#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-06-07 10:54:45 +0300 (Thu, 07 Jun 2018) $ #$Revision: 1012 $ #$URL: svn://172.16.1.111/rod/cif/1/00/04/1000468.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_1000468 loop_ _publ_author_name 'Burns, P. C.' 'Smith, J. V.' 'Steele, I. M.' _publ_section_title ; Arizona porphyry copper/hydrothermal deposits I. The structure of chenevixite and luetheite Note: Luetheite-chenevixite series Locality: Humboldt mine, Patagonia, Arizona ; _journal_name_full 'Mineralogical Magazine' _journal_page_first 25 _journal_page_last 30 _journal_paper_doi 10.1180/002646100549102 _journal_volume 64 _journal_year 2000 _chemical_compound_source R100177 _chemical_formula_sum 'Al0.635 As Cu Fe0.365 H2 O6' _chemical_name_mineral Luetheite _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb (1/2*x,y,-1/2*x+z)' _symmetry_space_group_name_H-M 'B 1 21 1' _cell_angle_alpha 90 _cell_angle_beta 89.99 _cell_angle_gamma 90 _cell_length_a 5.7012 _cell_length_b 5.1801 _cell_length_c 29.265 _cell_volume 864.277 _exptl_crystal_density_diffrn 4.211 _cod_original_formula_sum 'Cu (Al.635 Fe.365) As O6 H2' _cod_database_code 9009514 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type other _raman_measurement_device.excitation_laser_wavelength 532 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 15 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R100177.rod _rod_data_source.block 3500000 _rod_database.code 1000468 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9009514 COD http://www.crystallography.net/cod/9009514.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 132.4972 0.0000000E+00 132.9794 1.683871 133.4615 3.162396 133.9436 3.844308 134.4257 2.369594 134.9078 2.422174 135.3899 3.207573 135.8721 4.165749 136.3542 6.512115 136.8363 7.933349 137.3184 6.645218 137.8005 5.298156 138.2826 5.230469 138.7648 4.528767 139.2469 2.908060 139.7290 0.5743480 140.2111 0.9727270 140.6932 1.632191 141.1753 1.693178 141.6575 1.311958 142.1396 0.1706660 142.6217 0.5872840 143.1038 0.4319840 143.5859 0.7087210 144.0681 0.5963060 144.5502 1.535965 145.0323 4.250439 145.5144 5.917191 145.9965 5.877472 146.4786 5.762100 146.9608 5.916958 147.4429 6.429276 147.9250 6.970657 148.4071 7.973740 148.8892 8.847595 149.3713 8.657738 149.8535 6.371677 150.3356 4.049839 150.8177 2.177208 151.2998 0.6905520 151.7819 0.2016410 152.2640 0.2416650 152.7462 0.2894520 153.2283 0.8672560 153.7104 1.460495 154.1925 2.100784 154.6746 2.796394 155.1567 3.546021 155.6389 4.307922 156.1210 5.152718 156.6031 6.018120 157.0852 6.775139 157.5673 7.165054 158.0495 7.594620 158.5316 8.302834 159.0137 9.577515 159.4958 10.75928 159.9779 11.58205 160.4600 12.16382 160.9422 12.89102 161.4243 13.92029 161.9064 15.11417 162.3885 16.34509 162.8706 17.16080 163.3527 18.54080 163.8349 21.24851 164.3170 25.03261 164.7991 28.69216 165.2812 31.58094 165.7633 34.12239 166.2454 36.69189 166.7276 39.14392 167.2097 41.89551 167.6918 45.25415 168.1739 49.16089 168.6560 53.44882 169.1381 58.16504 169.6203 63.09772 170.1024 66.90540 170.5845 69.93962 171.0666 73.12610 171.5487 76.67719 172.0309 80.56623 172.5130 84.79102 172.9951 89.28345 173.4772 94.10545 173.9593 99.38967 174.4414 105.0649 174.9236 111.2520 175.4057 117.9379 175.8878 125.1775 176.3699 132.9471 176.8520 141.6501 177.3341 150.9458 177.8163 160.1413 178.2984 168.8835 178.7805 177.2881 