#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-06-07 11:17:23 +0300 (Thu, 07 Jun 2018) $ #$Revision: 1064 $ #$URL: svn://172.16.1.111/rod/cif/1/00/05/1000509.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_1000509 loop_ _publ_author_name 'Moore, P. B.' 'Araki, T.' _publ_section_title ; Armangite, Mn26[As6(OH)4O14][As6O18]2[CO3], a fluorite derivative structure ; _journal_name_full 'American Mineralogist' _journal_page_first 748 _journal_page_last 757 _journal_volume 64 _journal_year 1979 _chemical_compound_source R100054 _chemical_formula_sum 'C As18 Mn26 O57' _chemical_name_mineral Armangite _space_group_IT_number 147 _symmetry_space_group_name_Hall '-P 3' _symmetry_space_group_name_H-M 'P -3' _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_length_a 13.491 _cell_length_b 13.491 _cell_length_c 8.855 _cell_volume 1395.750 _exptl_crystal_density_diffrn 4.403 _cod_original_cell_volume 1395.749 _cod_original_formula_sum 'C Mn26 As18 O57' _cod_database_code 9000725 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type other _raman_measurement_device.excitation_laser_wavelength 532 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 15 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R100054.rod _rod_data_source.block 3500000 _rod_database.code 1000509 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9000725 COD http://www.crystallography.net/cod/9000725.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 90.49219 0.0000000E+00 90.97430 0.3546700 91.45642 0.7077350 91.93854 0.4084190 92.42065 3.0260000E-02 92.90277 0.5491480 93.38489 2.194471 93.86700 4.031059 94.34912 4.826683 94.83124 4.701622 95.31335 4.532866 95.79547 4.797688 96.27759 5.335066 96.75970 6.335534 97.24182 7.959343 97.72394 9.845300 98.20605 11.13552 98.68817 11.95148 99.17029 12.31567 99.65240 12.05516 100.1345 10.97181 100.6166 10.84955 101.0988 12.19863 101.5809 14.65259 102.0630 16.43222 102.5451 17.41941 103.0272 17.81269 103.5093 17.71414 103.9915 17.00088 104.4736 16.78475 104.9557 17.44835 105.4378 19.31101 105.9199 20.72611 106.4020 21.58824 106.8842 21.93084 107.3663 22.06705 107.8484 22.08216 108.3305 23.59863 108.8126 26.76711 109.2947 30.94555 109.7769 34.37634 110.2590 36.75762 110.7411 37.78134 111.2232 38.66264 111.7053 40.27359 112.1874 41.32092 112.6696 40.66885 113.1517 38.56546 113.6338 36.30990 114.1159 34.40220 114.5980 32.83969 115.0801 31.41214 115.5623 30.41246 116.0444 29.36460 116.5265 27.90060 117.0086 25.34122 117.4907 22.86320 117.9728 20.95318 118.4550 19.63962 118.9371 18.44037 119.4192 17.37086 119.9013 16.25506 120.3834 14.84795 120.8655 12.65122 121.3477 10.37690 121.8298 8.543664 122.3119 7.227041 122.7940 6.139192 123.2761 5.305730 123.7582 4.567570 124.2404 3.571419 124.7225 2.015265 125.2046 0.1325080 125.6867 1.918426 126.1688 4.316378 126.6509 6.393770 127.1331 7.117372 127.6152 6.721328 128.0973 6.367880 128.5794 7.098801 129.0615 8.471539 129.5436 9.418591 130.0258 9.627888 130.5079 