#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-06-07 11:28:26 +0300 (Thu, 07 Jun 2018) $
#$Revision: 1124 $
#$URL: svn://172.16.1.111/rod/cif/1/00/05/1000553.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000553
loop_
_publ_author_name
'Burns, P. C.'
'Smith, J. V.'
'Steele, I. M.'
_publ_section_title
;
 Arizona porphyry copper/hydrothermal deposits I. The structure of
 chenevixite and luetheite Note: Luetheite-chenevixite series Locality:
 Humboldt mine, Patagonia, Arizona
;
_journal_name_full               'Mineralogical Magazine'
_journal_page_first              25
_journal_page_last               30
_journal_paper_doi               10.1180/002646100549102
_journal_volume                  64
_journal_year                    2000
_chemical_compound_source        R100177
_chemical_formula_sum            'Al0.635 As Cu Fe0.365 H2 O6'
_chemical_name_mineral           Luetheite
_space_group_IT_number           4
_symmetry_space_group_name_Hall  'P 2yb (1/2*x,y,-1/2*x+z)'
_symmetry_space_group_name_H-M   'B 1 21 1'
_cell_angle_alpha                90
_cell_angle_beta                 89.99
_cell_angle_gamma                90
_cell_length_a                   5.7012
_cell_length_b                   5.1801
_cell_length_c                   29.265
_cell_volume                     864.277
_exptl_crystal_density_diffrn    4.211
_cod_original_formula_sum        'Cu (Al.635 Fe.365) As O6 H2'
_cod_database_code               9009514
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R100177.rod
_rod_data_source.block           3500000
_rod_database.code               1000553
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9009514 COD http://www.crystallography.net/cod/9009514.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
104.5868 0.0000000E+00
105.0690 1.972328
105.5511 4.322319
106.0332 6.212738
106.5153 6.809631
106.9974 7.339890
107.4795 5.426918
107.9617 3.231712
108.4438 0.8975180
108.9259 0.4876480
109.4080 0.3849870
109.8901 2.065987
110.3722 2.719116
110.8544 2.021606
111.3365 1.377716
111.8186 2.064915
112.3007 3.519485
112.7828 4.517895
113.2649 4.468895
113.7471 3.380646
114.2292 2.897655
114.7113 3.865200
115.1934 4.580715
115.6755 4.904854
116.1576 4.911812
116.6397 4.708595
117.1219 4.437725
117.6040 4.141369
118.0861 3.620544
118.5682 2.351662
119.0503 1.170799
119.5324 0.7506980
120.0146 1.196156
120.4967 1.953880
120.9788 2.297115
121.4609 1.755901
121.9430 1.465729
122.4251 1.809345
122.9073 2.331303
123.3894 2.341736
123.8715 1.512417
124.3536 0.3696670
124.8357 0.3457680
125.3178 1.878536
125.8000 3.268303
126.2821 3.805634
126.7642 3.653252
127.2463 3.428169
127.7284 3.442863
128.2105 3.589619
128.6927 3.889828
129.1748 4.555904
129.6569 5.042664
130.1390 5.413124
130.6211 5.620319
131.1032 5.901749
131.5854 6.580608
132.0675 7.316376
132.5496 7.923981
133.0317 8.464176
133.5138 8.855747
133.9959 8.690655
134.4781 7.338837
134.9602 6.393871
135.4423 6.636345
135.9244 7.441242
136.4065 7.957722
136.8886 7.618324
137.3708 6.514160
137.8529 5.852203
138.3350 6.321167
138.8171 6.587627
139.2992 6.165314
139.7813 5.262127
140.2635 4.382225
140.7456 3.953720
141.2277 4.026100
141.7098 4.173676
142.1919 4.508987
142.6740 4.811272
143.1561 4.878601
143.6383 4.731350
144.1204 4.649540
144.6025 4.972942
145.0846 5.794643
145.5667 6.354553
146.0488 6.572384
146.5310 6.537594
147.0131 6.287983
147.4952 5.798946
147.9773 5.251575
148.4594 4.947311
