#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-06-07 11:27:46 +0300 (Thu, 07 Jun 2018) $ #$Revision: 1112 $ #$URL: svn://172.16.1.111/rod/cif/1/00/05/1000544.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_1000544 loop_ _publ_author_name 'Basso, R.' 'Cabella, R.' 'Lucchetti, G.' 'Martinelli, A.' 'Palenzona, A.' _publ_section_title ; Vanadiocarpholite, Mn2+V3+Al(Si2O6)(OH)4, a new mineral from the Molinello mine, northern Apennines, Italy Note: sample VrC Locality: Molinello mine, northern Apennines, Italy ; _journal_name_full 'European Journal of Mineralogy' _journal_page_first 501 _journal_page_last 507 _journal_paper_doi 10.1127/0935-1221/2005/0017-0501 _journal_volume 17 _journal_year 2005 _chemical_compound_source R060608 _chemical_formula_sum 'Al3.02 H8 K0.012 Mg0.26 Mn1.74 O20 Si4 V0.98' _chemical_name_mineral Carpholite _space_group_IT_number 68 _symmetry_space_group_name_Hall '-C 2a 2ac' _symmetry_space_group_name_H-M 'C c c a :2' _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_length_a 13.840 _cell_length_b 20.452 _cell_length_c 5.143 _cell_volume 1455.755 _exptl_crystal_density_diffrn 3.076 _cod_original_sg_symbol_H-M 'C c c a' _cod_original_formula_sum 'K.012 (Mn1.74 Mg.26) Al3.02 V.98 Si4 O20 H8' _cod_database_code 9005714 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type helium-neon _raman_measurement_device.excitation_laser_wavelength 780 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 12 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R060608.rod _rod_data_source.block 3500000 _rod_database.code 1000544 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9005714 COD http://www.crystallography.net/cod/9005714.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 106.0234 0.0000000E+00 106.5055 0.2551270 106.9877 0.3930660 107.4698 8.579102 107.9519 27.37866 108.4340 49.00977 108.9161 68.42603 109.3982 87.70190 109.8804 110.8372 110.3625 136.7656 110.8446 164.6365 111.3267 198.4258 111.8088 249.0493 112.2909 300.9486 112.7731 353.6884 113.2552 402.3236 113.7373 424.8806 114.2194 418.0461 114.7015 368.8340 115.1836 317.8845 115.6658 262.2329 116.1479 207.3506 116.6300 156.9772 117.1121 111.6913 117.5942 71.77234 118.0763 41.15723 118.5584 20.68982 119.0406 6.175903 119.5227 3.028931 120.0048 7.024048 120.4869 5.747437 120.9690 1.830322 121.4511 13.96533 121.9333 26.41382 122.4154 38.40173 122.8975 49.47754 123.3796 59.21667 123.8617 67.19543 124.3438 72.19275 124.8260 71.02686 125.3081 67.41223 125.7902 64.01636 126.2723 60.61658 126.7544 58.60339 127.2365 59.85608 127.7187 63.22913 128.2008 70.46790 128.6829 84.49646 129.1650 101.5413 129.6471 117.0684 130.1292 129.2795 130.6114 137.1763 131.0935 138.4613 131.5756 130.3284 132.0577 120.0166 132.5398 108.8157 133.0219 97.21985 133.5041 84.94214 133.9862 71.52612 134.4683 56.36438 134.9504 45.09229 135.4325 40.92493 135.9146 37.89954 136.3968 32.12109 136.8789 23.49829 137.3610 15.12769 137.8431 11.12695 138.3252 13.28479 138.8073 14.34143 139.2895 13.13135 139.7716 11.56152 140.2537 11.90039 140.7358 14.80896 141.2179 17.43347 141.7000 18.01587 142.1821 17.11426 142.6643 16.00549 143.1464 15.22949 143.6285 14.70227 144.1106 13.78284 144.5927 11.53723 145.0748 9.884766 145.5570 10.74097 146.0391 13.99402 146.5212 16.81018 147.0033 15.66687 147.4854 9.929443 147.9675 6.081787 148.4497 7.969360 148.9318 10.48816 149.4139 