#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-06-07 11:26:05 +0300 (Thu, 07 Jun 2018) $
#$Revision: 1086 $
#$URL: svn://172.16.1.111/rod/cif/1/00/05/1000526.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000526
loop_
_publ_author_name
'Robinson, K.'
'Gibbs, G. V.'
'Ribbe, P. H.'
_publ_section_title
;
 The crystal structures of the humite minerals. IV. Clinohumite and
 titanclinohumite
;
_journal_name_full               'American Mineralogist'
_journal_page_first              43
_journal_page_last               49
_journal_volume                  58
_journal_year                    1973
_chemical_compound_source        R050183
_chemical_formula_sum            'Fe0.58 H2 Mg8.42 O18 Si4'
_chemical_name_mineral           Hydroxylclinohumite
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2xab'
_symmetry_space_group_name_H-M   'P 21/b 1 1'
_cell_angle_alpha                100.786
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   4.7441
_cell_length_b                   10.2501
_cell_length_c                   13.6635
_cell_volume                     652.684
_exptl_crystal_density_diffrn    3.253
_cod_original_cell_volume        652.683
_cod_original_formula_sum        'Mg8.42 Fe.58 Si4 O18 H2'
_cod_database_code               9000292
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R050183.rod
_rod_data_source.block           3500000
_rod_database.code               1000526
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9000292 COD http://www.crystallography.net/cod/9000292.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
130.5709 0.0000000E+00
131.0530 0.1977230
131.5351 0.5731510
132.0173 0.7251890
132.4994 0.6335300
132.9815 0.3806460
133.4636 0.2362670
133.9457 0.1820980
134.4278 0.3213960
134.9100 0.7635350
135.3921 1.337677
135.8742 1.899170
136.3563 2.330521
136.8384 2.580948
137.3205 2.377243
137.8027 1.809525
138.2848 1.299210
138.7669 1.699249
139.2490 2.730423
139.7311 3.300293
140.2132 2.792191
140.6953 1.904816
141.1775 1.449112
141.6596 1.717087
142.1417 2.197388
142.6238 2.504669
143.1059 2.683044
143.5880 2.550018
144.0702 1.781479
144.5523 1.171814
145.0344 1.354797
145.5165 2.620743
145.9986 3.957489
146.4807 4.399963
146.9629 3.722229
147.4450 2.896835
147.9271 2.193222
148.4092 1.634003
148.8913 1.171356
149.3734 0.7787780
149.8556 0.4764860
150.3377 0.3476100
150.8198 0.6350250
151.3019 0.8515320
151.7840 0.9963680
152.2661 1.114319
152.7483 1.022461
153.2304 0.8889160
153.7125 0.7143250
154.1946 0.5040440
154.6767 0.1468350
155.1588 0.1297910
155.6410 0.1857150
156.1231 6.5109000E-02
156.6052 6.1523002E-02
157.0873 6.9518998E-02
157.5694 4.1717999E-02
158.0515 0.1395570
158.5337 0.2107390
159.0158 0.2778930
159.4979 0.4288790
159.9800 0.6761320
160.4621 0.7624050
160.9442 0.2180330
161.4264 0.6952970
161.9085 1.156281
162.3906 0.5239720
162.8727 0.5569460
163.3548 0.9737240
163.8369 0.4870910
164.3191 0.2195890
164.8012 0.7583310
165.2833 1.152527
165.7654 1.418869
166.2475 1.541428
166.7296 1.534241
167.2118 1.471130
167.6939 1.231506
168.1760 1.089310
168.6581 1.245880
169.1402 1.608673
169.6223 1.944992
170.1045 2.083755
170.5866 2.023834
171.0687 1.781342
171.5508 1.155273
172.0329 0.5065770
172.5150 0.1987610
172.9971 0.8575290
173.4793 1.219223
173.9614 0.9545290
174.4435 0.1863250
174.9256 1.098419
175.4077 1.691452
175.8898 2.185135
176.3720 2.703308
176.8541 3.262222
177.3362 3.792007
177.8183 4.192688