148.9415 4.834602
149.4237 4.484268
149.9058 3.485165
150.3879 2.107811
150.8700 1.168770
151.3521 1.030861
151.8342 1.042160
152.3164 0.5510640
152.7985 0.3700290
153.2806 1.184406
153.7627 1.393772
154.2448 0.9844550
154.7269 0.7135890
155.2091 0.8477440
155.6912 1.024372
156.1733 1.073490
156.6554 0.9780620
157.1375 0.8078380
157.6196 0.6499670
158.1018 0.5318570
158.5839 0.3461040
159.0660 9.6938998E-02
159.5481 0.2167660
160.0302 0.6635510
160.5123 1.236366
160.9945 1.798382
161.4766 2.096371
161.9587 1.919868
162.4408 1.944118
162.9229 1.883186
163.4050 1.891186
163.8871 2.180477
164.3693 2.825581
164.8514 3.624489
165.3335 4.098072
165.8156 3.917152
166.2977 3.855778
166.7798 4.037182
167.2620 4.429024
167.7441 4.833584
168.2262 5.173836
168.7083 5.447132
169.1904 5.625740
169.6725 5.548859
170.1547 5.680099
170.6368 6.348309
171.1189 7.406467
171.6010 8.366825
172.0831 9.018631
172.5652 9.429165
173.0474 9.778267
173.5295 9.999496
174.0116 10.27850
174.4937 10.78131
174.9758 11.50761
175.4579 12.26622
175.9401 13.03535
176.4222 13.76013
176.9043 14.38411
177.3864 14.91420
177.8685 15.33485
178.3506 15.55749
178.8328 15.48812
179.3149 15.53813
179.7970 15.93298
180.2791 16.47660
180.7612 17.02201
181.2433 17.52134
181.7255 17.96013
182.2076 18.27169
182.6897 18.26932
183.1718 18.58112
183.6539 19.69821
184.1360 20.97173
184.6181 21.68048
185.1003 21.45512
185.5824 20.57631
186.0645 20.04205
186.5466 20.16957
187.0287 20.28289
187.5108 20.21793
187.9930 20.10688
188.4751 20.10035
188.9572 20.27886
189.4393 20.65134
189.9214 21.27261
190.4035 22.70491
190.8857 23.76217
191.3678 23.94749
191.8499 23.62000
192.3320 23.42931
192.8141 23.79575
193.2962 24.61915
193.7784 25.07893
194.2605 24.94210
194.7426 24.78193
195.2247 24.72453
195.7068 24.78888
196.1889 25.03714
196.6711 25.56932
197.1532 26.28421
197.6353 26.69530
198.1174 26.61308
198.5995 26.43847
199.0816 26.40020
199.5638 26.47723
200.0459 26.50195
200.5280 26.27868
201.0101 25.97205
201.4922 26.04744
201.9743 26.97935
202.4565 27.83888
202.9386 27.65526
203.4207 26.39583
203.9028 25.23930
204.3849 24.97907
204.8670 25.16758
205.3492 25.15297
205.8313 24.70486
206.3134 24.17418
206.7955 24.14115
207.2776 24.78934
207.7597 25.07236
208.2419 23.97521
208.7240 22.44997
209.2061 21.44689
209.6882 21.34314
210.1703 21.72958
210.6524 21.89264
211.1346 21.72868
211.6167 21.62991
212.0988 21.84853
212.5809 22.18150
213.0630 22.38586
213.5451 22.33107
214.0273 22.13909
214.5094 22.23002
214.9915 22.96808
215.4736 23.33956
215.9557 22.75014
216.4378 21.93079
216.9200 21.67728
217.4021 22.34815
217.8842 23.53728
218.3663 24.16756
218.8484 23.73574
219.3305 23.42014
219.8127 23.45331
220.2948 23.62194
220.7769 23.68959
221.2590 23.54950
221.7411 23.27748
222.2232 23.09318
222.7054 23.12623
223.1875 23.09078
223.6696 23.16888
224.1517 23.10059
224.6338 22.51108
225.1159 21.22841
225.5980 19.50916
226.0802 18.09390
226.5623 17.45076
227.0444 16.56258
227.5265 15.09287
228.0086 13.41143
228.4907 12.02476
228.9729 11.14902
229.4550 10.61192
229.9371 9.985527
230.4192 9.102997
230.9013 8.391884
231.3834 8.060478
231.8656 7.910892
232.3477 7.622581
232.8298 7.053532
233.3119 6.373173
233.7940 5.971882
234.2761 5.933178
234.7583 5.891586
235.2404 5.680153
235.7225 5.418377
236.2046 5.360302
236.6867 5.643436
237.1688 6.022186
237.6510 6.025784
238.1331 5.614670
238.6152 5.220772
239.0973 4.937679
239.5794 4.775669
