#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-06-07 10:54:25 +0300 (Thu, 07 Jun 2018) $
#$Revision: 1007 $
#$URL: svn://172.16.1.111/rod/cif/1/00/04/1000464.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000464
loop_
_publ_author_name
'Zubkova, N. V.'
'Pushcharovsky, D. Y.'
'Giester, G.'
'Tillmanns, E.'
'Pekov, I. V.'
'Kleimenov, D. A.'
_publ_section_title
;
 The crystal structure of arsentsumebite, Pb2Cu[(As,S)O4]2(OH) Locality:
 oxidation zone of the Berezovskoye gold deposit, Middle Urals, Russia
;
_journal_name_full               'Mineralogy and Petrology'
_journal_page_first              79
_journal_page_last               88
_journal_paper_doi               10.1007/s007100200016
_journal_volume                  75
_journal_year                    2002
_chemical_compound_source        R070629
_chemical_formula_sum            'As Cu H O9 Pb2 S'
_chemical_name_mineral           Arsentsumebite
_space_group_IT_number           11
_symmetry_space_group_name_Hall  '-P 2yb'
_symmetry_space_group_name_H-M   'P 1 21/m 1'
_cell_angle_alpha                90
_cell_angle_beta                 112.29
_cell_angle_gamma                90
_cell_length_a                   7.804
_cell_length_b                   5.890
_cell_length_c                   8.964
_cell_volume                     381.246
_exptl_crystal_density_diffrn    6.359
_cod_original_formula_sum        'Pb2 Cu (As S) (O9 H)'
_cod_database_code               9009849
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R070629.rod
_rod_data_source.block           3500000
_rod_database.code               1000464
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9009849 COD http://www.crystallography.net/cod/9009849.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
148.9056 0.0000000E+00
149.3877 15.56543
149.8698 50.72266
150.3519 80.45996
150.8340 56.11768
151.3161 5.295410
151.7983 11.77979
152.2804 32.89404
152.7625 96.91846
153.2446 150.7427
153.7267 191.6953
154.2088 221.5244
154.6909 235.6445
155.1731 230.3799
155.6552 231.9668
156.1373 247.2139
156.6194 271.4199
157.1015 298.6929
157.5836 340.3501
158.0658 375.0239
158.5479 389.0684
159.0300 364.5825
159.5121 355.9409
159.9942 398.9819
160.4763 471.4717
160.9585 522.1499
161.4406 510.4170
161.9227 483.1211
162.4048 472.5762
162.8869 496.9399
163.3690 528.3164
163.8512 548.9727
164.3333 561.3071
164.8154 586.2485
165.2975 661.7188
165.7796 745.1074
166.2617 791.7637
166.7439 734.1304
167.2260 667.9302
167.7081 664.4478
168.1902 729.7373
168.6723 800.2104
169.1544 840.0195
169.6366 856.4019
170.1187 862.0439
170.6008 854.0015
171.0829 842.1931
171.5650 839.4775
172.0471 851.8345
172.5293 861.5605
173.0114 848.2507
173.4935 817.5327
173.9756 789.4360
174.4577 783.7144
174.9398 790.3562
175.4220 790.3469
175.9041 767.5510
176.3862 737.7275
176.8683 743.9004
177.3504 798.7090
177.8326 855.8342
178.3147 851.1216
178.7968 810.4902
179.2789 783.7449
179.7610 806.1636
180.2431 851.8281
180.7253 873.7610
181.2074 865.1233
181.6895 836.8792
182.1716 829.4983
182.6537 854.7808
183.1358 899.5151
183.6180 951.3145
184.1001 1004.951
184.5822 1011.644
185.0643 965.9995
185.5464 906.5256
186.0285 862.5955
186.5107 836.7532
186.9928 825.4978
187.4749 826.2437
