#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-06-07 11:16:01 +0300 (Thu, 07 Jun 2018) $ #$Revision: 1042 $ #$URL: svn://172.16.1.111/rod/cif/1/00/04/1000495.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_1000495 loop_ _publ_author_name 'Zaitsev, A. N.' 'Chakhmouradian, A. R.' 'Siidra, O. I.' 'Spratt, J.' 'Williams, C. T.' 'Stanley, C. J.' 'Petrov, S. V.' 'Britvin, S. N.' 'Polyakova, E. A.' _publ_section_title ; Fluorine-, yttrium- and lanthanide-rich cerianite-(Ce) from carbonatitic rocks of the Kerimasi volcano and surrounding explosion craters, Gregory Rift, northern Tanzania ; _journal_name_full 'Mineralogical Magazine' _journal_page_first 2813 _journal_page_last 2822 _journal_paper_doi 10.1180/minmag.2011.075.6.2813 _journal_volume 75 _journal_year 2011 _chemical_compound_source 'Gregory Rift, northern Tanzania' _chemical_formula_sum 'Ce0.62 Dy0.02 Er0.01 F0.24 Gd0.02 La0.03 Nd0.06 O1.68 Pr0.01 Sm0.01 Y0.2 Yb0.02' _chemical_name_mineral Cerianite-(Ce) _space_group_IT_number 225 _symmetry_space_group_name_Hall '-F 4 2 3' _symmetry_space_group_name_H-M 'F m -3 m' _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_length_a 5.4203 _cell_length_b 5.4203 _cell_length_c 5.4203 _cell_volume 159.247 _exptl_crystal_density_diffrn 6.813 _cod_original_formula_sum '(Ce.62 Y.2 Nd.06 La.03 Pr.01 Sm.01 Gd.02 Dy.02 Er.01 Yb.02) O1.68 F.24' _cod_database_code 9016030 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type other _raman_measurement_device.excitation_laser_wavelength 532 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 15 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R050379.rod _rod_data_source.block 3500000 _rod_database.code 1000495 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9016030 COD http://www.crystallography.net/cod/9016030.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 145.3864 0.0000000E+00 145.8685 0.3320310 146.3506 0.6318890 146.8327 0.9400020 147.3148 0.7756120 147.7969 0.2148590 148.2791 6.3942000E-02 148.7612 5.1865000E-02 149.2433 0.4305950 149.7254 0.7822270 150.2075 1.163940 150.6896 1.475540 151.1718 1.665573 151.6539 1.536110 152.1360 1.573723 152.6181 1.876961 153.1002 2.365211 153.5823 2.797737 154.0645 3.236946 154.5466 3.587013 155.0287 3.790031 155.5108 3.830734 155.9929 3.712318 156.4750 3.325333 156.9572 2.746422 157.4393 2.279106 157.9214 1.932411 158.4035 1.736115 158.8856 1.706886 159.3677 2.027649 159.8499 2.337143 160.3320 2.507874 160.8141 2.565140 161.2962 2.659767 161.7783 2.908600 162.2604 3.202652 162.7426 3.521912 163.2247 3.854095 163.7068 4.191307 164.1889 4.098289 164.6710 3.664314 165.1531 3.247353 165.6353 2.856209 166.1174 2.537003 166.5995 2.367355 167.0816 2.502708 167.5637 2.688263 168.0458 2.754715 168.5280 2.839500 169.0101 2.866676 169.4922 3.292572 169.9743 3.893784 170.4564 4.329636 170.9385 4.520378 171.4207 4.452301 171.9028 3.980049 172.3849 3.079185 172.8670 2.248505 173.3491 1.913361 173.8312 1.915833 174.3134 1.954773 174.7955 1.917702 