240.0615 4.792072
240.5437 5.058380
241.0258 5.391895
241.5079 5.508801
241.9900 5.408703
242.4721 5.396465
242.9542 5.606293
243.4364 5.999462
243.9185 6.516834
244.4006 7.231728
244.8827 7.907772
245.3648 8.342190
245.8469 8.553791
246.3290 8.568790
246.8112 8.379719
247.2933 8.003181
247.7754 7.397182
248.2575 6.296501
248.7396 5.428135
249.2217 5.585266
249.7039 6.477730
250.1860 7.117126
250.6681 6.735313
251.1502 5.635002
251.6323 4.988255
252.1144 5.136730
252.5966 5.268314
253.0787 4.850132
253.5608 4.056866
254.0429 3.265678
254.5250 2.639175
255.0071 2.180622
255.4893 1.914879
255.9714 1.918423
256.4535 2.010456
256.9356 2.131557
257.4177 2.266361
257.8998 2.402351
258.3820 2.567665
258.8641 2.712322
259.3462 2.615692
259.8283 2.015102
260.3104 1.615856
260.7925 1.917282
261.2747 2.448669
261.7568 2.541180
262.2389 1.790157
262.7210 0.5309300
263.2031 0.2570760
263.6852 0.3374370
264.1674 0.3138960
264.6495 0.3236160
265.1316 0.3267560
265.6137 0.2692410
266.0958 0.1249080
266.5779 6.4960003E-02
267.0601 0.2122880
267.5422 0.3546220
268.0243 0.3701170
268.5064 0.2091140
268.9885 4.3892000E-02
269.4706 0.3924870
269.9528 0.8258550
270.4349 1.173538
270.9170 1.019516
271.3991 0.2058490
271.8812 0.7795680
272.3633 0.1695670
272.8455 0.7544560
273.3276 1.445072
273.8097 1.727543
274.2918 1.624149
274.7739 1.072155
275.2560 0.4149630
275.7382 1.288857
276.2202 1.273075
276.7024 0.9918330
277.1845 0.7134510
277.6666 0.5410190
278.1487 0.5570950
278.6308 0.8700330
279.1129 1.531265
279.5951 2.331398
280.0772 3.626022
280.5593 4.738308
281.0414 5.166531
281.5235 5.008400
282.0056 4.803303
282.4878 5.106594
282.9699 6.047981
283.4520 6.553791
283.9341 6.116428
284.4162 5.801300
284.8983 6.096027
285.3805 6.892735
285.8626 7.820232
286.3447 8.608646
286.8268 9.256721
287.3089 9.839916
287.7910 10.34739
288.2732 10.80785
288.7553 11.14710
289.2374 11.44714
289.7195 11.88765
290.2016 12.59958
290.6837 13.49165
291.1659 14.05902
291.6480 14.07670
292.1301 14.03146
292.6122 14.11192
293.0943 14.14714
293.5764 13.83945
294.0586 13.04050
294.5407 11.94957
295.0228 11.10279
295.5049 10.69347
295.9870 10.30832
296.4691 9.894577
296.9513 9.515247
297.4334 9.278473
297.9155 9.213634
298.3976 9.186489
298.8797 8.960182
299.3618 8.305965
299.8440 7.890316
300.3261 8.009857
300.8082 8.180866
301.2903 7.857414
301.7724 7.002392
302.2545 6.219463
302.7367 6.301620
303.2188 7.668957
303.7009 8.213783
304.1830 7.168209
304.6651 6.006367
305.1472 5.751431
305.6294 6.348278
306.1115 7.010647
306.5936 7.039394
307.0757 6.383938
307.5578 6.073811
308.0399 6.436340
308.5221 6.754761
309.0042 6.642971
309.4863 6.221214
309.9684 5.852890
310.4505 5.782249
310.9326 5.953876
311.4148 5.982235
311.8969 5.713654
312.3790 5.502758
312.8611 5.572826
313.3432 5.731289
313.8253 5.566185
314.3075 4.856503
314.7896 3.949329
315.2717 3.765999
315.7538 5.355648
316.2359 6.148247
316.7180 5.319492
317.2001 3.868488
317.6823 2.848209
318.1644 2.564518
318.6465 2.736053
319.1286 2.975918
319.6107 3.335793
320.0928 3.412582
320.5750 3.113766
321.0571 2.651424
321.5392 2.060364
322.0213 1.438831
322.5034 1.075584
322.9855 1.281651
323.4677 2.148861
323.9498 2.948792
324.4319 3.684505
324.9140 4.309349
325.3961 4.849834
325.8782 5.261314
326.3604 5.438919
326.8425 5.306328
327.3246 4.941551
327.8067 4.782211
328.2888 4.787785
328.7709 4.895050
329.2531 5.112495
329.7352 5.455643
330.2173 6.093094
330.6994 7.107174
