#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-06-07 10:54:08 +0300 (Thu, 07 Jun 2018) $
#$Revision: 1003 $
#$URL: svn://172.16.1.111/rod/cif/1/00/04/1000460.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000460
loop_
_publ_author_name
'Moore, P. B.'
'Araki, T.'
_publ_section_title
;
 Bahianite, Al5Sb3O14(O,OH)2, a novel hexagonal close-packed oxide
 structure Locality: Serra de Mangabeira, Bahia, Brazil
;
_journal_name_full
'Neues Jahrbuch fur Mineralogie, Abhandlungen'
_journal_page_first              113
_journal_page_last               125
_journal_volume                  126
_journal_year                    1976
_chemical_compound_source        R060433
_chemical_formula_sum            'Al4.76 Fe0.34 O16 Sb2.9'
_chemical_name_mineral           Bahianite
_space_group_IT_number           12
_symmetry_space_group_name_Hall  '-C 2y'
_symmetry_space_group_name_H-M   'C 1 2/m 1'
_cell_angle_alpha                90
_cell_angle_beta                 90.94
_cell_angle_gamma                90
_cell_length_a                   9.406
_cell_length_b                   11.541
_cell_length_c                   4.410
_cell_volume                     478.662
_exptl_crystal_density_diffrn    5.249
_cod_original_formula_sum        'Sb2.9 Fe.34 Al4.76 O16'
_cod_database_code               9009247
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R060433.rod
_rod_data_source.block           3500000
_rod_database.code               1000460
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9009247 COD http://www.crystallography.net/cod/9009247.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
140.2111 0.0000000E+00
140.6932 0.2310590
141.1753 0.3394930
141.6575 0.3352000
142.1396 0.6387610
142.6217 0.6619620
143.1038 0.3369620
143.5859 2.5288999E-02
144.0681 0.2394910
144.5502 0.3060400
145.0323 0.2397880
145.5144 2.5976000E-02
145.9965 0.3838420
146.4786 0.8404010
146.9608 1.277727
147.4429 1.699841
147.9250 2.155937
148.4071 2.705713
148.8892 3.265406
149.3713 3.682920
149.8535 3.815922
150.3356 3.956532
150.8177 4.167297
151.2998 4.407146
151.7819 4.801231
152.2640 5.388498
152.7462 6.128702
153.2283 6.927654
153.7104 7.405109
154.1925 8.244015
154.6746 9.755714
155.1567 12.47534
155.6389 14.91537
156.1210 16.77432
156.6031 18.22892
157.0852 19.74440
157.5673 21.40971
158.0495 23.15046
158.5316 24.93911
159.0137 26.62593
159.4958 28.54747
159.9779 30.87772
160.4600 33.54170
160.9422 36.29467
161.4243 39.04964
161.9064 41.86843
162.3885 44.75974
162.8706 47.50631
163.3527 50.63848
163.8349 54.62082
164.3170 59.29801
164.7991 63.92764
165.2812 68.96032
165.7633 73.44374
166.2454 76.52780
166.7276 78.10162
167.2097 78.06142
167.6918 76.21138
168.1739 72.61898
168.6560 67.76263
169.1381 60.85676
169.6203 53.10648
170.1024 45.40131
170.5845 38.60436
171.0666 32.85315
171.5487 28.05415
172.0309 24.18713
172.5130 21.10865
172.9951 19.10598
173.4772 17.75634
173.9593 16.40071
174.4414 14.72660
174.9236 12.95566
175.4057 11.17290
175.8878 9.355087
176.3699 8.016171
176.8520 7.859100
177.3341 8.488071
177.8163 9.051929
178.2984 9.166679
178.7805 9.005001
179.2626 8.724518
179.7447 8.304546
180.2268 8.011925
180.7090 8.175846
181.1911 8.698177
181.6732 9.280983
182.1553 9.801582
182.6374 10.28537
183.1195 10.66217
183.6017 10.88261
184.0838 11.31539
184.5659 12.62014
185.0480 14.62189
185.5301 16.51914
186.0123 17.84805
186.4944 18.76242
186.9765 19.65039
187.4586 20.51888
187.9407 21.42787
188.4228 22.50108
188.9050 23.71713