175.2776 1.832451 175.7597 1.724831 176.2418 1.594864 176.7239 1.457832 177.2061 1.368744 177.6882 1.290619 178.1703 1.123177 178.6524 0.7041470 179.1345 0.1919630 179.6166 0.1229930 180.0988 0.2045900 180.5809 0.2088320 181.0630 0.3665920 181.5451 0.6210400 182.0272 0.7414630 182.5093 0.4710460 182.9915 1.5838999E-02 183.4736 0.2709660 183.9557 0.2362060 184.4378 7.9948001E-02 184.9199 8.3899999E-04 185.4020 6.4389999E-03 185.8842 2.4780000E-02 186.3663 0.1010670 186.8484 0.2058260 187.3305 0.2495040 187.8126 0.1978150 188.2947 0.1608280 188.7769 0.4443210 189.2590 1.024147 189.7411 1.377899 190.2232 0.9798510 190.7053 9.3310000E-03 191.1874 0.5275880 191.6696 0.4189530 192.1517 4.6516001E-02 192.6338 0.4112470 193.1159 0.6736760 193.5980 0.8915630 194.0801 1.084488 194.5623 1.253265 195.0444 1.428047 195.5265 1.601608 196.0086 1.791069 196.4907 2.074142 196.9728 2.470573 197.4550 2.788567 197.9371 2.820290 198.4192 2.557549 198.9013 2.563622 199.3834 2.964699 199.8655 3.578857 200.3477 3.979378 200.8298 4.143440 201.3119 4.188423 201.7940 4.119301 202.2761 3.909355 202.7582 3.919121 203.2404 4.265915 203.7225 4.794006 204.2046 5.067223 204.6867 5.026077 205.1688 4.937569 205.6509 4.977325 206.1331 5.167343 206.6152 5.322189 207.0973 5.437889 207.5794 5.494354 208.0615 5.416786 208.5436 5.169456 209.0258 4.881294 209.5079 4.578377 209.9900 4.200218 210.4721 4.135406 210.9542 4.579544 211.4363 5.303680 211.9185 5.424911 212.4006 4.629875 212.8827 3.882660 213.3648 3.851936 213.8469 4.756218 214.3290 5.586418 214.8112 6.337097 215.2933 6.940056 215.7754 7.112343 216.2575 6.631310 216.7396 6.137138 217.2217 6.016586 217.7039 6.361115 218.1860 6.815834 218.6681 7.444519 219.1502 8.151192 219.6323 8.547691 220.1144 8.507332 220.5966 8.369278 221.0787 8.292030 221.5608 8.217110 222.0429 8.378792 222.5250 8.886940 223.0071 9.634720 223.4893 10.19774 223.9714 10.50536 224.4535 10.75240 224.9356 11.02906 225.4177 11.28704 225.8998 11.70824 226.3820 12.40356 226.8641 13.25849 227.3462 13.81522 227.8283 13.86436 228.3104 13.93217 228.7925 14.31976 229.2747 15.26823 229.7568 15.98766 230.2389 16.35293 230.7210 16.49168 231.2031 16.81607 231.6852 17.46228 232.1674 18.08979 232.6495 18.51329 233.1316 18.61008 233.6137 18.77063 234.0958 18.97997 234.5779 19.26076 235.0601 19.69591 235.5422 20.42120 236.0243 21.11320 236.5064 21.62276 236.9885 21.86388 237.4706 22.10160 237.9528 22.39649 238.4349 22.67999 238.9170 22.72647 239.3991 22.34800 239.8812 22.00580 240.3633 21.93693 240.8455 22.30579 241.3276 22.55701 241.8097 22.66338 242.2918 22.65101 242.7739 22.58367 243.2560 22.50117 243.7382 22.30807 244.2203 21.97420 244.7024 21.50771 245.1845 20.85223 245.6666 19.83716 246.1487 18.71516 246.6309 17.99914 247.1130 17.98064 247.5951 17.88080 248.0772 17.38730 248.5593 16.33351 249.0414 15.42010 249.5236 14.69600 250.0057 14.16467 250.4878 13.81033 250.9699 13.82185 251.4520 13.65085 251.9341 13.02747 252.4163 11.76799 252.8984 10.98443 253.3805 10.90927 