10.75244 149.8960 8.166138 150.3781 4.234497 150.8602 1.134644 151.3424 0.9097900 151.8245 2.222046 152.3066 2.606445 152.7887 2.602539 153.2708 2.852173 153.7529 3.543823 154.2351 4.151489 154.7172 3.339722 155.1993 0.2766110 155.6814 3.486450 156.1635 8.070801 156.6456 13.23352 157.1278 18.99573 157.6099 25.45276 158.0920 32.09753 158.5741 36.65479 159.0562 36.03345 159.5383 37.05103 160.0205 42.03418 160.5026 49.95312 160.9847 58.64380 161.4668 67.19922 161.9489 75.30945 162.4310 81.90881 162.9131 88.76636 163.3953 92.90125 163.8774 95.69373 164.3595 93.66296 164.8416 89.09058 165.3237 82.83081 165.8058 74.84460 166.2880 65.24646 166.7701 52.33752 167.2522 39.06604 167.7343 29.12573 168.2164 23.10413 168.6985 17.75641 169.1807 10.28790 169.6628 2.603210 170.1449 2.716858 170.6270 3.999939 171.1091 2.754944 171.5912 2.311523 172.0734 3.035339 172.5555 3.839233 173.0376 4.462769 173.5197 4.895081 174.0018 5.211914 174.4839 5.578674 174.9661 5.830017 175.4482 4.921448 175.9303 1.778076 176.4124 1.292236 176.8945 3.896423 177.3766 5.704163 177.8588 6.761047 178.3409 7.276428 178.8230 7.613586 179.3051 8.151672 179.7872 9.024963 180.2693 9.664612 180.7515 9.650879 181.2336 9.177979 181.7157 8.812744 182.1978 9.069031 182.6799 10.03540 183.1620 10.34979 183.6441 8.335632 184.1263 7.242371 184.6084 9.467896 185.0905 14.58319 185.5726 19.80347 186.0547 22.36597 186.5368 21.77246 187.0190 23.09735 187.5011 27.35785 187.9832 32.69397 188.4653 37.92291 188.9474 42.87927 189.4296 47.77008 189.9117 52.95001 190.3938 58.37860 190.8759 63.20166 191.3580 66.42853 191.8401 69.39355 192.3223 73.76392 192.8044 79.91058 193.2865 86.62244 193.7686 92.82031 194.2507 98.62036 194.7328 104.3926 195.2150 110.1887 195.6971 116.0565 196.1792 122.1866 196.6613 128.7310 197.1434 135.1038 197.6255 140.8287 198.1077 146.1094 198.5898 151.3234 199.0719 156.3234 199.5540 161.3186 200.0361 167.3436 200.5182 175.0922 201.0004 183.0176 201.4825 189.9736 201.9646 196.3569 202.4467 203.0911 202.9288 211.0105 203.4109 220.0986 203.8930 228.9218 204.3752 236.7483 204.8573 244.9776 205.3394 254.0283 205.8215 263.7930 206.3036 274.1696 206.7857 284.9924 207.2679 296.2366 207.7500 307.4876 208.2321 320.5094 208.7142 331.7480 209.1963 340.3976 209.6784 346.3285 210.1606 349.5941 210.6427 350.1896 211.1248 348.0876 211.6069 343.1911 212.0890 336.1215 212.5711 326.1725 213.0533 312.1976 213.5354 294.8448 214.0175 275.7976 214.4996 256.6432 214.9817 237.4417 215.4638 217.6655 215.9460 196.1654 216.4281 175.1306 216.9102 155.1850 217.3923 136.5762 217.8744 119.2563 218.3565 103.1895 218.8387 88.43542 219.3208 76.06165 219.8029 66.52777 220.2850 58.58942 220.7671 51.88440 221.2492 46.21661 221.7314 40.92462 222.2135 35.28241 222.6956 29.32281 223.1777 24.84546 223.6598 22.71582 224.1419 21.37476 224.6240 19.62494 225.1062 17.41553 225.5883 15.51526 226.0704 14.57227 226.5525 14.58801 227.0346 14.87177 227.5167 14.97766 227.9989 15.34229 228.4810 17.25421 228.9631 20.98206 229.4452 24.38263 229.9273 25.66223 230.4094 25.31006 230.8916 24.74310 231.3737 24.11945 231.8558 23.43585 232.3379 22.61139 232.8200 21.61597 233.3021 20.82623 233.7843 20.89838 234.2664 21.36786 234.7485 21.39404 235.2306 20.72980 235.7127 19.55292 236.1948 17.79327 236.6770 15.11676 237.1591 13.18304 237.6412 13.75299 238.1233 15.26569 238.6054 15.93665 239.0875 14.89459 239.5697 13.24512 240.0518 