9.395199 130.9900 9.137358 131.4721 8.867916 131.9542 8.641092 132.4363 8.735357 132.9185 9.041817 133.4006 8.770407 133.8827 7.457813 134.3648 5.463364 134.8469 4.067188 135.3290 3.436188 135.8112 2.665302 136.2933 0.6695290 136.7754 2.622631 137.2575 6.196739 137.7396 9.902767 138.2217 13.64457 138.7039 16.79477 139.1860 18.95114 139.6681 21.16292 140.1502 25.58114 140.6323 33.02303 141.1144 39.76746 141.5966 44.22181 142.0787 45.81898 142.5608 47.49123 143.0429 49.23783 143.5250 51.05310 144.0071 52.96252 144.4893 55.14997 144.9714 57.08801 145.4535 58.26969 145.9356 57.33768 146.4177 58.52248 146.8998 62.94009 147.3820 69.65442 147.8641 74.98251 148.3462 78.05638 148.8283 80.78881 149.3104 84.43694 149.7925 89.81290 150.2747 95.01776 150.7568 99.74476 151.2389 104.0443 151.7210 108.5466 152.2031 113.5194 152.6852 118.4764 153.1674 123.1806 153.6495 127.5799 154.1316 131.7159 154.6137 135.5104 155.0958 138.9583 155.5779 142.4160 156.0601 146.1865 156.5422 149.8789 157.0243 153.1019 157.5064 154.8406 157.9885 156.9823 158.4706 160.1064 158.9528 164.3180 159.4349 168.8966 159.9170 173.5374 160.3991 178.4797 160.8812 183.9995 161.3633 190.6393 161.8455 197.5020 162.3276 204.1609 162.8097 210.3739 163.2918 216.9209 163.7739 223.6035 164.2560 230.4464 164.7382 235.9116 165.2203 242.2922 165.7024 249.5393 166.1845 257.4005 166.6666 266.2094 167.1487 274.5233 167.6309 280.9855 168.1130 286.4738 168.5951 292.7054 169.0772 301.3083 169.5593 310.6303 170.0414 319.1485 170.5236 326.2605 171.0057 333.4198 171.4878 341.6562 171.9699 350.8958 172.4520 360.7145 172.9341 371.7074 173.4163 382.9486 173.8984 393.3284 174.3805 402.5587 174.8626 411.0132 175.3447 418.8762 175.8268 426.3304 176.3090 434.2894 176.7911 444.2917 177.2732 454.9716 177.7553 463.9262 178.2374 469.9630 178.7195 474.7065 179.2017 480.2249 179.6838 486.4905 180.1659 492.6427 180.6480 498.6534 181.1301 504.1164 181.6122 508.2003 182.0944 510.4592 182.5765 511.3166 183.0586 511.7085 183.5407 511.5881 184.0228 510.2734 184.5049 506.6283 184.9871 501.2365 185.4692 496.0643 185.9513 491.9720 186.4334 488.2991 186.9155 483.4685 187.3976 477.4751 187.8798 470.9772 188.3619 464.2435 188.8440 457.3668 189.3261 451.3416 189.8082 447.1939 190.2903 444.0888 190.7725 438.5955 191.2546 430.3211 191.7367 421.7357 192.2188 415.5474 192.7009 411.5587 193.1830 408.2151 193.6652 405.2387 194.1473 402.5165 194.6294 399.3639 195.1115 395.7735 195.5936 391.7424 196.0757 387.0106 196.5579 381.5431 197.0400 376.4116 197.5221 372.5293 198.0042 369.7470 198.4863 365.1405 198.9684 358.3081 199.4506 350.5805 199.9327 344.1448 200.4148 339.1331 200.8969 333.9459 201.3790 327.8716 201.8611 320.9089 202.3433 313.6299 202.8254 305.9251 203.3075 298.0302 203.7896 290.3822 204.2717 282.9074 204.7538 275.8038 205.2360 269.1831 205.7181 263.0674 206.2002 257.1728 206.6823 251.4789 207.1644 246.0251 207.6465 240.8870 208.1287 236.1396 208.6108 231.6101 209.0929 227.1547 209.5750 222.6600 210.0571 