#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-06-07 11:26:28 +0300 (Thu, 07 Jun 2018) $ #$Revision: 1092 $ #$URL: svn://172.16.1.111/rod/cif/1/00/05/1000530.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_1000530 loop_ _publ_author_name 'Zaitsev, A. N.' 'Chakhmouradian, A. R.' 'Siidra, O. I.' 'Spratt, J.' 'Williams, C. T.' 'Stanley, C. J.' 'Petrov, S. V.' 'Britvin, S. N.' 'Polyakova, E. A.' _publ_section_title ; Fluorine-, yttrium- and lanthanide-rich cerianite-(Ce) from carbonatitic rocks of the Kerimasi volcano and surrounding explosion craters, Gregory Rift, northern Tanzania ; _journal_name_full 'Mineralogical Magazine' _journal_page_first 2813 _journal_page_last 2822 _journal_paper_doi 10.1180/minmag.2011.075.6.2813 _journal_volume 75 _journal_year 2011 _chemical_compound_source 'Gregory Rift, northern Tanzania' _chemical_formula_sum 'Ce0.62 Dy0.02 Er0.01 F0.24 Gd0.02 La0.03 Nd0.06 O1.68 Pr0.01 Sm0.01 Y0.2 Yb0.02' _chemical_name_mineral Cerianite-(Ce) _space_group_IT_number 225 _symmetry_space_group_name_Hall '-F 4 2 3' _symmetry_space_group_name_H-M 'F m -3 m' _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_length_a 5.4203 _cell_length_b 5.4203 _cell_length_c 5.4203 _cell_volume 159.247 _exptl_crystal_density_diffrn 6.813 _cod_original_formula_sum '(Ce.62 Y.2 Nd.06 La.03 Pr.01 Sm.01 Gd.02 Dy.02 Er.01 Yb.02) O1.68 F.24' _cod_database_code 9016030 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type helium-neon _raman_measurement_device.excitation_laser_wavelength 780 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 12 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R050379.rod _rod_data_source.block 3500000 _rod_database.code 1000530 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9016030 COD http://www.crystallography.net/cod/9016030.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 144.5920 0.0000000E+00 145.0741 0.1049650 145.5563 0.4443820 146.0384 0.7800290 146.5205 1.124374 147.0026 1.268646 147.4847 0.8235930 147.9668 0.4498140 148.4490 0.4912260 148.9311 1.072083 149.4132 1.758438 149.8953 1.813202 150.3774 0.7309110 150.8595 2.3300000E-02 151.3417 0.1262210 151.8238 2.5832999E-02 152.3059 0.3431700 152.7880 0.7671810 153.2701 1.260345 153.7522 1.709747 154.2344 2.024139 154.7165 2.347855 155.1986 2.795410 155.6807 3.231125 156.1628 3.461411 156.6449 3.376953 157.1271 3.062454 157.6092 2.856216 158.0913 2.715851 158.5734 2.700211 159.0555 2.947281 159.5376 3.416840 160.0198 3.874313 160.5019 3.962753 160.9840 3.800629 161.4661 3.933914 161.9482 4.655380 162.4303 5.283981 162.9125 5.507843 163.3946 5.766907 163.8767 5.617935 164.3588 5.289505 164.8409 4.945404 165.3230 4.826950 165.8052 5.153641 166.2873 5.565872 166.7694 5.505310 167.2515 4.801315 167.7336 4.212021 168.2157 4.337418 168.6979 4.724228 169.1800 4.828415 169.6621 4.351776 170.1442 3.494003 170.6263 2.792755 171.1084 2.228409 171.5906 1.890625 172.0727 2.012177 172.5548 2.301132 173.0369 2.323242 173.5190 1.758514 174.0011 