178.3004 4.408035
178.7825 4.615860
179.2647 4.718781
179.7468 4.870117
180.2289 5.227753
180.7110 5.824356
181.1931 6.532043
181.6752 7.149673
182.1574 7.610428
182.6395 8.182968
183.1216 8.988922
183.6037 9.898346
184.0858 10.74234
184.5679 11.48080
185.0501 12.11703
185.5322 12.72423
186.0143 13.39130
186.4964 13.64636
186.9785 13.24571
187.4606 12.30464
187.9428 11.02725
188.4249 9.279999
188.9070 7.506378
189.3891 6.248291
189.8712 5.509232
190.3533 4.992126
190.8355 4.381409
191.3176 3.744415
191.7997 3.722488
192.2818 4.971085
192.7639 6.483963
193.2460 7.408386
193.7282 7.689789
194.2103 7.746674
194.6924 7.848022
195.1745 7.968002
195.6566 8.405350
196.1387 9.439438
196.6209 10.69780
197.1030 12.04298
197.5851 13.44597
198.0672 14.85201
198.5493 16.22736
199.0314 17.62108
199.5136 18.81485
199.9957 19.71761
200.4778 20.47900
200.9599 21.21307
201.4420 21.94035
201.9241 22.55597
202.4063 22.90044
202.8884 22.96811
203.3705 22.77701
203.8526 22.16216
204.3347 21.42776
204.8168 20.77281
205.2990 20.26720
205.7811 19.87547
206.2632 19.53917
206.7453 19.39267
207.2274 19.08694
207.7095 18.59143
208.1917 17.96764
208.6738 17.26602
209.1559 16.49448
209.6380 15.67499
210.1201 14.86824
210.6022 14.33385
211.0844 13.39230
211.5665 11.68608
212.0486 9.668503
212.5307 7.817673
213.0128 6.292679
213.4949 5.083496
213.9771 4.201675
214.4592 3.770615
214.9413 3.362000
215.4234 2.737015
215.9055 2.119659
216.3876 1.884064
216.8698 2.194031
217.3519 2.836258
217.8340 3.448532
218.3161 4.028381
218.7982 4.685638
219.2803 5.557892
219.7625 6.472885
220.2446 7.029587
220.7267 6.921082
221.2088 6.674835
221.6909 7.140305
222.1730 8.349915
222.6552 9.671509
223.1373 10.89859
223.6194 12.01199
224.1015 12.92932
224.5836 13.49577
225.0657 14.02460
225.5479 14.87000
226.0300 16.03757
226.5121 17.26666
226.9942 18.45691
227.4763 19.59027
227.9584 20.57854
228.4406 21.26880
228.9227 21.94173
229.4048 22.88266
229.8869 24.07751
230.3690 25.20656
230.8511 26.05038
231.3333 26.61258
231.8154 26.93623
232.2975 26.88168
232.7796 26.70132
233.2617 26.55109
233.7438 26.43398
234.2259 26.29065
234.7081 26.10342
235.1902 25.88052
235.6723 25.47621
236.1544 24.59268
236.6365 23.75526
237.1186 23.28143
237.6008 23.11160
238.0829 22.93219
238.5650 22.37753
239.0471 21.35907
239.5292 20.61772
240.0113 20.62973
240.4935 20.52225
240.9756 19.82550
241.4577 18.65057
241.9398 17.47873
242.4219 16.77444
242.9040 16.61053
243.3862 16.39816
243.8683 16.09201
244.3504 15.78439
244.8325 15.51103
245.3146 15.27095
245.7967 15.03531
246.2789 14.75923
246.7610 14.41479
247.2431 14.30280
247.7252 14.59064
248.2073 14.93388
248.6894 15.20300
249.1716 15.41565
249.6537 15.66733
250.1358 16.05814
250.6179 16.61023
251.1000 16.92683
251.5821 16.78859
252.0643 16.66354
252.5464 16.64510
253.0285 16.77144
253.5106 17.14397
253.9927 17.90953
254.4748 19.05841
254.9570 19.46899
255.4391 18.67767
255.9212 17.77637
256.4033 17.10970
256.8854 16.64438
257.3675 16.22690
257.8496 15.75977
258.3318 15.24992
258.8139 14.76160
259.2960 14.51639
259.7781 14.06488
260.2602 12.97606
260.7423 11.54767
261.2245 10.51974
261.7066 10.39421
262.1887 10.94403
262.6708 10.94934
263.1529 10.07748
263.6350 9.177887
264.1172 8.468201
264.5993 7.923981
265.0814 7.495346
265.5635 7.176147
266.0456 6.929306
266.5277 6.649811
267.0099 6.422867
267.4920 6.045227
267.9741 5.289474
268.4562 4.344009
268.9383 3.605637
269.4204 3.254974