218.8015 210.5392 215.5502 211.0214 212.9402 211.5035 211.2626 211.9856 210.9671 212.4677 210.4198 212.9498 208.5196 213.4319 204.5615 213.9140 202.4780 214.3962 203.0667 214.8783 205.0496 215.3604 205.2684 215.8425 202.8975 216.3246 200.6199 216.8067 199.8276 217.2889 201.1741 217.7710 201.6719 218.2531 200.9081 218.7352 199.4490 219.2173 198.7238 219.6994 199.1296 220.1816 199.4977 220.6637 199.3436 221.1458 198.6350 221.6279 197.4635 222.1100 195.6650 222.5921 193.4789 223.0743 191.5063 223.5564 189.9545 224.0385 188.2920 224.5206 186.3507 225.0027 184.1846 225.4848 181.4991 225.9670 177.9309 226.4491 173.9896 226.9312 171.0681 227.4133 169.8616 227.8954 168.5725 228.3775 166.3082 228.8597 162.4144 229.3418 159.0854 229.8239 156.6515 230.3060 154.6889 230.7881 152.0560 231.2702 148.2818 231.7524 144.4703 232.2345 141.1859 232.7166 138.6526 233.1987 136.0081 233.6808 133.3426 234.1629 130.5548 234.6451 127.2606 235.1272 123.1705 235.6093 119.0575 236.0914 115.2518 236.5735 111.8061 237.0556 108.5932 237.5378 105.7397 238.0199 103.0953 238.5020 100.2746 238.9841 97.15482 239.4662 94.00223 239.9483 90.77368 240.4305 86.91650 240.9126 84.42209 241.3947 83.88290 241.8768 84.51321 242.3589 84.40210 242.8410 83.33446 243.3232 81.85080 243.8053 80.12662 244.2874 77.96454 244.7695 76.09590 245.2516 74.55803 245.7337 73.24760 246.2159 71.96297 246.6980 70.64819 247.1801 69.46443 247.6622 68.47661 248.1443 67.71725 248.6264 67.09601 249.1086 66.63101 249.5907 66.26016 250.0728 65.86725 250.5549 65.41931 251.0370 65.04382 251.5191 64.81094 252.0013 64.79913 252.4834 64.63110 252.9655 64.10745 253.4476 63.43546 253.9297 63.14603 254.4118 63.68286 254.8940 64.01392 255.3761 63.58432 255.8582 62.01410 256.3403 61.01035 256.8224 60.81317 257.3046 61.06226 257.7867 61.15952 258.2688 61.01242 258.7509 60.78712 259.2330 60.59502 259.7151 60.46732 260.1973 60.40866 260.6794 60.50276 261.1615 60.54205 261.6436 60.19273 262.1257 59.23479 262.6078 58.36804 263.0900 57.88358 263.5721 57.82957 264.0542 57.70946 264.5363 57.62379 265.0184 57.31975 265.5005 56.31627 265.9827 54.32056 266.4648 52.36087 266.9469 50.83669 267.4290 49.79561 267.9111 48.40302 268.3932 46.61229 268.8754 44.63150 269.3575 42.58215 269.8396 40.28264 270.3217 38.49603 270.8038 37.55655 271.2859 37.40520 271.7681 37.08437 272.2502 36.61208 272.7323 35.93758 273.2144 35.00189 273.6965 33.76331 274.1786 32.43909 274.6608 30.92932 275.1429 29.33492 275.6250 28.41576 276.1071 28.33490 276.5892 28.46568 277.0714 28.29765 277.5535 27.81799 278.0356 27.11473 278.5177 26.05775 278.9998 24.82655 279.4819 24.18044 279.9641 24.16235 280.4462 24.51472 280.9283 25.32472 281.4104 26.63039 281.8925 27.06438 282.3746 26.14445 282.8568 24.42874 283.3389 23.54463 283.8210 23.57224 284.3031 23.79791 284.7852 23.82043 285.2673 23.63774 285.7495 23.10915 286.2316 22.08415 286.7137 20.88766 287.1958 20.32106 287.6779 20.40527 288.1600 20.39636 288.6422 19.53029 289.1243 17.99777 289.6064 