187.9570 839.0530
188.4391 837.9546
188.9212 815.0840
189.4034 782.8071
189.8855 752.4119
190.3676 723.8059
190.8497 701.4646
191.3318 691.1277
191.8139 691.8708
192.2961 692.3633
192.7782 694.6194
193.2603 693.2617
193.7424 668.5212
194.2245 616.6931
194.7066 558.9751
195.1888 516.4800
195.6709 489.7046
196.1530 457.9958
196.6351 410.4739
197.1172 352.1865
197.5993 320.8652
198.0815 322.9148
198.5636 333.8547
199.0457 325.9658
199.5278 298.1350
200.0099 259.2617
200.4920 205.4956
200.9742 136.8223
201.4563 85.80298
201.9384 52.13794
202.4205 36.32153
202.9026 49.57031
203.3847 102.9231
203.8668 138.6816
204.3490 121.3484
204.8311 41.07031
205.3132 20.71143
205.7953 62.12891
206.2774 83.36646
206.7595 72.10327
207.2417 28.60449
207.7238 17.71753
208.2059 53.38989
208.6880 81.12988
209.1701 84.79517
209.6522 54.49854
210.1344 0.5283200
210.6165 36.03833
211.0986 51.07520
211.5807 56.86938
212.0628 63.90137
212.5449 76.67065
213.0271 74.75635
213.5092 46.97729
213.9913 3.471191
214.4734 25.42334
214.9555 11.79785
215.4376 19.48022
215.9198 55.55811
216.4019 107.8792
216.8840 136.0649
217.3661 123.9358
217.8482 68.20947
218.3303 30.35913
218.8125 17.84863
219.2946 16.08154
219.7767 4.351807
220.2588 26.48340
220.7409 47.67432
221.2230 45.16040
221.7052 9.002686
222.1873 1.239746
222.6694 30.04761
223.1515 77.52539
223.6336 91.61450
224.1157 49.70142
224.5979 13.59937
225.0800 11.47632
225.5621 64.87207
226.0442 90.02734
226.5263 69.15015
227.0084 25.24194
227.4906 21.30420
227.9727 83.84424
228.4548 147.0156
228.9369 176.0566
229.4190 149.6731
229.9011 137.8901
230.3833 148.5117
230.8654 176.0632
231.3475 197.8867
231.8296 208.4785
232.3117 220.1638
232.7938 241.6531
233.2760 280.4199
233.7581 313.0122
234.2402 336.7390
234.7223 352.3079
235.2044 364.2412
235.6865 371.1233
236.1687 376.0859
236.6508 381.2722
237.1329 386.3464
237.6150 391.9377
238.0971 395.0786
238.5792 396.0051
239.0614 413.2292
239.5435 457.7764
240.0256 507.8008
240.5077 543.0034
240.9898 558.9072
241.4719 568.2488
241.9541 572.0862
242.4362 569.9077
242.9183 569.6270
243.4004 576.4446
243.8825 580.8196
244.3646 569.1711
244.8468 525.7217
245.3289 493.5259
245.8110 483.2578
246.2931 497.1870
246.7752 523.0664
247.2573 576.4976
247.7395 630.4851
248.2216 640.5933
248.7037 574.7085
249.1858 520.4565
249.6679 506.8062
250.1500 545.8259
250.6322 579.6868
251.1143 615.6052
251.5964 641.8423
252.0785 631.2722
252.5606 555.1206
253.0427 490.9844
253.5248 473.4919
254.0070 527.3325
254.4891 548.7219
254.9712 527.4631
255.4533 478.6892
255.9354 430.9150
256.4175 372.1282
256.8997 335.2771
257.3818 341.6667
257.8639 417.0186
258.3460 461.2590
258.8281 462.0073
259.3102 435.0830
259.7924 424.8118
260.2745 439.3843
260.7566 457.1306
261.2387 471.7114
261.7208 490.2048
262.2029 476.2766
262.6851 412.1980
263.1672 315.2468
263.6493 251.5146
264.1314 227.2297
264.6135 228.3770
265.0956 255.0200
265.5778 318.1646
266.0599 361.1619
266.5420 373.9077
267.0241 362.7769
267.5062 352.4819
267.9883 342.0334
268.4705 330.1208
268.9526 321.0471
269.4347 319.7778
269.9168 298.6301
270.3989 241.6218
270.8810 164.7119
271.3632 141.7676
271.8453 192.8315
272.3274 249.8923
272.8095 255.7905
273.2916 196.5977
273.7737 154.5586
274.2559 144.5793
