#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-06-07 10:54:45 +0300 (Thu, 07 Jun 2018) $
#$Revision: 1012 $
#$URL: svn://172.16.1.111/rod/cif/1/00/04/1000468.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000468
loop_
_publ_author_name
'Burns, P. C.'
'Smith, J. V.'
'Steele, I. M.'
_publ_section_title
;
 Arizona porphyry copper/hydrothermal deposits I. The structure of
 chenevixite and luetheite Note: Luetheite-chenevixite series Locality:
 Humboldt mine, Patagonia, Arizona
;
_journal_name_full               'Mineralogical Magazine'
_journal_page_first              25
_journal_page_last               30
_journal_paper_doi               10.1180/002646100549102
_journal_volume                  64
_journal_year                    2000
_chemical_compound_source        R100177
_chemical_formula_sum            'Al0.635 As Cu Fe0.365 H2 O6'
_chemical_name_mineral           Luetheite
_space_group_IT_number           4
_symmetry_space_group_name_Hall  'P 2yb (1/2*x,y,-1/2*x+z)'
_symmetry_space_group_name_H-M   'B 1 21 1'
_cell_angle_alpha                90
_cell_angle_beta                 89.99
_cell_angle_gamma                90
_cell_length_a                   5.7012
_cell_length_b                   5.1801
_cell_length_c                   29.265
_cell_volume                     864.277
_exptl_crystal_density_diffrn    4.211
_cod_original_formula_sum        'Cu (Al.635 Fe.365) As O6 H2'
_cod_database_code               9009514
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R100177.rod
_rod_data_source.block           3500000
_rod_database.code               1000468
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9009514 COD http://www.crystallography.net/cod/9009514.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
132.4972 0.0000000E+00
132.9794 1.683871
133.4615 3.162396
133.9436 3.844308
134.4257 2.369594
134.9078 2.422174
135.3899 3.207573
135.8721 4.165749
136.3542 6.512115
136.8363 7.933349
137.3184 6.645218
137.8005 5.298156
138.2826 5.230469
138.7648 4.528767
139.2469 2.908060
139.7290 0.5743480
140.2111 0.9727270
140.6932 1.632191
141.1753 1.693178
141.6575 1.311958
142.1396 0.1706660
142.6217 0.5872840
143.1038 0.4319840
143.5859 0.7087210
144.0681 0.5963060
144.5502 1.535965
145.0323 4.250439
145.5144 5.917191
145.9965 5.877472
146.4786 5.762100
146.9608 5.916958
147.4429 6.429276
147.9250 6.970657
148.4071 7.973740
148.8892 8.847595
149.3713 8.657738
149.8535 6.371677
150.3356 4.049839
150.8177 2.177208
151.2998 0.6905520
151.7819 0.2016410
152.2640 0.2416650
152.7462 0.2894520
153.2283 0.8672560
153.7104 1.460495
154.1925 2.100784
154.6746 2.796394
155.1567 3.546021
155.6389 4.307922
156.1210 5.152718
156.6031 6.018120
157.0852 6.775139
157.5673 7.165054
158.0495 7.594620
158.5316 8.302834
159.0137 9.577515
159.4958 10.75928
159.9779 11.58205
160.4600 12.16382
160.9422 12.89102
161.4243 13.92029
161.9064 15.11417
162.3885 16.34509
162.8706 17.16080
163.3527 18.54080
163.8349 21.24851
164.3170 25.03261
164.7991 28.69216
165.2812 31.58094
165.7633 34.12239
166.2454 36.69189
166.7276 39.14392
167.2097 41.89551
167.6918 45.25415
168.1739 49.16089
168.6560 53.44882
169.1381 58.16504
169.6203 63.09772
170.1024 66.90540
170.5845 69.93962
171.0666 73.12610
171.5487 76.67719
172.0309 80.56623
172.5130 84.79102
172.9951 89.28345
173.4772 94.10545
173.9593 99.38967
174.4414 105.0649
174.9236 111.2520
175.4057 117.9379
175.8878 125.1775
176.3699 132.9471
176.8520 141.6501
177.3341 150.9458
177.8163 160.1413
178.2984 168.8835
178.7805 177.2881
