 362.1778 15.03167 362.6599 15.13987 363.1421 16.63077 363.6242 18.01951 364.1063 19.37742 364.5884 20.14367 365.0705 19.72928 365.5526 15.02989 366.0348 12.19043 366.5169 13.74593 366.9990 19.36116 367.4811 23.21065 367.9632 23.96895 368.4453 23.49882 368.9275 22.77356 369.4096 20.17992 369.8917 18.97130 370.3738 20.47772 370.8559 23.46515 371.3380 24.23343 371.8202 21.28181 372.3023 18.20212 372.7844 16.34763 373.2665 15.93517 373.7487 15.96033 374.2308 16.84030 374.7129 17.69008 375.1950 17.31288 375.6771 15.37914 376.1592 13.41349 376.6414 11.82287 377.1235 10.54063 377.6056 8.813588 378.0877 6.567065 378.5698 4.425383 379.0519 2.979847 379.5341 2.242884 380.0162 1.597818 380.4983 1.008521 380.9804 0.4361500 381.4625 0.4843130 381.9446 1.751995 382.4268 2.537367 382.9089 1.734267 383.3910 1.6665000E-02 383.8731 0.4891590 384.3552 0.7242670 384.8373 2.244574 385.3195 2.104489 385.8016 0.9041380 386.2837 0.3334260 386.7658 2.287783 387.2479 4.748248 387.7300 4.808065 388.2122 2.542461 388.6943 6.9679998E-02 389.1764 1.337773 389.6585 1.927957 390.1406 1.828989 390.6227 0.4136380 391.1049 0.7282570 391.5870 3.0455001E-02 392.0691 1.873151 392.5512 3.082654 393.0333 2.244992 393.5154 0.7725250 393.9976 0.5856690 394.4797 1.870742 394.9618 2.566983 395.4439 2.011844 395.9260 0.8735840 396.4081 8.3972998E-02 396.8903 1.7317001E-02 397.3724 0.1067370 397.8545 0.3149600 398.3366 0.6371890 398.8188 0.4904800 399.3009 1.082834 399.7830 2.482579 400.2651 2.703997 400.7472 0.5927920 401.2293 0.9027840 401.7115 1.660738 402.1936 1.782075 402.6757 1.421033 403.1578 0.3663140 403.6399 0.8227060 404.1220 2.019774 404.6042 3.382855 405.0863 3.734799 405.5684 2.742548 406.0505 1.213805 406.5326 0.1915550 407.0147 0.2516830 407.4969 0.6745780 407.9790 1.408217 408.4611 2.155254 408.9432 1.387433 409.4253 1.066434 409.9074 3.348121 410.3896 3.889287 410.8717 3.010457 411.3538 1.966707 411.8359 0.7964080 412.3180 6.8325996E-02 412.8001 8.2277998E-02 413.2823 1.071705 413.7644 2.326324 414.2465 4.028757 414.7286 5.566847 415.2107 5.899236 415.6928 4.959940 416.1750 4.140522 416.6571 5.280849 417.1392 6.820374 417.6213 6.771324 418.1034 2.987422 418.5855 0.7015270 419.0677 2.285347 419.5498 2.054950 420.0319 0.9433630 420.5140 2.375756 420.9961 5.344735 421.4782 6.131813 421.9604 3.471889 422.4425 1.370305 422.9246 0.9599120 423.4067 1.485105 423.8889 1.961782 424.3710 2.975974 424.8531 3.304527 425.3352 2.055603 425.8173 0.7898580 426.2994 2.056790 426.7816 1.379998 427.2637 0.5095890 427.7458 3.475965 428.2279 8.960498 428.7100 11.93783 429.1921 11.14669 429.6743 8.261639 430.1564 7.392061 430.6385 9.166602 431.1206 10.48663 431.6027 9.384841 432.0848 6.077297 432.5670 5.847686 433.0491 9.253618 433.5312 13.50627 434.0133 15.28142 434.4954 15.05708 434.9775 15.99341 435.4597 19.21612 435.9418 23.58143 436.4239 26.76095 436.9060 28.98610 437.3881 31.95126 437.8702 38.13073 438.3524 45.16055 438.8345 48.94764 439.3166 48.50101 439.7987 48.31336 440.2808 52.43373 440.7629 59.17883 441.2451 65.74679 441.7272 71.06783 442.2093 