#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-06-07 11:17:46 +0300 (Thu, 07 Jun 2018) $
#$Revision: 1070 $
#$URL: svn://172.16.1.111/rod/cif/1/00/05/1000513.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000513
loop_
_publ_author_name
'Onac, B. P.'
'Effenberger, H. S.'
_publ_section_title
;
 Re-examination of berlinite (AlPO4) from the Cioclovina Cave, Romania
 Locality: Cioclovina Cave, Romania
;
_journal_name_full               'American Mineralogist'
_journal_page_first              1998
_journal_page_last               2001
_journal_paper_doi               10.2138/am.2007.2581
_journal_volume                  92
_journal_year                    2007
_chemical_compound_source        R130243
_chemical_formula_sum            'Al O4 P'
_chemical_name_mineral           Berlinite
_space_group_IT_number           152
_symmetry_space_group_name_Hall  'P 31 2"'
_symmetry_space_group_name_H-M   'P 31 2 1'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_length_a                   4.9458
_cell_length_b                   4.9458
_cell_length_c                   10.9526
_cell_volume                     232.018
_exptl_crystal_density_diffrn    2.618
_cod_original_formula_sum        'Al P O4'
_cod_database_code               9010367
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R130243.rod
_rod_data_source.block           3500000
_rod_database.code               1000513
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9010367 COD http://www.crystallography.net/cod/9010367.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
103.2825 0.0000000E+00
103.7646 0.2688520
104.2467 2.936440
104.7288 8.968597
105.2109 17.75333
105.6931 29.14253
106.1752 42.38460
106.6573 57.72511
107.1394 79.34709
107.6215 95.92461
108.1036 108.0860
108.5858 115.5191
109.0679 115.6103
109.5500 103.5857
110.0321 88.26334
110.5142 74.24951
110.9963 58.90282
111.4785 47.42764
111.9606 40.62629
112.4427 38.34586
112.9248 38.83721
113.4069 41.96617
113.8890 47.55644
114.3712 55.51534
114.8533 65.63441
115.3354 78.17326
115.8175 94.46105
116.2996 113.7982
116.7817 134.9768
117.2639 160.0443
117.7460 186.5995
118.2281 211.8342
118.7102 241.2513
119.1923 264.3557
119.6744 275.1703
120.1566 272.9781
120.6387 260.5793
121.1208 234.9255
121.6029 200.3590
122.0850 165.7577
122.5671 133.1079
123.0493 103.7124
123.5314 79.08459
124.0135 59.83878
124.4956 44.32228
124.9777 31.79139
125.4598 21.97588
125.9420 14.14290
126.4241 8.211998
126.9062 3.892929
127.3883 0.7211760
127.8704 1.239296
128.3525 2.306526
128.8347 2.754593
129.3168 2.607147
129.7989 2.268562
130.2810 2.020004
130.7631 1.842598
131.2452 1.651749
131.7274 1.388214
132.2095 1.113007
132.6916 1.050064
133.1737 1.231934
133.6558 1.385414
134.1379 1.183830
134.6201 0.6328350
135.1022 0.1511990
135.5843 0.1351780
136.0664 0.2444230
136.5485 0.2513500
137.0306 0.3173830
137.5128 1.531494
137.9949 3.929329
138.4770 6.913719
138.9591 9.484970
139.4412 11.36840
139.9233 12.23449
140.4055 12.56368
140.8876 12.72134
141.3697 12.96468
141.8518 13.40663
142.3339 13.91677
142.8160 14.90918
143.2982 16.64925
143.7803 19.43251
144.2624 21.93766
144.7445 23.89955
145.2266 25.66605
145.7087 28.00074
146.1909 31.50546
146.6730 34.86298
147.1551 37.57195
147.6372 39.22081
148.1193 40.87202
148.6014 42.50123
149.0836 44.12977
149.5657 45.89488
150.0478 47.66161
150.5299 49.63415
151.0120 51.91975
151.4941 54.56578
151.9763 57.43471
152.4584 60.46725
152.9405 63.70004
153.4226 67.36950
153.9047 71.43542
