#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-06-07 11:27:46 +0300 (Thu, 07 Jun 2018) $
#$Revision: 1112 $
#$URL: svn://172.16.1.111/rod/cif/1/00/05/1000544.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000544
loop_
_publ_author_name
'Basso, R.'
'Cabella, R.'
'Lucchetti, G.'
'Martinelli, A.'
'Palenzona, A.'
_publ_section_title
;
 Vanadiocarpholite, Mn2+V3+Al(Si2O6)(OH)4, a new mineral from the
 Molinello mine, northern Apennines, Italy Note: sample VrC Locality:
 Molinello mine, northern Apennines, Italy
;
_journal_name_full               'European Journal of Mineralogy'
_journal_page_first              501
_journal_page_last               507
_journal_paper_doi               10.1127/0935-1221/2005/0017-0501
_journal_volume                  17
_journal_year                    2005
_chemical_compound_source        R060608
_chemical_formula_sum
'Al3.02 H8 K0.012 Mg0.26 Mn1.74 O20 Si4 V0.98'
_chemical_name_mineral           Carpholite
_space_group_IT_number           68
_symmetry_space_group_name_Hall  '-C 2a 2ac'
_symmetry_space_group_name_H-M   'C c c a :2'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   13.840
_cell_length_b                   20.452
_cell_length_c                   5.143
_cell_volume                     1455.755
_exptl_crystal_density_diffrn    3.076
_cod_original_sg_symbol_H-M      'C c c a'
_cod_original_formula_sum        'K.012 (Mn1.74 Mg.26) Al3.02 V.98 Si4 O20 H8'
_cod_database_code               9005714
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R060608.rod
_rod_data_source.block           3500000
_rod_database.code               1000544
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9005714 COD http://www.crystallography.net/cod/9005714.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
106.0234 0.0000000E+00
106.5055 0.2551270
106.9877 0.3930660
107.4698 8.579102
107.9519 27.37866
108.4340 49.00977
108.9161 68.42603
109.3982 87.70190
109.8804 110.8372
110.3625 136.7656
110.8446 164.6365
111.3267 198.4258
111.8088 249.0493
112.2909 300.9486
112.7731 353.6884
113.2552 402.3236
113.7373 424.8806
114.2194 418.0461
114.7015 368.8340
115.1836 317.8845
115.6658 262.2329
116.1479 207.3506
116.6300 156.9772
117.1121 111.6913
117.5942 71.77234
118.0763 41.15723
118.5584 20.68982
119.0406 6.175903
119.5227 3.028931
120.0048 7.024048
120.4869 5.747437
120.9690 1.830322
121.4511 13.96533
121.9333 26.41382
122.4154 38.40173
122.8975 49.47754
123.3796 59.21667
123.8617 67.19543
124.3438 72.19275
124.8260 71.02686
125.3081 67.41223
125.7902 64.01636
126.2723 60.61658
126.7544 58.60339
127.2365 59.85608
127.7187 63.22913
128.2008 70.46790
128.6829 84.49646
129.1650 101.5413
129.6471 117.0684
130.1292 129.2795
130.6114 137.1763
131.0935 138.4613
131.5756 130.3284
132.0577 120.0166
132.5398 108.8157
133.0219 97.21985
133.5041 84.94214
133.9862 71.52612
134.4683 56.36438
134.9504 45.09229
135.4325 40.92493
135.9146 37.89954
136.3968 32.12109
136.8789 23.49829
137.3610 15.12769
137.8431 11.12695
138.3252 13.28479
138.8073 14.34143
139.2895 13.13135
139.7716 11.56152
140.2537 11.90039
140.7358 14.80896
141.2179 17.43347
141.7000 18.01587
142.1821 17.11426
142.6643 16.00549
143.1464 15.22949
143.6285 14.70227
144.1106 13.78284
144.5927 11.53723
145.0748 9.884766
145.5570 10.74097
146.0391 13.99402
146.5212 16.81018
147.0033 15.66687
147.4854 9.929443
147.9675 6.081787
148.4497 7.969360
148.9318 10.48816
149.4139 10.75244
149.8960 8.166138
150.3781 4.234497
150.8602 1.134644
151.3424 0.9097900
