#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-06-07 10:53:45 +0300 (Thu, 07 Jun 2018) $
#$Revision: 997 $
#$URL: svn://172.16.1.111/rod/cif/1/00/04/1000454.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000454
loop_
_publ_author_name
'Hazen, R. M.'
'Burnham, C. W.'
_publ_section_title
;
 The crystal structures of one-layer phlogopite and annite
;
_journal_name_full               'American Mineralogist'
_journal_page_first              889
_journal_page_last               900
_journal_volume                  58
_journal_year                    1973
_chemical_compound_source        R060204
_chemical_formula_sum
'Al1.282 Ca0.03 Cl0.05 F0.22 Fe2.43 H1.38 K0.88 Mg0.12 Mn0.03 Na0.07 O11.73 Si2.808 Ti0.21'
_chemical_name_mineral           Annite
_space_group_IT_number           12
_symmetry_space_group_name_Hall  '-C 2y'
_symmetry_space_group_name_H-M   'C 1 2/m 1'
_cell_angle_alpha                90
_cell_angle_beta                 100.63
_cell_angle_gamma                90
_cell_length_a                   5.3860
_cell_length_b                   9.3241
_cell_length_c                   10.2683
_cell_volume                     506.820
_exptl_crystal_density_diffrn    3.250
_cod_original_formula_sum
;Al1.282 Ca0.03 Cl0.05 F0.22 Fe2.43 H1.38 K0.88 Mg0.12 Mn0.03 Na0.07 O11.73
 Si2.808 Ti0.21
;
_cod_database_code               9000377
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R060204.rod
_rod_data_source.block           3500000
_rod_database.code               1000454
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9000377 COD http://www.crystallography.net/cod/9000377.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
145.5931 0.0000000E+00
146.0752 6.811035
146.5573 3.857056
147.0394 1.347595
147.5215 2.172424
148.0036 3.7842002E-02
148.4858 4.713501
148.9679 12.75745
149.4500 23.65320
149.9321 37.60345
150.4142 54.62653
150.8963 76.68494
151.3785 100.0947
151.8606 123.3655
152.3427 146.2160
152.8248 170.4233
153.3069 195.7087
153.7890 222.4171
154.2712 247.6349
154.7533 267.9414
155.2354 287.8130
155.7175 307.0833
156.1996 325.0269
156.6817 342.9514
157.1639 361.0673
157.6460 379.3416
158.1281 397.2724
158.6102 414.4991
159.0923 431.5482
159.5744 448.7053
160.0566 465.4932
160.5387 482.8517
161.0208 501.0854
161.5029 520.0111
161.9850 539.0687
162.4671 558.2686
162.9493 577.4685
163.4314 596.5000
163.9135 614.5536
164.3956 633.4965
164.8777 653.9882
165.3598 676.0846
165.8420 700.0204
166.3241 727.4261
166.8062 755.9167
167.2883 783.3522
167.7704 807.8710
168.2525 832.3168
168.7346 858.8642
169.2168 887.2081
169.6989 915.6609
170.1810 943.3960
170.6631 970.5906
171.1452 997.6132
171.6273 1025.664
172.1095 1052.409
172.5916 1075.871
173.0737 1096.226
173.5558 1115.193
174.0379 1134.927
174.5201 1153.929
175.0022 1170.115
175.4843 1182.840
175.9664 1192.402
176.4485 1198.609
176.9306 1201.573
177.4128 1202.201
177.8949 1202.276
178.3770 1200.649
178.8591 1194.733
179.3412 1182.024
179.8233 1164.867
180.3055 1147.204
180.7876 1128.985
181.2697 1108.637
181.7518 1083.015
182.2339 1053.642
182.7160 1024.410
183.1982 998.5009
183.6803 974.2309
184.1624 946.8990
184.6445 916.3533
185.1266 885.3348
185.6087 857.1959
186.0909 830.9174
186.5730 804.1625
187.0551 775.2363
187.5372 744.8691
188.0193 714.4359
188.5014 684.1650
188.9836 654.8385
189.4657 626.3809
189.9478 599.1434
190.4299 573.0927
190.9120 548.3351
191.3941 524.4406
191.8763 500.2687
192.3584 476.5343