154.3868 75.97839
154.8690 81.04153
155.3511 86.36656
155.8332 92.48644
156.3153 99.23177
156.7974 106.6863
157.2795 115.5186
157.7617 125.8077
158.2438 137.5608
158.7259 150.7840
159.2080 165.9406
159.6901 182.1317
160.1722 199.1093
160.6544 216.8779
161.1365 235.6601
161.6186 256.7458
162.1007 278.1530
162.5828 298.5546
163.0649 322.8228
163.5471 341.3149
164.0292 351.3091
164.5113 352.6767
164.9934 341.7065
165.4755 310.6372
165.9576 267.4987
166.4398 222.7346
166.9219 174.2902
167.4040 129.1839
167.8861 92.57764
168.3682 64.62597
168.8503 42.68690
169.3325 26.61971
169.8146 15.23116
170.2967 6.786095
170.7788 1.590149
171.2609 1.752083
171.7430 4.334568
172.2252 6.246563
172.7073 7.447456
173.1894 7.645336
173.6715 7.094509
174.1536 6.353329
174.6357 5.787945
175.1179 5.135399
175.6000 4.052597
176.0821 2.494366
176.5642 0.6503680
177.0463 1.331997
177.5284 3.466736
178.0106 5.758274
178.4927 8.307205
178.9748 11.00439
179.4569 13.59237
179.9390 16.04604
180.4211 18.48392
180.9033 21.08046
181.3854 23.82875
181.8675 26.61954
182.3496 29.31505
182.8317 32.00974
183.3138 35.11344
183.7960 38.70237
184.2781 42.53238
184.7602 46.12161
185.2423 49.54409
185.7244 53.03921
186.2065 56.92063
186.6887 61.16220
187.1708 65.59279
187.6529 70.14806
188.1350 74.97954
188.6171 80.18206
189.0992 85.80423
189.5814 91.93189
190.0635 98.60328
190.5456 105.8874
191.0277 113.5875
191.5098 121.6195
191.9919 130.2589
192.4741 139.9788
192.9562 150.7546
193.4383 162.1016
193.9204 173.8377
194.4025 185.9128
194.8846 197.6969
195.3668 209.3448
195.8489 220.4102
196.3310 230.2587
196.8131 239.0378
197.2952 245.4226
197.7773 248.0557
198.2595 246.8343
198.7416 244.6848
199.2237 241.5232
199.7058 238.0090
200.1879 235.8336
200.6700 234.9407
201.1522 235.5711
201.6343 237.8953
202.1164 241.9326
202.5985 247.5346
203.0806 254.6792
203.5627 263.3229
204.0449 273.3451
204.5270 284.8454
205.0091 297.3913
205.4912 310.5578
205.9733 324.1962
206.4554 339.4304
206.9376 356.7662
207.4197 375.6325
207.9018 394.4389
208.3839 412.9680
208.8660 432.0806
209.3481 452.3488
209.8303 474.2056
210.3124 495.7903
210.7945 517.0471
211.2766 537.7975
211.7587 558.2717
212.2408 578.9224
212.7230 598.4474
213.2051 616.2662
213.6872 632.4021
214.1693 646.8009
214.6514 659.3912
215.1335 670.1964
215.6157 678.7297
216.0978 684.7759
216.5799 689.0312
217.0620 691.7658
217.5441 692.4714
218.0262 693.0813
218.5084 693.6995
218.9905 694.3657
219.4726 695.3428
219.9547 696.9780
220.4368 698.3726
220.9189 698.9805
221.4011 698.7862
221.8832 697.9836
222.3653 696.8950
222.8474 695.2443
223.3295 691.6813
223.8116 686.2893
224.2938 679.0038
224.7759 669.6755
225.2580 658.0090
225.7401 645.1542
226.2222 630.7782
226.7043 615.2632
227.1865 599.4762
227.6686 583.6495
228.1507 567.6462
228.6328 551.4136
229.1149 534.6364
229.5970 518.1647
230.0792 502.3054
230.5613 486.9000
231.0434 471.7367
231.5255 457.1664
232.0076 442.7393
232.4897 428.4436
232.9719 414.6239
233.4540 400.2454
233.9361 384.8811
234.4182 368.9412
234.9003 353.5447
235.3824 338.7086
235.8646 324.2528
236.3467 310.0242
236.8288 295.7136
237.3109 282.2588
237.7930 269.7195
238.2751 257.9892
238.7573 247.1465
239.2394 237.2574
239.7215 228.1336
240.2036 219.6318
240.6857 211.8201
241.1678 204.4917
241.6500 197.7679
242.1321 191.5194
242.6142 185.2978
243.0963 179.1047
243.5784 172.9819
244.0605 167.0011
244.5427 161.1082
245.0248 155.4126
245.5069 149.9352
245.9890 144.6289
246.4711 139.5248
246.9532 134.7967