151.8245 2.222046
152.3066 2.606445
152.7887 2.602539
153.2708 2.852173
153.7529 3.543823
154.2351 4.151489
154.7172 3.339722
155.1993 0.2766110
155.6814 3.486450
156.1635 8.070801
156.6456 13.23352
157.1278 18.99573
157.6099 25.45276
158.0920 32.09753
158.5741 36.65479
159.0562 36.03345
159.5383 37.05103
160.0205 42.03418
160.5026 49.95312
160.9847 58.64380
161.4668 67.19922
161.9489 75.30945
162.4310 81.90881
162.9131 88.76636
163.3953 92.90125
163.8774 95.69373
164.3595 93.66296
164.8416 89.09058
165.3237 82.83081
165.8058 74.84460
166.2880 65.24646
166.7701 52.33752
167.2522 39.06604
167.7343 29.12573
168.2164 23.10413
168.6985 17.75641
169.1807 10.28790
169.6628 2.603210
170.1449 2.716858
170.6270 3.999939
171.1091 2.754944
171.5912 2.311523
172.0734 3.035339
172.5555 3.839233
173.0376 4.462769
173.5197 4.895081
174.0018 5.211914
174.4839 5.578674
174.9661 5.830017
175.4482 4.921448
175.9303 1.778076
176.4124 1.292236
176.8945 3.896423
177.3766 5.704163
177.8588 6.761047
178.3409 7.276428
178.8230 7.613586
179.3051 8.151672
179.7872 9.024963
180.2693 9.664612
180.7515 9.650879
181.2336 9.177979
181.7157 8.812744
182.1978 9.069031
182.6799 10.03540
183.1620 10.34979
183.6441 8.335632
184.1263 7.242371
184.6084 9.467896
185.0905 14.58319
185.5726 19.80347
186.0547 22.36597
186.5368 21.77246
187.0190 23.09735
187.5011 27.35785
187.9832 32.69397
188.4653 37.92291
188.9474 42.87927
189.4296 47.77008
189.9117 52.95001
190.3938 58.37860
190.8759 63.20166
191.3580 66.42853
191.8401 69.39355
192.3223 73.76392
192.8044 79.91058
193.2865 86.62244
193.7686 92.82031
194.2507 98.62036
194.7328 104.3926
195.2150 110.1887
195.6971 116.0565
196.1792 122.1866
196.6613 128.7310
197.1434 135.1038
197.6255 140.8287
198.1077 146.1094
198.5898 151.3234
199.0719 156.3234
199.5540 161.3186
200.0361 167.3436
200.5182 175.0922
201.0004 183.0176
201.4825 189.9736
201.9646 196.3569
202.4467 203.0911
202.9288 211.0105
203.4109 220.0986
203.8930 228.9218
204.3752 236.7483
204.8573 244.9776
205.3394 254.0283
205.8215 263.7930
206.3036 274.1696
206.7857 284.9924
207.2679 296.2366
207.7500 307.4876
208.2321 320.5094
208.7142 331.7480
209.1963 340.3976
209.6784 346.3285
210.1606 349.5941
210.6427 350.1896
211.1248 348.0876
211.6069 343.1911
212.0890 336.1215
212.5711 326.1725
213.0533 312.1976
213.5354 294.8448
214.0175 275.7976
214.4996 256.6432
214.9817 237.4417
215.4638 217.6655
215.9460 196.1654
216.4281 175.1306
216.9102 155.1850
217.3923 136.5762
217.8744 119.2563
218.3565 103.1895
218.8387 88.43542
219.3208 76.06165
219.8029 66.52777
220.2850 58.58942
220.7671 51.88440
221.2492 46.21661
221.7314 40.92462
222.2135 35.28241
222.6956 29.32281
223.1777 24.84546
223.6598 22.71582
224.1419 21.37476
224.6240 19.62494
225.1062 17.41553
225.5883 15.51526
226.0704 14.57227
226.5525 14.58801
227.0346 14.87177
227.5167 14.97766
227.9989 15.34229
228.4810 17.25421
228.9631 20.98206
229.4452 24.38263
229.9273 25.66223
230.4094 25.31006
230.8916 24.74310
231.3737 24.11945
231.8558 23.43585
232.3379 22.61139
232.8200 21.61597
233.3021 20.82623
233.7843 20.89838
234.2664 21.36786
234.7485 21.39404
235.2306 20.72980
235.7127 19.55292
236.1948 17.79327
236.6770 15.11676
237.1591 13.18304
237.6412 13.75299
238.1233 15.26569
238.6054 15.93665
239.0875 14.89459
239.5697 13.24512
240.0518 12.88733
240.5339 14.26709
241.0160 15.53388
241.4981 15.68207
241.9802 15.47461
242.4624 15.63934
242.9445 16.45374
243.4266 17.70410
243.9087 18.97260
244.3908 20.14343
244.8729 21.61163