179.2626 185.6718 179.7447 193.9301 180.2268 201.6703 180.7090 208.2304 181.1911 213.8132 181.6732 218.9361 182.1553 223.5775 182.6374 227.9481 183.1195 232.4406 183.6017 237.2002 184.0838 241.6981 184.5659 245.1123 185.0480 247.6665 185.5301 250.7226 186.0123 255.1770 186.4944 260.6522 186.9765 265.8680 187.4586 270.8604 187.9407 275.5053 188.4228 279.4205 188.9050 282.6636 189.3871 286.1272 189.8692 290.1326 190.3513 294.4662 190.8334 299.2482 191.3155 304.3427 191.7977 310.1275 192.2798 317.3592 192.7619 326.0251 193.2440 335.2350 193.7261 344.7500 194.2082 354.5054 194.6904 364.3188 195.1725 374.0496 195.6546 384.1341 196.1367 395.5761 196.6188 408.6250 197.1009 420.5070 197.5831 430.0096 198.0652 437.2258 198.5473 441.7420 199.0294 443.6184 199.5115 442.8122 199.9937 438.7501 200.4758 431.1568 200.9579 422.0240 201.4400 412.2246 201.9221 401.7321 202.4042 390.9834 202.8864 379.7077 203.3685 368.4527 203.8506 358.5013 204.3327 350.0429 204.8148 342.4257 205.2969 335.4687 205.7791 329.2560 206.2612 323.1794 206.7433 317.4632 207.2254 311.6726 207.7075 304.3144 208.1896 294.6463 208.6718 285.5216 209.1539 278.7306 209.6360 274.9352 210.1181 270.2566 210.6002 264.0162 211.0823 257.0392 211.5645 251.6342 212.0466 247.9789 212.5287 245.4547 213.0108 243.8811 213.4929 243.4759 213.9750 243.0777 214.4572 242.4357 214.9393 242.0969 215.4214 243.3149 215.9035 246.0611 216.3856 250.0011 216.8678 255.0227 217.3499 261.3417 217.8320 268.5447 218.3141 276.7543 218.7962 285.5217 219.2783 293.5987 219.7605 300.5409 220.2426 307.6578 220.7247 315.7016 221.2068 325.3231 221.6889 333.6901 222.1710 341.0801 222.6532 347.0773 223.1353 350.2010 223.6174 350.6928 224.0995 348.1932 224.5816 342.2173 225.0637 331.4887 225.5459 320.4886 226.0280 309.9103 226.5101 299.0053 226.9922 285.5749 227.4743 268.0042 227.9564 250.2843 228.4386 234.2670 228.9207 221.4279 229.4028 207.2198 229.8849 190.3851 230.3670 172.3915 230.8492 156.8762 231.3313 144.4975 231.8134 133.8051 232.2955 124.0345 232.7776 115.2420 233.2597 107.6465 233.7419 101.5865 234.2240 96.61145 234.7061 91.63412 235.1882 86.22440 235.6703 81.48421 236.1524 77.88237 236.6346 75.75984 237.1167 74.03647 237.5988 72.63004 238.0809 71.63876 238.5630 71.35907 239.0451 72.18704 239.5273 73.12126 240.0094 73.62897 240.4915 73.12195 240.9736 73.73694 241.4557 75.70428 241.9378 78.68138 242.4200 81.93689 242.9021 85.34305 243.3842 89.28610 243.8663 93.97583 244.3484 99.63458 244.8306 105.4523 245.3127 111.6911 245.7948 117.8970 246.2769 123.0984 246.7590 126.6073 247.2411 130.1907 247.7233 134.6200 248.2054 140.4089 248.6875 145.1497 249.1696 148.5947 249.6517 151.1228 250.1338 153.4131 250.6160 156.0229 251.0981 157.4105 251.5802 157.0686 252.0623 154.8951 252.5444 151.4846 253.0265 146.4557 253.5087 140.5277 253.9908 134.7827 254.4729 129.2479 254.9550 123.7584 255.4371 118.1195 255.9192 112.2613 256.4014 107.2079 256.8835 103.0671 257.3656 99.62430 257.8477 96.55235 258.3298 93.92209 258.8120 91.46136 259.2941 88.89349 259.7762 86.13365 260.2583 84.72975 260.7404 85.18932 261.2225 86.35260 261.7047 87.12447 262.1868 87.64331 262.6689 87.39319 263.1510 86.27061 263.6331 84.28506 264.1152 81.46988 264.5974 77.84317 265.0795 73.37282 265.5616 68.05136 266.0437 61.62067 266.5258 54.92720 267.0079 48.00264 267.4901 40.86946 267.9722 34.27835 268.4543 28.27422 268.9364 22.60162 269.4185 16.85605 269.9006 