75.68153 442.6914 79.07432 443.1735 81.67616 443.6556 85.74706 444.1378 93.64931 444.6199 102.1258 445.1020 108.9889 445.5841 112.9905 446.0662 117.9382 446.5483 125.0169 447.0305 133.1236 447.5126 140.5934 447.9947 146.9118 448.4768 153.0338 448.9590 159.0483 449.4411 164.9534 449.9232 171.3565 450.4053 179.0373 450.8874 186.0389 451.3695 190.9402 451.8517 193.7048 452.3338 194.3854 452.8159 192.9730 453.2980 189.4898 453.7801 183.4772 454.2622 174.8211 454.7444 165.1489 455.2265 154.7068 455.7086 143.8083 456.1907 134.3868 456.6728 126.5389 457.1549 119.1615 457.6371 111.5839 458.1192 103.9000 458.6013 95.87139 459.0834 87.29363 459.5655 78.71716 460.0476 70.11083 460.5298 61.89758 461.0119 55.66584 461.4940 53.83986 461.9761 53.20500 462.4582 50.69003 462.9403 45.80320 463.4225 41.93118 463.9046 41.88569 464.3867 43.07973 464.8688 43.05617 465.3509 40.37609 465.8330 37.75674 466.3152 35.42281 466.7973 33.38706 467.2794 31.83809 467.7615 29.23240 468.2436 28.83553 468.7257 32.54666 469.2079 41.75890 469.6900 47.80543 470.1721 49.29536 470.6542 48.86551 471.1363 49.36318 471.6184 51.06467 472.1006 52.62902 472.5827 53.83926 473.0648 54.62382 473.5469 55.33653 474.0291 56.05288 474.5112 56.08357 474.9933 54.44840 475.4754 51.65095 475.9575 49.87446 476.4396 49.12684 476.9218 49.44818 477.4039 52.05164 477.8860 55.87892 478.3681 58.32078 478.8502 58.22950 479.3323 56.76802 479.8145 54.53704 480.2966 51.85688 480.7787 49.99257 481.2608 51.00422 481.7429 52.05688 482.2250 50.79841 482.7072 46.27424 483.1893 41.76091 483.6714 38.76629 484.1535 36.34266 484.6356 33.61964 485.1177 30.68955 485.5999 27.32761 486.0820 23.04736 486.5641 18.28363 487.0462 14.43117 487.5283 11.27955 488.0104 9.492333 488.4926 10.05366 488.9747 13.83168 489.4568 13.89255 489.9389 8.589072 490.4210 2.523277 490.9031 1.405375 491.3853 5.551467 491.8674 8.809029 492.3495 9.724915 492.8316 9.185129 493.3137 8.947970 493.7958 8.974118 494.2780 9.089274 494.7601 8.986289 495.2422 8.907129 495.7243 9.549763 496.2064 10.99673 496.6885 12.06594 497.1707 11.36673 497.6528 9.846315 498.1349 8.948627 498.6170 9.502172 499.0992 10.17646 499.5813 10.37235 500.0634 10.14996 500.5455 9.689940 501.0276 8.053798 501.5097 7.080204 501.9919 8.035476 502.4740 11.45871 502.9561 13.53879 503.4382 13.11926 503.9203 11.69447 504.4024 10.32571 504.8846 8.888185 505.3667 7.846518 505.8488 7.504654 506.3309 7.427530 506.8130 6.480888 507.2951 4.369159 507.7773 2.776572 508.2594 2.545408 508.7415 3.401255 509.2236 3.765007 509.7057 3.617061 510.1878 3.342235 510.6700 3.107977 511.1521 3.015995 511.6342 3.689879 512.1163 5.599978 512.5984 6.898141 513.0806 4.334868 513.5627 0.2614420 514.0448 2.584917 514.5269 0.5623080 515.0090 2.724431 515.4911 3.627130 515.9733 2.410297 516.4554 1.186482 516.9375 0.4941070 517.4196 0.1888780 517.9017 0.3654310 518.3839 1.692481 518.8660 1.795341 519.3481 1.101235 519.8302 0.5067630 520.3123 1.134725 520.7944 0.7499170 521.2766 1.811538 521.7587 1.357336 522.2408 0.3134090 522.7229 2.456979 523.2050 5.418708 523.6871 7.302735 