245.3550 24.26202
245.8372 26.85962
246.3193 28.27734
246.8014 28.11157
247.2835 26.90961
247.7656 25.44214
248.2477 23.38129
248.7299 21.88354
249.2120 21.87030
249.6941 22.00446
250.1762 21.09430
250.6583 18.81006
251.1404 16.02295
251.6226 14.12897
252.1047 13.34064
252.5868 13.07275
253.0689 12.97455
253.5510 13.46307
254.0331 15.03906
254.5153 17.75085
254.9974 20.93268
255.4795 23.58600
255.9616 25.46350
256.4437 27.30670
256.9258 29.16364
257.4080 30.98053
257.8901 32.93732
258.3722 34.96051
258.8543 36.59766
259.3364 37.20209
259.8185 36.43713
260.3007 35.39697
260.7828 34.26373
261.2649 32.77216
261.7470 30.66779
262.2291 27.97217
262.7112 25.01514
263.1934 22.18719
263.6755 19.67322
264.1576 16.55188
264.6397 12.19659
265.1218 7.887756
265.6039 4.240295
266.0861 1.336121
266.5682 0.9952390
267.0503 2.885864
267.5324 4.286682
268.0145 5.452332
268.4966 6.454590
268.9788 7.216431
269.4609 7.914429
269.9430 8.392883
270.4251 8.086426
270.9072 6.364441
271.3893 3.148254
271.8715 1.165588
272.3536 1.752625
272.8357 1.994751
273.3178 0.8781740
273.7999 1.579102
274.2820 5.188538
274.7642 9.977661
275.2463 15.81750
275.7284 21.00824
276.2105 24.46179
276.6926 28.59277
277.1747 34.65582
277.6568 42.00360
278.1389 49.23499
278.6211 55.60553
279.1032 61.27185
279.5853 66.91077
280.0674 73.75299
280.5495 79.19763
281.0316 83.13989
281.5138 85.21216
281.9959 84.56879
282.4780 80.73010
282.9601 74.34644
283.4422 66.77045
283.9243 56.43677
284.4065 47.92712
284.8886 42.94940
285.3707 40.15442
285.8528 37.53619
286.3349 34.40424
286.8170 31.52649
287.2992 30.36743
287.7813 31.40796
288.2634 32.30975
288.7455 32.53467
289.2276 32.50732
289.7097 32.70929
290.1919 33.24731
290.6740 34.04114
291.1561 35.15295
291.6382 36.68903
292.1203 37.61469
292.6024 37.88678
293.0846 37.46014
293.5667 36.09955
294.0488 33.78351
294.5309 31.12500
295.0130 28.52173
295.4951 26.02466
295.9773 24.15948
296.4594 23.11432
296.9415 22.56903
297.4236 22.35175
297.9057 22.44281
298.3878 22.76508
298.8700 23.30511
299.3521 24.03772
299.8342 24.76331
300.3163 25.33374
300.7984 26.02808
301.2805 26.92780
301.7627 28.06378
302.2448 29.62012
302.7269 31.83746
303.2090 34.46033
303.6911 36.69714
304.1732 38.38483
304.6554 40.00427
305.1375 41.83923
305.6196 43.77850
306.1017 45.43323
306.5838 46.52911
307.0659 47.53943
307.5481 49.61017
308.0302 53.17889
308.5123 55.95239
308.9944 56.68274
309.4765 56.24133
309.9586 56.01782
310.4408 56.32690
310.9229 57.07263
311.4050 58.27917
311.8871 59.96094
312.3692 61.56842
312.8513 63.29132
313.3335 64.74072
313.8156 65.35901
314.2977 65.03949
314.7798 64.32568
315.2619 63.61554
315.7440 62.91089
316.2262 62.28430
316.7083 61.98907
317.1904 61.59644
317.6725 60.84509
318.1546 59.70258
318.6367 57.96478
319.1188 55.05182
319.6010 51.49780
320.0831 49.57062
320.5652 50.59595
321.0473 52.03827
321.5294 52.39105
322.0115 51.80707
322.4937 51.19800
322.9758 51.01398
323.4579 51.20642
323.9400 51.54303
324.4221 51.92181
324.9042 52.47418
325.3864 52.90076
325.8685 53.57208
326.3506 55.32153
326.8327 58.52570
327.3148 62.35608
327.7969 65.61023
328.2791 68.26550
328.7612 70.87213
329.2433 73.44775
329.7254 76.06183
330.2075 78.75476
330.6896 81.50598
331.1718 84.35870
331.6539 87.13214
332.1360 89.81860
332.6181 93.54224
333.1002 98.91260
333.5823 104.8359
334.0645 110.4500
334.5466 115.7770
335.0287 121.5496
335.5108 128.2560
335.9929 135.8654
336.4750 143.7045
336.9572 151.5063
337.4393 159.8432
337.9214 169.1364
338.4035 179.1761
338.8856 189.4700