0.7026060 174.4833 3.2623000E-02 174.9654 0.1886900 175.4475 0.2450410 175.9296 0.2340240 176.4117 0.1975860 176.8938 0.1826170 177.3760 0.2239070 177.8581 0.3223110 178.3402 0.4492190 178.8223 0.7526700 179.3044 0.9400790 179.7865 0.7914890 180.2687 0.4064940 180.7508 0.1055760 181.2329 0.2059630 181.7150 0.7670440 182.1971 0.8674930 182.6792 7.8720003E-02 183.1614 0.7447200 183.6435 1.026367 184.1256 0.7795100 184.6077 0.5103610 185.0898 0.6753850 185.5719 1.317276 186.0541 1.919464 186.5362 2.520447 187.0183 3.048096 187.5004 3.453812 187.9825 3.736511 188.4646 3.843033 188.9468 3.488800 189.4289 2.839935 189.9110 2.631668 190.3931 3.389481 190.8752 4.576828 191.3573 5.392105 191.8395 5.747314 192.3216 5.809891 192.8037 5.432053 193.2858 4.843292 193.7679 4.610031 194.2500 5.232758 194.7322 6.433060 195.2143 7.326569 195.6964 7.826065 196.1785 8.089615 196.6606 7.996872 197.1427 7.758377 197.6249 7.850937 198.1070 8.748901 198.5891 10.34775 199.0712 11.59112 199.5533 12.35147 200.0354 12.84071 200.5176 12.92659 200.9997 12.79720 201.4818 12.84587 201.9639 13.46005 202.4460 14.66591 202.9281 15.51692 203.4103 15.56795 203.8924 15.64088 204.3745 16.13919 204.8566 16.89485 205.3387 17.42813 205.8208 17.27913 206.3030 16.35017 206.7851 15.65038 207.2672 15.31659 207.7493 15.05513 208.2314 14.74139 208.7135 14.39435 209.1957 14.13069 209.6778 14.09814 210.1599 14.36192 210.6420 14.27127 211.1241 13.59776 211.6062 12.84410 212.0884 12.14816 212.5705 11.57684 213.0526 11.28221 213.5347 11.48425 214.0168 12.26970 214.4989 12.53162 214.9811 11.71527 215.4632 10.85214 215.9453 10.66040 216.4274 11.15985 216.9095 11.86880 217.3916 12.43228 217.8737 12.83080 218.3559 13.08844 218.8380 12.99672 219.3201 12.90240 219.8022 13.14615 220.2843 13.75418 220.7664 14.43022 221.2486 14.92804 221.7307 15.29630 222.2128 15.71957 222.6949 16.34082 223.1770 16.96893 223.6591 17.32411 224.1413 17.35509 224.6234 17.41893 225.1055 17.83817 225.5876 18.46861 226.0697 19.05815 226.5518 19.44574 227.0340 19.80304 227.5161 20.42542 227.9982 21.39198 228.4803 22.34619 228.9624 23.07805 229.4445 23.66684 229.9267 24.20082 230.4088 24.67635 230.8909 25.13646 231.3730 25.68819 231.8551 26.40674 232.3372 27.00179 232.8194 27.19957 233.3015 27.28430 233.7836 27.63402 234.2657 28.48836 234.7478 29.56160 235.2299 30.15364 235.7121 29.96164 236.1942 29.88617 236.6763 30.18773 237.1584 30.71365 237.6405 31.39658 238.1227 32.25751 238.6048 33.11218 239.0869 33.41339 239.5690 32.64671 240.0511 32.17928 240.5332 32.64703 241.0154 33.36189 241.4975 33.62669 241.9796 33.14326 242.4617 32.21172 242.9438 31.60475 243.4259 31.63342 243.9081 31.49954 244.3902 30.98930 244.8723 30.35422 245.3544 29.87444 245.8365 29.65118 246.3186 29.51700 246.8008 29.07365 247.2829 28.02446 247.7650 27.07675 248.2471 26.29021 248.7292 25.59578 249.2113 24.94817 249.6935 24.32697 250.1756 23.71091 250.6577 23.05988 251.1398 22.40254 251.6219 21.65785 252.1040 20.55855 252.5862 19.52020 253.0683 19.07758 253.5504 