189.3871 24.93346
189.8692 25.97333
190.3513 26.90150
190.8334 28.13943
191.3155 29.75816
191.7977 31.53045
192.2798 32.97131
192.7619 34.08158
193.2440 35.49200
193.7261 37.46487
194.2082 39.99762
194.6904 43.26756
195.1725 47.40886
195.6546 52.04566
196.1367 56.18291
196.6188 59.77129
197.1009 63.76146
197.5831 68.88933
198.0652 75.06872
198.5473 80.97927
199.0294 86.83263
199.5115 91.99527
199.9937 95.22940
200.4758 96.47591
200.9579 96.05208
201.4400 93.60732
201.9221 88.97013
202.4042 84.95580
202.8864 82.19444
203.3685 79.67239
203.8506 74.64838
204.3327 66.63856
204.8148 58.29612
205.2969 50.70282
205.7791 43.70819
206.2612 38.57496
206.7433 35.60430
207.2254 34.34409
207.7075 33.79069
208.1896 34.07247
208.6718 34.68205
209.1539 35.25658
209.6360 35.63470
210.1181 36.78060
210.6002 38.89136
211.0823 41.71658
211.5645 44.55875
212.0466 47.37646
212.5287 50.34880
213.0108 53.49472
213.4929 56.72434
213.9750 60.57301
214.4572 65.20547
214.9393 70.42465
215.4214 75.82371
215.9035 81.43657
216.3856 87.18012
216.8678 92.92973
217.3499 98.82002
217.8320 104.5980
218.3141 110.4146
218.7962 116.0165
219.2783 120.5551
219.7605 123.9224
220.2426 126.3108
220.7247 127.8520
221.2068 128.7097
221.6889 128.3031
222.1710 126.6322
222.6532 123.6754
223.1353 119.5042
223.6174 114.3529
224.0995 107.5346
224.5816 98.43767
225.0637 85.80268
225.5459 73.81389
226.0280 62.49191
226.5101 51.88098
226.9922 42.41562
227.4743 33.75941
227.9564 26.63025
228.4386 21.46169
228.9207 19.16070
229.4028 16.81237
229.8849 14.19050
230.3670 11.52555
230.8492 9.401550
231.3313 7.947929
231.8134 6.863960
232.2955 6.045822
232.7776 5.653503
233.2597 5.174080
233.7419 4.532387
234.2240 3.822105
234.7061 3.298264
235.1882 2.994949
235.6703 2.827164
236.1524 2.719879
236.6346 2.482391
237.1167 2.770905
237.5988 3.742981
238.0809 5.177971
238.5630 6.598869
239.0451 7.980553
239.5273 9.365730
240.0094 10.69567
240.4915 11.70088
240.9736 13.37850
241.4557 15.88180
241.9378 18.99307
242.4200 22.31754
242.9021 26.18451
243.3842 29.80717
243.8663 32.85700
244.3484 35.13650
244.8306 37.43246
245.3127 39.70757
245.7948 41.99691
246.2769 44.34108
246.7590 46.65303
247.2411 49.15833
247.7233 51.93463
248.2054 55.04632
248.6875 58.09122
249.1696 60.84305
249.6517 63.71411
250.1338 67.31831
250.6160 71.82449
251.0981 76.69606
251.5802 81.52945
252.0623 86.06480
252.5444 92.04391
253.0265 99.56983
253.5087 108.4146
253.9908 118.0521
254.4729 128.3292
254.9550 139.8492
255.4371 153.1491
255.9192 168.3960
256.4014 183.1375
256.8835 197.5599
257.3656 211.2946
257.8477 224.8879
258.3298 240.2541
258.8120 251.3767
259.2941 257.7849
259.7762 259.7188
260.2583 251.7474
260.7404 230.9748
261.2225 203.7937
261.7047 175.3769
262.1868 143.6849
262.6689 115.9473
263.1510 93.72870
263.6331 77.11579
264.1152 62.69601
264.5974 50.64346
265.0795 40.67381
265.5616 33.04384
266.0437 28.11647
266.5258 23.96935
267.0079 20.41189
267.4901 17.36610
267.9722 14.40343
268.4543 11.44709
268.9364 8.670998
269.4185 6.188461
269.9006 3.991943
270.3828 2.131798
270.8649 0.6144710
271.3470 0.5707630
271.8291 1.469841
272.3112 2.071121
272.7933 2.427231
273.2755 2.505219
273.7576 2.270081
274.2397 2.086609
274.7218 2.059090
275.2039 2.125748
275.6860 2.109100
276.1682 2.036575
276.6503 1.807838
277.1324 1.292427
277.6145 0.4763490
278.0966 0.3767240
278.5787 1.240509
279.0609 2.061447
279.5430 2.582092
280.0251 2.712639
280.5072 3.165497
280.9893 4.600639
281.4715 7.012337
281.9536 8.602325
