#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-06-07 11:16:56 +0300 (Thu, 07 Jun 2018) $
#$Revision: 1057 $
#$URL: svn://172.16.1.111/rod/cif/1/00/05/1000505.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000505
loop_
_publ_author_name
'Robinson, K.'
'Gibbs, G. V.'
'Ribbe, P. H.'
_publ_section_title
;
 The crystal structures of the humite minerals. IV. Clinohumite and
 titanclinohumite
;
_journal_name_full               'American Mineralogist'
_journal_page_first              43
_journal_page_last               49
_journal_volume                  58
_journal_year                    1973
_chemical_compound_source        R060559
_chemical_formula_sum            'Fe0.58 H2 Mg8.42 O18 Si4'
_chemical_name_mineral           Hydroxylclinohumite
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2xab'
_symmetry_space_group_name_H-M   'P 21/b 1 1'
_cell_angle_alpha                100.786
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   4.7441
_cell_length_b                   10.2501
_cell_length_c                   13.6635
_cell_volume                     652.684
_exptl_crystal_density_diffrn    3.253
_cod_original_cell_volume        652.683
_cod_original_formula_sum        'Mg8.42 Fe.58 Si4 O18 H2'
_cod_database_code               9000292
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R060559.rod
_rod_data_source.block           3500000
_rod_database.code               1000505
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9000292 COD http://www.crystallography.net/cod/9000292.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
89.78320 0.0000000E+00
90.26532 0.3890690
90.74744 2.863434
91.22955 6.234711
91.71167 11.68634
92.19379 23.57230
92.67590 40.54584
93.15802 53.20987
93.64014 51.91983
94.12225 40.91095
94.60437 32.99713
95.08649 31.60950
95.56860 33.19839
96.05072 33.43231
96.53284 33.40866
97.01495 34.06976
97.49707 33.81290
97.97919 30.87497
98.46130 25.57220
98.94342 19.15646
99.42554 13.11115
99.90765 11.00375
100.3898 14.36636
100.8719 19.66489
101.3540 20.70093
101.8361 16.67377
102.3182 11.91931
102.8004 7.545746
103.2825 3.375610
103.7646 0.4255980
104.2467 1.130249
104.7288 1.590820
105.2109 1.402496
105.6931 1.328308
106.1752 0.2786250
106.6573 4.227966
107.1394 11.56561
107.6215 19.40787
108.1036 30.24481
108.5858 42.73608
109.0679 48.17426
109.5500 41.16287
110.0321 30.94971
110.5142 22.61261
110.9963 16.16562
111.4785 11.62042
111.9606 9.807678
112.4427 10.61487
112.9248 11.61624
113.4069 12.11490
113.8890 12.95752
114.3712 14.06165
114.8533 14.73407
115.3354 16.41171
115.8175 20.44034
116.2996 27.27402
116.7817 32.58002
117.2639 33.46579
117.7460 32.58832
118.2281 33.64975
118.7102 39.87851
119.1923 44.97833
119.6744 46.33875
120.1566 42.48062
120.6387 38.61829
121.1208 38.26071
121.6029 39.55042
122.0850 40.67319
122.5671 38.52164
123.0493 36.01062
123.5314 37.03201
124.0135 43.82486
124.4956 50.12521
124.9777 49.01233
125.4598 41.87527
125.9420 33.93839
126.4241 27.93002
126.9062 23.50208
127.3883 20.05811
127.8704 17.53314
128.3525 15.85422
128.8347 15.10062
129.3168 15.24597
129.7989 15.76877
130.2810 16.37708
130.7631 17.04617
131.2452 17.83405
131.7274 19.17120
132.2095 20.44427
132.6916 19.67355
133.1737 16.64499
133.6558 13.04135
134.1379 10.38077
134.6201 8.656158
135.1022 7.265381
135.5843 6.121857
136.0664 5.194092
136.5485 4.101410
137.0306 2.644318
137.5128 1.507843
137.9949 1.397156
138.4770 2.286072
138.9591 4.441620
139.4412 8.617432
139.9233 15.05478
140.4055 19.60446
140.8876 22.30341
141.3697 23.04626