253.8626 11.13000 254.3447 11.02730 254.8268 10.44281 255.3090 9.861496 255.7911 9.454567 256.2732 9.259819 256.7553 8.886833 257.2374 8.221619 257.7195 7.489166 258.2017 6.966072 258.6838 6.700043 259.1659 6.530060 259.6480 6.442734 260.1301 6.442848 260.6122 6.422615 261.0944 6.456581 261.5765 6.374748 262.0586 5.926758 262.5407 4.929451 263.0228 4.159752 263.5049 3.843224 263.9871 3.956818 264.4692 4.017288 264.9513 3.941200 265.4334 3.845436 265.9155 3.894844 266.3976 4.183891 266.8798 4.363220 267.3619 4.276436 267.8440 3.962555 268.3261 3.692131 268.8082 3.425293 269.2903 3.374237 269.7725 3.833733 270.2546 4.966003 270.7367 5.753876 271.2188 5.878838 271.7009 5.550201 272.1830 5.649132 272.6652 6.330246 273.1473 7.141052 273.6294 7.758698 274.1115 8.151611 274.5936 8.443855 275.0757 8.613060 275.5579 8.746384 276.0400 9.128212 276.5221 9.793808 277.0042 10.52037 277.4863 11.20983 277.9684 11.85800 278.4506 12.41949 278.9327 12.80058 279.4148 13.15893 279.8969 13.89902 280.3790 15.10465 280.8611 16.22515 281.3433 16.88979 281.8254 17.08892 282.3075 17.40526 282.7896 17.87099 283.2717 18.40757 283.7538 18.79504 284.2360 19.03166 284.7181 19.48090 285.2002 20.42872 285.6823 21.79760 286.1644 22.85603 286.6465 23.51868 287.1287 24.13180 287.6108 25.20699 288.0929 26.71539 288.5750 28.14293 289.0571 29.29475 289.5392 30.22266 290.0214 31.03493 290.5035 31.70647 290.9856 32.43261 291.4677 33.43420 291.9498 34.68709 292.4319 36.01056 292.9141 37.43919 293.3962 38.86914 293.8783 40.03848 294.3604 40.93991 294.8425 41.73067 295.3246 42.66008 295.8068 43.62220 296.2889 44.20372 296.7710 44.18541 297.2531 43.90078 297.7352 44.02121 298.2173 44.47857 298.6995 44.69136 299.1816 44.16451 299.6637 43.08941 300.1458 41.83739 300.6279 40.40515 301.1100 38.94510 301.5922 37.78056 302.0743 36.80721 302.5564 35.61487 303.0385 33.62650 303.5206 31.36945 304.0027 29.63221 304.4849 28.61998 304.9670 27.75416 305.4491 26.56226 305.9312 25.10736 306.4133 23.54025 306.8954 21.76025 307.3776 20.00063 307.8597 18.56460 308.3418 17.48264 308.8239 16.47742 309.3060 15.26469 309.7881 13.99814 310.2703 12.95207 310.7524 12.50539 311.2345 12.11101 311.7166 11.19713 312.1987 9.789589 312.6808 8.750763 313.1630 9.110771 313.6451 9.883118 314.1272 10.00622 314.6093 8.482178 315.0914 6.837799 315.5735 5.780983 316.0557 5.244476 316.5378 4.875946 317.0199 4.568108 317.5020 4.345436 317.9841 4.260254 318.4662 4.611053 318.9484 4.666191 319.4305 4.002174 319.9126 2.842270 320.3947 1.771919 320.8768 0.7770390 321.3589 5.3307001E-02 321.8411 0.2156070 322.3232 0.2839970 322.8053 0.5209350 323.2874 1.7850000E-03 323.7695 0.8519360 324.2516 1.345032 324.7338 0.9136050 325.2159 0.5373230 325.6980 0.5593720 326.1801 1.099091 326.6622 1.577591 327.1443 2.038315 327.6265 2.376602 328.1086 2.483673 328.5907 1.876740 329.0728 1.599243 329.5549 2.005295 330.0370 3.105286 330.5192 3.729218 331.0013 3.552628 331.4834 3.180084 331.9655 3.031525 332.4476 3.310104 332.9297 3.456253 333.4119 