#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-06-07 11:27:50 +0300 (Thu, 07 Jun 2018) $
#$Revision: 1113 $
#$URL: svn://172.16.1.111/rod/cif/1/00/05/1000545.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000545
loop_
_publ_author_name
'Abraham, F.'
'Dion, C.'
'Tancret, N.'
'Saadi, M.'
_publ_section_title
;
 Ag2(UO2)2V2O8: a new compound with the carnotite structure. Synthesis,
 structure and properties
;
_journal_name_full               'Advanced Materials Research'
_journal_page_first              511
_journal_page_last               520
_journal_volume                  1
_journal_year                    1994
_chemical_compound_source        R070647
_chemical_formula_structural     Ag2(UO2)2V2O8
_chemical_formula_sum            'Ag O6 U V'
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 100.56
_cell_angle_gamma                90
_cell_length_a                   5.8952
_cell_length_b                   8.3541
_cell_length_c                   10.4142
_cell_volume                     504.203
_exptl_crystal_density_diffrn    6.492
_cod_original_formula_sum        'Ag U V O6'
_cod_database_code               9012859
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R070647.rod
_rod_data_source.block           3500000
_rod_database.code               1000545
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9012859 COD http://www.crystallography.net/cod/9012859.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
121.9340 0.0000000E+00
122.4161 3.328125
122.8982 12.67969
123.3804 46.46777
123.8625 106.0391
124.3446 189.3984
124.8267 244.5820
125.3088 246.3438
125.7909 202.9854
126.2731 195.8174
126.7552 237.2451
127.2373 269.5957
127.7194 288.9453
128.2015 311.3047
128.6837 384.5508
129.1658 393.0820
129.6479 313.2354
130.1300 298.4268
130.6121 275.8975
131.0942 244.9502
131.5764 241.1797
132.0585 283.7070
132.5406 348.9072
133.0227 357.5781
133.5048 321.0449
133.9869 282.6826
134.4691 186.7090
134.9512 76.53906
135.4333 9.347656
135.9154 20.73340
136.3975 98.49805
136.8796 127.0107
137.3618 78.28906
137.8439 18.96387
138.3260 5.860352
138.8081 6.975586
139.2902 28.64746
139.7723 36.40625
140.2545 30.91504
140.7366 20.22070
141.2187 1.222656
141.7008 25.07031
142.1829 44.46582
142.6650 59.77441
143.1472 65.37695
143.6293 44.08691
144.1114 2.603516
144.5935 24.73535
145.0756 5.854492
145.5577 41.64062
146.0399 53.97852
146.5220 6.862305
147.0041 72.29980
147.4862 84.84570
147.9683 46.21582
148.4504 2.585938
148.9326 28.96777
149.4147 31.48633
149.8968 28.10742
150.3789 3.930664
150.8610 13.97461
151.3431 3.529297
151.8252 39.30957
152.3074 90.64551
152.7895 111.8242
153.2716 87.19336
153.7537 65.02441
154.2358 51.06543
154.7179 41.78320
155.2001 36.48340
155.6822 34.92383
156.1643 33.22949
156.6464 19.48730
157.1285 17.32812
157.6106 55.38574
158.0928 77.47852
158.5749 102.2383
159.0570 159.9229
159.5391 271.6680
160.0212 430.4072
160.5033 550.4199
160.9855 604.2568
161.4676 653.8252
161.9497 709.8877
162.4318 776.1338
162.9139 859.3369
163.3960 968.6045
163.8782 1105.056
164.3603 1220.794
164.8424 1284.960
165.3245 1354.519
165.8066 1479.328
166.2887 1660.187
166.7709 1836.693
167.2530 1939.122
167.7351 1969.764
168.2172 2047.019
168.6993 2216.959
169.1814 2426.970
169.6636 2616.769
170.1457 2778.233
170.6278 2918.394
171.1099 3040.128
171.5920 3146.676
172.0741 3244.517
172.5563 3333.447
173.0384 3415.581
173.5205 3496.763
174.0026 3581.582
174.4847 3660.737
174.9668 3726.681
175.4490 3780.332