247.4354 129.9095
247.9175 124.6671
248.3996 118.8748
248.8817 113.2642
249.3638 107.8259
249.8459 102.5771
250.3281 97.55575
250.8102 92.78241
251.2923 88.18685
251.7744 83.68138
252.2565 79.27885
252.7386 75.08417
253.2208 71.04775
253.7029 67.25875
254.1850 63.81958
254.6671 60.87335
255.1492 57.97819
255.6313 54.99324
256.1135 51.88868
256.5956 48.94120
257.0777 46.14175
257.5598 43.54119
258.0419 41.27646
258.5240 39.55989
259.0062 37.75210
259.4883 35.58002
259.9704 33.03623
260.4525 30.85025
260.9346 29.14923
261.4167 27.69455
261.8989 26.20275
262.3810 24.64254
262.8631 23.15095
263.3452 21.81097
263.8273 20.61179
264.3094 19.41461
264.7916 18.13588
265.2737 16.89614
265.7558 15.82058
266.2379 14.98241
266.7200 14.09812
267.2021 13.06750
267.6843 11.92201
268.1664 10.87962
268.6485 9.925835
269.1306 9.113388
269.6127 8.567314
270.0948 8.384041
270.5770 8.017715
271.0591 7.314907
271.5412 6.369553
272.0233 5.612770
272.5054 5.106403
272.9875 4.658756
273.4697 4.129791
273.9518 3.494835
274.4339 2.903160
274.9160 2.374794
275.3981 1.902367
275.8802 1.433300
276.3624 0.9570620
276.8445 0.5618590
277.3266 0.3626520
277.8087 0.3822400
278.2908 0.2428780
278.7729 0.1282920
279.2551 0.6238250
279.7372 1.010654
280.2193 1.289768
280.7014 1.459980
281.1835 1.460556
281.6656 1.295986
282.1478 1.281712
282.6299 1.460205
283.1120 1.733032
283.5941 1.951218
284.0762 2.115330
284.5583 2.234962
285.0405 2.332985
285.5226 2.398956
286.0047 2.332951
286.4868 2.110233
286.9689 1.829788
287.4510 1.623745
287.9332 1.486755
288.4153 1.352097
288.8974 1.195396
289.3795 1.016911
289.8616 0.8250390
290.3438 0.6093600
290.8259 0.3843460
291.3080 0.2027240
291.7901 4.6246000E-02
292.2722 0.2264290
292.7543 0.7466660
293.2365 1.387825
293.7186 1.804752
294.2007 1.990505
294.6828 2.166031
295.1649 2.431053
295.6470 2.824890
296.1292 3.527328
296.6113 4.724155
297.0934 6.077641
297.5755 7.006866
298.0576 7.548603
298.5397 8.092705
299.0219 8.926773
299.5040 9.956669
299.9861 10.96421
300.4682 11.89642
300.9503 12.89416
301.4324 14.19557
301.9146 15.73838
302.3967 17.29474
302.8788 18.71282
303.3609 20.05111
303.8430 21.39897
304.3251 22.80218
304.8073 24.08590
305.2894 25.13375
305.7715 25.94280
306.2536 26.53393
306.7357 27.08130
307.2178 27.32095
307.7000 26.92397
308.1821 25.83488
308.6642 24.39549
309.1463 22.67682
309.6284 20.80790
310.1105 18.96311
310.5927 17.19325
311.0748 15.51916
311.5569 13.81183
312.0390 12.08198
312.5211 10.79253
313.0032 10.76064
313.4854 11.08078
313.9675 10.79168
314.4496 9.056820
314.9317 7.112221
315.4138 5.374950
315.8959 3.870743
316.3781 2.687706
316.8602 2.035351
317.3423 1.633587
317.8244 1.278503
318.3065 0.8545760
318.7886 0.5731430
319.2708 0.6495970
319.7529 0.9441830
320.2350 1.063778
320.7171 0.6398810
321.1992 0.2003710
321.6813 2.0992000E-02
322.1635 0.2479170
322.6456 0.4795530
323.1277 0.6081090
323.6098 0.6984980
324.0919 0.8600160
324.5740 1.198883
325.0562 1.527718
325.5383 1.780636
326.0204 1.931519
326.5025 2.101650
326.9846 2.193897
327.4667 2.352051
327.9489 2.731564
328.4310 3.590115
328.9131 4.384361
329.3952 5.034950
329.8773 5.540096
330.3594 5.987396
330.8416 6.185032
331.3237 6.482025
331.8058 7.147812
332.2879 8.356476
332.7700 9.719341
333.2521 11.20952
333.7343 12.82111
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334.6985 16.66183
335.1806 18.65645
335.6627 20.47148
336.1448 22.23265
336.6270 23.36641
337.1091 23.85003
337.5912 23.69240
338.0733 22.80432
338.5554 21.05868