282.4357 9.145004
282.9178 9.173553
283.3999 9.576889
283.8820 10.38174
284.3642 11.25587
284.8463 11.97549
285.3284 12.57730
285.8105 13.49574
286.2926 14.78402
286.7747 16.22902
287.2569 17.41698
287.7390 18.36931
288.2211 19.70547
288.7032 21.93290
289.1853 24.78825
289.6674 26.99273
290.1496 28.45602
290.6317 29.93492
291.1138 32.51650
291.5959 36.02962
292.0780 39.18128
292.5602 41.53252
293.0423 43.27203
293.5244 44.87140
294.0065 46.32750
294.4886 47.54477
294.9707 48.70755
295.4529 49.63257
295.9350 49.70540
296.4171 48.99233
296.8992 47.12837
297.3813 42.95319
297.8634 36.65371
298.3456 30.06389
298.8277 24.36145
299.3098 19.45708
299.7919 15.21134
300.2740 11.64977
300.7561 8.701706
301.2383 6.509689
301.7204 4.970284
302.2025 3.766541
302.6846 2.775749
303.1667 1.958260
303.6488 1.215942
304.1310 0.5126800
304.6131 2.5696000E-02
305.0952 0.1190110
305.5773 9.3070999E-02
306.0594 0.2167510
306.5415 0.3830570
307.0237 0.9653930
307.5058 0.5724410
307.9879 1.014091
308.4700 2.665802
308.9521 3.443161
309.4343 3.709122
309.9164 4.123337
310.3985 5.123116
310.8806 6.279335
311.3627 7.265221
311.8448 8.073128
312.3270 8.856354
312.8091 9.664841
313.2912 10.51570
313.7733 11.42921
314.2554 12.15277
314.7375 13.16486
315.2197 14.81436
315.7018 17.05647
316.1839 19.38390
316.6660 21.85552
317.1481 24.17923
317.6302 26.07372
318.1124 27.15562
318.5945 28.21545
319.0766 29.51508
319.5587 31.00854
320.0408 32.55489
320.5229 34.58372
321.0051 36.32148
321.4872 37.36649
321.9693 37.67963
322.4514 37.23017
322.9335 35.81663
323.4156 33.65125
323.8978 31.14226
324.3799 28.12122
324.8620 24.97663
325.3441 21.76905
325.8262 18.41869
326.3083 15.37378
326.7905 12.78123
327.2726 10.46601
327.7547 8.245171
328.2368 5.814133
328.7189 3.766838
329.2010 2.286385
329.6832 1.421280
330.1653 0.5599670
330.6474 0.4421390
331.1295 1.319435
331.6116 1.856361
332.0938 1.932304
332.5759 1.855972
333.0580 1.540962
333.5401 1.051842
334.0222 0.9633940
334.5043 1.575760
334.9865 2.152199
335.4686 2.202728
335.9507 1.465485
336.4328 1.001709
336.9149 1.037254
337.3970 1.292244
337.8792 0.9732440
338.3613 0.1118160
338.8434 1.241814
339.3255 2.064301
339.8076 2.520233
340.2898 3.196419
340.7719 4.194397
341.2540 5.252548
341.7361 5.982040
342.2182 6.341568
342.7003 6.624489
343.1825 6.745628
343.6646 6.823868
344.1467 7.814293
344.6288 9.875923
345.1109 12.09014
345.5930 13.40213
346.0752 13.90471
346.5573 14.74947
347.0394 16.33949
347.5215 18.33641
348.0036 19.91428
348.4857 21.08191
348.9679 22.48550
349.4500 24.76037
349.9321 27.68008
350.4142 30.60085
350.8963 33.47089
351.3784 36.22505
351.8606 38.84369
352.3427 41.25864
352.8248 43.27119
353.3069 44.84222
353.7890 45.88484
354.2711 46.34949
354.7533 46.24918
355.2354 45.43877
355.7175 43.85603
356.1996 41.47101
356.6817 38.23071
357.1638 33.22155
357.6460 27.99941
358.1281 23.67360
358.6102 20.23512
359.0923 17.13297
359.5744 13.94322
360.0565 11.02672
360.5387 8.753128
361.0208 7.553261
361.5029 6.598297
361.9850 5.423981
362.4671 4.163177
362.9492 3.325211
363.4314 3.351715
363.9135 3.672554
364.3956 3.950203
364.8777 4.122116
365.3598 4.356293
365.8419 4.683998
366.3241 5.077484
366.8062 5.596077
367.2883 5.998604
367.7704 6.766777
368.2526 8.157509
368.7347 10.32428
369.2168 12.26629
369.6989 13.90264
370.1810 15.35806
370.6631 16.72571
371.1453 17.66020
371.6274 19.02785
372.1095 20.99846
372.5916 23.52471
373.0737 26.26691
373.5558 29.55026
374.0380 32.60226
374.5201 34.96022