192.8405 453.9489
193.3226 432.6401
193.8047 412.8976
194.2868 393.3809
194.7690 373.0585
195.2511 352.1396
195.7332 332.0663
196.2153 312.8549
196.6974 294.5652
197.1795 278.1034
197.6617 263.4567
198.1438 249.7427
198.6259 236.8140
199.1080 224.7273
199.5901 212.2691
200.0722 199.1531
200.5544 186.1608
201.0365 175.0759
201.5186 166.0247
202.0007 157.5576
202.4828 149.0771
202.9649 140.5692
203.4471 131.4818
203.9292 122.3207
204.4113 113.2478
204.8934 104.2631
205.3755 95.28381
205.8576 87.24249
206.3398 80.78644
206.8219 76.16156
207.3040 71.30872
207.7861 66.11151
208.2682 60.82123
208.7503 56.04327
209.2325 51.96155
209.7146 47.99524
210.1967 43.88220
210.6788 39.57275
211.1609 35.37213
211.6430 31.25354
212.1252 27.25476
212.6073 23.49432
213.0894 19.94409
213.5715 16.75397
214.0536 13.98071
214.5357 11.58801
215.0179 9.770569
215.5000 8.741638
215.9821 8.118164
216.4642 6.998474
216.9463 5.181824
217.4284 3.321533
217.9105 1.638000
218.3927 0.1461180
218.8748 1.116638
219.3569 2.034790
219.8390 2.791260
220.3211 3.899475
220.8032 5.669312
221.2854 7.232849
221.7675 8.224243
222.2496 8.381653
222.7317 8.740723
223.2138 9.415100
223.6959 10.23804
224.1781 10.92950
224.6602 11.57642
225.1423 11.92419
225.6244 11.80322
226.1065 11.08728
226.5886 10.33936
227.0708 9.587585
227.5529 8.796082
228.0350 7.812378
228.5171 6.271545
228.9992 5.149170
229.4813 4.830872
229.9635 5.458984
230.4456 6.538696
230.9277 8.730286
231.4098 11.00952
231.8919 11.32068
232.3740 8.653076
232.8562 5.603271
233.3383 2.868713
233.8204 8.9050002E-02
234.3025 1.121582
234.7846 5.7128999E-02
235.2667 2.182495
235.7489 3.651855
236.2310 4.427185
236.7131 4.282898
237.1952 2.779602
237.6773 0.9074710
238.1594 2.805725
238.6416 1.911438
239.1237 0.1492310
239.6058 0.7183230
240.0879 0.9080810
240.5700 2.866577
241.0521 4.600525
241.5343 6.024414
242.0164 7.576233
242.4985 9.414551
242.9806 11.25629
243.4627 12.62793
243.9448 13.10986
244.4270 13.83862
244.9091 15.21661
245.3912 17.41888
245.8733 19.17163
246.3554 20.17328
246.8375 20.97302
247.3197 22.35168
247.8018 24.82587
248.2839 26.86591
248.7660 27.88947
249.2481 27.69196
249.7302 28.52173
250.2124 30.90607
250.6945 33.67639
251.1766 35.45966
251.6587 35.62628
252.1408 36.13043
252.6229 37.57318
253.1051 40.06134
253.5872 41.86523
254.0693 42.27203
254.5514 42.80048
255.0335 45.40265
255.5156 51.80011
255.9978 56.39862
256.4799 57.46039
256.9620 55.01569
257.4441 54.37360
257.9262 56.29883
258.4083 58.96283
258.8904 60.60693
259.3726 60.53217
259.8547 61.26050
260.3368 63.46130
260.8189 66.96240
261.3010 69.71399
261.7831 71.50659
262.2653 72.89905
262.7474 74.15417
263.2295 74.93225
263.7116 76.66168
264.1937 80.01312
264.6758 84.52972
265.1580 87.54401
265.6401 88.43787
266.1222 88.99152
266.6043 90.55737
267.0864 93.59607
267.5685 96.02368
268.0507 97.45056
268.5328 98.18835
269.0149 99.45721
269.4970 101.4475
269.9791 103.4622
270.4612 105.0120
270.9434 105.9097
271.4255 107.2651
271.9076 109.3619
272.3897 111.8151
272.8718 113.6823
273.3539 114.9125
273.8361 115.6907
274.3182 116.0283
274.8003 115.8716
275.2824 114.6821
275.7645 115.2613
276.2466 115.2416
276.7288 114.6553
277.2109 111.8055
277.6930 111.8787
278.1751 110.7805
278.6572 109.6343
279.1393 110.1188
279.6215 105.7108
280.1036 103.3513
280.5857 100.6989
281.0678 97.77087
281.5499 94.43115
282.0320 90.55627
282.5142 86.19165
282.9963 82.15167
283.4784 78.52661
283.9605 75.10028