3.349533 333.8940 3.067764 334.3761 2.983658 334.8582 3.265305 335.3403 3.492172 335.8224 3.387344 336.3046 2.715393 336.7867 2.455521 337.2688 2.796951 337.7509 3.428070 338.2330 3.741837 338.7151 3.723648 339.1973 3.422592 339.6794 2.696106 340.1615 1.508713 340.6436 0.8715210 341.1257 0.9034580 341.6078 1.236206 342.0900 1.451401 342.5721 1.547043 343.0542 1.540146 343.5363 1.408035 344.0184 1.179733 344.5005 0.9861300 344.9827 0.8393250 345.4648 0.6602330 345.9469 0.3219150 346.4290 0.1477510 346.9111 0.4479370 347.3932 0.4639890 347.8754 0.3621220 348.3575 0.3958440 348.8396 0.5652310 349.3217 0.9262540 349.8038 1.614655 350.2859 2.511078 350.7681 3.382111 351.2502 4.242905 351.7323 4.903854 352.2144 4.862808 352.6965 4.386963 353.1786 4.277634 353.6608 5.352371 354.1429 6.826355 354.6250 7.666824 355.1071 7.816788 355.5892 7.871185 356.0714 8.270004 356.5535 8.876480 357.0356 9.488617 357.5177 10.09995 357.9998 10.64139 358.4819 10.87677 358.9641 10.90106 359.4462 11.23904 359.9283 12.40840 360.4104 13.87746 360.8925 15.22914 361.3746 16.45294 361.8568 17.39938 362.3389 17.65561 362.8210 17.57584 363.3031 17.97676 363.7852 19.57410 364.2673 21.33830 364.7495 22.73674 365.2316 23.55429 365.7137 24.59972 366.1958 26.34644 366.6779 28.27881 367.1600 29.80835 367.6422 30.25032 368.1243 30.92488 368.6064 32.28285 369.0885 34.38403 369.5706 36.01216 370.0527 36.63216 370.5349 37.20612 371.0170 38.38966 371.4991 40.51930 371.9812 42.67857 372.4633 44.91710 372.9454 47.15137 373.4276 49.00111 373.9097 50.29425 374.3918 51.54543 374.8739 52.90120 375.3560 54.31973 375.8381 56.15451 376.3203 58.53586 376.8024 61.13303 377.2845 63.42218 377.7666 65.31058 378.2487 67.15421 378.7308 68.97334 379.2130 70.81404 379.6951 72.83087 380.1772 75.11418 380.6593 77.46327 381.1414 79.69411 381.6235 81.77855 382.1057 83.93065 382.5878 86.31454 383.0699 88.71291 383.5520 90.55368 384.0341 91.88518 384.5162 93.30176 384.9984 95.40315 385.4805 97.85855 385.9626 99.96133 386.4447 101.6557 386.9268 103.1632 387.4089 104.4997 387.8911 105.7572 388.3732 107.2236 388.8553 109.3913 389.3374 111.6817 389.8195 113.4463 390.3016 114.6525 390.7838 115.7748 391.2659 117.2089 391.7480 118.6726 392.2301 119.8461 392.7122 120.5358 393.1943 121.0301 393.6765 121.3306 394.1586 121.5735 394.6407 122.0047 395.1228 123.1723 395.6049 124.1254 396.0870 124.3280 396.5692 123.4548 397.0513 122.7795 397.5334 122.8711 398.0155 123.2359 398.4976 123.1912 398.9797 122.3459 399.4619 121.3584 399.9440 120.3907 400.4261 119.4445 400.9082 118.2330 401.3903 116.8079 401.8724 115.0705 402.3546 112.8737 402.8367 109.8466 403.3188 107.2283 403.8009 105.2498 404.2830 103.6504 404.7651 101.7353 405.2473 99.40877 405.7294 97.09332 406.2115 94.95197 406.6936 93.00623 407.1757 91.10715 407.6578 89.21872 408.1400 87.46790 408.6221 86.03668 409.1042 84.91852 409.5863 83.82291 410.0684 82.80838 410.5505 81.66331 411.0327 79.53891 411.5148 76.46553 411.9969 73.66200 412.4790 72.08748 412.9611 71.39587 413.4432 