141.8518 21.35663
142.3339 16.31543
142.8160 10.93576
143.2982 6.205566
143.7803 2.107208
144.2624 1.144104
144.7445 3.392914
145.2266 4.830750
145.7087 5.900085
146.1909 6.886444
146.6730 7.155182
147.1551 6.285522
147.6372 2.056702
148.1193 0.6050720
148.6014 1.020538
149.0836 0.2247010
149.5657 1.084534
150.0478 1.344757
150.5299 1.388306
151.0120 1.375549
151.4941 1.833344
151.9763 1.639618
152.4584 0.1851810
152.9405 2.169800
153.4226 3.658478
153.9047 2.563477
154.3868 1.586517
154.8690 2.192841
155.3511 6.873016
155.8332 10.66486
156.3153 12.71484
156.7974 13.10602
157.2795 12.73190
157.7617 10.66455
158.2438 8.547852
158.7259 7.538055
159.2080 9.219971
159.6901 10.73279
160.1722 10.65817
160.6544 9.111694
161.1365 8.729858
161.6186 11.99332
162.1007 16.24054
162.5828 19.15726
163.0649 18.74948
163.5471 17.88147
164.0292 18.00320
164.5113 19.14859
164.9934 20.37280
165.4755 20.86542
165.9576 21.16409
166.4398 21.89539
166.9219 23.33649
167.4040 25.34372
167.8861 27.94247
168.3682 31.14996
168.8503 34.36264
169.3325 37.36420
169.8146 40.11972
170.2967 42.51688
170.7788 45.14059
171.2609 47.06586
171.7430 47.41302
172.2252 46.11612
172.7073 43.61826
173.1894 39.25351
173.6715 33.87198
174.1536 29.47018
174.6357 27.26874
175.1179 26.34149
175.6000 25.69659
176.0821 25.27557
176.5642 24.98105
177.0463 24.52710
177.5284 24.07104
178.0106 24.08459
178.4927 25.23187
178.9748 26.92899
179.4569 28.08286
179.9390 28.52289
180.4211 28.77097
180.9033 29.17035
181.3854 29.82809
181.8675 31.17740
182.3496 33.86353
182.8317 37.40247
183.3138 40.85669
183.7960 44.08188
184.2781 47.20032
184.7602 50.44913
185.2423 53.80743
185.7244 56.78476
186.2065 59.41647
186.6887 61.52188
187.1708 62.58118
187.6529 62.65265
188.1350 61.41672
188.6171 58.06433
189.0992 52.60330
189.5814 46.16150
190.0635 38.95508
190.5456 31.09171
191.0277 23.85959
191.5098 17.23157
191.9919 11.43893
192.4741 7.196808
192.9562 4.542755
193.4383 2.813263
193.9204 1.565063
194.4025 0.8111270
194.8846 1.026031
195.3668 2.501038
195.8489 4.770355
196.3310 6.529388
196.8131 7.700836
197.2952 9.292480
197.7773 12.02185
198.2595 15.84680
198.7416 19.90805
199.2237 24.00006
199.7058 28.29559
200.1879 33.18796
200.6700 38.74991
201.1522 44.77707
201.6343 51.36789
202.1164 58.60452
202.5985 65.17682
203.0806 70.97690
203.5627 76.01105
204.0449 80.01935
204.5270 82.90689
205.0091 85.33273
205.4912 88.14105
205.9733 91.48981
206.4554 93.30682
206.9376 92.94604
207.4197 90.90710
207.9018 89.00305
208.3839 87.24625
208.8660 85.65390
209.3481 84.08719
209.8303 82.42355
210.3124 81.79034
210.7945 82.84995
211.2766 84.90823
211.7587 85.53265
212.2408 84.83170
212.7230 82.50177
213.2051 78.18652
213.6872 71.50293
214.1693 63.71268
214.6514 54.61761
215.1335 44.50040
215.6157 34.93051
216.0978 25.49701
216.5799 17.20422
217.0620 10.77057
217.5441 6.668030
218.0262 2.992859
218.5084 0.5877080
218.9905 3.918030
219.4726 6.033478
219.9547 6.527557
220.4368 6.526611
220.9189 6.809265
221.4011 7.694031
221.8832 7.976440
222.3653 7.491760
222.8474 6.324463
223.3295 4.777527
223.8116 2.899963
224.2938 0.6485600
224.7759 2.000122
225.2580 5.011414
225.7401 8.439880
226.2222 12.37970
226.7043 16.73120
227.1865 21.28784
227.6686 25.74182
228.1507 30.68542
228.6328 36.49713
229.1149 43.63904
229.5970 50.47449
230.0792 56.53595
230.5613 62.22180
231.0434 68.92822
231.5255 77.05731
232.0076 85.48865
232.4897 93.58386
232.9719 101.3992
233.4540 108.7430
233.9361 115.6259
234.4182 122.0831
234.9003 128.4073
235.3824 134.9728
235.8646 140.8751