10.76367 270.3828 5.903717 270.8649 2.863098 271.3470 1.180054 271.8291 1.614487 272.3112 6.100601 272.7933 10.27605 273.2755 12.40260 273.7576 12.14238 274.2397 12.37608 274.7218 13.74994 275.2039 15.65701 275.6860 16.05754 276.1682 14.61882 276.6503 12.93037 277.1324 12.22324 277.6145 12.64943 278.0966 12.00543 278.5787 9.884674 279.0609 6.883667 279.5430 4.176010 280.0251 1.776016 280.5072 0.3807530 280.9893 1.999084 281.4715 3.073776 281.9536 5.356750 282.4357 9.144928 282.9178 13.72740 283.3999 17.93469 283.8820 21.74341 284.3642 25.53522 284.8463 29.21349 285.3284 32.87915 285.8105 37.55118 286.2926 43.33704 286.7747 49.84656 287.2569 56.80966 287.7390 64.19591 288.2211 71.31116 288.7032 77.67015 289.1853 83.48793 289.6674 89.92023 290.1496 97.07065 290.6317 104.3662 291.1138 111.4534 291.5959 118.2833 292.0780 124.2834 292.5602 129.5300 293.0423 133.7961 293.5244 136.3697 294.0065 137.2114 294.4886 136.9643 294.9707 136.2432 295.4529 134.9267 295.9350 132.5233 296.4171 128.5175 296.8992 123.6972 297.3813 119.3936 297.8634 115.6000 298.3456 112.0385 298.8277 108.4185 299.3098 104.9108 299.7919 101.8911 300.2740 99.41754 300.7561 97.54137 301.2383 96.38531 301.7204 95.92435 302.2025 96.13020 302.6846 97.03674 303.1667 98.57710 303.6488 100.6200 304.1310 103.0471 304.6131 106.2255 305.0952 110.8283 305.5773 116.4998 306.0594 122.2551 306.5415 127.6929 307.0237 132.9259 307.5058 138.4763 307.9879 144.5400 308.4700 149.6064 308.9521 152.2995 309.4343 153.2413 309.9164 153.6192 310.3985 154.5743 310.8806 154.7304 311.3627 153.1110 311.8448 149.6572 312.3270 144.6876 312.8091 137.8849 313.2912 129.8349 313.7733 121.2291 314.2554 111.4951 314.7375 101.9747 315.2197 93.43799 315.7018 85.75183 316.1839 78.39627 316.6660 70.84024 317.1481 63.62549 317.6302 57.25465 318.1124 51.51762 318.5945 46.97614 319.0766 44.13901 319.5587 42.71231 320.0408 41.61746 320.5229 40.20769 321.0051 39.25157 321.4872 39.22079 321.9693 40.52780 322.4514 42.12421 322.9335 43.79523 323.4156 45.67778 323.8978 47.98062 324.3799 50.85567 324.8620 53.98470 325.3441 57.30502 325.8262 60.88626 326.3083 64.37497 326.7905 67.93993 327.2726 71.29831 327.7547 74.07776 328.2368 75.62320 328.7189 77.27644 329.2010 79.44797 329.6832 82.12573 330.1653 84.07312 330.6474 85.71857 331.1295 86.39761 331.6116 85.57301 332.0938 82.25357 332.5759 78.91199 333.0580 75.77925 333.5401 72.96024 334.0222 70.73061 334.5043 69.77068 334.9865 68.38885 335.4686 65.34134 335.9507 59.79094 336.4328 55.10056 336.9149 51.52919 337.3970 48.90956 337.8792 46.84457 338.3613 45.17245 338.8434 44.05569 339.3255 43.55896 339.8076 43.71082 340.2898 44.41927 340.7719 45.77052 341.2540 47.42252 341.7361 48.68024 342.2182 49.44481 342.7003 51.54829 343.1825 55.95013 343.6646 62.34558 344.1467 68.15498 344.6288 73.18712 345.1109 78.84192 345.5930 87.24428 346.0752 97.99976 346.5573 108.1134 347.0394 116.6895 347.5215 124.4005 348.0036 133.3075 348.4857 143.3280 348.9679 152.7412 349.4500 161.2437 349.9321 168.2663 350.4142 172.0124 350.8963 171.9217 351.3784 169.3550 351.8606 165.0959 352.3427 159.5944 352.8248 154.4077 353.3069 150.1400 353.7890 146.8815 354.2711 144.5529 354.7533 143.1000 355.2354 143.0543 355.7175 145.4720 356.1996 149.5622 356.6817 153.9453 357.1638 157.7222 357.6460 161.7996 358.1281 167.0609 358.6102 173.4182 359.0923 180.0327 359.5744 186.9204 360.0565 193.5531 360.5387 199.4317 