524.1693 6.391681 524.6514 2.996678 525.1335 1.306360 525.6156 1.512061 526.0977 1.970251 526.5798 0.8836060 527.0620 1.323437 527.5441 1.277320 528.0262 0.6063260 528.5083 1.910147 528.9904 1.498721 529.4725 9.3448997E-02 529.9547 0.4815130 530.4368 1.754997 530.9189 4.127082 531.4010 4.055661 531.8831 1.547570 532.3652 0.9418840 532.8474 6.064458 533.3295 11.85876 533.8116 15.26352 534.2937 15.66572 534.7758 13.94974 535.2579 8.528589 535.7401 1.890595 536.2222 2.173815 536.7043 1.504512 537.1864 1.390202 537.6685 1.568376 538.1506 1.891638 538.6328 0.8586740 539.1149 1.927510 539.5970 3.239189 540.0791 0.3750480 540.5612 3.189986 541.0433 6.457007 541.5255 5.246356 542.0076 3.167347 542.4897 3.763728 542.9718 6.048471 543.4539 8.149631 543.9360 9.599303 544.4182 10.42922 544.9003 10.13741 545.3824 9.150666 545.8645 8.458716 546.3466 8.461469 546.8287 8.780010 547.3109 9.068648 547.7930 9.281975 548.2751 10.30377 548.7572 13.63599 549.2393 16.76253 549.7214 18.38553 550.2036 18.41663 550.6857 17.10971 551.1678 13.78124 551.6499 9.911728 552.1320 7.851933 552.6141 8.026496 553.0963 7.333272 553.5784 4.608199 554.0605 1.004599 554.5426 0.3130260 555.0247 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0.2342180 927.7014 0.7219690 928.1835 2.846390 928.6656 3.620074 929.1478 3.107472 929.6299 4.8333999E-02 930.1120 3.885196 930.5941 7.942122 931.0762 3.987761 931.5583 0.4484100 932.0405 2.326792 932.5226 0.8682050 933.0047 0.6604460 933.4868 8.308670 933.9689 16.66484 934.4510 21.30065 934.9332 22.50950 935.4153 20.71048 935.8974 16.17512 936.3795 13.62595 936.8616 16.54930 937.3438 20.72827 937.8259 21.76141 938.3080 21.07400 938.7901 21.01246 939.2722 24.28283 939.7543 25.13266 940.2365 21.67622 940.7186 17.12346 941.2007 16.47733 941.6828 19.33009 942.1649 20.42638 942.6470 18.94004 943.1292 17.05953 943.6113 16.84638 944.0934 17.25567 944.5755 17.29033 945.0576 16.78092 945.5397 16.25772 946.0219 16.11624 946.5040 15.50832 946.9861 14.07120 947.4682 11.80484 947.9503 8.061327 948.4324 2.959702 948.9146 0.7962490 949.3967 1.601778 949.8788 1.007600 950.3609 0.4748830 950.8430 2.263510 951.3251 3.262839 951.8073 4.130224 952.2894 3.349126 952.7715 0.3227540 953.2536 0.5566570 953.7357 0.3734570 954.2179 1.108211 954.7000 7.5266004E-02 955.1821 1.711227 955.6642 0.6470950 956.1464 0.5430210 956.6285 1.654106 957.1106 1.315648 957.5927 0.9342030 958.0748 0.4552770 958.5569 1.376397 959.0391 1.229073 959.5212 1.366088 960.0033 0.5133730 960.4854 0.7496850 960.9675 1.852951 961.4496 1.031497 961.9318 2.168819 962.4139 0.1278120 962.8960 0.6385480 963.3781 0.8930430 963.8602 3.320371 964.3423 9.125316 964.8245 11.97005 965.3066 10.24266 965.7887 6.289722 966.2708 1.299832 966.7529 2.398122 967.2350 1.503667 967.7172 8.404136 968.1993 16.12216 968.6814 16.00759 969.1635 13.74598 969.6456 12.85833 970.1277 13.25140 970.6099 15.63541 971.0920 19.94348 971.5741 25.77102 972.0562 34.08928 972.5383 42.98006 973.0204 48.42847 973.5026 51.30612 973.9847 56.38531 974.4668 67.04635 974.9489 78.04922 975.4310 87.66136 