375.0022 36.34422
375.4843 37.91921
375.9664 39.86331
376.4485 41.88542
376.9307 43.50676
377.4128 44.73364
377.8949 45.69777
378.3770 46.46211
378.8591 46.97092
379.3412 46.62602
379.8234 45.26155
380.3055 43.83322
380.7876 43.39584
381.2697 43.89731
381.7518 44.72028
382.2339 45.72769
382.7161 46.93959
383.1982 48.56870
383.6803 50.56670
384.1624 52.41158
384.6445 53.38187
385.1266 53.91225
385.6088 55.18147
386.0909 57.50945
386.5730 60.04956
387.0551 61.73784
387.5372 62.79335
388.0193 63.83044
388.5015 65.67352
388.9836 67.31876
389.4657 67.55120
389.9478 66.33104
390.4299 64.80679
390.9120 63.60853
391.3942 62.60244
391.8763 61.60812
392.3584 59.86208
392.8405 58.72192
393.3226 59.16216
393.8047 60.97972
394.2869 62.99918
394.7690 64.66209
395.2511 66.39801
395.7332 68.47940
396.2154 70.89363
396.6975 73.87453
397.1796 77.77047
397.6617 82.21395
398.1438 86.56138
398.6259 90.21040
399.1081 94.28626
399.5902 99.17090
400.0723 104.9657
400.5544 110.8881
401.0365 116.9550
401.5186 123.1573
402.0008 129.4036
402.4829 135.6512
402.9650 142.0943
403.4471 148.7986
403.9292 155.7387
404.4113 162.5945
404.8935 169.2672
405.3756 176.1689
405.8577 183.6144
406.3398 191.6187
406.8219 199.4920
407.3040 207.1429
407.7862 214.8609
408.2683 223.5165
408.7504 233.1640
409.2325 242.0935
409.7146 249.7204
410.1967 256.9675
410.6789 262.4334
411.1610 268.6096
411.6431 273.7190
412.1252 277.3323
412.6073 279.2305
413.0894 278.7619
413.5716 275.9380
414.0537 270.4329
414.5358 261.3459
415.0179 249.1479
415.5000 235.0560
415.9821 219.4840
416.4643 202.6479
416.9464 184.0444
417.4285 163.5517
417.9106 144.1028
418.3927 127.3285
418.8748 112.7111
419.3570 99.93385
419.8391 89.61597
420.3212 80.23656
420.8033 70.95481
421.2854 61.98160
421.7675 54.03627
422.2497 47.56255
422.7318 41.99550
423.2139 37.17056
423.6960 33.34676
424.1781 29.66782
424.6602 25.99374
425.1424 22.44243
425.6245 19.22528
426.1066 16.42101
426.5887 13.89262
427.0709 11.59601
427.5530 9.530418
428.0351 7.936417
428.5172 6.947029
428.9993 6.223671
429.4814 5.533936
429.9636 4.866249
430.4457 4.292511
430.9278 3.872223
431.4099 3.494606
431.8920 2.841782
432.3741 1.852524
432.8563 1.031677
433.3384 0.7660680
433.8205 0.9274520
434.3026 0.5248950
434.7847 0.5168150
435.2668 1.533417
435.7490 1.650261
436.2311 1.134491
436.7132 0.9630970
437.1953 1.517509
437.6774 2.355827
438.1595 2.928551
438.6417 3.275696
439.1238 3.563347
439.6059 3.963768
440.0880 4.318344
440.5701 4.419121
441.0522 4.211685
441.5344 3.971336
442.0165 3.937294
442.4986 3.948700
442.9807 3.809242
443.4628 3.262108
443.9449 2.739578
444.4271 2.498871
444.9092 2.470131
445.3913 2.244667
445.8734 1.349106
446.3555 0.5269620
446.8376 0.1935650
447.3198 0.7609410
447.8019 1.055954
448.2840 0.8965070
448.7661 0.5194930
449.2482 0.2674790
449.7303 0.3258130
450.2125 0.1845400
450.6946 0.3818440
451.1767 1.324234
451.6588 1.816971
452.1409 1.711357
452.6230 1.514633
453.1052 1.674049
453.5873 2.246964
454.0694 2.327019
454.5515 1.649490
455.0337 0.8545070
455.5158 1.085617
455.9979 2.291573
456.4800 3.675125
456.9621 4.993164
457.4442 6.236877
457.9264 7.417320
458.4085 8.528381
458.8906 9.526657
459.3727 10.12447
459.8548 10.63913
460.3369 11.55463
460.8191 13.00040
461.3012 14.84043
461.7833 17.13223
462.2654 19.73695
462.7475 22.35315
463.2296 24.58455
463.7118 27.04547
464.1939 30.21953
464.6760 34.17132
465.1581 37.99694
465.6402 41.25281
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