19.34328 254.0325 19.76897 254.5146 19.43159 254.9967 17.67686 255.4789 16.33556 255.9610 15.63979 256.4431 15.22322 256.9252 14.81657 257.4073 14.34525 257.8894 13.81157 258.3716 13.20738 258.8537 12.46991 259.3358 11.86401 259.8179 11.44562 260.3000 11.11641 260.7821 10.76611 261.2643 10.38847 261.7464 10.11627 262.2285 10.11040 262.7106 10.43933 263.1927 10.73256 263.6748 11.03903 264.1570 11.27005 264.6391 11.29141 265.1212 11.10112 265.6033 10.87871 266.0854 10.78609 266.5675 10.83408 267.0497 10.94020 267.5318 11.13094 268.0139 11.33418 268.4960 11.44835 268.9781 11.48572 269.4602 11.66374 269.9424 12.23389 270.4245 13.10358 270.9066 13.66112 271.3887 13.48262 271.8708 13.26355 272.3529 13.56541 272.8351 14.37390 273.3172 15.31828 273.7993 16.23790 274.2814 17.12129 274.7635 17.95744 275.2456 18.62198 275.7278 19.33511 276.2099 20.29060 276.6920 21.46127 277.1741 22.60298 277.6562 23.59514 278.1383 24.46198 278.6205 25.25471 279.1026 25.89185 279.5847 26.61064 280.0668 27.51422 280.5489 28.60788 281.0310 29.99451 281.5132 31.99097 281.9953 34.07564 282.4774 35.49892 282.9595 36.19635 283.4416 36.68178 283.9237 37.05063 284.4059 37.38448 284.8880 38.09995 285.3701 39.44965 285.8522 41.04762 286.3343 42.46567 286.8164 43.70973 287.2986 44.96767 287.7807 46.37816 288.2628 47.88014 288.7449 49.26680 289.2270 50.47749 289.7091 51.68188 290.1913 53.06474 290.6734 54.57336 291.1555 56.06218 291.6376 57.51482 292.1197 58.88423 292.6018 60.04521 293.0840 60.90259 293.5661 61.74339 294.0482 62.81390 294.5303 63.99554 295.0124 65.09027 295.4945 66.01515 295.9767 66.80063 296.4588 67.63080 296.9409 68.69249 297.4230 69.14903 297.9051 68.06987 298.3872 66.28424 298.8694 64.71333 299.3515 63.65683 299.8336 62.84413 300.3157 62.08018 300.7978 61.45944 301.2799 60.27803 301.7621 57.88376 302.2442 54.96465 302.7263 52.03056 303.2084 49.14983 303.6905 46.36183 304.1726 43.68314 304.6548 41.11909 305.1369 38.67139 305.6190 36.40369 306.1011 34.19777 306.5832 31.90305 307.0653 29.52220 307.5475 27.32179 308.0296 25.67307 308.5117 24.51447 308.9938 22.99998 309.4759 20.58629 309.9580 18.33719 310.4402 17.08244 310.9223 16.62335 311.4044 16.17584 311.8865 15.17529 312.3686 13.76520 312.8507 12.56133 313.3329 11.62045 313.8150 10.81526 314.2971 10.15401 314.7792 9.550262 315.2613 8.824860 315.7434 7.800781 316.2256 6.664139 316.7077 5.858704 317.1898 5.509674 317.6719 5.129501 318.1540 4.431732 318.6361 3.614792 319.1183 2.884384 319.6004 2.301300 320.0825 1.816376 320.5646 1.353806 321.0467 0.9014590 321.5288 0.5513920 322.0110 0.5019230 322.4931 0.4634860 322.9752 0.1592710 323.4573 0.4597020 323.9394 1.095993 324.4215 1.431992 324.9037 1.475327 325.3858 1.606293 325.8679 1.908051 326.3500 2.307632 326.8321 2.852585 327.3142 3.491821 327.7964 3.944443 328.2785 3.924408 328.7606 3.529358 329.2427 3.208893 329.7248 2.929214 330.2069 2.834885 330.6891 3.071289 331.1712 3.532181 331.6533 4.011551 332.1354 4.520355 332.6175 4.937592 333.0996 4.919098 333.5818 