975.9131 97.17923 976.3953 109.3451 976.8774 123.8989 977.3595 140.0190 977.8416 156.9972 978.3237 176.9657 978.8058 204.6758 979.2880 235.2035 979.7701 262.4194 980.2522 282.5941 980.7343 308.9726 981.2164 342.2095 981.6985 381.7402 982.1807 429.6302 982.6628 483.8185 983.1449 533.8926 983.6270 580.9492 984.1091 632.0865 984.5912 690.3941 985.0734 754.7198 985.5555 827.1765 986.0376 905.6418 986.5197 983.1649 987.0018 1056.117 987.4839 1140.601 987.9661 1240.301 988.4482 1348.403 988.9303 1457.799 989.4124 1567.822 989.8945 1677.766 990.3766 1788.977 990.8588 1889.818 991.3409 1979.126 991.8230 2052.648 992.3051 2110.877 992.7872 2152.741 993.2693 2171.835 993.7515 2168.211 994.2336 2139.583 994.7157 2081.875 995.1978 2000.769 995.6799 1896.074 996.1620 1772.436 996.6442 1642.266 997.1263 1499.906 997.6084 1363.799 998.0905 1233.480 998.5726 1112.842 999.0547 1005.604 999.5369 910.7739 1000.019 825.3881 1000.501 749.2021 1000.983 680.3416 1001.465 615.6017 1001.947 558.2006 1002.430 512.7258 1002.912 479.2552 1003.394 447.9503 1003.876 417.3358 1004.358 393.0495 1004.840 377.6631 1005.322 368.6888 1005.804 362.2511 1006.287 357.9637 1006.769 354.6766 1007.251 352.0883 1007.733 350.4720 1008.215 351.7693 1008.697 352.6223 1009.179 350.4060 1009.661 345.1487 1010.143 336.0372 1010.626 322.8405 1011.108 306.0891 1011.590 284.3378 1012.072 260.7588 1012.554 237.8861 1013.036 215.7643 1013.518 194.3800 1014.000 174.2661 1014.483 153.8064 1014.965 132.0746 1015.447 110.7640 1015.929 93.15287 1016.411 78.69554 1016.893 65.53326 1017.375 52.88522 1017.857 42.34137 1018.339 35.15557 1018.822 29.89613 1019.304 25.42371 1019.786 21.51578 1020.268 19.47788 1020.750 19.86510 1021.232 19.42300 1021.714 14.45373 1022.196 8.553924 1022.679 9.039710 1023.161 13.46991 1023.643 14.74601 1024.125 5.349381 1024.607 1.059441 1025.089 1.234961 1025.571 1.608362 1026.053 3.025024 1026.535 3.252823 1027.018 4.541270 1027.500 7.258039 1027.982 9.028768 1028.464 7.794452 1028.946 4.868445 1029.428 0.2516050 1029.910 2.231948 1030.392 1.232921 1030.875 0.8884790 1031.357 2.650193 1031.839 0.7075260 1032.321 1.499330 1032.803 0.9086470 1033.285 7.0628002E-02 1033.767 3.865125 1034.249 5.895714 1034.731 12.22454 1035.214 9.391837 1035.696 4.076820 1036.178 0.6959930 1036.660 0.7154870 1037.142 0.7250790 1037.624 0.6208280 1038.106 2.016159 1038.588 2.934550 1039.071 3.292020 1039.553 2.069528 1040.035 0.2730460 1040.517 1.127106 1040.999 5.345663 1041.481 10.79042 1041.963 17.64546 1042.445 24.43276 1042.927 28.86852 1043.410 31.98727 1043.892 35.64377 1044.374 40.10653 1044.856 45.49082 1045.338 53.65228 1045.820 60.51212 1046.302 62.49720 1046.784 61.68164 1047.266 70.51426 1047.749 88.19659 1048.231 104.8866 1048.713 115.8973 1049.195 125.5386 1049.677 136.6746 1050.159 148.8954 1050.641 161.5909 1051.123 173.7631 1051.606 189.4837 1052.088 209.5562 1052.570 230.6873 1053.052 249.7702 1053.534 268.9543 1054.016 292.4820 1054.498 320.0139 1054.980 349.3499 1055.463 376.8926 1055.945 410.2392 1056.427 451.7376 1056.909 498.1640 