175.9311 3830.150
176.4132 3893.654
176.8953 3969.889
177.3774 4005.912
177.8595 3952.935
178.3417 3886.474
178.8238 3852.486
179.3059 3855.380
179.7880 3883.404
180.2701 3908.707
180.7522 3933.407
181.2344 3949.184
181.7165 3944.483
182.1986 3937.306
182.6807 3936.414
183.1628 3944.568
183.6449 3962.102
184.1271 3991.313
184.6092 4038.561
185.0913 4086.713
185.5734 4130.445
186.0555 4175.570
186.5376 4226.244
187.0198 4284.451
187.5019 4349.421
187.9840 4419.717
188.4661 4486.642
188.9482 4573.275
189.4303 4701.522
189.9125 4844.504
190.3946 4963.831
190.8767 5039.245
191.3588 5086.266
191.8409 5182.432
192.3230 5355.639
192.8052 5543.727
193.2873 5758.878
193.7694 5983.439
194.2515 6186.799
194.7336 6347.830
195.2157 6465.447
195.6979 6547.015
196.1800 6593.107
196.6621 6617.408
197.1442 6626.795
197.6263 6618.109
198.1084 6582.662
198.5906 6513.324
199.0727 6408.174
199.5548 6282.595
200.0369 6139.688
200.5190 5978.349
201.0011 5788.039
201.4833 5573.741
201.9654 5362.755
202.4475 5167.482
202.9296 4991.510
203.4117 4836.488
203.8938 4730.532
204.3760 4631.786
204.8581 4488.385
205.3402 4294.027
205.8223 4111.877
206.3044 4001.177
206.7865 3945.939
207.2687 3893.081
207.7508 3815.791
208.2329 3742.772
208.7150 3712.825
209.1971 3731.271
209.6792 3778.709
210.1614 3850.933
210.6435 3941.174
211.1256 4037.153
211.6077 4127.885
212.0898 4221.006
212.5719 4332.771
213.0541 4462.895
213.5362 4615.140
214.0183 4806.050
214.5004 5020.447
214.9825 5220.732
215.4646 5367.460
215.9468 5478.287
216.4289 5629.223
216.9110 5854.842
217.3931 6076.361
217.8752 6248.396
218.3573 6381.698
218.8395 6506.346
219.3216 6633.791
219.8037 6765.351
220.2858 6925.387
220.7679 7163.831
221.2500 7376.365
221.7322 7502.816
222.2143 7560.321
222.6964 7606.934
223.1785 7693.293
223.6606 7822.012
224.1427 7931.412
224.6249 8011.385
225.1070 8078.406
225.5891 8126.229
226.0712 8162.794
226.5533 8210.711
227.0354 8304.264
227.5176 8457.733
227.9997 8552.927
228.4818 8577.111
228.9639 8555.455
229.4460 8493.520
229.9281 8391.966
230.4103 8248.737
230.8924 8063.855
231.3745 7837.774
231.8566 7544.635
232.3387 7128.401
232.8208 6697.384
233.3030 6290.170
233.7851 5911.309
234.2672 5554.269
234.7493 5209.732
235.2314 4870.522
235.7135 4573.991
236.1957 4339.272
236.6778 4119.599
237.1599 3884.660
237.6420 3637.597
238.1241 3410.657
238.6062 3243.868
239.0884 3154.860
239.5705 3068.474
240.0526 2964.351
240.5347 2879.321
241.0168 2836.230
241.4989 2835.616
241.9811 2865.826
242.4632 2911.864
242.9453 2981.871
243.4274 3042.948
243.9095 3085.429
244.3916 3127.204
244.8738 3172.278
245.3559 3224.633
245.8380 3297.530
246.3201 3410.088
246.8022 3582.532
247.2843 3730.059
247.7665 3829.044
248.2486 3922.907
248.7307 4041.850
249.2128 4189.849
249.6949 4352.848
250.1770 4518.231
250.6592 4692.745
251.1413 4838.915
251.6234 4946.953
252.1055 5035.116
252.5876 5112.747
253.0697 5182.343
253.5519 5251.422
254.0340 5332.818
254.5161 5438.786
254.9982 5491.281
255.4803 5461.938
255.9624 5399.379
256.4445 5340.322
256.9267 5289.766
257.4088 5230.452
257.8909 5141.469
258.3730 5013.802
258.8551 4900.694
259.3372 4805.574
259.8194 4723.154
260.3015 4653.649
260.7836 4596.021
261.2657 4540.035
261.7478 4476.992
262.2299 4405.815
262.7121 4326.381
263.1942 4225.539
263.6763 4125.418
264.1584 4039.291
264.6405 3969.420
265.1227 3922.394
265.6048 3912.765
266.0869 3943.695
266.5690 3949.398
267.0511 3908.821
267.5332 3855.762
268.0154 3815.529
268.4975 3790.271
268.9796 3774.301