274.7380 160.9419
275.2201 176.1702
275.7022 194.1152
276.1843 208.7546
276.6664 209.5967
277.1486 193.2163
277.6307 190.6028
278.1128 213.7185
278.5949 253.9680
279.0770 272.4688
279.5591 263.8130
280.0413 250.9578
280.5234 260.8569
281.0055 294.7686
281.4876 312.5449
281.9697 293.9160
282.4518 253.9670
282.9340 261.5559
283.4161 324.5984
283.8982 399.7534
284.3803 444.4512
284.8624 459.2349
285.3445 475.7148
285.8267 501.5662
286.3088 535.4844
286.7909 573.1711
287.2730 613.7222
287.7551 660.4187
288.2372 722.3438
288.7194 796.7339
289.2015 862.8940
289.6836 912.6558
290.1657 950.0859
290.6478 980.7812
291.1299 1003.682
291.6121 1033.955
292.0942 1088.234
292.5763 1163.721
293.0584 1248.086
293.5405 1346.080
294.0226 1445.870
294.5048 1521.142
294.9869 1571.695
295.4690 1610.159
295.9511 1640.089
296.4332 1666.575
296.9153 1706.498
297.3975 1775.879
297.8796 1856.387
298.3617 1909.034
298.8438 1933.738
299.3259 1971.679
299.8080 2080.042
300.2902 2230.024
300.7723 2357.460
301.2544 2422.832
301.7365 2461.358
302.2186 2519.799
302.7007 2597.175
303.1829 2675.275
303.6650 2733.032
304.1471 2781.167
304.6292 2837.908
305.1113 2927.913
305.5934 3018.150
306.0756 3069.344
306.5577 3083.728
307.0398 3096.811
307.5219 3134.410
308.0040 3187.988
308.4861 3242.328
308.9683 3303.851
309.4504 3353.122
309.9325 3367.925
310.4146 3351.520
310.8967 3341.543
311.3788 3369.528
311.8610 3411.968
312.3431 3443.497
312.8252 3451.691
313.3073 3451.530
313.7894 3452.123
314.2715 3451.770
314.7537 3439.547
315.2358 3401.118
315.7179 3351.693
316.2000 3305.958
316.6821 3273.428
317.1642 3242.000
317.6464 3206.858
318.1285 3168.280
318.6106 3131.809
319.0927 3094.809
319.5748 3062.863
320.0569 3040.387
320.5391 3044.643
321.0212 3041.987
321.5033 3018.611
321.9854 2977.059
322.4675 2943.445
322.9496 2927.924
323.4318 2918.266
323.9139 2906.030
324.3960 2883.029
324.8781 2865.263
325.3602 2850.146
325.8423 2839.288
326.3245 2847.468
326.8066 2899.724
327.2887 2954.991
327.7708 2989.864
328.2529 2982.422
328.7350 2981.543
329.2171 2991.539
329.6992 3010.874
330.1814 3029.897
330.6635 3044.046
331.1456 3062.380
331.6277 3090.147
332.1098 3130.777
332.5919 3176.540
333.0741 3239.410
333.5562 3308.040
334.0383 3333.414
334.5204 3297.493
335.0025 3248.058
335.4846 3207.276
335.9668 3169.233
336.4489 3160.610
336.9310 3194.724
337.4131 3253.985
337.8952 3288.823
338.3773 3299.869
338.8595 3290.846
339.3416 3255.670
339.8237 3189.427
340.3058 3137.250
340.7879 3110.392
341.2701 3088.062
341.7522 3016.429
342.2343 2889.884
342.7164 2767.247
343.1985 2685.949
343.6806 2642.841
344.1628 2600.878
344.6449 2562.697
345.1270 2514.405
345.6091 2421.327
346.0912 2287.737
346.5733 2158.839
347.0555 2062.071
347.5376 1987.870
348.0197 1900.314
348.5018 1793.421
348.9839 1689.058
349.4660 1626.857
349.9482 1593.794
350.4303 1539.819
350.9124 1416.229
351.3945 1265.192
351.8766 1150.372
352.3587 1075.919
352.8409 1025.454
353.3230 1003.010
353.8051 993.4749
354.2872 967.7517
354.7693 902.6589
355.2514 822.5117
355.7336 743.9070
356.2157 667.3311
356.6978 604.7515
357.1799 581.5728
357.6620 571.9119
358.1441 541.3794
358.6263 448.5847
359.1084 355.7236
359.5905 298.5898
360.0726 275.7258
360.5547 260.2307
361.0368 245.6472