284.4426 71.38898
284.9247 67.37372
285.4069 64.00433
285.8890 61.87469
286.3711 60.72113
286.8532 58.89374
287.3353 56.25165
287.8174 53.34570
288.2996 50.88812
288.7817 48.75128
289.2638 46.28064
289.7459 43.31470
290.2280 40.23541
290.7101 37.63464
291.1923 35.50879
291.6744 33.44214
292.1565 30.62531
292.6386 27.19183
293.1207 24.38019
293.6028 22.61462
294.0850 21.55042
294.5671 20.68054
295.0492 20.04272
295.5313 19.24841
296.0134 17.56366
296.4955 15.17749
296.9777 12.90326
297.4598 10.92163
297.9419 9.401001
298.4240 8.633545
298.9061 8.500000
299.3882 8.446777
299.8704 8.333923
300.3525 8.051208
300.8346 7.221741
301.3167 5.706848
301.7988 4.175903
302.2809 3.428894
302.7631 3.277832
303.2452 3.098877
303.7273 2.373108
304.2094 1.528503
304.6915 1.312317
305.1736 1.811096
305.6558 2.238098
306.1379 1.552979
306.6200 0.3167720
307.1021 0.4081420
307.5842 0.2277220
308.0663 1.294739
308.5485 1.908508
309.0306 2.064270
309.5127 2.145569
309.9948 2.370422
310.4769 2.680054
310.9590 3.014343
311.4412 3.527527
311.9233 3.874817
312.4054 3.755615
312.8875 3.224548
313.3696 2.600403
313.8517 1.831909
314.3339 1.189514
314.8160 0.9593510
315.2981 1.597778
315.7802 2.089111
316.2623 1.706726
316.7444 0.7780760
317.2266 0.1457520
317.7087 0.4500730
318.1908 0.9971920
318.6729 1.354736
319.1550 1.407593
319.6371 1.409546
320.1193 1.270935
320.6014 1.150696
321.0835 1.302246
321.5656 2.127808
322.0477 2.958679
322.5298 3.618591
323.0120 4.149292
323.4941 4.127930
323.9762 2.998657
324.4583 1.439331
324.9404 0.1853640
325.4225 0.6043700
325.9047 1.130676
326.3868 1.336914
326.8689 1.216492
327.3510 1.073059
327.8331 0.9432370
328.3152 0.7740480
328.7974 0.5277100
329.2795 0.3740230
329.7616 8.9844003E-02
330.2437 1.207153
330.7258 2.773254
331.2079 3.657227
331.6901 3.428467
332.1722 2.928772
332.6543 2.514526
333.1364 1.912048
333.6185 1.931396
334.1006 2.942261
334.5828 4.460754
335.0649 5.306152
335.5470 5.094910
336.0291 4.878662
336.5112 5.150024
336.9933 6.111084
337.4755 6.430176
337.9576 5.749878
338.4397 4.856384
338.9218 4.845093
339.4039 5.910034
339.8860 7.223694
340.3681 8.743652
340.8503 10.41504
341.3324 11.29645
341.8145 11.28302
342.2966 10.79260
342.7787 9.960144
343.2608 8.755859
343.7430 8.140503
344.2251 8.449463
344.7072 9.374817
345.1893 9.957886
345.6714 10.15405
346.1535 10.55646
346.6357 11.65637
347.1178 13.36407
347.5999 15.31226
348.0820 17.69977
348.5641 19.75214
349.0462 19.92816
349.5284 18.44696
350.0105 16.97888
350.4926 16.43701
350.9747 16.53088
351.4568 16.58777
351.9389 16.55627
352.4211 16.72168
352.9032 17.70428
353.3853 19.13800
353.8674 20.13245
354.3495 20.07703
354.8316 19.57489
355.3138 19.24463
355.7959 19.08618
356.2780 19.07037
356.7601 19.37311
357.2422 19.74188
357.7243 19.83221
358.2065 19.44733
358.6886 18.93701
359.1707 18.41998
359.6528 17.93469
360.1349 17.63300
360.6170 17.97925
361.0992 18.29016
361.5813 17.92566
362.0634 16.50616
362.5455 15.37708
363.0276 15.32416
363.5097 15.86017
363.9919 16.23810
364.4740 16.13538
364.9561 15.88031
365.4382 15.70160
365.9203 15.62256
366.4024 15.36426
366.8846 14.62952
367.3667 13.79962
367.8488 13.18915
368.3309 13.34204
368.8130 13.15497
369.2951 12.17841
369.7773 10.59473
370.2594 9.638733
370.7415 9.787964
371.2236 10.09912
371.7057 10.17041
372.1878 10.06042
372.6700 9.587280
373.1521 8.513306
373.6342 7.220215
374.1163 6.491699
374.5984 6.650085
375.0805 6.714172
375.5627 6.423157
376.0448 5.758301