269.9026 3.148331
270.3847 2.987762
270.8668 2.759293
271.3489 2.535263
271.8310 2.359818
272.3131 2.203384
272.7953 2.020966
273.2774 1.810455
273.7595 1.539215
274.2416 1.118011
274.7237 0.5390320
275.2058 3.1493999E-02
275.6880 0.7902070
276.1701 1.461365
276.6522 1.436478
277.1343 0.4405210
277.6164 0.8179320
278.0985 1.420288
278.5807 1.442841
279.0628 1.410629
279.5449 1.284378
280.0270 1.246536
280.5091 1.720490
280.9912 2.892044
281.4734 4.027176
281.9555 4.184875
282.4376 3.613266
282.9197 3.308258
283.4018 3.783188
283.8839 4.547821
284.3661 4.969406
284.8482 4.990646
285.3303 4.777954
285.8124 4.272308
286.2945 3.618912
286.7766 3.189560
287.2588 3.184357
287.7409 3.372879
288.2230 3.516754
288.7051 3.614075
289.1872 3.681870
289.6693 3.621582
290.1515 3.572693
290.6336 3.830139
291.1157 4.728607
291.5978 5.587036
292.0799 5.581482
292.5620 4.704315
293.0442 3.998413
293.5263 4.070023
294.0084 4.501312
294.4905 4.639755
294.9726 4.287872
295.4547 4.053757
295.9369 4.591522
296.4190 5.834213
296.9011 6.886169
297.3832 7.444229
297.8653 7.680984
298.3474 7.732559
298.8296 7.563293
299.3117 7.582840
299.7938 8.166580
300.2759 9.218552
300.7580 10.19315
301.2401 10.83746
301.7223 11.58565
302.2044 12.92163
302.6865 14.77872
303.1686 16.54370
303.6507 17.82822
304.1328 18.78098
304.6150 19.79454
305.0971 20.82327
305.5792 22.09142
306.0613 24.06203
306.5434 26.41177
307.0255 28.22632
307.5077 28.94989
307.9898 28.97217
308.4719 28.98553
308.9540 28.96445
309.4361 29.05383
309.9182 29.33264
310.4003 29.77032
310.8824 30.36295
311.3646 31.17961
311.8467 32.08661
312.3288 32.83093
312.8109 33.34607
313.2930 33.94189
313.7751 34.76154
314.2573 35.79417
314.7394 37.01186
315.2215 38.37793
315.7036 40.03873
316.1857 42.23445
316.6678 44.91837
317.1500 47.41881
317.6321 49.59647
318.1142 51.46478
318.5963 53.16356
319.0784 54.71657
319.5605 55.71420
320.0427 55.80789
320.5248 55.08134
321.0069 53.95959
321.4890 52.29480
321.9711 50.52621
322.4532 49.06516
322.9354 47.86765
323.4175 46.69882
323.8996 45.59775
324.3817 44.42470
324.8638 42.72595
325.3459 40.26428
325.8281 37.76135
326.3102 35.83151
326.7923 34.27765
327.2744 32.67256
327.7565 30.61458
328.2386 28.55956
328.7208 27.32738
329.2029 27.06267
329.6850 26.80951
330.1671 25.93098
330.6492 24.76585
331.1313 23.81369
331.6135 23.26657
332.0956 22.78542
332.5777 21.96175
333.0598 20.81577
333.5419 19.87776
334.0240 19.46471
334.5062 19.29030
334.9883 18.97716
335.4704 18.50735
335.9525 17.89236
336.4346 17.07729
336.9167 16.11072
337.3989 15.15848
337.8810 14.16739
338.3631 13.36043
338.8452 13.09515
339.3273 13.31340
339.8094 13.36658
340.2916 12.91115
340.7737 12.15358
341.2558 11.38741
341.7379 10.60333
342.2200 9.989777
342.7021 9.883698
343.1843 10.10110
343.6664 10.06651
344.1485 9.402710
344.6306 8.613464
345.1127 8.269180
345.5948 8.360886
346.0770 8.365738
346.5591 7.866928
347.0412 7.116364
347.5233 6.812180
348.0054 7.265488
348.4875 7.667740
348.9697 7.463837
349.4518 6.802139
349.9339 6.181351
350.4160 5.784866
350.8981 5.499084
351.3802 5.084015
351.8624 4.481247
352.3445 4.063278
352.8266 4.079559
353.3087 4.313141
353.7908 4.467804
354.2729 4.493622
354.7551 4.366196
355.2372 3.999832
355.7193 3.387238
356.2014 2.868271
356.6835 2.537766
357.1656 2.270569
357.6478 1.947815
358.1299 1.574295
358.6120 1.248093
359.0941 1.053802
359.5762 0.9681240
360.0583 0.8107450
360.5405 0.5487670