361.5190 230.6086
362.0011 213.7332
362.4832 200.3767
362.9653 179.3115
363.4474 143.3057
363.9295 94.52124
364.4117 48.29053
364.8938 4.174561
365.3759 45.21021
365.8580 64.06982
366.3401 29.76196
366.8222 8.245361
367.3044 13.00439
367.7865 37.44336
368.2686 52.30054
368.7507 41.90259
369.2328 34.90063
369.7149 44.96045
370.1971 93.57007
370.6792 122.6108
371.1613 128.3367
371.6434 115.5994
372.1255 94.66943
372.6076 59.79272
373.0898 26.42334
373.5719 0.1267090
374.0540 20.62842
374.5361 29.62134
375.0182 22.49390
375.5003 8.634277
375.9825 2.655273
376.4646 4.972656
376.9467 13.95947
377.4288 35.87598
377.9109 69.41919
378.3930 73.70483
378.8752 41.33032
379.3573 1.895752
379.8394 6.382324
380.3215 15.52222
380.8036 43.13477
381.2857 72.59033
381.7679 100.8694
382.2500 115.8962
382.7321 116.4490
383.2142 120.8118
383.6963 150.4902
384.1784 198.7976
384.6606 245.3635
385.1427 287.2498
385.6248 320.9932
386.1069 340.9453
386.5890 347.4192
387.0711 342.8247
387.5533 316.4475
388.0354 283.9546
388.5175 268.2266
388.9996 285.9875
389.4817 303.9993
389.9638 298.3713
390.4460 272.8167
390.9281 238.9216
391.4102 179.6514
391.8923 128.6533
392.3744 117.1106
392.8565 172.6023
393.3387 212.4446
393.8208 197.5806
394.3029 146.1843
394.7850 91.52734
395.2671 25.31909
395.7492 27.76025
396.2314 55.31567
396.7135 51.08472
397.1956 40.76782
397.6777 18.01514
398.1598 5.781738
398.6419 16.47559
399.1241 8.422363
399.6062 21.30225
400.0883 5.529785
400.5704 42.47339
401.0525 64.32324
401.5346 43.19702
402.0168 12.50903
402.4989 1.479248
402.9810 17.95850
403.4631 35.54907
403.9452 51.94434
404.4273 66.45947
404.9095 73.06958
405.3916 68.48828
405.8737 65.44067
406.3558 74.77197
406.8379 97.40405
407.3200 114.8020
407.8022 122.3584
408.2843 127.4971
408.7664 154.8220
409.2485 204.2019
409.7306 235.2866
410.2127 210.1750
410.6949 146.6626
411.1770 102.8225
411.6591 81.22925
412.1412 83.43799
412.6233 126.4131
413.1054 197.3579
413.5876 259.0605
414.0697 294.6765
414.5518 311.0671
415.0339 308.2205
415.5160 285.8792
415.9981 269.7070
416.4803 275.6355
416.9624 299.6907
417.4445 336.3552
417.9266 412.0764
418.4087 474.9294
418.8908 480.6946
419.3730 440.3486
419.8551 427.3727
420.3372 491.6122
420.8193 580.6404
421.3014 657.4075
421.7835 711.9011
422.2657 760.5199
422.7478 796.0549
423.2299 825.5402
423.7120 873.7493
424.1941 968.2532
424.6762 1064.534
425.1584 1142.774
425.6404 1193.523
426.1226 1253.839
426.6047 1327.926
427.0868 1410.724
427.5689 1493.454
428.0510 1573.842
428.5331 1653.072
429.0153 1730.568
429.4974 1806.543
429.9795 1899.691
430.4616 2011.734
430.9437 2137.367
431.4258 2271.244
431.9080 2412.468
432.3901 2555.027
432.8722 2692.245
433.3543 2834.260
433.8364 3016.965
434.3185 3238.785
434.8007 3465.661
435.2828 3669.245
435.7649 3858.017
436.2470 4057.169
436.7291 4272.123
437.2112 4483.227
437.6934 4684.091
438.1755 4867.253
438.6576 5000.070
439.1397 5046.044
439.6218 5045.735
440.1039 5044.982
440.5861 5051.807
441.0682 5006.246
441.5503 4836.980
442.0324 4608.864
442.5145 4396.914
442.9966 4229.663
443.4788 4077.465
443.9609 3932.714
444.4430 3794.350
444.9251 3660.723
445.4072 3511.042
445.8893 3379.919
446.3715 3288.431
446.8536 3287.177
447.3357 3262.451
447.8178 3208.773