4.287521 334.0639 3.789139 334.5460 4.039474 335.0281 4.552826 335.5102 4.785675 335.9923 4.555038 336.4745 4.105545 336.9566 3.726852 337.4387 3.434296 337.9208 2.982239 338.4029 1.968079 338.8850 1.003983 339.3671 0.7634580 339.8492 1.337128 340.3314 2.047089 340.8135 2.448578 341.2956 2.564651 341.7777 2.505936 342.2598 2.173248 342.7419 1.839233 343.2241 1.802277 343.7062 1.996078 344.1883 2.090088 344.6704 1.984268 345.1525 1.660889 345.6346 0.9839320 346.1168 0.1856380 346.5989 1.275940 347.0810 1.724060 347.5631 1.810013 348.0452 2.011139 348.5273 2.491241 349.0095 3.097870 349.4916 3.752563 349.9737 4.457947 350.4558 4.912155 350.9379 4.814804 351.4200 4.461639 351.9022 4.306992 352.3843 4.354568 352.8664 4.646011 353.3485 5.261566 353.8306 6.156616 354.3127 7.185349 354.7949 8.389069 355.2770 9.587708 355.7591 10.54446 356.2412 11.26549 356.7233 11.97491 357.2054 12.76797 357.6876 13.59396 358.1697 14.34384 358.6518 14.98682 359.1339 15.67171 359.6160 16.46416 360.0981 17.40009 360.5803 18.61911 361.0624 20.53056 361.5445 22.43390 362.0266 23.60863 362.5087 24.14374 362.9908 24.76279 363.4730 25.85004 363.9551 27.32124 364.4372 28.88957 364.9193 30.54097 365.4014 32.28433 365.8835 34.12029 366.3657 36.03938 366.8478 38.07390 367.3299 40.24924 367.8120 42.43875 368.2941 44.44479 368.7762 46.22990 369.2584 48.00468 369.7405 49.60292 370.2226 51.30586 370.7047 53.41248 371.1868 55.96469 371.6689 58.75554 372.1511 61.72388 372.6332 64.87962 373.1153 67.41519 373.5974 68.97470 374.0795 70.34880 374.5616 71.68521 375.0438 73.14238 375.5259 75.08780 376.0080 77.73508 376.4901 80.91216 376.9722 84.03526 377.4543 87.35269 377.9365 90.29559 378.4186 92.62225 378.9007 94.62598 379.3828 96.53899 379.8649 98.46259 380.3470 100.4902 380.8292 102.7618 381.3113 105.4473 381.7934 107.8034 382.2755 109.6329 382.7576 111.4038 383.2397 113.3812 383.7219 115.5280 384.2040 117.6137 384.6861 119.4375 385.1682 121.0152 385.6503 122.6078 386.1324 124.2719 386.6146 125.9739 387.0967 127.8288 387.5788 129.6487 388.0609 131.2239 388.5430 132.4398 389.0251 133.3126 389.5073 133.8679 389.9894 133.9008 390.4715 134.0413 390.9536 134.5568 391.4357 135.0768 391.9178 135.3593 392.4000 135.3231 392.8821 135.0327 393.3642 134.5496 393.8463 133.8964 394.3284 133.2736 394.8105 132.7572 395.2927 132.1559 395.7748 131.4944 396.2569 130.7420 396.7390 129.7451 397.2211 128.3133 397.7032 126.6616 398.1854 125.5390 398.6675 125.3945 399.1496 124.4854 399.6317 121.6037 400.1138 118.2253 400.5959 115.4481 401.0781 113.4452 401.5602 111.5928 402.0423 109.3554 402.5244 106.7759 403.0065 104.1812 403.4886 101.5616 403.9708 99.02811 404.4529 96.71863 404.9350 94.54736 405.4171 92.24544 405.8992 89.58588 406.3813 86.79807 406.8635 84.19547 407.3456 81.77435 407.8277 79.54189 408.3098 77.49945 408.7919 75.64398 409.2740 73.99225 409.7562 72.63214 410.2383 71.23384 410.7204 69.49557 411.2025 67.54639 411.6846 65.74686 412.1667 64.18625 412.6489 62.77747 413.1310 61.38045 413.6131 59.98224 