361.0208 204.5140 361.5029 208.7173 361.9850 212.1820 362.4671 214.7630 362.9492 215.9386 363.4314 215.3921 363.9135 213.4950 364.3956 210.3919 364.8777 205.9259 365.3598 200.6420 365.8419 194.8715 366.3241 188.3203 366.8062 180.5713 367.2883 170.5885 367.7704 160.3445 368.2526 150.4175 368.7347 140.9113 369.2168 130.9953 369.6989 119.9045 370.1810 108.8186 370.6631 98.58484 371.1453 89.47513 371.6274 80.78479 372.1095 72.25357 372.5916 63.94870 373.0737 56.63492 373.5558 50.53278 374.0380 44.99667 374.5201 39.60968 375.0022 34.38065 375.4843 29.40881 375.9664 24.57547 376.4485 20.11186 376.9307 16.44695 377.4128 13.74164 377.8949 11.28021 378.3770 8.752960 378.8591 6.192566 379.3412 4.136414 379.8234 2.681625 380.3055 1.451309 380.7876 3.2837000E-02 381.2697 1.751938 381.7518 3.106491 382.2339 3.855835 382.7161 4.203934 383.1982 4.686478 383.6803 5.287216 384.1624 5.680710 384.6445 5.534668 385.1266 4.993378 385.6088 4.387909 386.0909 3.745956 386.5730 3.119614 387.0551 2.625854 387.5372 2.212585 388.0193 1.723495 388.5015 0.8823240 388.9836 3.1128000E-02 389.4657 0.5215760 389.9478 0.7615970 390.4299 0.6116490 390.9120 0.2485200 391.3942 1.448471 391.8763 2.517990 392.3584 3.235367 392.8405 3.843872 393.3226 4.406403 393.8047 4.943817 394.2869 5.553024 394.7690 6.690292 395.2511 7.627136 395.7332 7.877014 396.2154 7.109375 396.6975 6.189178 397.1796 5.442062 397.6617 4.622910 398.1438 3.324310 398.6259 1.146393 399.1081 1.186554 399.5902 3.483459 400.0723 5.722870 400.5544 8.040100 401.0365 10.10458 401.5186 12.49916 402.0008 15.67218 402.4829 19.79393 402.9650 24.41930 403.4471 29.67178 403.9292 35.40872 404.4113 40.87941 404.8935 45.99559 405.3756 51.11844 405.8577 56.63452 406.3398 62.66695 406.8219 67.77582 407.3040 71.82431 407.7862 75.20668 408.2683 78.64711 408.7504 82.17120 409.2325 85.03569 409.7146 86.73947 410.1967 87.64471 410.6789 89.18613 411.1610 91.39810 411.6431 93.46259 412.1252 94.40370 412.6073 94.60852 413.0894 95.03654 413.5716 95.63867 414.0537 97.02573 414.5358 100.0860 415.0179 104.5823 415.5000 109.8536 415.9821 115.0106 416.4643 120.9748 416.9464 128.9481 417.4285 139.0629 417.9106 149.9031 418.3927 160.1786 418.8748 170.8019 419.3570 182.6693 419.8391 196.9946 420.3212 211.8554 420.8033 226.2924 421.2854 240.5566 421.7675 256.0878 422.2497 274.0356 422.7318 292.8578 423.2139 311.5321 423.6960 329.3940 424.1781 348.2626 424.6602 368.0287 425.1424 388.9575 425.6245 411.2429 426.1066 434.8904 426.5887 459.5105 427.0709 485.1237 427.5530 511.7279 428.0351 537.9242 428.5172 563.8809 428.9993 589.5908 429.4814 615.4000 429.9636 641.8298 430.4457 666.4099 430.9278 689.1391 431.4099 709.7042 431.8920 727.4164 432.3741 742.4165 432.8563 754.6254 433.3384 764.3608 433.8205 771.4406 434.3026 774.5270 434.7847 773.6575 435.2668 768.8232 435.7490 760.0868 436.2311 747.3572 436.7132 730.3652 437.1953 708.0936 437.6774 682.8079 438.1595 656.5908 438.6417 629.4883 439.1238 601.8267 439.6059 573.2532 440.0880 544.5848 440.5701 516.5165 441.0522 488.9363 441.5344 462.4395 442.0165 437.4233 442.4986 413.7046 442.9807 391.1797 443.4628 369.0536 443.9449 348.8543 444.4271 331.4979 444.9092 316.7181 445.3913 302.9186 445.8734 290.0684 446.3555 278.1736 446.8376 267.3178 447.3198 257.6982 447.8019 248.6487 448.2840 240.2507 448.7661 232.3720 449.2482 224.9440 449.7303 218.3735 450.2125 211.7158 450.6946 204.6787 451.1767 