12.88733 240.5339 14.26709 241.0160 15.53388 241.4981 15.68207 241.9802 15.47461 242.4624 15.63934 242.9445 16.45374 243.4266 17.70410 243.9087 18.97260 244.3908 20.14343 244.8729 21.61163 245.3550 24.26202 245.8372 26.85962 246.3193 28.27734 246.8014 28.11157 247.2835 26.90961 247.7656 25.44214 248.2477 23.38129 248.7299 21.88354 249.2120 21.87030 249.6941 22.00446 250.1762 21.09430 250.6583 18.81006 251.1404 16.02295 251.6226 14.12897 252.1047 13.34064 252.5868 13.07275 253.0689 12.97455 253.5510 13.46307 254.0331 15.03906 254.5153 17.75085 254.9974 20.93268 255.4795 23.58600 255.9616 25.46350 256.4437 27.30670 256.9258 29.16364 257.4080 30.98053 257.8901 32.93732 258.3722 34.96051 258.8543 36.59766 259.3364 37.20209 259.8185 36.43713 260.3007 35.39697 260.7828 34.26373 261.2649 32.77216 261.7470 30.66779 262.2291 27.97217 262.7112 25.01514 263.1934 22.18719 263.6755 19.67322 264.1576 16.55188 264.6397 12.19659 265.1218 7.887756 265.6039 4.240295 266.0861 1.336121 266.5682 0.9952390 267.0503 2.885864 267.5324 4.286682 268.0145 5.452332 268.4966 6.454590 268.9788 7.216431 269.4609 7.914429 269.9430 8.392883 270.4251 8.086426 270.9072 6.364441 271.3893 3.148254 271.8715 1.165588 272.3536 1.752625 272.8357 1.994751 273.3178 0.8781740 273.7999 1.579102 274.2820 5.188538 274.7642 9.977661 275.2463 15.81750 275.7284 21.00824 276.2105 24.46179 276.6926 28.59277 277.1747 34.65582 277.6568 42.00360 278.1389 49.23499 278.6211 55.60553 279.1032 61.27185 279.5853 66.91077 280.0674 73.75299 280.5495 79.19763 281.0316 83.13989 281.5138 85.21216 281.9959 84.56879 282.4780 80.73010 282.9601 74.34644 283.4422 66.77045 283.9243 56.43677 284.4065 47.92712 284.8886 42.94940 285.3707 40.15442 285.8528 37.53619 286.3349 34.40424 286.8170 31.52649 287.2992 30.36743 287.7813 31.40796 288.2634 32.30975 288.7455 32.53467 289.2276 32.50732 289.7097 32.70929 290.1919 33.24731 290.6740 34.04114 291.1561 35.15295 291.6382 36.68903 292.1203 37.61469 292.6024 37.88678 293.0846 37.46014 293.5667 36.09955 294.0488 33.78351 294.5309 31.12500 295.0130 28.52173 295.4951 26.02466 295.9773 24.15948 296.4594 23.11432 296.9415 22.56903 297.4236 22.35175 297.9057 22.44281 298.3878 22.76508 298.8700 23.30511 299.3521 24.03772 299.8342 24.76331 300.3163 25.33374 300.7984 26.02808 301.2805 26.92780 301.7627 28.06378 302.2448 29.62012 302.7269 31.83746 303.2090 34.46033 303.6911 36.69714 304.1732 38.38483 304.6554 40.00427 305.1375 41.83923 305.6196 43.77850 306.1017 45.43323 306.5838 46.52911 307.0659 47.53943 307.5481 49.61017 308.0302 53.17889 308.5123 55.95239 308.9944 56.68274 309.4765 56.24133 309.9586 56.01782 310.4408 56.32690 310.9229 57.07263 311.4050 58.27917 311.8871 59.96094 312.3692 61.56842 312.8513 63.29132 313.3335 64.74072 313.8156 65.35901 314.2977 65.03949 314.7798 64.32568 315.2619 63.61554 315.7440 62.91089 316.2262 62.28430 316.7083 61.98907 317.1904 61.59644 317.6725 60.84509 318.1546 59.70258 318.6367 57.96478 319.1188 55.05182 319.6010 51.49780 320.0831 49.57062 320.5652 50.59595 321.0473 52.03827 321.5294 52.39105 322.0115 51.80707 322.4937 51.19800 322.9758 51.01398 323.4579 51.20642 323.9400 51.54303 324.4221 51.92181 324.9042 52.47418 325.3864 52.90076 325.8685 53.57208 326.3506 55.32153 326.8327 58.52570 327.3148 62.35608 327.7969 65.61023 328.2791 68.26550 328.7612 70.87213 329.2433 73.44775 329.7254 76.06183 330.2075 78.75476 