414.0952 58.87030 414.5773 58.31242 415.0594 57.91443 415.5416 57.21005 416.0237 56.23868 416.5058 55.54607 416.9879 55.56592 417.4700 56.13824 417.9521 56.37781 418.4343 56.00793 418.9164 55.69666 419.3985 55.53491 419.8806 55.56761 420.3627 55.94547 420.8448 56.71191 421.3270 57.57162 421.8091 58.04613 422.2912 57.82700 422.7733 58.13324 423.2554 59.36880 423.7375 60.73029 424.2197 61.59677 424.7018 62.12363 425.1839 62.92786 425.6660 64.46759 426.1481 66.64560 426.6302 68.86206 427.1124 70.97081 427.5945 73.29924 428.0766 76.12048 428.5587 79.05136 429.0408 81.71976 429.5229 84.01247 430.0051 86.13284 430.4872 88.26273 430.9693 90.25400 431.4514 92.83350 431.9335 96.71466 432.4156 100.6127 432.8978 103.7350 433.3799 106.4456 433.8620 109.7856 434.3441 114.5398 434.8262 120.2263 435.3083 125.3912 435.7905 129.7673 436.2726 134.3155 436.7547 139.3219 437.2368 144.7208 437.7189 150.5045 438.2010 156.6809 438.6832 163.1257 439.1653 169.9352 439.6474 176.9808 440.1295 183.5411 440.6116 189.1743 441.0938 194.9176 441.5759 201.5027 442.0580 208.8410 442.5401 216.9199 443.0222 226.4025 443.5043 236.1300 443.9865 245.0791 444.4686 253.2450 444.9507 260.8699 445.4328 267.8194 445.9149 274.5447 446.3970 282.0847 446.8792 290.6044 447.3613 299.2196 447.8434 307.8621 448.3255 316.3963 448.8076 324.5992 449.2897 332.4838 449.7719 340.3080 450.2540 348.3569 450.7361 356.6835 451.2182 364.5942 451.7003 372.0537 452.1824 379.2715 452.6646 386.2179 453.1467 392.9983 453.6288 399.8872 454.1109 407.0249 454.5930 413.9276 455.0751 419.7210 455.5573 424.3826 456.0394 427.8580 456.5215 429.8449 457.0036 431.0751 457.4857 432.1136 457.9678 432.8520 458.4500 432.7699 458.9321 431.4564 459.4142 428.9806 459.8963 425.7505 460.3784 421.8533 460.8605 416.9052 461.3427 410.6797 461.8248 403.5294 462.3069 395.6175 462.7890 387.0027 463.2711 378.1176 463.7532 369.6817 464.2354 361.5374 464.7175 352.3419 465.1996 341.4815 465.6817 330.2966 466.1638 319.6402 466.6459 309.3890 467.1281 299.2406 467.6102 289.0665 468.0923 279.0319 468.5744 269.3627 469.0565 259.9731 469.5386 250.9795 470.0208 242.5323 470.5029 234.3465 470.9850 225.8755 471.4671 216.9041 471.9492 208.6536 472.4313 201.8426 472.9135 195.6287 473.3956 189.0184 473.8777 181.9793 474.3598 175.1513 474.8419 169.1176 475.3240 163.7609 475.8062 158.0493 476.2883 151.2189 476.7704 144.9947 477.2525 140.0556 477.7346 135.7769 478.2167 131.5533 478.6989 127.1570 479.1810 122.5861 479.6631 117.6595 480.1452 112.1918 480.6273 107.4989 481.1094 104.2711 481.5916 101.1395 482.0737 97.62926 482.5558 93.91486 483.0379 90.35779 483.5200 87.12439 484.0021 84.06232 484.4843 80.89502 484.9664 77.60411 485.4485 74.20668 485.9306 70.36737 486.4127 66.72333 486.8948 63.74942 487.3770 61.38101 487.8591 59.22035 488.3412 57.13292 488.8233 55.08333 489.3054 53.04669 489.7875 51.05376 490.2697 48.89700 490.7518 46.34515 491.2339 43.65251 491.7160 41.26663 492.1981 39.23271 492.6802 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