269.4617 3768.597
269.9438 3771.387
270.4259 3753.170
270.9081 3694.714
271.3902 3627.881
271.8723 3588.349
272.3544 3574.749
272.8365 3539.688
273.3186 3437.247
273.8008 3273.137
274.2829 3139.226
274.7650 3071.234
275.2471 3008.263
275.7292 2907.109
276.2113 2767.995
276.6935 2606.090
277.1756 2424.322
277.6577 2226.464
278.1398 2048.125
278.6219 1907.552
279.1040 1770.909
279.5862 1609.383
280.0683 1426.164
280.5504 1250.972
281.0325 1102.536
281.5146 978.7178
281.9967 860.1270
282.4789 752.5303
282.9610 644.0508
283.4431 520.4170
283.9252 385.7773
284.4073 267.3135
284.8894 184.2842
285.3716 125.3975
285.8537 51.54688
286.3358 45.79199
286.8179 146.4385
287.3000 247.6592
287.7821 345.6748
288.2643 421.1475
288.7464 461.1934
289.2285 476.6523
289.7106 498.0723
290.1927 532.9102
290.6748 560.1377
291.1570 568.2637
291.6391 560.5645
292.1212 547.2812
292.6033 533.0146
293.0854 513.8984
293.5675 481.2002
294.0497 430.5889
294.5318 380.1807
295.0139 340.1807
295.4960 305.5615
295.9781 263.9590
296.4602 209.9863
296.9424 150.2861
297.4245 101.0615
297.9066 68.73340
298.3887 18.39258
298.8708 69.83203
299.3529 181.5762
299.8351 287.9414
300.3172 377.9600
300.7993 474.1104
301.2814 618.7617
301.7635 815.3486
302.2456 1000.977
302.7278 1151.258
303.2099 1285.221
303.6920 1422.447
304.1741 1565.456
304.6562 1722.817
305.1383 1914.521
305.6205 2142.580
306.1026 2355.268
306.5847 2524.440
307.0668 2686.606
307.5489 2885.654
308.0310 3127.805
308.5132 3372.699
308.9953 3579.864
309.4774 3747.703
309.9595 3933.462
310.4416 4153.675
310.9237 4382.450
311.4059 4601.139
311.8880 4808.036
312.3701 5009.738
312.8522 5210.181
313.3343 5409.077
313.8164 5616.183
314.2986 5874.992
314.7807 6102.363
315.2628 6233.825
315.7449 6284.751
316.2270 6331.904
316.7091 6432.906
317.1913 6564.397
317.6734 6595.094
318.1555 6486.313
318.6376 6337.129
319.1197 6174.042
319.6018 5998.089
320.0840 5811.700
320.5661 5620.062
321.0482 5414.329
321.5303 5165.254
322.0124 4853.960
322.4945 4533.527
322.9767 4211.846
323.4588 3888.485
323.9409 3554.666
324.4230 3204.134
324.9051 2861.802
325.3872 2576.789
325.8694 2385.040
326.3515 2190.098
326.8336 1970.611
327.3157 1753.692
327.7978 1563.320
328.2799 1406.689
328.7621 1280.847
329.2442 1181.554
329.7263 1118.704
330.2084 1064.571
330.6905 1014.186
331.1726 975.4688
331.6548 957.5859
332.1369 959.6182
332.6190 968.9805
333.1011 971.2002
333.5832 960.9824
334.0653 975.9834
334.5475 1019.584
335.0296 1079.737
335.5117 1156.685
335.9938 1245.949
336.4759 1338.598
336.9580 1427.504
337.4402 1512.792
337.9223 1603.427
338.4044 1687.672
338.8865 1789.134
339.3686 1912.845
339.8507 2058.825
340.3329 2228.960
340.8150 2427.054
341.2971 2644.735
341.7792 2846.807
342.2613 3006.022
342.7434 3184.104
343.2256 3391.972
343.7077 3619.053
344.1898 3848.277
344.6719 4073.413
345.1540 4298.833
345.6361 4536.518
346.1183 4795.509
346.6004 5055.991
347.0825 5325.956
347.5646 5590.079
348.0467 5832.200
348.5288 6050.569
349.0110 6268.236
349.4931 6511.295
349.9752 6785.148
350.4573 7068.565
350.9394 7367.114
351.4215 7675.333
351.9037 7990.783
352.3858 8314.845
352.8679 8651.824
353.3500 9014.405
353.8321 9400.631
354.3142 9749.608
354.7964 10017.42
355.2785 10298.18
355.7606 10639.64
356.2427 11020.82
356.7248 11398.68
357.2069 11741.18
357.6891 12060.77
358.1712 12392.45
358.6533 12747.52
359.1354 13092.62
359.6175 13405.08
360.0996 13703.71
360.5818 14010.79
361.0639 14337.24
361.5460 14665.29
362.0281 14966.44
362.5102 15238.84