17.47488 290.0885 18.39067 290.5706 19.58676 291.0527 18.97954 291.5349 16.68224 292.0170 14.32829 292.4991 12.80408 292.9812 11.95093 293.4633 11.39540 293.9454 11.20094 294.4276 10.93214 294.9097 9.869461 295.3918 8.159485 295.8739 6.558853 296.3560 5.553879 296.8381 4.910767 297.3203 4.079636 297.8024 3.028580 298.2845 2.034149 298.7666 1.482819 299.2487 1.264374 299.7308 1.015747 300.2130 0.6606750 300.6951 0.1588750 301.1772 0.7211610 301.6593 1.972855 302.1414 3.123337 302.6235 3.646439 303.1057 3.753357 303.5878 3.840576 304.0699 4.023590 304.5520 4.302933 305.0341 4.765533 305.5162 5.378052 305.9984 5.921417 306.4805 6.136642 306.9626 6.198608 307.4447 6.328384 307.9268 6.674194 308.4089 7.080399 308.8911 7.572678 309.3732 8.049004 309.8553 8.149025 310.3374 7.134514 310.8195 5.920403 311.3016 5.581993 311.7838 6.672218 312.2659 7.784821 312.7480 7.894394 313.2301 7.303795 313.7122 6.772873 314.1943 6.848640 314.6765 6.967026 315.1586 6.622917 315.6407 5.543549 316.1228 4.714508 316.6049 4.849762 317.0870 5.516388 317.5692 5.993515 318.0513 6.002655 318.5334 5.790634 319.0155 5.389450 319.4976 4.756874 319.9797 4.292587 320.4619 4.292313 320.9440 4.476295 321.4261 4.526695 321.9082 4.654228 322.3903 4.369255 322.8724 3.328400 323.3546 1.510612 323.8367 0.1096800 324.3188 1.427208 324.8009 2.445221 325.2830 3.156784 325.7651 3.037994 326.2473 3.207832 326.7294 3.961906 327.2115 5.224594 327.6936 6.378891 328.1757 7.365364 328.6578 8.247261 329.1400 9.056473 329.6221 9.745583 330.1042 10.41646 330.5863 11.07488 331.0684 11.71523 331.5505 12.33330 332.0327 13.14004 332.5148 13.67377 332.9969 13.65372 333.4790 12.68862 333.9611 12.25854 334.4432 12.48312 334.9254 13.17402 335.4075 14.07075 335.8896 15.38602 336.3717 16.48753 336.8538 17.11962 337.3359 17.23532 337.8180 17.47399 338.3001 17.94183 338.7823 18.37420 339.2644 18.41521 339.7465 17.96272 340.2286 17.56114 340.7107 17.32686 341.1928 17.24873 341.6750 17.34206 342.1571 17.66893 342.6392 17.93074 343.1213 17.77988 343.6034 17.20842 344.0855 16.88805 344.5677 17.05047 345.0498 17.40337 345.5319 17.10642 346.0140 16.13373 346.4961 15.24908 346.9782 15.09520 347.4604 15.50069 347.9425 15.60634 348.4246 15.27578 348.9067 14.80712 349.3888 14.73837 349.8709 14.97322 350.3531 14.97054 350.8352 14.32858 351.3173 13.29779 351.7994 12.24509 352.2815 11.16763 352.7636 10.32445 353.2458 10.15975 353.7279 10.41468 354.2100 10.52508 354.6921 10.02513 355.1742 9.447449 355.6563 9.603745 356.1385 10.39242 356.6206 10.77850 357.1027 9.423439 357.5848 7.498009 358.0669 6.432480 358.5490 7.142235 359.0312 7.979172 359.5133 7.867989 359.9954 7.005348 360.4775 6.052353 360.9596 5.063080 361.4417 4.280602 361.9239 3.927521 362.4060 4.203247 362.8881 4.395233 363.3702 4.215813 363.8523 3.783539 364.3344 3.296028 364.8166 2.438713 365.2987 1.872047 365.7808 2.071053 366.2629 3.208397 366.7450 3.757820 367.2271 2.724365 367.7093 1.394714 368.1914 0.9483180 368.6735 2.488121 369.1556 