70.88431 413.9254 70.53716 414.4075 70.03436 414.8896 68.76196 415.3717 67.05170 415.8538 65.69261 416.3359 65.34525 416.8181 65.34430 417.3002 65.09210 417.7823 64.57878 418.2644 64.11508 418.7465 63.83490 419.2286 63.69888 419.7108 63.66951 420.1929 63.70737 420.6750 63.88217 421.1571 64.35512 421.6392 64.99503 422.1213 65.45216 422.6035 65.38782 423.0856 65.33224 423.5677 65.49489 424.0498 65.91597 424.5319 66.47699 425.0140 67.24236 425.4962 68.12065 425.9783 69.01974 426.4604 69.89589 426.9425 70.85646 427.4246 71.82625 427.9067 72.86885 428.3889 74.40176 428.8710 76.62090 429.3531 78.97725 429.8352 81.16370 430.3173 83.06865 430.7994 85.24890 431.2816 87.79053 431.7637 90.48126 432.2458 92.87575 432.7279 94.94482 433.2100 97.14632 433.6921 99.57234 434.1743 102.2715 434.6564 105.4756 435.1385 109.2376 435.6206 113.0453 436.1027 116.2293 436.5848 119.1177 437.0670 122.6269 437.5491 127.0117 438.0312 131.8902 438.5133 137.0955 438.9954 142.5231 439.4775 147.8775 439.9597 152.8398 440.4418 157.7750 440.9239 163.0333 441.4060 168.6383 441.8881 174.3697 442.3702 179.9699 442.8524 185.6310 443.3345 191.5834 443.8166 198.0130 444.2987 204.5862 444.7808 211.2338 445.2629 217.9472 445.7451 224.7613 446.2272 231.6575 446.7093 238.5081 447.1914 245.2487 447.6735 251.8899 448.1556 258.5636 448.6378 264.9842 449.1199 271.5005 449.6020 278.5615 450.0841 286.5080 450.5662 294.0975 451.0483 301.0975 451.5305 307.6176 452.0126 314.0454 452.4947 320.5024 452.9768 326.6394 453.4589 332.2662 453.9410 337.4106 454.4232 342.5252 454.9053 347.8493 455.3874 352.6049 455.8695 355.7500 456.3516 357.3803 456.8337 358.3177 457.3159 358.8910 457.7980 358.9315 458.2801 358.1102 458.7622 356.4528 459.2443 354.0547 459.7264 351.1966 460.2086 347.5728 460.6907 342.6294 461.1728 336.0997 461.6549 329.2021 462.1370 323.5373 462.6191 318.0698 463.1013 311.3928 463.5834 301.8632 464.0655 291.9325 464.5476 282.5333 465.0297 273.7546 465.5118 265.5206 465.9940 258.3363 466.4761 251.4086 466.9582 244.4036 467.4403 237.3794 467.9224 230.0269 468.4045 222.0277 468.8867 213.8588 469.3688 206.0809 469.8509 198.9999 470.3330 191.9932 470.8151 184.7074 471.2972 177.2757 471.7794 171.3238 472.2615 167.2731 472.7436 163.3950 473.2257 158.2771 473.7078 151.8672 474.1899 146.1525 474.6721 141.3363 475.1542 136.9880 475.6363 132.5471 476.1184 128.0265 476.6005 123.5064 477.0826 118.9226 477.5648 114.4230 478.0469 110.1754 478.5290 106.1695 479.0111 102.3108 479.4932 98.55394 479.9753 94.89841 480.4575 91.36490 480.9396 87.99002 481.4217 84.59590 481.9038 80.93272 482.3859 77.27116 482.8680 74.06248 483.3502 72.05557 483.8323 69.93993 484.3144 67.15021 484.7965 63.74323 485.2786 60.37073 485.7607 56.79951 486.2429 53.59175 486.7250 51.07782 487.2071 49.81784 487.6892 48.10153 488.1713 45.70256 488.6534 43.01210 489.1356 40.52893 489.6177 38.24095 490.0998 36.19011 490.5819 34.45595 491.0640 32.92696 491.5461 31.01793 492.0283 28.66393 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