339.0375 18.95193
339.5197 16.54653
340.0018 13.84414
340.4839 11.61134
340.9660 9.948547
341.4481 8.604610
341.9302 7.298191
342.4124 6.010963
342.8945 4.925209
343.3766 4.131966
343.8587 3.588364
344.3408 3.038914
344.8229 2.480991
345.3051 1.972851
345.7872 1.621216
346.2693 1.393204
346.7514 1.033890
347.2335 0.4142300
347.7156 0.2587890
348.1978 0.5120510
348.6799 0.3751640
349.1620 0.2166820
349.6441 0.2675670
350.1262 0.4800910
350.6083 0.7772290
351.0905 1.181427
351.5726 1.557091
352.0547 1.733009
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353.5010 1.746620
353.9832 1.743999
354.4653 1.595463
354.9474 1.293823
355.4295 0.9645040
355.9116 0.8245580
356.3937 0.6936110
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357.3580 0.5722200
357.8401 1.628990
358.3222 2.693947
358.8043 3.772938
359.2864 4.836174
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361.2149 9.250034
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364.5897 25.60228
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365.5540 30.56484
366.0361 33.38725
366.5182 36.47924
367.0003 39.88134
367.4824 43.28234
367.9645 47.31842
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369.8930 70.80291
370.3751 78.45749
370.8572 87.08513
371.3394 96.23890
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372.3036 119.7162
372.7857 134.0984
373.2678 149.5640
373.7499 168.3675
374.2321 184.5051
374.7142 195.0057
375.1963 199.3452
375.6784 199.8148
376.1605 194.4120
376.6426 187.6772
377.1248 186.5166
377.6069 191.2025
378.0890 199.9059
378.5711 214.2129
379.0532 232.6915
379.5353 245.5324
380.0175 253.6276
380.4996 252.2297
380.9817 233.3332
381.4638 198.9174
381.9459 163.7434
382.4280 129.7121
382.9102 98.40877
383.3923 73.99061
383.8744 56.00091
384.3565 41.89727
384.8386 30.96321
385.3207 22.61612
385.8029 16.31045
386.2850 12.09679
386.7671 9.024040
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388.6956 0.6915130
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391.1061 3.100769
391.5883 3.389072
392.0704 3.545799
392.5525 3.532330
393.0346 3.447002
393.5167 3.305618
393.9988 3.121872
394.4810 2.932068
394.9631 2.911659
395.4452 2.761234
395.9273 2.300659
396.4094 1.422401
396.8915 0.5106960
397.3737 0.3375700
397.8558 1.190884
398.3379 2.133358
398.8200 2.924412
399.3021 4.070950
399.7842 5.717793
400.2664 7.859703
400.7485 10.16946
401.2306 12.69389
401.7127 15.30814
402.1948 17.92342
402.6769 20.50654
403.1591 23.13553
403.6412 25.76108
404.1233 28.45655
404.6054 31.51618
405.0875 34.98933
405.5696 38.50502
406.0518 41.86568
406.5339 45.08029
407.0160 48.73053
407.4981 52.77490
407.9802 57.20283
408.4623 61.84686
408.9445 66.73835
409.4266 72.47590
409.9087 79.18671
410.3908 86.87586
410.8729 95.53354
411.3550 105.1968
411.8372 115.6159
412.3193 126.6058
412.8014 138.3447
413.2835 151.2852
413.7656 165.5667
414.2477 181.0273
414.7299 197.9331
415.2120 215.9211
415.6941 233.5481
416.1762 251.4753
416.6583 268.0597
417.1404 282.8398
417.6226 295.7707
418.1047 303.8695
418.5868 305.7508
419.0689 301.9168
419.5510 292.6758
420.0331 276.0605
420.5153 256.8015
420.9974 234.8935
421.4795 211.6385
421.9616 191.2225
422.4437 174.3871
422.9258 160.6257
423.4080 149.9864
423.8901 142.7855
424.3722 137.1331
424.8543 133.2516
425.3364 130.6905
425.8185 129.0196
426.3007 127.9858
426.7828 128.2078
427.2649 129.9238
427.7470 133.0017
428.2291 136.5930
428.7112 140.2453
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