3.784180 369.6377 4.255402 370.1198 4.021019 370.6020 4.134552 371.0841 4.896194 371.5662 5.808693 372.0483 6.560242 372.5304 7.069519 373.0125 7.614227 373.4947 8.260574 373.9768 8.956299 374.4589 9.552086 374.9410 9.942749 375.4231 10.37116 375.9052 10.96376 376.3874 11.75224 376.8695 12.66580 377.3516 13.82849 377.8337 14.96150 378.3158 15.61252 378.7979 15.66757 379.2801 16.10872 379.7622 17.48579 380.2443 19.45102 380.7264 20.31781 381.2085 20.00507 381.6906 19.44113 382.1728 19.21638 382.6549 19.32512 383.1370 19.92740 383.6191 21.15485 384.1012 22.63556 384.5833 23.68513 385.0655 24.38908 385.5476 25.29507 386.0297 27.09511 386.5118 29.22578 386.9939 30.64789 387.4760 31.21230 387.9582 31.45885 388.4403 31.79742 388.9224 32.20334 389.4045 32.62009 389.8866 32.72301 390.3687 33.03954 390.8509 34.22343 391.3330 36.18806 391.8151 38.04199 392.2972 39.31868 392.7793 40.18069 393.2614 40.74933 393.7436 40.72653 394.2257 40.87221 394.7078 41.66147 395.1899 42.87592 395.6720 43.94182 396.1541 44.53166 396.6363 45.05057 397.1184 45.67796 397.6005 46.43867 398.0826 47.29404 398.5647 48.52216 399.0468 49.74695 399.5290 50.51221 400.0111 50.14134 400.4932 50.01158 400.9753 50.54112 401.4574 51.72784 401.9395 52.35727 402.4217 51.98984 402.9038 51.53325 403.3859 51.69296 403.8680 53.04860 404.3501 53.56656 404.8322 52.74457 405.3144 51.16847 405.7965 50.47319 406.2786 50.89197 406.7607 51.40422 407.2428 51.55826 407.7249 51.34370 408.2071 51.16821 408.6892 51.08966 409.1713 50.88245 409.6534 50.09993 410.1355 48.77638 410.6176 47.73122 411.0998 47.41136 411.5819 47.41379 412.0640 46.55505 412.5461 44.86816 413.0282 43.32887 413.5103 43.13832 413.9925 43.62326 414.4746 43.22588 414.9567 41.42615 415.4388 39.33929 415.9209 38.27974 416.4030 37.93582 416.8852 37.37756 417.3673 35.74513 417.8494 33.90436 418.3315 32.58467 418.8136 31.83652 419.2957 31.25249 419.7779 30.59398 420.2600 30.04321 420.7421 29.75789 421.2242 30.38519 421.7063 30.62370 422.1884 29.67714 422.6706 27.89674 423.1527 26.66151 423.6348 27.08492 424.1169 27.59917 424.5990 27.35947 425.0811 25.66742 425.5633 24.49489 426.0454 24.27209 426.5275 24.58177 427.0096 24.76100 427.4917 24.63972 427.9738 24.55553 428.4560 24.55565 428.9381 24.65097 429.4202 24.95168 429.9023 25.54134 430.3844 26.14162 430.8665 26.50537 431.3487 26.57141 431.8308 26.78056 432.3129 27.20372 432.7950 27.73961 433.2771 28.11108 433.7592 28.29929 434.2414 28.65675 434.7235 29.48869 435.2056 30.63889 435.6877 31.47990 436.1698 31.99835 436.6519 32.32892 437.1341 32.54596 437.6162 32.66890 438.0983 32.76616 438.5804 32.89381 439.0625 32.95010 439.5446 32.78128 440.0268 32.43118 440.5089 32.05782 440.9910 31.78636 441.4731 31.51640 441.9552 31.20367 442.4373 30.88013 442.9195 30.31691 443.4016 29.24664 443.8837 27.92137 444.3658 26.64732 444.8479 25.50391 445.3300 24.43689 445.8122 23.48653 446.2943 22.63269 446.7764 21.64551 447.2585 20.22586 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