448.2999 3131.338
448.7820 3042.158
449.2642 2939.199
449.7463 2831.615
450.2284 2725.573
450.7105 2626.037
451.1926 2499.566
451.6747 2330.603
452.1569 2159.058
452.6390 2042.617
453.1211 1986.863
453.6032 1926.164
454.0853 1831.389
454.5674 1721.167
455.0496 1663.992
455.5317 1663.140
456.0138 1664.329
456.4959 1613.286
456.9780 1525.928
457.4601 1444.798
457.9423 1378.734
458.4244 1327.403
458.9065 1299.186
459.3886 1287.824
459.8707 1271.788
460.3528 1241.612
460.8350 1204.304
461.3171 1155.032
461.7992 1093.383
462.2813 1030.642
462.7634 961.6833
463.2455 899.0100
463.7277 857.4962
464.2098 874.5962
464.6919 882.1807
465.1740 854.9189
465.6561 792.3262
466.1382 730.4943
466.6204 666.8293
467.1025 610.5178
467.5846 567.0024
468.0667 551.5344
468.5488 523.3890
469.0309 473.2864
469.5131 411.9221
469.9952 368.2598
470.4773 347.4307
470.9594 332.7991
471.4415 318.4535
471.9236 304.1948
472.4058 288.1237
472.8879 270.4421
473.3700 251.2811
473.8521 229.1259
474.3342 204.5233
474.8163 184.2019
475.2985 172.8689
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1243.792 113.1820
1244.274 104.3312
1244.756 104.6339
1245.239 112.8851
1245.721 110.5973
1246.203 94.60486
1246.685 77.16882
1247.167 52.77063
1247.649 33.45532
1248.131 9.999146
1248.613 9.265869
1249.096 6.691284
1249.578 59.94336
1250.060 83.14160
1250.542 47.98376
1251.024 22.24219
1251.506 24.03369
1251.988 39.93591
1252.470 52.52979
1252.953 63.27039
1253.435 77.69507
1253.917 98.52673
1254.399 95.75891
1254.881 58.52637
1255.363 30.96082
1255.845 31.71118
1256.327 47.19897
1256.809 62.46252
1257.292 75.34778
1257.774 85.55811
1258.256 95.94666
1258.738 93.99194
1259.220 75.89148
1259.702 56.73584
1260.184 47.65356
1260.666 41.43091
1261.148 30.42896
1261.631 17.40271
1262.113 4.643188
1262.595 12.03528
1263.077 7.352051
1263.559 21.71216
1264.041 55.59827
1264.523 90.69495
1265.005 115.3656
1265.487 108.6716
1265.970 84.40344
1266.452 65.20947
1266.934 49.61890
1267.416 53.55408
1267.898 78.47717
1268.380 101.7954
1268.862 110.6561
1269.344 109.3846
1269.827 96.16968
1270.309 76.49792
1270.791 58.24158
1271.273 39.26355
1271.755 40.10120
1272.237 61.30676
1272.719 81.43347
1273.201 80.42334
1273.683 79.68628
1274.166 102.5197
1274.648 89.53003
1275.130 117.7507
1275.612 78.64966
1276.094 57.39075
1276.576 57.28894
1277.058 53.51416
1277.540 12.00500
1278.022 16.53040
1278.505 3.609009
1278.987 31.02197
1279.469 57.20911
1279.951 75.50977
1280.433 87.72009
1280.915 94.01038
1281.397 94.96521
1281.879 84.12122
1282.362 73.94934
1282.844 68.40955
1283.326 63.87183
1283.808 60.52551
1284.290 58.02673
1284.772 53.33032
1285.254 45.66699
1285.736 50.00098
1286.219 87.20801
1286.701 110.2955
1287.183 101.8669
1287.665 81.37366
1288.147 85.92004
1288.629 102.0109
1289.111 102.1542
1289.593 70.06506
1290.075 57.20874
1290.557 72.89868
1291.040 86.77954
1291.522 90.23853
1292.004 89.60632
1292.486 86.38586
1292.968 88.13257
1293.450 112.8423
1293.932 169.6138
1294.414 181.6012
1294.897 142.9219
1295.379 91.60498
1295.861 29.54248
1296.343 10.11475
1296.825 38.47974
1297.307 112.2014
1297.789 131.5989
1298.271 95.41345
1298.754 54.86511
1299.236 65.91943
1299.718 60.69055
1300.200 25.38574
1300.682 0.0000000E+00