179.2626 185.6718
179.7447 193.9301
180.2268 201.6703
180.7090 208.2304
181.1911 213.8132
181.6732 218.9361
182.1553 223.5775
182.6374 227.9481
183.1195 232.4406
183.6017 237.2002
184.0838 241.6981
184.5659 245.1123
185.0480 247.6665
185.5301 250.7226
186.0123 255.1770
186.4944 260.6522
186.9765 265.8680
187.4586 270.8604
187.9407 275.5053
188.4228 279.4205
188.9050 282.6636
189.3871 286.1272
189.8692 290.1326
190.3513 294.4662
190.8334 299.2482
191.3155 304.3427
191.7977 310.1275
192.2798 317.3592
192.7619 326.0251
193.2440 335.2350
193.7261 344.7500
194.2082 354.5054
194.6904 364.3188
195.1725 374.0496
195.6546 384.1341
196.1367 395.5761
196.6188 408.6250
197.1009 420.5070
197.5831 430.0096
198.0652 437.2258
198.5473 441.7420
199.0294 443.6184
199.5115 442.8122
199.9937 438.7501
200.4758 431.1568
200.9579 422.0240
201.4400 412.2246
201.9221 401.7321
202.4042 390.9834
202.8864 379.7077
203.3685 368.4527
203.8506 358.5013
204.3327 350.0429
204.8148 342.4257
205.2969 335.4687
205.7791 329.2560
206.2612 323.1794
206.7433 317.4632
207.2254 311.6726
207.7075 304.3144
208.1896 294.6463
208.6718 285.5216
209.1539 278.7306
209.6360 274.9352
210.1181 270.2566
210.6002 264.0162
211.0823 257.0392
211.5645 251.6342
212.0466 247.9789
212.5287 245.4547
213.0108 243.8811
213.4929 243.4759
213.9750 243.0777
214.4572 242.4357
214.9393 242.0969
215.4214 243.3149
215.9035 246.0611
216.3856 250.0011
216.8678 255.0227
217.3499 261.3417
217.8320 268.5447
218.3141 276.7543
218.7962 285.5217
219.2783 293.5987
219.7605 300.5409
220.2426 307.6578
220.7247 315.7016
221.2068 325.3231
221.6889 333.6901
222.1710 341.0801
222.6532 347.0773
223.1353 350.2010
223.6174 350.6928
224.0995 348.1932
224.5816 342.2173
225.0637 331.4887
225.5459 320.4886
226.0280 309.9103
226.5101 299.0053
226.9922 285.5749
227.4743 268.0042
227.9564 250.2843
228.4386 234.2670
228.9207 221.4279
229.4028 207.2198
229.8849 190.3851
230.3670 172.3915
230.8492 156.8762
231.3313 144.4975
231.8134 133.8051
232.2955 124.0345
232.7776 115.2420
233.2597 107.6465
233.7419 101.5865
234.2240 96.61145
234.7061 91.63412
235.1882 86.22440
235.6703 81.48421
236.1524 77.88237
236.6346 75.75984
237.1167 74.03647
237.5988 72.63004
238.0809 71.63876
238.5630 71.35907
239.0451 72.18704
239.5273 73.12126
240.0094 73.62897
240.4915 73.12195
240.9736 73.73694
241.4557 75.70428
241.9378 78.68138
242.4200 81.93689
242.9021 85.34305
243.3842 89.28610
243.8663 93.97583
244.3484 99.63458
244.8306 105.4523
245.3127 111.6911
245.7948 117.8970
246.2769 123.0984
246.7590 126.6073
247.2411 130.1907
247.7233 134.6200
248.2054 140.4089
248.6875 145.1497
249.1696 148.5947
249.6517 151.1228
250.1338 153.4131
250.6160 156.0229
251.0981 157.4105
251.5802 157.0686
252.0623 154.8951
252.5444 151.4846
253.0265 146.4557
253.5087 140.5277
253.9908 134.7827
254.4729 129.2479
254.9550 123.7584
255.4371 118.1195
255.9192 112.2613
256.4014 107.2079
256.8835 103.0671
257.3656 99.62430
257.8477 96.55235
258.3298 93.92209
258.8120 91.46136
259.2941 88.89349
259.7762 86.13365
260.2583 84.72975
260.7404 85.18932
261.2225 86.35260
261.7047 87.12447
262.1868 87.64331
262.6689 87.39319
263.1510 86.27061
263.6331 84.28506
264.1152 81.46988
264.5974 77.84317
265.0795 73.37282
265.5616 68.05136
266.0437 61.62067
266.5258 54.92720
267.0079 48.00264
267.4901 40.86946
267.9722 34.27835
268.4543 28.27422
268.9364 22.60162
269.4185 16.85605
269.9006 10.76367
270.3828 5.903717
270.8649 2.863098
271.3470 1.180054
271.8291 1.614487
272.3112 6.100601
272.7933 10.27605