236.3467 145.5496
236.8288 148.3040
237.3109 151.4428
237.7930 155.6534
238.2751 160.1866
238.7573 162.6207
239.2394 162.4791
239.7215 160.8835
240.2036 158.2068
240.6857 153.9973
241.1678 149.7767
241.6500 146.0847
242.1321 142.2466
242.6142 136.3162
243.0963 127.2849
243.5784 117.6591
244.0605 108.3621
244.5427 98.83795
245.0248 90.99207
245.5069 85.24530
245.9890 81.00208
246.4711 76.93658
246.9532 72.44684
247.4354 69.09106
247.9175 67.54688
248.3996 68.12970
248.8817 69.48053
249.3638 71.52875
249.8459 74.39771
250.3281 78.45416
250.8102 84.41205
251.2923 90.34497
251.7744 95.49609
252.2565 99.36145
252.7386 104.4376
253.2208 111.4618
253.7029 119.1477
254.1850 125.5947
254.6671 130.3870
255.1492 134.7573
255.6313 139.0653
256.1135 143.3552
256.5956 147.1403
257.0777 150.4703
257.5598 153.1700
258.0419 154.9736
258.5240 155.7703
259.0062 155.8342
259.4883 155.1597
259.9704 153.7255
260.4525 151.9174
260.9346 149.7330
261.4167 147.2052
261.8989 144.3257
262.3810 141.0178
262.8631 137.6590
263.3452 134.4470
263.8273 131.3519
264.3094 127.8553
264.7916 123.8787
265.2737 119.5938
265.7558 115.0126
266.2379 110.0027
266.7200 105.2898
267.2021 101.1786
267.6843 97.55396
268.1664 93.00885
268.6485 87.20905
269.1306 81.18451
269.6127 75.87695
270.0948 71.43158
270.5770 67.07312
271.0591 62.71155
271.5412 58.36163
272.0233 53.94867
272.5054 49.44128
272.9875 45.10272
273.4697 41.23523
273.9518 37.89832
274.4339 34.33728
274.9160 30.24261
275.3981 26.01129
275.8802 22.81311
276.3624 20.80115
276.8445 19.29883
277.3266 17.98077
277.8087 16.89343
278.2908 16.23639
278.7729 16.14160
279.2551 16.31683
279.7372 16.01831
280.2193 15.15778
280.7014 14.65027
281.1835 15.18945
281.6656 16.75983
282.1478 18.03143
282.6299 18.91144
283.1120 19.43152
283.5941 19.44012
284.0762 18.89758
284.5583 18.68646
285.0405 19.47595
285.5226 21.12555
286.0047 22.22119
286.4868 22.67261
286.9689 22.80957
287.4510 22.91052
287.9332 22.99652
288.4153 23.45685
288.8974 24.54193
289.3795 26.11945
289.8616 27.65948
290.3438 29.13104
290.8259 30.71393
291.3080 32.84534
291.7901 35.36310
292.2722 37.42706
292.7543 38.70319
293.2365 39.35144
293.7186 39.68030
294.2007 39.68488
294.6828 39.42230
295.1649 39.01233
295.6470 38.39026
296.1292 37.29065
296.6113 35.51477
297.0934 33.39087
297.5755 31.23853
298.0576 29.08472
298.5397 27.29370
299.0219 26.25299
299.5040 25.74530
299.9861 25.29517
300.4682 24.76794
300.9503 24.37421
301.4324 24.13708
301.9146 24.17322
302.3967 24.95032
302.8788 27.13409
303.3609 30.12982
303.8430 33.13068
304.3251 36.08472
304.8073 38.81183
305.2894 41.11365
305.7715 43.05585
306.2536 44.86792
306.7357 46.94318
307.2178 48.76898
307.7000 49.77570
308.1821 49.88702
308.6642 49.40015
309.1463 48.24377
309.6284 46.67371
310.1105 45.07349
310.5927 43.37799
311.0748 41.89221
311.5569 40.98706
312.0390 40.66071
312.5211 40.18146
313.0032 38.62561
313.4854 36.89160
313.9675 35.95703
314.4496 35.86707
314.9317 36.91388
315.4138 39.51288
315.8959 43.52136
316.3781 48.08295
316.8602 52.86346
317.3423 57.99982
317.8244 63.60638
318.3065 69.95502
318.7886 76.41766
319.2708 82.78607
319.7529 89.07837
320.2350 95.37030
320.7171 102.5311
321.1992 108.9785
321.6813 113.8994
322.1635 116.9641
322.6456 118.9869
323.1277 120.2556
323.6098 120.5457
324.0919 119.4809
324.5740 115.7147
325.0562 111.7676
325.5383 108.5803
326.0204 106.5898
326.5025 103.7454
326.9846 98.81812
327.4667 93.44391
327.9489 89.30450
328.4310 87.84839
328.9131 86.03766
329.3952 83.43085
329.8773 80.02448
330.3594 76.15881