330.6896 81.50598 331.1718 84.35870 331.6539 87.13214 332.1360 89.81860 332.6181 93.54224 333.1002 98.91260 333.5823 104.8359 334.0645 110.4500 334.5466 115.7770 335.0287 121.5496 335.5108 128.2560 335.9929 135.8654 336.4750 143.7045 336.9572 151.5063 337.4393 159.8432 337.9214 169.1364 338.4035 179.1761 338.8856 189.4700 339.3677 199.8615 339.8499 210.1774 340.3320 219.7651 340.8141 227.5510 341.2962 236.5793 341.7783 248.4108 342.2604 261.4601 342.7426 274.1478 343.2247 285.9860 343.7068 296.1793 344.1889 303.5643 344.6710 307.4585 345.1531 309.6552 345.6353 311.1287 346.1174 310.2181 346.5995 305.4557 347.0816 296.8816 347.5637 285.4796 348.0458 272.1039 348.5280 256.6241 349.0101 239.6722 349.4922 220.1937 349.9743 200.5908 350.4564 181.5809 350.9385 163.4045 351.4207 146.1207 351.9028 129.7712 352.3849 114.5933 352.8670 101.5479 353.3491 92.09363 353.8312 82.98163 354.3134 73.65369 354.7955 64.55670 355.2776 56.12823 355.7597 48.54236 356.2418 41.75092 356.7239 35.58472 357.2061 29.88232 357.6882 25.32227 358.1703 22.39307 358.6524 20.11005 359.1345 17.85486 359.6166 15.54956 360.0987 13.52289 360.5808 12.17908 361.0630 11.66754 361.5451 10.33643 362.0272 6.834534 362.5093 3.966492 362.9914 2.970032 363.4735 3.273499 363.9557 3.750854 364.4378 3.719849 364.9199 3.324341 365.4020 3.154297 365.8841 3.034790 366.3662 3.450806 366.8484 4.802795 367.3305 6.511597 367.8126 8.074524 368.2947 9.313721 368.7768 10.29596 369.2589 11.08453 369.7411 11.57812 370.2232 12.15369 370.7053 12.73047 371.1874 13.46033 371.6695 14.45917 372.1516 15.70337 372.6338 17.12024 373.1159 18.92059 373.5980 21.05072 374.0801 21.63397 374.5622 19.65070 375.0443 17.24054 375.5265 15.00732 376.0086 12.86523 376.4907 10.69202 376.9728 8.437805 377.4549 6.048401 377.9370 3.189026 378.4192 0.6249390 378.9013 3.507507 379.3834 4.159302 379.8655 4.168091 380.3476 4.760681 380.8297 6.176514 381.3119 7.734741 381.7940 8.795227 382.2761 9.366089 382.7582 9.695374 383.2403 9.880493 383.7224 9.701294 384.2046 8.978210 384.6867 7.802185 385.1688 6.498169 385.6509 5.259094 386.1330 4.014343 386.6151 2.747986 387.0973 1.649231 387.5794 0.1542970 388.0615 4.070801 388.5436 8.778381 389.0257 12.29755 389.5078 13.77673 389.9900 14.86511 390.4721 17.04346 390.9542 20.18811 391.4363 23.18024 391.9184 25.26611 392.4005 27.56464 392.8827 31.85638 393.3648 38.27448 393.8469 44.45471 394.3290 48.95953 394.8111 52.81567 395.2932 57.68250 395.7754 63.89209 396.2575 70.46381 396.7396 76.36218 397.2217 81.78027 397.7038 88.51392 398.1859 97.41327 398.6681 107.0437 399.1501 116.2682 399.6323 125.3782 400.1144 135.5776 400.5965 147.5696 401.0786 160.8610 401.5607 174.0436 402.0428 188.2424 402.5250 200.4704 403.0071 210.2631 403.4892 217.7972 403.9713 223.4004 404.4534 227.0820 404.9355 228.2197 405.4177 225.9257 405.8998 219.7036 406.3819 212.0676 406.8640 203.3945 407.3461 193.2155 407.8282 180.1161 408.3104 165.2375 408.7925 151.1687 409.2746 139.3931 409.7567 129.6136 410.2388 120.1918 410.7209 110.1422 411.2031 101.9179 411.6852 96.22241 412.1673 92.11127 412.6494 88.66077 413.1315 85.63629 413.6136 83.44800 414.0958 82.80835 414.5779 84.12585 415.0600 85.34186 415.5421 85.39661 416.0242 86.35419 416.5063 89.44299 416.9885 94.13934 417.4706 99.13031 417.9527 103.7377 418.4348 107.9142 418.9169 111.6486 419.3990 115.2293 419.8812 117.6389 420.3633 117.7148 420.8454 117.0032 