339.3677 199.8615
339.8499 210.1774
340.3320 219.7651
340.8141 227.5510
341.2962 236.5793
341.7783 248.4108
342.2604 261.4601
342.7426 274.1478
343.2247 285.9860
343.7068 296.1793
344.1889 303.5643
344.6710 307.4585
345.1531 309.6552
345.6353 311.1287
346.1174 310.2181
346.5995 305.4557
347.0816 296.8816
347.5637 285.4796
348.0458 272.1039
348.5280 256.6241
349.0101 239.6722
349.4922 220.1937
349.9743 200.5908
350.4564 181.5809
350.9385 163.4045
351.4207 146.1207
351.9028 129.7712
352.3849 114.5933
352.8670 101.5479
353.3491 92.09363
353.8312 82.98163
354.3134 73.65369
354.7955 64.55670
355.2776 56.12823
355.7597 48.54236
356.2418 41.75092
356.7239 35.58472
357.2061 29.88232
357.6882 25.32227
358.1703 22.39307
358.6524 20.11005
359.1345 17.85486
359.6166 15.54956
360.0987 13.52289
360.5808 12.17908
361.0630 11.66754
361.5451 10.33643
362.0272 6.834534
362.5093 3.966492
362.9914 2.970032
363.4735 3.273499
363.9557 3.750854
364.4378 3.719849
364.9199 3.324341
365.4020 3.154297
365.8841 3.034790
366.3662 3.450806
366.8484 4.802795
367.3305 6.511597
367.8126 8.074524
368.2947 9.313721
368.7768 10.29596
369.2589 11.08453
369.7411 11.57812
370.2232 12.15369
370.7053 12.73047
371.1874 13.46033
371.6695 14.45917
372.1516 15.70337
372.6338 17.12024
373.1159 18.92059
373.5980 21.05072
374.0801 21.63397
374.5622 19.65070
375.0443 17.24054
375.5265 15.00732
376.0086 12.86523
376.4907 10.69202
376.9728 8.437805
377.4549 6.048401
377.9370 3.189026
378.4192 0.6249390
378.9013 3.507507
379.3834 4.159302
379.8655 4.168091
380.3476 4.760681
380.8297 6.176514
381.3119 7.734741
381.7940 8.795227
382.2761 9.366089
382.7582 9.695374
383.2403 9.880493
383.7224 9.701294
384.2046 8.978210
384.6867 7.802185
385.1688 6.498169
385.6509 5.259094
386.1330 4.014343
386.6151 2.747986
387.0973 1.649231
387.5794 0.1542970
388.0615 4.070801
388.5436 8.778381
389.0257 12.29755
389.5078 13.77673
389.9900 14.86511
390.4721 17.04346
390.9542 20.18811
391.4363 23.18024
391.9184 25.26611
392.4005 27.56464
392.8827 31.85638
393.3648 38.27448
393.8469 44.45471
394.3290 48.95953
394.8111 52.81567
395.2932 57.68250
395.7754 63.89209
396.2575 70.46381
396.7396 76.36218
397.2217 81.78027
397.7038 88.51392
398.1859 97.41327
398.6681 107.0437
399.1501 116.2682
399.6323 125.3782
400.1144 135.5776
400.5965 147.5696
401.0786 160.8610
401.5607 174.0436
402.0428 188.2424
402.5250 200.4704
403.0071 210.2631
403.4892 217.7972
403.9713 223.4004
404.4534 227.0820
404.9355 228.2197
405.4177 225.9257
405.8998 219.7036
406.3819 212.0676
406.8640 203.3945
407.3461 193.2155
407.8282 180.1161
408.3104 165.2375
408.7925 151.1687
409.2746 139.3931
409.7567 129.6136
410.2388 120.1918
410.7209 110.1422
411.2031 101.9179
411.6852 96.22241
412.1673 92.11127
412.6494 88.66077
413.1315 85.63629
413.6136 83.44800
414.0958 82.80835
414.5779 84.12585
415.0600 85.34186
415.5421 85.39661
416.0242 86.35419
416.5063 89.44299
416.9885 94.13934
417.4706 99.13031
417.9527 103.7377
418.4348 107.9142
418.9169 111.6486
419.3990 115.2293
419.8812 117.6389
420.3633 117.7148
420.8454 117.0032
421.3275 117.2042
421.8096 118.7708
422.2917 119.8757
422.7739 117.9240
423.2560 113.1290
423.7381 109.9908
424.2202 109.7939
424.7023 110.6074
425.1844 110.9985
425.6666 111.0760
426.1487 111.2350
426.6308 111.3887
427.1129 111.8311
427.5950 112.9574
428.0771 114.7720
428.5593 117.2600
429.0414 120.3522
429.5235 124.2279
430.0056 128.9838
430.4877 134.7140
430.9698 141.1317
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