197.2747 451.6588 190.1861 452.1409 183.5515 452.6230 176.7448 453.1052 169.2468 453.5873 160.9392 454.0694 153.4388 454.5515 147.1147 455.0337 141.1664 455.5158 134.1805 455.9979 126.2274 456.4800 118.9268 456.9621 113.1350 457.4442 108.2070 457.9264 102.7814 458.4085 96.89987 458.8906 90.93018 459.3727 84.94553 459.8548 79.17688 460.3369 74.25220 460.8191 70.57208 461.3012 66.97702 461.7833 62.14922 462.2654 56.71635 462.7475 52.00177 463.2296 48.83345 463.7118 46.26732 464.1939 43.76915 464.6760 41.27425 465.1581 39.18690 465.6402 37.96051 466.1223 37.00060 466.6045 35.91078 467.0866 34.11833 467.5687 32.83620 468.0508 32.36899 468.5329 32.41769 469.0150 32.30006 469.4972 31.79538 469.9793 31.46666 470.4614 31.50453 470.9435 31.92247 471.4256 32.46179 471.9077 33.11005 472.3899 33.91199 472.8720 34.92513 473.3541 36.17165 473.8362 37.46606 474.3183 38.72493 474.8004 40.12218 475.2826 42.14990 475.7647 44.76175 476.2468 47.28140 476.7289 49.07961 477.2110 50.61768 477.6931 52.98245 478.1753 56.18944 478.6574 59.61230 479.1395 62.54738 479.6216 65.34219 480.1037 68.66962 480.5858 73.14874 481.0680 77.57480 481.5501 80.82672 482.0322 83.36749 482.5143 86.17261 482.9964 89.87624 483.4786 93.71805 483.9607 97.27127 484.4428 100.4500 484.9249 103.9545 485.4070 108.1682 485.8892 112.5490 486.3713 116.7297 486.8534 121.0154 487.3355 124.5351 487.8176 127.0904 488.2997 128.9727 488.7819 130.7878 489.2640 132.6248 489.7461 134.0265 490.2282 134.7631 490.7103 134.9032 491.1924 135.2602 491.6746 135.9256 492.1567 136.4025 492.6388 136.2125 493.1209 135.4237 493.6030 134.5311 494.0851 133.5339 494.5673 132.5154 495.0494 131.4729 495.5315 130.4912 496.0136 129.9003 496.4957 130.4914 496.9778 131.1804 497.4600 130.6187 497.9421 128.8935 498.4242 126.9500 498.9063 125.2789 499.3884 123.6835 499.8705 121.9619 500.3527 120.1005 500.8348 118.0971 501.3169 115.9686 501.7990 113.7409 502.2811 111.4273 502.7632 109.3321 503.2454 106.8683 503.7275 103.6086 504.2096 99.68292 504.6917 96.32385 505.1738 93.85739 505.6559 91.57889 506.1381 89.19998 506.6202 86.75079 507.1023 84.04408 507.5844 80.98630 508.0665 77.85451 508.5486 74.98537 509.0308 72.36263 509.5129 70.26999 509.9950 69.01764 510.4771 68.07219 510.9592 66.04128 511.4413 63.04811 511.9235 60.21349 512.4056 58.34435 512.8877 57.04539 513.3698 55.72850 513.8519 54.34940 514.3340 52.94420 514.8162 51.54590 515.2983 50.13542 515.7804 48.67273 516.2625 46.85828 516.7446 45.35667 517.2267 44.74068 517.7089 44.65941 518.1910 44.25874 518.6731 42.97653 519.1552 41.70348 519.6373 40.79497 520.1194 40.28305 520.6016 39.70360 521.0837 38.98898 521.5658 38.29300 522.0479 37.85646 522.5300 37.99086 523.0121 37.16084 523.4943 34.93535 523.9764 32.14180 524.4585 30.36862 524.9406 29.67940 525.4227 28.78650 525.9048 27.18123 526.3870 25.08995 526.8691 22.88910 527.3513 20.58829 527.8334 18.49747 528.3155 17.07603 528.7976 15.88544 529.2797 14.13866 529.7618 11.60278 530.2440 9.289612 530.7261 8.287079 531.2082 7.828217 531.6903 6.960022 532.1724 4.662155 532.6545 2.641754 533.1367 1.555862 533.6188 1.196747 534.1009 0.7525480 534.5830 4.2699999E-04 535.0651 0.7444460 535.5472 1.418640 536.0294 2.070496 536.5115 2.314568 536.9936 1.834991 537.4757 1.387512 537.9578 1.698624 538.4399 2.935455 538.9221 3.908424 539.4042 4.483490 539.8863 4.798180 540.3684 5.069633 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