376.5269 4.765442
377.0090 3.121338
377.4911 1.634766
377.9732 1.369385
378.4554 2.572876
378.9375 3.403198
379.4196 3.376709
379.9017 2.752502
380.3838 2.432373
380.8659 2.436584
381.3481 2.601196
381.8302 2.838989
382.3123 3.148682
382.7944 3.548523
383.2765 4.102234
383.7586 4.608643
384.2408 4.526123
384.7229 3.983093
385.2050 3.697723
385.6871 4.424561
386.1692 5.606232
386.6513 5.945190
387.1335 5.300140
387.6156 4.651855
388.0977 4.725067
388.5798 5.492493
389.0619 6.837891
389.5440 9.234497
390.0262 11.41635
390.5083 11.85596
390.9904 10.98660
391.4725 10.36407
391.9546 10.98471
392.4367 11.93857
392.9189 12.52173
393.4010 12.58124
393.8831 12.45010
394.3652 12.01215
394.8473 11.51962
395.3294 11.34467
395.8116 12.19806
396.2937 12.96378
396.7758 12.98309
397.2579 12.11392
397.7400 11.81406
398.2221 12.87811
398.7043 14.37872
399.1864 15.57077
399.6685 16.13272
400.1506 16.66837
400.6327 17.21378
401.1148 17.73175
401.5970 18.13834
402.0791 18.37393
402.5612 18.54111
403.0433 18.62473
403.5254 18.66586
404.0075 18.81110
404.4897 19.15646
404.9718 19.55566
405.4539 19.78638
405.9360 19.83371
406.4181 19.77444
406.9002 19.56525
407.3824 19.24661
407.8645 19.04395
408.3466 18.91074
408.8287 17.96650
409.3108 19.29004
409.7929 20.01483
410.2751 20.17301
410.7572 18.06761
411.2393 18.88517
411.7214 18.53133
412.2035 18.30042
412.6856 18.09598
413.1678 18.14850
413.6499 18.35300
414.1320 18.60034
414.6141 18.92151
415.0962 18.91144
415.5783 17.67365
416.0605 15.89554
416.5426 14.85147
417.0247 15.46490
417.5068 16.58466
417.9889 17.51517
418.4710 18.18942
418.9532 18.28394
419.4353 17.07361
419.9174 15.52380
420.3995 14.45621
420.8816 14.17673
421.3637 12.76617
421.8459 13.77637
422.3280 14.18786
422.8101 14.03277
423.2922 11.61407
423.7743 12.11836
424.2564 11.45123
424.7386 10.73602
425.2207 11.65168
425.7028 9.562232
426.1849 10.45203
426.6670 10.15258
427.1491 10.39740
427.6313 9.463558
428.1134 8.893798
428.5955 9.368042
429.0776 9.577240
429.5597 9.556366
430.0418 9.192383
430.5240 8.321716
431.0061 6.890442
431.4882 5.794037
431.9703 5.122986
432.4524 4.613922
432.9345 3.857666
433.4167 2.834503
433.8988 2.251862
434.3809 2.425537
434.8630 3.018280
435.3451 3.236877
435.8272 3.093475
436.3094 2.838623
436.7915 2.458282
437.2736 2.095032
437.7557 2.288483
438.2378 3.205414
438.7199 3.947723
439.2020 3.415070
439.6841 2.045807
440.1663 0.7369080
440.6484 0.4845580
441.1305 1.241333
441.6126 0.7876890
442.0947 0.6365970
442.5768 1.575256
443.0590 0.5600890
443.5411 0.8267210
444.0232 1.219299
444.5053 0.3020020
444.9874 1.327026
445.4695 0.3423770
445.9517 1.495605
446.4338 2.333099
446.9159 0.1688840
447.3980 1.395386
447.8801 0.8170780
448.3622 2.130646
448.8444 3.579926
449.3265 2.345093
449.8086 0.6453860
450.2907 4.7455002E-02
450.7728 0.8251650
451.2549 1.480652
451.7371 1.980560
452.2192 2.104767
452.7013 1.038788
453.1834 1.724396
453.6655 3.776794
454.1476 3.934967
454.6298 2.383514
455.1119 1.120300
455.5940 0.1825870
456.0761 0.6147460
456.5582 1.519348
457.0403 2.467682
457.5225 3.059998
458.0046 3.157135
458.4867 2.952637
458.9688 2.817505
459.4509 2.659271
459.9330 2.082642
460.4152 0.3754270
460.8973 1.632904
461.3794 2.949371
461.8615 3.530823
462.3436 3.729065
462.8257 3.346252
463.3079 2.881805
463.7900 2.910095
464.2721 4.024628
464.7542 5.140167
465.2363 5.979218
465.7184 6.506226
466.2006 6.616119
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