273.2755 12.40260
273.7576 12.14238
274.2397 12.37608
274.7218 13.74994
275.2039 15.65701
275.6860 16.05754
276.1682 14.61882
276.6503 12.93037
277.1324 12.22324
277.6145 12.64943
278.0966 12.00543
278.5787 9.884674
279.0609 6.883667
279.5430 4.176010
280.0251 1.776016
280.5072 0.3807530
280.9893 1.999084
281.4715 3.073776
281.9536 5.356750
282.4357 9.144928
282.9178 13.72740
283.3999 17.93469
283.8820 21.74341
284.3642 25.53522
284.8463 29.21349
285.3284 32.87915
285.8105 37.55118
286.2926 43.33704
286.7747 49.84656
287.2569 56.80966
287.7390 64.19591
288.2211 71.31116
288.7032 77.67015
289.1853 83.48793
289.6674 89.92023
290.1496 97.07065
290.6317 104.3662
291.1138 111.4534
291.5959 118.2833
292.0780 124.2834
292.5602 129.5300
293.0423 133.7961
293.5244 136.3697
294.0065 137.2114
294.4886 136.9643
294.9707 136.2432
295.4529 134.9267
295.9350 132.5233
296.4171 128.5175
296.8992 123.6972
297.3813 119.3936
297.8634 115.6000
298.3456 112.0385
298.8277 108.4185
299.3098 104.9108
299.7919 101.8911
300.2740 99.41754
300.7561 97.54137
301.2383 96.38531
301.7204 95.92435
302.2025 96.13020
302.6846 97.03674
303.1667 98.57710
303.6488 100.6200
304.1310 103.0471
304.6131 106.2255
305.0952 110.8283
305.5773 116.4998
306.0594 122.2551
306.5415 127.6929
307.0237 132.9259
307.5058 138.4763
307.9879 144.5400
308.4700 149.6064
308.9521 152.2995
309.4343 153.2413
309.9164 153.6192
310.3985 154.5743
310.8806 154.7304
311.3627 153.1110
311.8448 149.6572
312.3270 144.6876
312.8091 137.8849
313.2912 129.8349
313.7733 121.2291
314.2554 111.4951
314.7375 101.9747
315.2197 93.43799
315.7018 85.75183
316.1839 78.39627
316.6660 70.84024
317.1481 63.62549
317.6302 57.25465
318.1124 51.51762
318.5945 46.97614
319.0766 44.13901
319.5587 42.71231
320.0408 41.61746
320.5229 40.20769
321.0051 39.25157
321.4872 39.22079
321.9693 40.52780
322.4514 42.12421
322.9335 43.79523
323.4156 45.67778
323.8978 47.98062
324.3799 50.85567
324.8620 53.98470
325.3441 57.30502
325.8262 60.88626
326.3083 64.37497
326.7905 67.93993
327.2726 71.29831
327.7547 74.07776
328.2368 75.62320
328.7189 77.27644
329.2010 79.44797
329.6832 82.12573
330.1653 84.07312
330.6474 85.71857
331.1295 86.39761
331.6116 85.57301
332.0938 82.25357
332.5759 78.91199
333.0580 75.77925
333.5401 72.96024
334.0222 70.73061
334.5043 69.77068
334.9865 68.38885
335.4686 65.34134
335.9507 59.79094
336.4328 55.10056
336.9149 51.52919
337.3970 48.90956
337.8792 46.84457
338.3613 45.17245
338.8434 44.05569
339.3255 43.55896
339.8076 43.71082
340.2898 44.41927
340.7719 45.77052
341.2540 47.42252
341.7361 48.68024
342.2182 49.44481
342.7003 51.54829
343.1825 55.95013
343.6646 62.34558
344.1467 68.15498
344.6288 73.18712
345.1109 78.84192
345.5930 87.24428
346.0752 97.99976
346.5573 108.1134
347.0394 116.6895
347.5215 124.4005
348.0036 133.3075
348.4857 143.3280
348.9679 152.7412
349.4500 161.2437
349.9321 168.2663
350.4142 172.0124
350.8963 171.9217
351.3784 169.3550
351.8606 165.0959
352.3427 159.5944
352.8248 154.4077
353.3069 150.1400
353.7890 146.8815
354.2711 144.5529
354.7533 143.1000
355.2354 143.0543
355.7175 145.4720
356.1996 149.5622
356.6817 153.9453
357.1638 157.7222
357.6460 161.7996
358.1281 167.0609
358.6102 173.4182
359.0923 180.0327
359.5744 186.9204
360.0565 193.5531
360.5387 199.4317
361.0208 204.5140
361.5029 208.7173
361.9850 212.1820
362.4671 214.7630
362.9492 215.9386
363.4314 215.3921
363.9135 213.4950
364.3956 210.3919
364.8777 205.9259
365.3598 200.6420
365.8419 194.8715
366.3241 188.3203
366.8062 180.5713
367.2883 170.5885