421.3275 117.2042 421.8096 118.7708 422.2917 119.8757 422.7739 117.9240 423.2560 113.1290 423.7381 109.9908 424.2202 109.7939 424.7023 110.6074 425.1844 110.9985 425.6666 111.0760 426.1487 111.2350 426.6308 111.3887 427.1129 111.8311 427.5950 112.9574 428.0771 114.7720 428.5593 117.2600 429.0414 120.3522 429.5235 124.2279 430.0056 128.9838 430.4877 134.7140 430.9698 141.1317 431.4520 148.1424 431.9341 155.7079 432.4162 163.7470 432.8983 172.1794 433.3804 181.2778 433.8625 191.4582 434.3447 202.8584 434.8268 214.4648 435.3089 225.4140 435.7910 237.2271 436.2731 250.9592 436.7552 266.3210 437.2374 282.4873 437.7195 299.0495 438.2016 315.7662 438.6837 331.5179 439.1658 347.0476 439.6479 360.6594 440.1301 374.0258 440.6122 384.4620 441.0943 389.2745 441.5764 387.9543 442.0585 381.8195 442.5406 372.2414 443.0227 359.1196 443.5049 343.0142 443.9870 321.5276 444.4691 299.5804 444.9512 277.9076 445.4333 257.1120 445.9154 237.6030 446.3976 219.6238 446.8797 202.9239 447.3618 187.0698 447.8439 171.9796 448.3260 157.9442 448.8081 144.9544 449.2903 133.1140 449.7724 122.4237 450.2545 112.8633 450.7366 104.5423 451.2187 97.88770 451.7008 92.64819 452.1830 87.86957 452.6651 83.47440 453.1472 79.71539 453.6293 76.69592 454.1114 74.48895 454.5935 73.39902 455.0757 73.84857 455.5578 74.60681 456.0399 74.57709 456.5220 73.94995 457.0041 73.57864 457.4862 73.66367 457.9684 74.18527 458.4505 75.18082 458.9326 76.65442 459.4147 78.63507 459.8968 81.19641 460.3789 84.05151 460.8611 87.54858 461.3432 91.45688 461.8253 94.23892 462.3074 94.63354 462.7895 93.42499 463.2716 93.99872 463.7538 97.73779 464.2359 101.2792 464.7180 104.4502 465.2001 107.1839 465.6822 109.1855 466.1643 110.4892 466.6465 111.6971 467.1286 113.5528 467.6107 116.2032 468.0928 118.2748 468.5749 119.5875 469.0570 120.4940 469.5392 121.0280 470.0213 121.2078 470.5034 121.1564 470.9855 120.9482 471.4676 120.2076 471.9497 118.1856 472.4319 114.6905 472.9140 110.8021 473.3961 106.7556 473.8782 102.2540 474.3603 96.67859 474.8424 90.39426 475.3246 84.66711 475.8067 80.74219 476.2888 77.75012 476.7709 73.56592 477.2530 67.98627 477.7351 62.63385 478.2173 58.46271 478.6994 54.86490 479.1815 50.70370 479.6636 45.57602 480.1457 41.23309 480.6278 39.23141 481.1100 38.43768 481.5920 36.56717 482.0742 33.16907 482.5563 29.87451 483.0384 28.27045 483.5205 28.33688 484.0026 27.63324 484.4847 25.58392 484.9669 23.44205 485.4490 21.48288 485.9311 19.81525 486.4132 18.68442 486.8953 18.17035 487.3774 17.94052 487.8596 17.46631 488.3417 16.67819 488.8238 15.80508 489.3059 14.75128 489.7880 13.72348 490.2701 12.94824 490.7523 12.28275 491.2344 11.33646 491.7165 9.808960 492.1986 8.050262 492.6807 7.094269 493.1628 7.265930 493.6450 7.353973 494.1271 7.230743 494.6092 6.853363 495.0913 6.066193 495.5734 4.917236 496.0555 3.769958 496.5377 2.927429 497.0198 2.282227 497.5019 1.475494 497.9840 0.4115600 498.4661 0.4077150 498.9482 0.7562560 499.4304 0.6472780 499.9125 8.7279998E-02 500.3946 1.149445 500.8767 2.284332 501.3588 3.096497 501.8409 3.509521 502.3231 3.226166 502.8052 2.177124 503.2873 1.031128 503.7694 0.3944700 504.2515 0.2836300 504.7336 0.3979490 505.2158 1.296875 505.6979 1.775146 506.1800 1.004974 506.6621 0.3432620 507.1442 1.225616 507.6263 1.274261 508.1085 0.9103090 508.5906 0.7668760 509.0727 0.9089360 509.5548 1.043518 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