1057.391 544.6614 1057.873 591.1743 1058.355 638.0089 1058.837 685.4243 1059.319 730.9526 1059.802 772.1643 1060.284 809.9558 1060.766 845.9435 1061.248 879.8270 1061.730 903.9202 1062.212 917.5146 1062.694 925.2981 1063.176 929.1440 1063.658 927.6266 1064.141 915.2867 1064.623 897.0933 1065.105 881.8065 1065.587 875.4661 1066.069 864.1592 1066.551 850.5765 1067.033 825.7502 1067.515 781.7632 1067.998 720.5095 1068.480 653.1849 1068.962 579.7610 1069.444 501.3205 1069.926 409.3171 1070.408 323.0840 1070.890 252.8121 1071.372 195.5945 1071.854 149.0669 1072.337 114.1590 1072.819 85.31915 1073.301 62.41785 1073.783 44.80824 1074.265 34.33944 1074.747 27.54416 1075.229 21.28077 1075.711 15.41014 1076.193 10.86196 1076.676 8.398036 1077.158 5.246169 1077.640 0.1156270 1078.122 5.069894 1078.604 3.691601 1079.086 4.405999 1079.568 4.669518 1080.051 2.401728 1080.533 2.044310 1081.015 4.319241 1081.497 0.3977700 1081.979 4.239965 1082.461 6.936460 1082.943 7.094853 1083.425 5.055968 1083.907 2.940624 1084.390 2.412881 1084.872 1.184170 1085.354 2.850492 1085.836 2.825483 1086.318 1.716731 1086.800 5.588736 1087.282 8.060512 1087.764 8.689404 1088.246 8.873116 1088.729 8.590630 1089.211 9.098468 1089.693 11.98847 1090.175 16.80243 1090.657 22.59709 1091.139 31.10925 1091.621 36.59568 1092.103 37.55319 1092.586 37.68528 1093.068 43.40894 1093.550 52.21001 1094.032 57.78830 1094.514 59.36201 1094.996 62.23701 1095.478 70.10516 1095.960 78.23381 1096.443 85.05558 1096.925 90.73854 1097.407 95.35014 1097.889 99.32173 1098.371 105.0201 1098.853 113.4581 1099.335 122.0258 1099.817 130.7124 1100.299 137.1843 1100.781 139.2010 1101.264 136.7692 1101.746 131.7654 1102.228 123.9239 1102.710 116.7077 1103.192 112.4668 1103.674 108.9647 1104.156 103.0792 1104.638 96.44409 1105.121 91.86917 1105.603 93.48326 1106.085 89.34498 1106.567 77.20721 1107.049 65.50965 1107.531 61.82649 1108.013 62.89748 1108.495 62.16590 1108.978 60.08545 1109.460 58.97933 1109.942 60.20154 1110.424 61.91387 1110.906 64.09402 1111.388 65.71726 1111.870 64.39685 1112.352 61.11526 1112.834 60.76158 1113.317 63.62588 1113.799 66.21843 1114.281 65.96840 1114.763 65.49983 1115.245 66.47724 1115.727 68.06033 1116.209 67.63535 1116.691 65.35754 1117.173 64.43491 1117.656 65.75269 1118.138 67.91054 1118.620 70.83420 1119.102 73.31079 1119.584 74.53027 1120.066 74.45208 1120.548 71.11628 1121.030 63.72494 1121.513 59.90324 1121.995 64.13174 1122.477 69.30807 1122.959 64.65053 1123.441 55.93830 1123.923 51.72529 1124.405 55.86937 1124.887 56.39395 1125.370 51.36892 1125.852 47.92309 1126.334 52.02390 1126.816 59.63280 1127.298 63.36272 1127.780 63.99903 1128.262 63.14325 1128.744 59.20115 1129.226 57.21715 1129.709 59.14975 1130.191 60.68401 1130.673 57.09285 1131.155 49.95687 1131.637 45.18622 1132.119 42.71594 1132.601 41.47523 1133.083 41.05395 1133.566 41.68304 1134.048 44.98603 1134.530 47.98978 1135.012 45.85592 1135.494 39.19426 1135.976 33.79347 1136.458 30.54305 1136.940 28.85909 1137.422 30.20963 1137.905 31.46419 1138.387 30.47381 1138.869 27.63237 