367.7704 160.3445
368.2526 150.4175
368.7347 140.9113
369.2168 130.9953
369.6989 119.9045
370.1810 108.8186
370.6631 98.58484
371.1453 89.47513
371.6274 80.78479
372.1095 72.25357
372.5916 63.94870
373.0737 56.63492
373.5558 50.53278
374.0380 44.99667
374.5201 39.60968
375.0022 34.38065
375.4843 29.40881
375.9664 24.57547
376.4485 20.11186
376.9307 16.44695
377.4128 13.74164
377.8949 11.28021
378.3770 8.752960
378.8591 6.192566
379.3412 4.136414
379.8234 2.681625
380.3055 1.451309
380.7876 3.2837000E-02
381.2697 1.751938
381.7518 3.106491
382.2339 3.855835
382.7161 4.203934
383.1982 4.686478
383.6803 5.287216
384.1624 5.680710
384.6445 5.534668
385.1266 4.993378
385.6088 4.387909
386.0909 3.745956
386.5730 3.119614
387.0551 2.625854
387.5372 2.212585
388.0193 1.723495
388.5015 0.8823240
388.9836 3.1128000E-02
389.4657 0.5215760
389.9478 0.7615970
390.4299 0.6116490
390.9120 0.2485200
391.3942 1.448471
391.8763 2.517990
392.3584 3.235367
392.8405 3.843872
393.3226 4.406403
393.8047 4.943817
394.2869 5.553024
394.7690 6.690292
395.2511 7.627136
395.7332 7.877014
396.2154 7.109375
396.6975 6.189178
397.1796 5.442062
397.6617 4.622910
398.1438 3.324310
398.6259 1.146393
399.1081 1.186554
399.5902 3.483459
400.0723 5.722870
400.5544 8.040100
401.0365 10.10458
401.5186 12.49916
402.0008 15.67218
402.4829 19.79393
402.9650 24.41930
403.4471 29.67178
403.9292 35.40872
404.4113 40.87941
404.8935 45.99559
405.3756 51.11844
405.8577 56.63452
406.3398 62.66695
406.8219 67.77582
407.3040 71.82431
407.7862 75.20668
408.2683 78.64711
408.7504 82.17120
409.2325 85.03569
409.7146 86.73947
410.1967 87.64471
410.6789 89.18613
411.1610 91.39810
411.6431 93.46259
412.1252 94.40370
412.6073 94.60852
413.0894 95.03654
413.5716 95.63867
414.0537 97.02573
414.5358 100.0860
415.0179 104.5823
415.5000 109.8536
415.9821 115.0106
416.4643 120.9748
416.9464 128.9481
417.4285 139.0629
417.9106 149.9031
418.3927 160.1786
418.8748 170.8019
419.3570 182.6693
419.8391 196.9946
420.3212 211.8554
420.8033 226.2924
421.2854 240.5566
421.7675 256.0878
422.2497 274.0356
422.7318 292.8578
423.2139 311.5321
423.6960 329.3940
424.1781 348.2626
424.6602 368.0287
425.1424 388.9575
425.6245 411.2429
426.1066 434.8904
426.5887 459.5105
427.0709 485.1237
427.5530 511.7279
428.0351 537.9242
428.5172 563.8809
428.9993 589.5908
429.4814 615.4000
429.9636 641.8298
430.4457 666.4099
430.9278 689.1391
431.4099 709.7042
431.8920 727.4164
432.3741 742.4165
432.8563 754.6254
433.3384 764.3608
433.8205 771.4406
434.3026 774.5270
434.7847 773.6575
435.2668 768.8232
435.7490 760.0868
436.2311 747.3572
436.7132 730.3652
437.1953 708.0936
437.6774 682.8079
438.1595 656.5908
438.6417 629.4883
439.1238 601.8267
439.6059 573.2532
440.0880 544.5848
440.5701 516.5165
441.0522 488.9363
441.5344 462.4395
442.0165 437.4233
442.4986 413.7046
442.9807 391.1797
443.4628 369.0536
443.9449 348.8543
444.4271 331.4979
444.9092 316.7181
445.3913 302.9186
445.8734 290.0684
446.3555 278.1736
446.8376 267.3178
447.3198 257.6982
447.8019 248.6487
448.2840 240.2507
448.7661 232.3720
449.2482 224.9440
449.7303 218.3735
450.2125 211.7158
450.6946 204.6787
451.1767 197.2747
451.6588 190.1861
452.1409 183.5515
452.6230 176.7448
453.1052 169.2468
453.5873 160.9392
454.0694 153.4388
454.5515 147.1147
455.0337 141.1664
455.5158 134.1805
455.9979 126.2274
456.4800 118.9268
456.9621 113.1350
457.4442 108.2070
457.9264 102.7814
458.4085 96.89987
458.8906 90.93018
459.3727 84.94553
459.8548 79.17688
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