361.0226 0.2565920
361.5047 6.9885001E-02
361.9868 0.4053190
362.4689 0.7317050
362.9510 1.060440
363.4332 1.306229
363.9153 1.213989
364.3974 0.4991150
364.8795 2.8152000E-02
365.3616 1.2573000E-02
365.8438 0.2478940
366.3259 0.5673220
366.8080 0.9223330
367.2901 1.246964
367.7722 1.461655
368.2543 1.542664
368.7365 1.583466
369.2186 1.699875
369.7007 1.679260
370.1828 1.261078
370.6649 0.5575260
371.1470 4.6112001E-02
371.6291 0.2684940
372.1112 0.1350250
372.5934 6.7474000E-02
373.0755 0.6273800
373.5576 0.9182740
374.0397 0.6096800
374.5218 1.3580000E-03
375.0039 0.4706570
375.4861 0.6214900
375.9682 0.6151890
376.4503 0.8296810
376.9324 1.632843
377.4145 2.056046
377.8966 1.758926
378.3788 1.351181
378.8609 1.292419
379.3430 1.630188
379.8251 2.098343
380.3072 2.424957
380.7893 2.602478
381.2715 2.678665
381.7536 2.451767
382.2357 2.321289
382.7178 2.474945
383.1999 2.822311
383.6820 3.169403
384.1642 3.392105
384.6463 3.534012
385.1284 3.772522
385.6105 4.170959
386.0926 4.567108
386.5747 5.000854
387.0569 5.384674
387.5390 5.644440
388.0211 5.758881
388.5032 5.735046
388.9853 5.465912
389.4674 4.828171
389.9496 4.638916
390.4317 5.625229
390.9138 6.557220
391.3959 6.693222
391.8780 6.169281
392.3601 5.670792
392.8423 5.834946
393.3244 6.461807
393.8065 6.517136
394.2886 5.724548
394.7707 4.899414
395.2528 4.310883
395.7350 3.955994
396.2171 3.901749
396.6992 4.274811
397.1813 4.725708
397.6634 4.728561
398.1455 4.255524
398.6277 4.005203
399.1098 4.373291
399.5919 4.912750
400.0740 5.148056
400.5561 5.057999
401.0382 4.860153
401.5204 4.669388
402.0025 4.462067
402.4846 4.092468
402.9667 3.439011
403.4488 2.977798
403.9309 3.303543
404.4131 4.210968
404.8952 4.991425
405.3773 5.568649
405.8594 5.936325
406.3415 5.822723
406.8236 5.350739
407.3058 5.427017
407.7879 6.693497
408.2700 8.623123
408.7521 9.877808
409.2342 10.37169
409.7163 10.51112
410.1985 10.04225
410.6806 9.419525
411.1627 9.345093
411.6448 9.988861
412.1269 10.96954
412.6090 11.87402
413.0912 12.69701
413.5733 13.41000
414.0554 14.05447
414.5375 14.55756
415.0196 14.86986
415.5017 15.00233
415.9839 14.96371
416.4660 14.73039
416.9481 14.37837
417.4302 14.27715
417.9123 14.62772
418.3944 14.99323
418.8766 15.35510
419.3587 15.68102
419.8408 15.95007
420.3229 16.15909
420.8050 16.32640
421.2871 16.44012
421.7693 16.40891
422.2514 16.82431
422.7335 18.40630
423.2156 19.66461
423.6977 19.65906
424.1798 18.83156
424.6620 18.29744
425.1441 18.83934
425.6262 20.14320
426.1083 21.01552
426.5904 21.19160
427.0725 21.47452
427.5547 22.29327
428.0368 23.15248
428.5189 23.61005
429.0010 23.61702
429.4831 23.55884
429.9652 23.83327
430.4474 24.38420
430.9295 24.69987
431.4116 24.75302
431.8937 24.60764
432.3758 24.37169
432.8579 24.01176
433.3400 23.42859
433.8221 22.48456
434.3043 21.32384
434.7864 20.14226
435.2685 18.92242
435.7506 17.91759
436.2327 17.26385
436.7148 16.82970
437.1970 16.39305
437.6791 15.89815
438.1612 15.50607
438.6433 15.38937
439.1254 15.44728
439.6075 15.50285
440.0897 15.53754
440.5718 15.46449
441.0539 15.15274
441.5360 14.60158
442.0181 14.12283
442.5002 13.56967
442.9824 13.23650
443.4645 13.46414
443.9466 14.09843
444.4287 14.70822
444.9108 15.08224
445.3929 15.19748
445.8751 15.01387
446.3572 14.35007
446.8393 13.67159
447.3214 12.90642
447.8035 12.19193
448.2856 11.65134
448.7678 11.29688
449.2499 11.06133
449.7320 10.91136
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