1139.351 23.69195 1139.833 18.20676 1140.315 17.64202 1140.797 24.10078 1141.279 30.17981 1141.761 28.22333 1142.244 23.53801 1142.726 20.21415 1143.208 18.57145 1143.690 18.83784 1144.172 21.33181 1144.654 23.69899 1145.136 25.39841 1145.618 26.10990 1146.101 23.64278 1146.583 20.80653 1147.065 21.58663 1147.547 27.62401 1148.029 31.38227 1148.511 32.74221 1148.993 31.53843 1149.475 26.74900 1149.958 20.74242 1150.440 16.49624 1150.922 14.18769 1151.404 14.77908 1151.886 21.10410 1152.368 23.11020 1152.850 18.91943 1153.332 12.98577 1153.814 7.401196 1154.297 2.734476 1154.779 0.3231070 1155.261 2.106038 1155.743 2.223724 1156.225 1.810313 1156.707 3.810751 1157.189 1.998780 1157.671 0.4175930 1158.153 0.6901200 1158.636 0.6634830 1159.118 2.293539 1159.600 3.893893 1160.082 4.584518 1160.564 1.902318 1161.046 0.1225810 1161.528 0.7088580 1162.010 2.264980 1162.493 1.638066 1162.975 0.6538230 1163.457 1.276675 1163.939 6.6757999E-02 1164.421 2.501450 1164.903 8.694230 1165.385 13.24790 1165.867 13.41150 1166.349 10.70259 1166.832 6.230562 1167.314 0.3155840 1167.796 1.191137 1168.278 2.372712 1168.760 5.738369 1169.242 3.270094 1169.724 1.380968 1170.206 5.943062 1170.688 13.62728 1171.171 15.74659 1171.653 12.42357 1172.135 8.980968 1172.617 6.197096 1173.099 5.340518 1173.581 10.20664 1174.063 15.11822 1174.545 14.29545 1175.028 9.410235 1175.510 9.383459 1175.992 14.54570 1176.474 16.08784 1176.956 11.08708 1177.438 4.667402 1177.920 0.7223670 1178.402 1.663552 1178.885 3.146221 1179.367 1.760109 1179.849 2.626073 1180.331 0.2719140 1180.813 1.050189 1181.295 2.769762 1181.777 2.689558 1182.259 0.7229940 1182.741 1.932992 1183.224 0.1361140 1183.706 1.497769 1184.188 0.6043620 1184.670 3.144454 1185.152 7.071408 1185.634 9.893060 1186.116 12.12441 1186.598 14.20640 1187.081 15.96811 1187.563 17.27723 1188.045 18.42038 1188.527 16.67100 1189.009 11.18192 1189.491 7.265150 1189.973 8.536410 1190.455 12.01670 1190.938 15.21578 1191.420 17.68834 1191.902 18.74394 1192.384 18.52565 1192.866 15.68874 1193.348 9.431504 1193.830 4.763089 1194.312 5.755400 1194.794 9.772141 1195.276 14.32872 1195.759 18.33553 1196.241 20.09002 1196.723 18.23734 1197.205 16.70302 1197.687 15.34987 1198.169 15.09264 1198.651 18.32420 1199.133 21.68796 1199.616 19.63075 1200.098 14.11909 1200.580 10.26463 1201.062 9.671698 1201.544 8.585876 1202.026 6.570364 1202.508 5.037027 1202.990 4.995370 1203.473 6.310137 1203.955 10.04235 1204.437 15.02065 1204.919 17.53797 1205.401 16.75840 1205.883 14.16631 1206.365 9.334916 1206.847 4.931713 1207.329 4.728183 1207.812 5.640337 1208.294 3.149129 1208.776 1.634114 1209.258 1.933545 1209.740 3.726742 1210.222 3.001824 1210.704 1.047367 1211.186 1.625088 1211.668 0.6226810 1212.151 1.554626 1212.633 0.7038730 1213.115 6.479197 1213.597 9.475150 1214.079 8.573749 1214.561 6.893529 1215.043 4.465163 1215.525 2.974880 1216.008 6.520027 1216.490 10.50034 1216.972 7.182306 1217.454 1.411127 1217.936 1.358184 1218.418 1.523480 1218.900 7.683593 1219.382 12.36839 1219.865 15.20014 1220.347 14.89347 