331.1815 8.194454
331.6636 8.553207
332.1458 7.078514
332.6279 6.300346
333.1100 6.842758
333.5921 7.826157
334.0742 8.454906
334.5563 8.496468
335.0385 8.192524
335.5206 7.864922
336.0027 7.423508
336.4848 7.216343
336.9669 7.299370
337.4490 7.540531
337.9312 7.929649
338.4133 8.419636
338.8954 8.860790
339.3775 9.082859
339.8596 9.042797
340.3417 9.340092
340.8239 10.43475
341.3060 11.34408
341.7881 11.58186
342.2702 11.37275
342.7523 11.18517
343.2344 11.30115
343.7166 11.68592
344.1987 12.17257
344.6808 12.90210
345.1629 13.57893
345.6450 14.13436
346.1271 14.63721
346.6093 15.18340
347.0914 15.80113
347.5735 16.42284
348.0556 16.90812
348.5377 17.20182
349.0198 17.44946
349.5020 17.71884
349.9841 17.90303
350.4662 17.97605
350.9483 17.90685
351.4304 17.61209
351.9125 16.96873
352.3947 15.91673
352.8768 14.92442
353.3589 13.62256
353.8410 12.74441
354.3231 12.77265
354.8052 13.43073
355.2874 14.17190
355.7695 14.66301
356.2516 14.89402
356.7337 14.78255
357.2158 13.82649
357.6979 13.21870
358.1800 13.51857
358.6621 14.10628
359.1443 14.24216
359.6264 13.64499
360.1085 12.73222
360.5906 12.32435
361.0727 12.78021
361.5548 12.79210
362.0370 11.87589
362.5191 10.77615
363.0012 9.936562
363.4833 9.392403
363.9654 8.925114
364.4475 8.269958
364.9297 7.402355
365.4118 6.778940
365.8939 6.794821
366.3760 6.616665
366.8581 5.568655
367.3402 4.099760
367.8224 3.168230
368.3045 3.495043
368.7866 4.615297
369.2687 5.156723
369.7508 4.951992
370.2329 4.509554
370.7151 3.794350
371.1972 3.045311
371.6793 2.494904
372.1614 2.221561
372.6435 2.105125
373.1256 2.052429
373.6078 2.074783
374.0899 2.006422
374.5720 1.831087
375.0541 1.522762
375.5362 0.9116130
376.0183 5.8568999E-02
376.5005 0.5249820
376.9826 0.2626300
377.4647 0.5720200
377.9468 0.9480190
378.4289 0.6962870
378.9110 0.2179850
379.3932 0.3355690
379.8753 0.9086880
380.3574 1.393381
380.8395 1.807844
381.3216 2.072395
381.8037 2.045397
382.2859 1.722534
382.7680 1.310513
383.2501 0.7313120
383.7322 0.2390060
384.2143 0.2801270
384.6964 1.054371
385.1786 1.680922
385.6607 1.501284
386.1428 0.7826310
386.6249 0.2309190
387.1070 2.3031000E-02
387.5891 2.1470999E-02
388.0713 3.7636001E-02
388.5534 3.0634001E-02
389.0355 0.1721820
389.5176 0.6961940
389.9997 1.261036
390.4818 1.504309
390.9640 1.418222
391.4461 1.207262
391.9282 0.9091430
392.4103 0.6204410
392.8924 0.7773090
393.3745 1.994278
393.8567 2.946798
394.3388 2.951826
394.8209 2.344021
395.3030 1.689854
395.7851 1.164152
396.2672 0.8679830
396.7494 1.012239
397.2315 1.827187
397.7136 2.549313
398.1957 3.119812
398.6778 3.609241
399.1599 4.105404
399.6420 4.600258
400.1241 4.971447
400.6063 5.074604
401.0884 4.894508
401.5705 4.996086
402.0526 5.691730
402.5347 6.282719
403.0168 6.433203
403.4990 6.363207
403.9811 6.467146
404.4632 6.936863
404.9453 7.596001
405.4274 8.014050
405.9095 8.056524
406.3917 8.063931
406.8738 7.803087
407.3559 7.688299
407.8380 8.220499
408.3201 9.323694
408.8022 10.31467
409.2844 10.41969
409.7665 9.555376
410.2486 9.138058
410.7307 9.649508
411.2128 10.10585
411.6949 10.05354
412.1771 9.787714
412.6592 9.847473
413.1413 10.54966
413.6234 11.54490
414.1055 12.01873
414.5876 11.73903
415.0698 11.65242
415.5519 12.08589
416.0340 12.72271
416.5161 13.40301
416.9982 14.09886
417.4803 14.77364
417.9625 15.38594
418.4446 15.94527
418.9267 16.53068
419.4088 17.13260
419.8909 17.78493
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