362.9923 15509.55
363.4745 15764.00
363.9566 16038.33
364.4387 16370.56
364.9208 16770.20
365.4029 17184.99
365.8850 17576.32
366.3672 17948.56
366.8493 18335.76
367.3314 18748.16
367.8135 19171.30
368.2956 19602.09
368.7777 20038.35
369.2599 20444.57
369.7420 20796.31
370.2241 21108.73
370.7062 21404.54
371.1883 21686.54
371.6704 21952.58
372.1526 22208.08
372.6347 22449.53
373.1168 22655.44
373.5989 22853.63
374.0810 22994.31
374.5631 23037.83
375.0453 22985.41
375.5274 22861.77
376.0095 22679.77
376.4916 22431.76
376.9737 22103.59
377.4558 21691.84
377.9380 21215.14
378.4201 20676.77
378.9022 20075.41
379.3843 19411.79
379.8664 18686.20
380.3485 17906.44
380.8307 17098.99
381.3128 16246.46
381.7949 15390.30
382.2770 14485.01
382.7591 13599.99
383.2412 12828.02
383.7234 12178.18
384.2055 11572.44
384.6876 10918.99
385.1697 10188.78
385.6518 9533.461
386.1339 8965.809
386.6161 8448.062
387.0982 7964.788
387.5803 7514.224
388.0624 7103.917
388.5445 6736.981
389.0266 6411.122
389.5088 6110.795
389.9909 5846.226
390.4730 5599.892
390.9551 5348.680
391.4372 5122.075
391.9193 4964.012
392.4015 4895.332
392.8836 4881.981
393.3657 4851.633
393.8478 4783.713
394.3299 4748.524
394.8120 4764.384
395.2942 4806.002
395.7763 4856.951
396.2584 4916.128
396.7405 4995.828
397.2226 5105.017
397.7047 5242.937
398.1869 5424.064
398.6690 5697.199
399.1511 5957.140
399.6332 6132.684
400.1153 6245.805
400.5974 6361.960
401.0796 6503.353
401.5617 6674.517
402.0438 6894.836
402.5259 7175.908
403.0080 7461.028
403.4901 7716.643
403.9723 7958.303
404.4544 8207.678
404.9365 8475.122
405.4186 8740.541
405.9007 8986.195
406.3828 9213.890
406.8650 9436.565
407.3471 9665.052
407.8292 9879.837
408.3113 10053.39
408.7934 10188.15
409.2755 10285.22
409.7577 10356.59
410.2398 10384.74
410.7219 10347.51
411.2040 10241.22
411.6861 10066.55
412.1682 9817.877
412.6504 9485.831
413.1325 9127.969
413.6146 8735.548
414.0967 8325.927
414.5788 7906.855
415.0609 7477.659
415.5431 7027.325
416.0252 6544.326
416.5073 6042.390
416.9894 5577.648
417.4715 5156.517
417.9536 4763.969
418.4358 4414.125
418.9179 4085.629
419.4000 3750.116
419.8821 3400.383
420.3642 3055.820
420.8463 2746.587
421.3285 2483.903
421.8106 2230.078
422.2927 1972.882
422.7748 1735.466
423.2569 1532.926
423.7390 1362.118
424.2212 1207.701
424.7033 1058.263
425.1854 915.6338
425.6675 785.9282
426.1496 664.5522
426.6317 567.4902
427.1139 497.7192
427.5960 453.1069
428.0781 440.6650
428.5602 476.7109
429.0423 507.4180
429.5244 452.0908
430.0066 308.5684
430.4887 178.2158
430.9708 88.97266
431.4529 26.36279
431.9350 28.57959
432.4171 76.19922
432.8993 113.8672
433.3814 135.0903
433.8635 146.7642
434.3456 163.4590
434.8277 188.0239
435.3098 208.5664
435.7920 212.0894
436.2741 200.2192
436.7562 197.4526
437.2383 212.3638
437.7204 229.4229
438.2025 242.4741
438.6847 250.5522
439.1668 250.9160
439.6489 241.2764
440.1310 225.7432
440.6131 215.5928
441.0952 223.5698
441.5774 218.6958
442.0595 185.7383
442.5416 147.3828
443.0237 123.9336
443.5058 118.8853
443.9879 124.3779
444.4701 134.1128
444.9522 150.7007
445.4343 152.4619
445.9164 126.1245
446.3985 98.09082
446.8806 74.31250
447.3628 55.17725
447.8449 39.56494
448.3270 26.46875
448.8091 17.35352
449.2912 17.56104
449.7733 31.93555
450.2555 42.10889
450.7376 47.11230
451.2197 43.66553
451.7018 23.31201
452.1839 14.90820
452.6660 49.40332
453.1482 57.87988
453.6303 46.50391
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1280.460 0.0000000E+00