1220.829 13.14310 1221.311 11.51831 1221.793 10.41179 1222.275 10.42187 1222.757 11.96563 1223.239 13.24624 1223.721 14.04296 1224.203 14.18249 1224.686 13.43652 1225.168 12.29338 1225.650 10.18333 1226.132 7.877160 1226.614 7.383524 1227.096 9.029570 1227.578 10.71618 1228.061 11.95409 1228.543 13.17105 1229.025 14.99254 1229.507 16.80240 1229.989 17.85603 1230.471 18.18323 1230.953 18.71857 1231.435 19.44155 1231.917 20.34974 1232.400 21.56228 1232.882 22.21355 1233.364 21.65752 1233.846 20.02705 1234.328 17.14636 1234.810 13.24725 1235.292 8.538774 1235.774 2.874960 1236.256 3.161669 1236.739 12.97048 1237.221 19.77596 1237.703 6.978819 1238.185 4.311483 1238.667 6.244710 1239.149 1.916480 1239.631 0.4612900 1240.113 1.563031 1240.596 0.5639760 1241.078 0.6877880 1241.560 0.9988430 1242.042 1.156728 1242.524 0.1224010 1243.006 0.1785900 1243.488 6.560295 1243.970 9.051723 1244.453 8.027485 1244.935 6.482571 1245.417 4.523118 1245.899 4.144241 1246.381 8.139884 1246.863 12.46854 1247.345 14.86653 1247.827 15.92614 1248.309 17.63661 1248.792 19.63871 1249.274 19.99533 1249.756 17.96408 1250.238 16.33108 1250.720 19.21453 1251.202 19.08561 1251.684 10.79246 1252.166 0.6781110 1252.648 1.039975 1253.131 6.116045 1253.613 10.11856 1254.095 8.280061 1254.577 5.836390 1255.059 2.395934 1255.541 1.596424 1256.023 5.785590 1256.505 12.12177 1256.988 13.46136 1257.470 10.80611 1257.952 8.810729 1258.434 7.825697 1258.916 7.897792 1259.398 9.611564 1259.880 10.87785 1260.362 11.34232 1260.844 12.23750 1261.327 14.81752 1261.809 17.55383 1262.291 17.79617 1262.773 14.85767 1263.255 12.39460 1263.737 10.03765 1264.219 10.03617 1264.701 13.46369 1265.183 18.18251 1265.666 21.96460 1266.148 25.10730 1266.630 27.20725 1267.112 28.25960 1267.594 33.83947 1268.076 45.06260 1268.558 51.53051 1269.040 49.12311 1269.523 44.81609 1270.005 45.21756 1270.487 44.60436 1270.969 43.79102 1271.451 41.24273 1271.933 39.57524 1272.415 39.17147 1272.897 38.84284 1273.380 36.83284 1273.862 34.60082 1274.344 34.46077 1274.826 33.66020 1275.308 30.02477 1275.790 24.41193 1276.272 18.27287 1276.754 12.38246 1277.236 11.72463 1277.719 18.62043 1278.201 23.67086 1278.683 18.24315 1279.165 11.56820 1279.647 6.902928 1280.129 4.126777 1280.611 5.571302 1281.093 9.107590 1281.576 7.187988 1282.058 1.784129 1282.540 1.691182 1283.022 2.664243 1283.504 9.044256 1283.986 8.978702 1284.468 5.986187 1284.950 4.270367 1285.432 4.009533 1285.915 6.455168 1286.397 11.58296 1286.879 14.06509 1287.361 12.94753 1287.843 10.69275 1288.325 7.155507 1288.807 5.294961 1289.289 11.19043 1289.771 18.57590 1290.254 20.57488 1290.736 17.27752 1291.218 13.64523 1291.700 9.302610 1292.182 7.866434 1292.664 10.27497 1293.146 14.28888 1293.628 12.14247 1294.111 8.990023 1294.593 8.987526 1295.075 10.41201 1295.557 9.571505 1296.039 6.657346 1296.521 3.272527 1297.003 1.5158000E-02 1297.485 0.4239160 1297.968 6.527097 1298.450 10.43403 1298.932 6.287549 1299.414 0.1490850 1299.896 0.2115610 1300.378 5.750892 1300.860 6.204281 1301.342 2.087960 1301.824 0.0000000E+00