330.8416 71.44421
331.3237 66.65289
331.8058 62.32886
332.2879 58.50287
332.7700 55.09790
333.2521 52.32526
333.7343 49.96423
334.2164 46.90564
334.6985 42.90375
335.1806 38.63416
335.6627 34.35974
336.1448 29.97729
336.6270 26.05444
337.1091 22.79669
337.5912 19.91046
338.0733 16.54834
338.5554 12.37537
339.0375 8.945923
339.5197 7.198059
340.0018 7.281250
340.4839 6.531616
340.9660 4.772400
341.4481 2.613831
341.9302 0.8016360
342.4124 0.6825560
342.8945 1.854248
343.3766 2.732056
343.8587 3.255066
344.3408 3.087036
344.8229 2.088440
345.3051 1.125305
345.7872 1.403259
346.2693 2.713684
346.7514 3.291809
347.2335 2.523987
347.7156 1.054260
348.1978 0.2185670
348.6799 5.0415002E-02
349.1620 0.4689940
349.6441 1.694702
350.1262 3.273621
350.6083 4.195129
351.0905 4.249695
351.5726 4.039795
352.0547 4.220276
352.5368 4.709717
353.0189 5.240540
353.5010 5.454285
353.9832 5.713806
354.4653 6.708191
354.9474 8.507996
355.4295 10.03809
355.9116 10.46417
356.3937 10.10657
356.8759 9.415833
357.3580 8.033264
357.8401 6.797241
358.3222 6.407837
358.8043 6.744629
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359.7686 7.346497
360.2507 7.392334
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361.2149 6.482300
361.6970 6.135437
362.1791 6.914124
362.6613 8.386353
363.1434 9.564575
363.6255 9.680115
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364.5897 10.33997
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365.5540 12.85504
366.0361 14.86945
366.5182 17.08923
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367.4824 21.17847
367.9645 22.56207
368.4467 22.64697
368.9288 21.36646
369.4109 20.73334
369.8930 21.16028
370.3751 21.93469
370.8572 22.55688
371.3394 22.61200
371.8215 23.25909
372.3036 24.92230
372.7857 27.22858
373.2678 28.83508
373.7499 29.49969
374.2321 29.89453
374.7142 30.28680
375.1963 30.65167
375.6784 31.05237
376.1605 31.39282
376.6426 31.88373
377.1248 33.16125
377.6069 35.51862
378.0890 36.90723
378.5711 36.31781
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379.5353 32.71893
380.0175 32.43842
380.4996 32.11963
380.9817 30.51093
381.4638 27.78558
381.9459 25.27649
382.4280 23.30493
382.9102 21.66010
383.3923 19.93640
383.8744 18.14545
384.3565 16.64020
384.8386 15.76941
385.3207 15.32434
385.8029 14.90387
386.2850 14.42731
386.7671 14.13477
387.2492 14.32715
387.7313 14.88873
388.2134 15.56769
388.6956 16.40741
389.1777 17.21460
389.6598 17.74402
390.1419 18.01776
390.6240 18.36639
391.1061 19.14349
391.5883 20.04572
392.0704 20.73132
392.5525 20.83765
393.0346 21.09760
393.5167 22.20490
393.9988 23.77448
394.4810 24.72711
394.9631 24.42682
395.4452 23.61914
395.9273 22.59784
396.4094 21.29077
396.8915 20.10547
397.3737 19.32141
397.8558 18.62268
398.3379 17.61945
398.8200 16.14313
399.3021 14.47809
399.7842 12.65106
400.2664 10.65253
400.7485 8.489471
401.2306 6.005768
401.7127 3.530548
402.1948 1.236908
402.6769 1.076630
403.1591 2.699493
403.6412 3.369965
404.1233 3.468597
404.6054 3.926147
405.0875 4.800476
405.5696 5.720306
406.0518 6.749847
406.5339 7.922821
407.0160 7.996246
407.4981 6.770966
407.9802 4.975861
408.4623 3.367432
408.9445 1.932739
409.4266 0.5807190
409.9087 0.6269840
410.3908 1.850403
410.8729 3.450226
411.3550 5.434326
411.8372 7.672852
412.3193 10.26486
412.8014 13.04541
413.2835 15.59641
413.7656 17.82190
414.2477 20.02512
414.7299 22.54269
415.2120 25.28021
415.6941 27.95963
416.1762 30.40079
416.6583 32.76874
417.1404 35.03790
417.6226 37.24231
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